KR20120021904A - Furniture manufacturing method using eco-friendly flame retardant - Google Patents

Furniture manufacturing method using eco-friendly flame retardant Download PDF

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KR20120021904A
KR20120021904A KR1020100081042A KR20100081042A KR20120021904A KR 20120021904 A KR20120021904 A KR 20120021904A KR 1020100081042 A KR1020100081042 A KR 1020100081042A KR 20100081042 A KR20100081042 A KR 20100081042A KR 20120021904 A KR20120021904 A KR 20120021904A
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weight
parts
furniture
flame retardant
composition
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KR1020100081042A
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Korean (ko)
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KR101203514B1 (en
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임종상
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(주)으뜸퍼니처
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02—Processes; Apparatus
    • B27K3/0228—Spraying apparatus, e.g. tunnels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27M—WORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M3/00—Manufacture or reconditioning of specific semi-finished or finished articles
    • B27M3/18—Manufacture or reconditioning of specific semi-finished or finished articles of furniture or of doors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00—Purpose of the treatment
    • B27K2240/30—Fireproofing

Abstract

PURPOSE: Furniture manufacturing method using echo frame proofing agent is provided to have flameproof ability, flame retardancy and waterproof ability by spraying flame proofing agent composition, and then spraying flame retardant compostion and waterproof coating agent. CONSTITUTION: Furniture manufacturing method using echo frame proofing agent comprises a step of preparing flame proofing agent composition by mixing primary ammonium phosphate, boric acid, sodium hydroxide and water; a step of preparing mixed composition by mixing phytoncide, nano-silver material, mixed liquid of hot water extraction of a mistletoe; a step of manufacturing a first compostion by mixing the flame proofing agent composition and the mixed composition, and then spraying the mixture to woody material; and a step of manufacturing furniture by drying the first compostion.

Description

친환경 방염제를 이용한 가구 제조 방법{.}Furniture manufacturing method using eco-friendly flame retardant {.}

본 발명은 친환경 방염제를 이용한 가구 제조 방법에 관한 것으로, 보다 상세하게는 수용성 방염제 조성물과 피톤치드, 은나노 물질, 겨우살이나무 열수추출물 혼합액을 분사한 목질재료를 이용하여 가구를 제조함으로써, 가구 자체에 방염처리가 되는 동시에 피톤치드나 은나노 또는 겨우살이나무의 친환경적 효능이 발휘되고, 난연 및 발수용 코팅제를 더 분사함으로써, 방염성과 더불어 난연성 및 발수성의 기능이 있는 가구를 제조 할 수 있는 친환경 방염제를 이용한 가구 제조 방법에 관한 것이다.The present invention relates to a method of manufacturing furniture using an eco-friendly flame retardant, and more particularly, by producing a furniture using a wood material sprayed with a water-soluble flame retardant composition and phytoncide, silver nano material, mistletoe hot water extract mixture, flame retardant treatment on the furniture itself At the same time, the eco-friendly efficacy of phytoncide, silver nano or mistletoe wood is exhibited, and by spraying more flame retardant and water repellent coatings, furniture manufacturing method using eco-friendly flame retardant that can produce furniture with flame-retardant and water-repellent function. It is about.

본 발명은 친환경 방염제를 이용한 가구 제조 방법에 관한 것이다. The present invention relates to a method of manufacturing furniture using an environmentally friendly flame retardant.

기존의 가구는 일반 목질재료를 사용하여 제작함으로써 화재에 약하고 장시간 사용하면 목질재료에 습기가 스며들어 가구의 뒤틀림 현상이 발생하였다.Existing furniture is made of general wood materials, so it is vulnerable to fire. When used for a long time, the wood material gets wet, causing warping of furniture.

또한, 가구 제작 시 사용되는 페인트나 인체에 유해한 화학 물질이 함유된 접착제 등에 의하여 면역력이 약한 노인이나 어린이의 접촉 시 아토피 또는 알레르기 질환 등의 각종 질환이 유발될 수도 있다. In addition, various diseases such as atopic or allergic diseases may be induced when the elderly or children with weak immunity are contacted by paints used for making furniture or adhesives containing harmful chemicals to the human body.

상술한 문제점을 해결하기 위해 안출된 본 발명의 목적은 수용성 방염제 조성물과 피톤치드, 은나노 물질, 겨우살이나무 열수추출물 혼합액을 분사한 목질재료를 이용하여 가구를 제조함으로써, 가구 자체에 방염처리가 되는 동시에 피톤치드나 은나노 또는 겨우살이나무의 친환경적 효능이 발휘되는 친환경 방염제를 이용한 가구 제조 방법을 제공하기 위한 것이다.An object of the present invention devised to solve the above problems is to produce furniture by spraying the water-soluble flame retardant composition and phytoncide, silver nano material, mistletoe hot water extract mixture, wood furniture, flame retardant treatment at the same time phytoncide It is to provide a furniture manufacturing method using an eco-friendly flame retardant that exhibits the eco-friendly effects of silver nano or mistletoe.

