KR20120047815A - 가스 감지 시스템 - Google Patents
가스 감지 시스템 Download PDFInfo
- Publication number
- KR20120047815A KR20120047815A KR1020110111101A KR20110111101A KR20120047815A KR 20120047815 A KR20120047815 A KR 20120047815A KR 1020110111101 A KR1020110111101 A KR 1020110111101A KR 20110111101 A KR20110111101 A KR 20110111101A KR 20120047815 A KR20120047815 A KR 20120047815A
- Authority
- KR
- South Korea
- Prior art keywords
- gas
- sensing
- fiber
- sensing layer
- individual
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000001514 detection method Methods 0.000 title claims abstract description 22
- 239000000835 fiber Substances 0.000 claims abstract description 162
- 230000003287 optical effect Effects 0.000 claims abstract description 52
- 238000012546 transfer Methods 0.000 claims abstract description 39
- 239000007789 gas Substances 0.000 claims description 374
- 239000000463 material Substances 0.000 claims description 48
- 238000000034 method Methods 0.000 claims description 18
- 230000008542 thermal sensitivity Effects 0.000 claims description 14
- 239000003017 thermal stabilizer Substances 0.000 claims description 13
- 239000013307 optical fiber Substances 0.000 claims description 6
- 239000011540 sensing material Substances 0.000 claims description 5
- CRQQGFGUEAVUIL-UHFFFAOYSA-N chlorothalonil Chemical compound ClC1=C(Cl)C(C#N)=C(Cl)C(C#N)=C1Cl CRQQGFGUEAVUIL-UHFFFAOYSA-N 0.000 claims 1
- 238000002347 injection Methods 0.000 claims 1
- 239000007924 injection Substances 0.000 claims 1
- 239000010410 layer Substances 0.000 description 115
- 230000035945 sensitivity Effects 0.000 description 31
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 26
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 23
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 17
- 229910052739 hydrogen Inorganic materials 0.000 description 15
- 229910002092 carbon dioxide Inorganic materials 0.000 description 13
- 239000001569 carbon dioxide Substances 0.000 description 13
- 230000008859 change Effects 0.000 description 12
- 239000001257 hydrogen Substances 0.000 description 12
- 230000000694 effects Effects 0.000 description 11
- 230000004044 response Effects 0.000 description 10
- 229910052759 nickel Inorganic materials 0.000 description 9
- 239000000203 mixture Substances 0.000 description 8
- 239000011241 protective layer Substances 0.000 description 7
- 229910052725 zinc Inorganic materials 0.000 description 7
- 239000011701 zinc Substances 0.000 description 7
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910002091 carbon monoxide Inorganic materials 0.000 description 4
- 238000005253 cladding Methods 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 239000005350 fused silica glass Substances 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 230000003595 spectral effect Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 239000002657 fibrous material Substances 0.000 description 2
- -1 for example Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 230000001939 inductive effect Effects 0.000 description 2
- 229910052763 palladium Inorganic materials 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 description 1
- 239000005751 Copper oxide Substances 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 229910001252 Pd alloy Inorganic materials 0.000 description 1
- 206010057040 Temperature intolerance Diseases 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000003491 array Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 229910000431 copper oxide Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 230000008543 heat sensitivity Effects 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen(.) Chemical compound [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000010944 silver (metal) Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/41—Refractivity; Phase-affecting properties, e.g. optical path length
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