또한, 본 발명의 다른 목적은 목질재료에 방염제 조성물을 분사한 후 난연 및 발수용 코팅제를 더 분사함으로써, 방염성과 더불어 난연성 및 발수성의 기능이 있는 목질재료를 이용하여 가구를 제조할 수 있는 친환경 방염제를 이용한 가구 제조 방법을 제공하기 위함이다.In addition, another object of the present invention by spraying the flame retardant composition to the wood material and further spraying a flame retardant and water repellent coating, an eco-friendly flame retardant that can produce furniture using a wood material with a flame retardant and flame retardant and water-repellent function In order to provide a furniture manufacturing method using.

상기한 바와 같은 목적을 달성하기 위한 본 발명의 특징에 따르면, 본 발명은 제일인산암모늄, 붕산, 수산화나트륨 및 물을 혼합하여 제조한 방염제 조성물과, 피톤치드, 은나노 물질 및 겨우살이나무 열수추출물을 혼합한 혼합 조성물을 혼합하여 제조한 제1조성물을 목질재료에 분사한 후 건조하여 가구를 제조하는 것을 특징으로 한다.According to a feature of the present invention for achieving the object as described above, the present invention is a flame retardant composition prepared by mixing ammonium phosphate, boric acid, sodium hydroxide and water, phytoncide, silver nano material and mistletoe hot water extract The first composition prepared by mixing the mixed composition is sprayed on a wood material, and then dried to manufacture furniture.

또한, 콜로이달 실리카 및 물을 혼합한 후 질산으로 pH를 조정한 제1혼합용액과, 이소프로필알콜, 하이드로프로필 셀룰로스용액, 노말핵산, 메틸이소부틸케톤, 퓸드 실리카 및 황토를 혼합한 제2혼합용액을 교반하여 제조한 제2조성물을, 제1조성물을 분사하여 건조한 목질재료에 더 분사한 후 건조하여 가구를 제조하는 것을 특징으로 한다.In addition, a first mixture solution of which colloidal silica and water are mixed and then pH-adjusted with nitric acid, and a second mixture of isopropyl alcohol, hydropropyl cellulose solution, normal nucleic acid, methyl isobutyl ketone, fumed silica, and ocher The second composition prepared by stirring the solution is sprayed on the first composition to further dry wood material, and then dried to manufacture furniture.

또한, 겨우살이나무 열수추출물은 건조된 겨우살이나무 절편에 물을 10배 중량만큼 첨가하고 300℃로 가열한 후, 끓기 시작하면 200℃의 온도로 낮춰 첨가된 물이 50 내지 60 중량% 증발될 때까지 우려냄으로써 제조되는 것을 특징으로 한다.In addition, the mistletoe hot water extract was added to the dried mistletoe wood by 10 times the weight of water and heated to 300 ℃, and then started boiling to lower the temperature of 200 ℃ until the added water is evaporated 50 to 60% by weight It is characterized by being manufactured by boiling.

또한, 제1조성물은, 제일인산암모늄 11 내지 25 중량부와 붕산 0.1 내지 3 중량부와 수산화나트륨 1 내지 7 중량부와 피톤치드 5 내지 20 중량부와 은나노 5 내지 20 중량부 및 겨우살이나무 열수추출물 5 내지 20 중량부가 포함되는 것을 특징으로 한다.In addition, the first composition is 11 to 25 parts by weight of ammonium phosphate, 0.1 to 3 parts by weight of boric acid, 1 to 7 parts by weight of sodium hydroxide, 5 to 20 parts by weight of phytoncide, 5 to 20 parts by weight of silver nano and mistletoe hot water extract 5 To 20 parts by weight is included.

또한, 제2조성물은, 콜로이달 실리카 10 내지 45 중량부 및 물 55 내지 90 중량부가 포함되어 혼합된 후 질산으로 pH를 3.0 내지 4.5로 조정한 제1혼합용액과, 하이드로프로필 셀룰로스용액 5 내지 8 중량부와 노말핵산 1 내지 7 중량부와 메틸이소부틸케톤 10 내지 20중량부와 퓸드 실리카 0.1 내지 3 중량부 및 황토 5 내지 20중량부가 포함된 제2혼합용액을 혼합한 후 2시간 내지 3시간 동안 교반하여 제조하는 것을 특징으로 한다.In addition, the second composition includes 10 to 45 parts by weight of colloidal silica and 55 to 90 parts by weight of water, and then mixed with a first mixture solution having a pH adjusted to 3.0 to 4.5 with nitric acid and a hydropropyl cellulose solution 5 to 8 2 to 3 hours after mixing the second mixture solution containing 1 to 7 parts by weight of normal nucleic acid, 10 to 20 parts by weight of methyl isobutyl ketone, 0.1 to 3 parts by weight of fumed silica and 5 to 20 parts by weight of ocher It is characterized by preparing for stirring.

이상 살펴본 바와 같은 본 발명에 따르면, 수용성 방염제 조성물과 피톤치드, 은나노 물질, 겨우살이나무 열수추출물 혼합액을 분사한 목질재료를 이용하여 가구를 제조함으로써, 가구 자체에 방염처리가 되는 동시에 피톤치드나 은나노 또는 겨우살이나무의 친환경적 효능이 발휘되는 친환경 방염제를 이용한 가구 제조 방법을 제공할 수 있다.According to the present invention as described above, by producing a furniture using a water-based flame retardant composition and phytoncide, silver nano material, wood material sprayed mistletoe hot water extract mixture, the furniture itself is flame-resistant and at the same time phytoncide or silver nano or mistletoe It can provide a furniture manufacturing method using an environmentally friendly flame retardant exhibiting the eco-friendly efficacy of.

여기서, 피톤치드(phytoncide)는 식물이 병균, 해충, 곰팡이등에 저항하려고 내뿜거나 분비하는 물질로, 이러한 피톤치드는 편백나무, 측백나무 등에서 특히 많이 추출되며 방향성이 있는 항생물질의 총칭을 피톤치드라 하며 테르핀(terpene) 계통의 유기 화합물을 말한다. 최근에 많이 각광받고 있는 삼림욕이란 피톤치드가 휘산되어 있는 상태의 대기에 인간이 접하는 것으로서, 삼림욕을 통해 피톤치드를 흡수하면 해충, 병균, 곰팡이, 박테리아 등에는 치명적이지만 인간에게는 유익하기 때문이다. 또한, 피톤치드의 효능은 스트레스 완화작용, 강한 향균작용, 소취작용 및 유해물질 중화, 진정작용, 알레르기 및 피부 질환 개선 작업, 면역기능 증대 작용, 장과 심폐기능 강화 등의 효능을 갖는다.Here, phytoncide (phytoncide) is a substance that plants exhale or secrete to resist germs, pests, fungi, etc., these phytoncide is particularly extracted from cypress, cypress, etc., and the general term of directional antibiotics are called phytoncide and terpin Refers to organic compounds of the terpene family. Recently, forest baths, which have been widely spotlighted, are in contact with the atmosphere in which the phytoncide is volatilized, and the absorption of the phytoncide through the forest bath is fatal to pests, germs, molds, bacteria, etc., but is beneficial to humans. In addition, phytoncide has the effects of stress relief, strong antibacterial action, deodorant action and neutralization of harmful substances, sedation, allergy and skin disease improvement, immune function enhancement, intestinal and cardiopulmonary function enhancement.

그리고, 은나노 물질에서 은(silver)은 단세포 동물(바이러스, 박테리아, 곰팡이)등의 세포속으로 침투하여 호흡할 때 필요한 효소의 기능을 정지시켜 질식 및 소멸 시키는 작용을 한다. 또한, 은나노의 효능은 다음과 같은데 탈취 향균 작용으로 곰팡이, 박테리아, 무좀균 등에 침투하여 사멸하는 기능을 하며 인체에서 분비되는 땀, 노폐물의 냄새를 분해하는 기능을 하고, 전자파 차폐 기능이 있으며, 전기 전도도가 금 다음으로 뛰어나 정전기 발생을 억제하고, 항온 단열기능을 하며, 향균 및 살균 기능으로 세균의 세포막을 파괴 또는 세포의 기능을 교란시키며, 활성 산소를 발생하는 등의 효능을 갖는다.In addition, silver (silver) in the silver nanomaterials acts to suffocate and extinguish by stopping the function of the enzyme required to penetrate into cells such as unicellular animals (viruses, bacteria, fungi). In addition, the effects of silver nano are as follows: Deodorant antibacterial function to penetrate and kill fungi, bacteria, athlete's foot, etc., and to decompose the smell of sweat and waste products secreted by the human body, electromagnetic shielding function, electrical conductivity It is superior to poultry, which suppresses the generation of static electricity, has a constant-temperature insulation function, and has the effect of destroying bacterial cell membranes or disrupting the function of cells with antibacterial and bactericidal functions, and generating free radicals.

또한, 겨우살이 나무는 노박덩굴과의 상록관목으로 흔히 관상용이나 산울타리용으로 심으며 한국, 일본, 중국 등지에 분포하며, 독성이 전혀 없고 강력한 항암식물의 일종으로 약재로도 쓰이고 있다. 겨우살이 나무는 살균작용과 더불어 몸을 따듯하게 하는 효능이 있어 감기 등의 기관지 질환에도 탁월한 효능을 갖는다.Mistletoe trees are evergreen shrubs with vines and are often planted for ornamental or hedge, distributed in Korea, Japan, and China, and are also used as medicinal herbs as nontoxic and powerful anticancer plants. Mistletoe tree has the effect of sterilizing and warming the body, so it has an excellent effect on bronchial diseases such as cold.