- G01N21/7703—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator using reagent-clad optical fibres or optical waveguides
- G01N21/774—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator using reagent-clad optical fibres or optical waveguides the reagent being on a grating or periodic structure
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
- G01N33/0009—General constructional details of gas analysers, e.g. portable test equipment
- G01N33/0027—General constructional details of gas analysers, e.g. portable test equipment concerning the detector
- G01N33/0036—General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
- G01N33/004—CO or CO2
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
- G01N33/0009—General constructional details of gas analysers, e.g. portable test equipment
- G01N33/0027—General constructional details of gas analysers, e.g. portable test equipment concerning the detector
- G01N33/0036—General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component
- G01N33/005—H2
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/75—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated
- G01N21/77—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
- G01N21/78—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
- G01N21/783—Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour for analysing gases
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Pathology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Plasma & Fusion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/913,950 US8542955B2 (en) | 2010-10-28 | 2010-10-28 | Gas detection system incorporating fiber gas sensors having fiber bragg gratings |
| US12/913,950 | 2010-10-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20120047815A true KR20120047815A (ko) | 2012-05-14 |
Family
ID=45373440
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020110111101A Ceased KR20120047815A (ko) | 2010-10-28 | 2011-10-28 | 가스 감지 시스템 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8542955B2 (enExample) |
| JP (1) | JP2012098279A (enExample) |
| KR (1) | KR20120047815A (enExample) |
| DE (1) | DE102011054715A1 (enExample) |
| GB (1) | GB2485059B (enExample) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8639066B2 (en) * | 2011-09-29 | 2014-01-28 | General Electric Company | Nano-structured trampoline fiber gas sensor |
| FR2985315B1 (fr) * | 2011-12-30 | 2014-03-14 | Andra | Dispositif de detection et/ou de dosage d'hydrogene et procede de detection et/ou de dosage d'hydrogene |
| WO2014123519A1 (en) | 2013-02-06 | 2014-08-14 | Empire Technology Development Llc | Devices, systems, and methods for detecting odorants |
| US20160138963A1 (en) * | 2013-06-17 | 2016-05-19 | Empire Technology Development Llc | Graded films |
| CN103675217B (zh) * | 2013-12-30 | 2015-11-18 | 中国科学院电子学研究所 | 一种气体检测方法及装置 |
| CN103868879B (zh) * | 2014-03-18 | 2016-05-11 | 天津大学 | 基于光纤布喇格光栅的多种气体浓度传感器 |
| CN104458798B (zh) * | 2014-11-04 | 2017-01-18 | 大连理工大学 | 一种高压低温导热系数、传热系数的原位测试方法 |
| CN105044033B (zh) * | 2014-12-10 | 2017-12-05 | 中国计量学院 | 一种强度解调型光纤气体传感装置及其传感方法 |
| WO2016136905A1 (ja) | 2015-02-27 | 2016-09-01 | 国立研究開発法人物質・材料研究機構 | 母材と粒状材料を混合した受容体層を被覆したセンサ |
| CN105388113B (zh) * | 2015-11-20 | 2019-05-31 | 上海斐讯数据通信技术有限公司 | 气体检测设备 |
| KR102271697B1 (ko) * | 2016-08-18 | 2021-07-02 | 네바다 나노테크 시스템즈 인코포레이티드 | 물질의 적어도 하나의 속성을 결정하기 위한 시스템 및 방법 |
| US11371893B2 (en) | 2016-11-10 | 2022-06-28 | Ryan Seeley | Optical sensor and systems and methods |
| ES2824497T3 (es) | 2016-11-11 | 2021-05-12 | Carrier Corp | Detección basada en fibra óptica de alta sensibilidad |
| ES2841313T3 (es) | 2016-11-11 | 2021-07-08 | Carrier Corp | Detección basada en fibra óptica de alta sensibilidad |
| CN108844991B (zh) * | 2018-05-22 | 2020-09-11 | 太原理工大学 | 混凝土板件传热系数测定装置及方法 |
| CN109358010A (zh) * | 2018-10-31 | 2019-02-19 | 榆林学院 | 一种利用光纤有源内腔法测雾霾主要成分的装置及方法 |
| CN109459425B (zh) * | 2018-12-13 | 2021-05-11 | 云南电网有限责任公司电力科学研究院 | 一种应用于光纤气体传感的光纤适配装置 |