또한, 본 발명에 따르면 목질재료에 방염제 조성물을 분사한 후 난연 및 발수용 코팅제를 더 분사함으로써, 방염성과 더불어 난연성 및 발수성의 기능이 있는 목질재료를 이용하여 가구를 제조함으로써, 화재로부터 강하고 물이 잘 스미지 않아 장시간 사용하여도 뒤틀림 현상이 없는 가구를 제작할 수 있는 친환경 방염제를 이용한 가구 제조 방법을 제공할 수 있다. In addition, according to the present invention by spraying a flame retardant composition to the wood material and further spraying a flame retardant and water repellent coating, by producing a furniture using wood materials having a flame retardant and flame retardant and water-repellent function, strong and water from fire It can provide a method of manufacturing furniture using an eco-friendly flame retardant that can produce furniture without distortion, even if it is not used well for a long time.

이때, 난연 및 발수용 코팅제 조성물 제조시 황토 분말을 주입함으로써 황토 성분에 의하여 실내의 공기가 정화되어 인체에 유익하며 친환경적인 황토에서 고율의 원적외선이 방사되어 세포의 생리작용을 활발히 하고 열에너지를 방출시키면서 체온을 높이는 작용을 하여 인체의 모세혈관을 확장하고 혈액순환을 활성화하면서 신진대사를 강화, 조직 재생력을 증가시키며, 실내의 습기가 많을 때는 습기를 흡수해두었다가 건조해지면 습기를 발산하여 실내의 습도를 자동으로 조절하고, 실내의 음식냄새, 담배냄새 등 기타 유해한 냄새를 신속히 흡수하여 주변을 항시 쾌적하게 하며, 피부건조증과 손상된 피부장벽을 개선시키는데 도움을 주어 아토피 피부염에도 탁월한 효능을 갖는다.At this time, by injecting ocher powder when preparing the coating composition for flame retardant and water-repellent, the indoor air is purified by the ocher component, which is beneficial to the human body. It increases the body's capillaries, activates blood circulation, enhances metabolism, increases tissue regeneration, and absorbs moisture when there is a lot of moisture in the room, and then releases moisture when it dries. It automatically adjusts, quickly absorbs indoor odors and other harmful odors to keep the surroundings pleasant all the time, and helps to improve skin dryness and damaged skin barriers.

기타 실시예들의 구체적인 사항들은 상세한 설명에 포함되어 있다.Specific details of other embodiments are included in the detailed description.

본 발명의 이점 및 특징, 그리고 그것들을 달성하는 방법은 상세하게 후술되어 있는 실시예들을 참조하면 명확해질 것이다.Advantages and features of the present invention and methods for achieving them will be apparent with reference to the embodiments described below in detail.

그러나 본 발명은 이하에서 개시되는 실시예들에 한정되는 것이 아니라 서로 다른 다양한 형태로 구현될 수 있으며, 단지 본 실시예들은 본 발명의 개시가 완전하도록 하고, 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자에게 발명의 범주를 완전하게 알려주기 위해 제공되는 것이며, 본 발명은 청구항의 범주에 의해 정의될 뿐이다. However, the present invention is not limited to the embodiments disclosed below, but can be implemented in various different forms, and only the embodiments make the disclosure of the present invention complete, and the general knowledge in the art to which the present invention belongs. It is provided to fully inform the person having the scope of the invention, which is defined only by the scope of the claims.

본 발명의 바람직한 실시예에 따른 친환경 방염제를 이용한 가구 제조 방법은 제일인산암모늄, 붕산, 수산화나트륨 및 물을 혼합하여 제조한 방염제 조성물과 피톤치드, 은나노 물질 및 겨우살이나무 열수추출물을 혼합한 혼합액을 혼합하여 제조한 제1조성물을 목질재료에 분사한 후 건조하여 가구를 제조한다.Furniture manufacturing method using an eco-friendly flame retardant according to a preferred embodiment of the present invention by mixing a flame retardant composition prepared by mixing the first ammonium phosphate, boric acid, sodium hydroxide and water and a mixture of phytoncide, silver nano material and mistletoe hot water extract The manufactured first composition is sprayed onto wood materials and dried to manufacture furniture.

이때, 상기 제1조성물은 제일인산암모늄 11 내지 25 중량부와 붕산 0.1 내지 3 중량부와 수산화나트륨 1 내지 7 중량부와 피톤치드 5 내지 20 중량부와 은나노 5 내지 20 중량부 및 겨우살이나무 열수추출물 5 내지 20 중량부가 포함되고, 나머지는 물이 포함되어 혼합 제조된다. At this time, the first composition is 11 to 25 parts by weight of ammonium phosphate, 0.1 to 3 parts by weight of boric acid, 1 to 7 parts by weight of sodium hydroxide, 5 to 20 parts by weight of phytoncide, 5 to 20 parts by weight of silver nano and mistletoe hot water extract 5 To 20 parts by weight, the remainder is mixed with water to prepare.

여기서, 상기 겨우살이나무 열수추출물은 건조된 겨우살이나무 절편에 물을 10배 중량만큼 첨가하고 300℃로 가열한 후, 끓기 시작하면 200℃의 온도로 낮춰 첨가된 물이 50%정도 증발될 때까지 우려냄으로써 겨우살이나무 열수추출물을 제조한다. 즉, 첨가된 물이 50 내지 60 중량% 증발될 때라 함은 첨가된 물이 50ℓ인 경우 25ℓ 정도로 줄어들 때까지 증발시킴을 의미하고 소요되는 시간은 약 5~10시간 정도 걸린다. 이와 같은 장시간에 걸친 가열에 의해 더욱 진한 겨우살이나무 열수추출물이 제조된다.Here, the mistletoe hot water extract is added to the dried mistletoe wood by 10 times the weight of water and heated to 300 ℃, when boiling starts to lower the temperature of 200 ℃ until the added water is evaporated about 50% Mistletoe hot water extracts are prepared. That is, when the added water is evaporated 50 to 60% by weight means that the evaporated water is reduced to about 25 L when the added water is 50 L and the time required is about 5 to 10 hours. By heating for a long time, a deeper mistletoe hot water extract is produced.

또한, 상기 피톤치드 및 은나노는 기 공지된 것이므로 이에대한 상세한 제조방법은 생략하기로 한다.In addition, since the phytoncide and silver nano are known, a detailed manufacturing method thereof will be omitted.

상기한 바와 같은 배합비를 통하여 제조된 제1조성물은 방염효과만을 나타내기 위하여 피톤치드 은나노 및 겨우살이나무 열수추출물을 제외하여 사용이 가능하고, 도포방법으로서는 스프레이, 롤러, 침적 등의 기법을 이용하는 것이 바람직하다.The first composition prepared through the compounding ratio as described above may be used except for phytoncide silver nano and mistletoe hot water extract in order to exhibit only a flame retardant effect, and it is preferable to use a technique such as spraying, rollers, or deposition as a coating method. .

또한, 상기 제1조성물을 분사하여 건조한 목질재료에 콜로이달 실리카 및 물을 혼합한 후 질산으로 pH를 조정한 제1혼합용액과 이소프로필알콜, 하이드로프로필 셀룰로스용액, 노말핵산, 메틸이소부틸케톤, 퓸드 실리카(fumed silica), 황토를 혼합한 제2혼합용액을 교반하여 제조한 제2조성물을 더 분사한 후 건조하여 가구를 제조할 수도 있다.In addition, by spraying the first composition, the first mixed solution and the isopropyl alcohol, hydropropyl cellulose solution, normal nucleic acid, methyl isobutyl ketone, the pH of which is adjusted with nitric acid after mixing colloidal silica and water to dry wood material, The second composition prepared by stirring the second mixture solution of fumed silica and ocher may be further sprayed and then dried to manufacture furniture.

이때, 제2조성물은 콜로이달 실리카 10 내지 45 중량부 및 물 55 내지 90 중량부가 포함되어 혼합된 후 질산으로 pH를 3.0 내지 4.5로 조정한 제1혼합용액과, 하이드로프로필 셀룰로스용액 5 내지 8 중량부와 노말핵산 1 내지 7 중량부와 메틸이소부틸케톤 10 내지 20중량부와 퓸드 실리카 0.1 내지 3 중량부 및 황토 5 내지 20중량부가 포함되고, 나머지는 이소프로필알콜이 포함되어 혼합된 제2혼합용액을 혼합한 후 2시간 내지 3시간 동안 교반하여 제조된다.At this time, the second composition includes 10 to 45 parts by weight of colloidal silica and 55 to 90 parts by weight of water, and then mixed with the first mixture solution, the pH of which is adjusted to 3.0 to 4.5 with nitric acid, and 5 to 8 weight of hydropropyl cellulose solution. Part, 1 to 7 parts by weight of normal nucleic acid, 10 to 20 parts by weight of methyl isobutyl ketone, 0.1 to 3 parts by weight of fumed silica and 5 to 20 parts by weight of ocher, and the second mixture is mixed with isopropyl alcohol. The solution is prepared by stirring for 2 to 3 hours after mixing.

또한, 본 발명은 제1조성물을 분사하여 건조한 목질재료를 사용하여 방염 기능이 있는 가구를 제작할 수도 있지만, 여기에 난연 및 발수 기능이 있는 가구를 제작하기 위해 상기 제2조성물을 더 분사하여 건조한 목질재료를 이용하여 가구를 제작할 수도 있다.
In addition, the present invention may be a furniture having a flame retardant function using a dry wood material by spraying the first composition, but the wood is further sprayed by the second composition to produce a furniture having a flame retardant and water-repellent function You can also make furniture using materials.