| US11385130B2 (en) | 2019-02-22 | 2022-07-12 | Ryan Seeley | Multi-spectral feature sensing techniques and sensors for determining a phase shift by comparing a measured narrowband response to a known wideband response |
| US11137271B2 (en) | 2019-02-22 | 2021-10-05 | Ryan Seeley | Multi-spectral features sensing techniques and sensors comprising plural gratings with plural chirp slopes |
| CN110006851B (zh) * | 2019-04-24 | 2019-11-15 | 山东大学 | 一种光纤光栅气敏传感用的气体在线监测装置及方法 |
| US12276533B2 (en) * | 2022-03-02 | 2025-04-15 | Halliburton Energy Services, Inc. | Materials and diagnostics for hydrogen service environments |
| WO2025101732A1 (en) * | 2023-11-08 | 2025-05-15 | Cummins Inc. | Sensor systems including hydrogen concentration sensors and cooling apparatus |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5218347A (en) | 1991-11-12 | 1993-06-08 | Lindale Industries, Inc. | Apparatus for detecting hazardous gases |
| JPH09113501A (ja) * | 1995-10-16 | 1997-05-02 | Kurabe Ind Co Ltd | 一酸化炭素ガス検知用検知材料及び一酸化炭素ガス検知方法 |
| US5767411A (en) * | 1996-12-31 | 1998-06-16 | Cidra Corporation | Apparatus for enhancing strain in intrinsic fiber optic sensors and packaging same for harsh environments |
| JP3285511B2 (ja) * | 1997-05-15 | 2002-05-27 | 株式会社豊田中央研究所 | ガス分析試験装置 |
| TW537879B (en) | 2001-05-23 | 2003-06-21 | Ind Tech Res Inst | Diagnosing device by breath test including a multi-array of sensors |
| NO316775B1 (no) * | 2001-06-11 | 2004-05-03 | Optoplan As | Fremgangsmate for belegging av en fiber med fiberoptisk Bragg-Gitter (FBG) |
| US7140232B2 (en) | 2002-12-16 | 2006-11-28 | Radiodetection Limited | Method and apparatus for multiple gas sensor |
| JP2005156831A (ja) * | 2003-11-25 | 2005-06-16 | Hitachi Cable Ltd | 光ファイバセンサの製造方法及び光ファイバセンサ |
| US7239778B2 (en) | 2004-01-23 | 2007-07-03 | University Of Pittsburgh - Of The Commonwealth System Of Higher Education | Active in-fiber optic components powered by in-fiber light |
| US7421162B2 (en) * | 2005-03-22 | 2008-09-02 | General Electric Company | Fiber optic sensing device and method of making and operating the same |
| GB2430027A (en) | 2005-09-09 | 2007-03-14 | Kidde Ip Holdings Ltd | Fibre bragg temperature sensors |
| US7151872B1 (en) | 2005-11-22 | 2006-12-19 | General Electric Company | Method, system and module for monitoring a power generating system |
| WO2008136870A2 (en) | 2006-12-18 | 2008-11-13 | University Of Pittsburgh - Of The Commonwealth System Of Higher Education | Fiber optic gas sensor |
| GB0707303D0 (en) | 2007-04-17 | 2007-05-23 | Faculte Polytechnique De Mons | Gas sensor |
| US7567734B2 (en) * | 2007-08-09 | 2009-07-28 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Industry, Through The Communications Research Centre Canada | Ridge waveguide optical sensor incorporating a Bragg grating |
| US7489835B1 (en) * | 2008-03-28 | 2009-02-10 | General Electric Company | Sensing system with fiber gas sensor |
| US8547553B2 (en) * | 2010-03-17 | 2013-10-01 | General Electric Company | Fiber optic hydrogen purity sensor and system |
| WO2011120147A1 (en) * | 2010-03-30 | 2011-10-06 | University Of Victoria Innovation And Development Corporation | Multi-point pressure sensor and uses thereof |
| US8467977B2 (en) * | 2010-07-29 | 2013-06-18 | General Electric Company | Fiber optic carbon dioxide purity sensor package and system |
-
2010
- 2010-10-28 US US12/913,950 patent/US8542955B2/en not_active Expired - Fee Related
-
2011
- 2011-10-20 JP JP2011230219A patent/JP2012098279A/ja active Pending
- 2011-10-21 DE DE102011054715A patent/DE102011054715A1/de not_active Withdrawn
- 2011-10-26 GB GB1118484.3A patent/GB2485059B/en not_active Expired - Fee Related
- 2011-10-28 KR KR1020110111101A patent/KR20120047815A/ko not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| GB2485059B (en) | 2017-05-10 |
| GB2485059A (en) | 2012-05-02 |
| JP2012098279A (ja) | 2012-05-24 |
| DE102011054715A1 (de) | 2012-05-03 |
| US20120103066A1 (en) | 2012-05-03 |
| GB201118484D0 (en) | 2011-12-07 |
| US8542955B2 (en) | 2013-09-24 |
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