실험예Experimental Example : 제1조성물 및 제2조성물의 제조 비율에 따른 방염, 난연 및 : Flame retardant, flame retardant and 발수Water repellent 성능 비교 Performance Comparison

실험예
성분Experimental Example
ingredient 실험 예 1Experimental Example 1 실험 예 2Experimental Example 2 실험 예 3Experimental Example 3 제일인산암모늄Ammonium Phosphate 10 중량부10 parts by weight 19 중량부19 parts by weight 26 중량부26 parts by weight 붕산Boric acid 0.1 중량부0.1 parts by weight 0.1 중량부0.1 parts by weight 0.1 중량부0.1 parts by weight 수산화나트륨Sodium hydroxide 1 중량부1 part by weight 1 중량부1 part by weight 1 중량부1 part by weight 물water 나머지Remainder 나머지Remainder 나머지Remainder 방염 성능Flameproof performance 나쁨Bad 매우 우수Very good 보통usually

즉, 제일인산암모늄의 양이 10중량부 이하이면 충분한 방염성능을 기대하기 어렵고, 26중량부 이상이면 도장 후 표면에 석출되므로, 제일인산암모늄은 19중량부인 것이 가장 바람직하다.
That is, if the amount of ammonium monophosphate is 10 parts by weight or less, it is difficult to expect sufficient flame retardant performance, and if it is 26 parts by weight or more, it is precipitated on the surface after coating, so that ammonium monophosphate is most preferably 19 parts by weight.

실험예
성분 Experimental Example
ingredient 실험 예 1Experimental Example 1 실험 예 2Experimental Example 2 실험 예 3Experimental Example 3 콜로이달 실리카Colloidal silica 50 중량부50 parts by weight 15 중량부15 parts by weight 9 중량부9 parts by weight 물water 50 중량부50 parts by weight 85 중량부85 parts by weight 91 중량부91 parts by weight 난연 및 Flame retardant and 발수Water repellent 성능 Performance 나쁨Bad 매우 우수Very good 보통usually

즉, 콜로이달 실리카의 함량이 9중량부 이하이면 건조속도가 감소되며, 50중량부 이상이면 내수성이 감소된다.
That is, when the content of colloidal silica is 9 parts by weight or less, the drying rate is reduced, and when 50 parts by weight or more, the water resistance is reduced.

실시예Example : [표 1] 내지 [표 2] [Table 1] to [Table 2] 에서의In 실험 예 2에 의한  By Experimental Example 2 목질재료Wood materials 제조 방법 Manufacturing method

제1조성물은 제일인산암모늄, 붕산, 수산화나트륨 및 물을 혼합하여 제조한 방염제 조성물과, 피톤치드, 은나노 물질 및 겨우살이나무 열수추출물을 혼합한 혼합액을 혼합하여 제조한다.The first composition is prepared by mixing a flame retardant composition prepared by mixing ammonium phosphate, boric acid, sodium hydroxide and water, and a mixed solution of phytoncide, silver nano material and mistletoe hot water extract.

위 제1조성물의 조성 비율은 제일인산암모늄 19중량부, 붕산 0.1중량부, 수산화나트륨 1중량부, 물 49.9중량부, 피톤치드 10중량부, 은나노 10중량부, 겨우살이나무 열수추출물 10중량부로 한다.
The composition ratio of the first composition is 19 parts by weight of ammonium phosphate, 0.1 parts by weight of boric acid, 1 part by weight of sodium hydroxide, 49.9 parts by weight of water, 10 parts by weight of phytoncide, 10 parts by weight of silver nano, and 10 parts by weight of mistletoe hot water extract.

제2조성물은 콜로이달 실리카와 물을 혼한합 후 질산으로 pH를 조정하여 제조한 제1혼합용액과, 이소프로필알콜, 하이드로프로필 셀룰로스용액, 노말핵산, 메틸이소부틸케톤, 퓸드 실리카, 황토를 혼합한 제2혼합용액을 혼합한 후 약 2시간반 동안 교반하여 반응시켜 제조된 제품을 사용한다.The second composition is a mixture of colloidal silica and water mixed with a first mixture solution prepared by adjusting the pH with nitric acid, isopropyl alcohol, hydropropyl cellulose solution, normal nucleic acid, methyl isobutyl ketone, fumed silica, ocher One second mixed solution is mixed and then stirred for about two and a half hours to use a product prepared by reacting.

여기서, 제1혼합용액의 조성 비율은 콜로이달 실리카(HS40, DUPONT) 15중량부, 물 85중량부의 비율로 혼합한 후 질산(시약급, 덕산화학)으로 pH를 3.5로 조정하여 제조한다.Herein, the composition ratio of the first mixed solution is prepared by mixing 15 parts by weight of colloidal silica (HS40, DUPONT) and 85 parts by weight of water, and then adjusting the pH to 3.5 with nitric acid (reagent, Duksan Chemical).

또한, 제2혼합용액의 조성 비율은 이소프로필알콜 63중량부, 하이드로프로필 셀룰로스용액(고형분 1.5%, 이소프로필 알콜 용매사용) 7중량부, 노말핵산 3중량부, 메틸이소부틸케톤 15중량부, 퓸드 실리카(fumed silica) 2중량부, 황토 10중량부로 하여 제조한다.
The composition ratio of the second mixed solution is 63 parts by weight of isopropyl alcohol, 7 parts by weight of hydropropyl cellulose solution (1.5% solids, isopropyl alcohol solvent), 3 parts by weight of normal nucleic acid, 15 parts by weight of methyl isobutyl ketone, 2 parts by weight of fumed silica and 10 parts by weight of ocher are prepared.

위와 같이 제조된 제1조성물 및 제2조성물을 이용한 방염 및 난연?발수 코팅처리공정으로서는 1차로 가구재료(무늬목, 목질재료 등) 표면에 제1조성물을 분사한 뒤 30 내지 80℃의 온도범위에서 1 내지 7분 정도 건조시킨다.Flame-retardant, flame-retardant and water-repellent coating process using the first composition and the second composition prepared as described above in the temperature range of 30 to 80 ℃ after spraying the first composition on the surface of the furniture material (wood veneer, wood material, etc.) first Dry for 1 to 7 minutes.

1차 분사에 의해 방염성이 부여된 가구재료에 2차로 제2조성물을 분사한 뒤 40 내지 120℃범위에서 약 5 내지 25분 동안 건조시키면 방염성과 더불어 난연성?및 발수성의 특징을 갖는 가구재료가 되는데 이를 이용하여 가구 제품의 제조를 완성하는 것이다.After spraying the second composition on the furniture material given flame retardancy by the first spraying and drying it for about 5 to 25 minutes in the range of 40 to 120 ° C, it becomes a furniture material having the characteristics of flame retardancy and flame retardancy and water repellency. Using this to complete the manufacture of furniture products.

상기 방염성, 난연성 및 발수성의 특징을 갖는 가구재료는 가구 조립 단계 전 목질의 상태에서 제1조성물을 분사함으로써 방염처리가 되는 동시에 친환경적 효능을 발휘할 뿐 아니라, 제2조성물을 더 분사하여 코팅작업을 함으로써 최종적으로 방염, 난연 및 발수처리가 된 재료를 이용하여 가구를 조립하여 옷장, 침대, 책상, 식탁 등의 다양한 목질의 가구제품에 적용될 수 있다.
Furniture material having the characteristics of flame retardant, flame retardant and water repellent is not only flame retardant treatment by spraying the first composition in the state of wood before the furniture assembly step, but also to show the eco-friendly effect, by spraying the second composition further by coating Finally, the furniture is assembled using flame retardant, flame retardant, and water repellent materials, and can be applied to various wooden furniture products such as wardrobes, beds, desks, and dining tables.

본 발명이 속하는 기술분야의 통상의 지식을 가진 자는 본 발명이 그 기술적 사상이나 필수적인 특징을 변경하지 않고서 다른 구체적인 형태로 실시될 수 있다는 것을 이해할 수 있을 것이다. 그러므로 이상에서 기술한 실시예들은 모든 면에서 예시적인 것이며 한정적이 아닌 것으로 이해해야만 한다. 본 발명의 범위는 상기 상세한 설명보다는 후술하는 특허청구의 범위에 의하여 나타내어지며, 특허청구의 범위의 의미 및 범위 그리고 그 균등 개념으로부터 도출되는 모든 변경 또는 변형된 형태가 본 발명의 범위에 포함되는 것으로 해석되어야 한다.Those skilled in the art will appreciate that the present invention can be embodied in other specific forms without changing the technical spirit or essential features of the present invention. It is therefore to be understood that the above-described embodiments are illustrative in all aspects and not restrictive. The scope of the present invention is indicated by the scope of the following claims rather than the detailed description, and all changes or modifications derived from the meaning and scope of the claims and the equivalent concept are included in the scope of the present invention. Should be interpreted.

Claims (5)

제일인산암모늄, 붕산, 수산화나트륨 및 물을 혼합하여 제조한 방염제 조성물과, 피톤치드, 은나노 물질 및 겨우살이나무 열수추출물을 혼합한 혼합 조성물을 혼합하여 제조한 제1조성물을 목질재료에 분사한 후 건조하여 가구를 제조하는 것을 특징으로 하는 친환경 방염제를 이용한 가구 제조 방법.Spraying the first composition prepared by mixing a flame retardant composition prepared by mixing ammonium phosphate, boric acid, sodium hydroxide and water, and a mixed composition obtained by mixing phytoncide, silver nano material and mistletoe hot water extract on wood materials, and then drying. Furniture manufacturing method using an eco-friendly flame retardant, characterized in that for producing furniture. 제 1항에 있어서,
콜로이달 실리카 및 물을 혼합한 후 질산으로 pH를 조정한 제1혼합용액과,
이소프로필알콜, 하이드로프로필 셀룰로스용액, 노말핵산, 메틸이소부틸케톤, 퓸드 실리카 및 황토를 혼합한 제2혼합용액을 교반하여 제조한 제2조성물을, 제1조성물을 분사하여 건조한 목질재료에 더 분사한 후 건조하여 가구를 제조하는 것을 특징으로 하는 친환경 방염제를 이용한 가구 제조 방법.The method of claim 1,
A first mixed solution in which pH is adjusted with nitric acid after mixing colloidal silica and water;
A second composition prepared by stirring isopropyl alcohol, a hydropropyl cellulose solution, a second mixed solution of normal nucleic acid, methyl isobutyl ketone, fumed silica, and ocher is further sprayed onto the dried wood material by spraying the first composition. Method of manufacturing furniture using an environmentally friendly flame retardant, characterized in that after drying to produce furniture. 제 1항에 있어서,
겨우살이나무 열수추출물은 건조된 겨우살이나무 절편에 물을 10배 중량만큼 첨가하고 300℃로 가열한 후, 끓기 시작하면 200℃의 온도로 낮춰 첨가된 물이 50 내지 60 중량% 증발될 때까지 우려냄으로써 제조되는 것을 특징으로 하는 친환경 방염제를 이용한 가구 제조 방법.The method of claim 1,
Mistletoe hot water extract is added to the dried mistletoe wood by 10 times the weight of water, heated to 300 ℃, and then boiled down to a temperature of 200 ℃ by boiling until the added water is evaporated 50 to 60% by weight Furniture manufacturing method using an environmentally friendly flame retardant, characterized in that the production. 제 1항에 있어서,
제1조성물은,
제일인산암모늄 11 내지 25 중량부와 붕산 0.1 내지 3 중량부와 수산화나트륨 1 내지 7 중량부와 피톤치드 5 내지 20 중량부와 은나노 5 내지 20 중량부 및 겨우살이나무 열수추출물 5 내지 20 중량부가 포함되는 것을 특징으로 하는 친환경 방염제를 이용한 가구 제조 방법.The method of claim 1,
The first composition,
11 to 25 parts by weight of ammonium phosphate, 0.1 to 3 parts by weight of boric acid, 1 to 7 parts by weight of sodium hydroxide, 5 to 20 parts by weight of phytoncide, 5 to 20 parts by weight of silver nano and 5 to 20 parts by weight of mistletoe hot water extract Furniture manufacturing method using an eco-friendly flame retardant characterized in that. 제 2항에 있어서,
제2조성물은,
콜로이달 실리카 10 내지 45 중량부 및 물 55 내지 90 중량부가 포함되어 혼합된 후 질산으로 pH를 3.0 내지 4.5로 조정한 제1혼합용액과,
하이드로프로필 셀룰로스용액 5 내지 8 중량부와 노말핵산 1 내지 7 중량부와 메틸이소부틸케톤 10 내지 20중량부와 퓸드 실리카 0.1 내지 3 중량부 및 황토 5 내지 20중량부가 포함된 제2혼합용액을 혼합한 후 2시간 내지 3시간 동안 교반하여 제조하는 것을 특징으로 하는 친환경 방염제를 이용한 가구 제조 방법.The method of claim 2,
The second composition,
10 to 45 parts by weight of colloidal silica and 55 to 90 parts by weight of water are mixed and mixed with a first mixed solution adjusted to pH 3.0 to 4.5 with nitric acid,
Mixing a second mixed solution containing 5 to 8 parts by weight of hydropropyl cellulose solution, 1 to 7 parts by weight of normal nucleic acid, 10 to 20 parts by weight of methyl isobutyl ketone, 0.1 to 3 parts by weight of fumed silica and 5 to 20 parts by weight of ocher Method of manufacturing furniture using an environmentally friendly flame retardant, characterized in that by stirring for 2 hours to 3 hours.
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CN104400849A (en) * 2014-10-16 2015-03-11 阜南县永兴工艺品有限公司 Long-acting soaking solution containing nano silver and used for modification of bamboo strip and use method thereof
KR102517137B1 (en) * 2022-10-18 2023-04-04 전북대학교산학협력단 Silicified wood with flame retardancy and method of manufacturing the same

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KR101932004B1 (en) * 2017-06-30 2018-12-24 주식회사 승화가구 Method for manufacturing of wood panel for eco-friendly furniture and furniture using the same
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CN104400849A (en) * 2014-10-16 2015-03-11 阜南县永兴工艺品有限公司 Long-acting soaking solution containing nano silver and used for modification of bamboo strip and use method thereof
KR102517137B1 (en) * 2022-10-18 2023-04-04 전북대학교산학협력단 Silicified wood with flame retardancy and method of manufacturing the same

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