KR20100138933A - 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 - Google Patents

공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 Download PDF

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KR20100138933A
KR20100138933A KR1020107020746A KR20107020746A KR20100138933A KR 20100138933 A KR20100138933 A KR 20100138933A KR 1020107020746 A KR1020107020746 A KR 1020107020746A KR 20107020746 A KR20107020746 A KR 20107020746A KR 20100138933 A KR20100138933 A KR 20100138933A
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South Korea
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hfc
composition
distillation
entrainer
mixture
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Korean (ko)
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제프리 피. 크납
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이 아이 듀폰 디 네모아 앤드 캄파니
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
KR1020107020746A 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 Ceased KR20100138933A (ko)

Applications Claiming Priority (2)

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US3035908P 2008-02-21 2008-02-21
US61/030,359 2008-02-21

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KR1020167027807A Division KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

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KR20100138933A true KR20100138933A (ko) 2010-12-31

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KR1020107020746A Ceased KR20100138933A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020197003238A Ceased KR20190016124A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020167027807A Active KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020187007744A Active KR101946378B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

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KR1020197003238A Ceased KR20190016124A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020167027807A Active KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020187007744A Active KR101946378B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

Country Status (10)

Country Link
EP (1) EP2247561B1 (https=)
JP (1) JP2011513227A (https=)
KR (4) KR20100138933A (https=)
CN (1) CN101952230B (https=)
BR (1) BRPI0906014A2 (https=)
CA (1) CA2713086A1 (https=)
ES (1) ES2463670T3 (https=)
MX (1) MX2010009080A (https=)
RU (1) RU2476416C2 (https=)
WO (1) WO2009105512A1 (https=)

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KR20140117682A (ko) * 2012-02-03 2014-10-07 아르끄마 프랑스 2,3,3,3-테트라플루오로프로펜 제조방법
CN104100687A (zh) * 2013-04-09 2014-10-15 喜来健株式会社 温热治疗仪用自动张力调节装置
KR20200098688A (ko) * 2018-01-08 2020-08-20 허니웰 인터내셔날 인코포레이티드 1234yf로의 244bb 탈염화수소화 동안 불순물의 형성을 감소시키는 시스템 및 방법

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US8766020B2 (en) * 2008-07-31 2014-07-01 Honeywell International Inc. Process for producing 2,3,3,3-tetrafluoropropene
JP5439177B2 (ja) 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法
EP4328213A3 (en) * 2006-10-27 2024-04-03 Honeywell International Inc. A high purity 2,3,3,3-tetrafluoropropene
WO2011052559A1 (ja) * 2009-10-27 2011-05-05 昭和電工株式会社 フッ素含有化合物の精製方法
KR101458679B1 (ko) * 2009-11-10 2014-11-05 다이킨 고교 가부시키가이샤 2,3,3,3-테트라플루오로프로펜의 정제 방법
WO2011099604A2 (en) * 2010-02-12 2011-08-18 Daikin Industries, Ltd. Process for producing fluorine-containing alkene
WO2012011609A1 (en) 2010-07-23 2012-01-26 Daikin Industries, Ltd. Purification method of 2,3,3,3-tetrafluoropropene
US8518293B2 (en) 2010-09-03 2013-08-27 Honeywell International Inc. 1,3,3,3-tetrafluoropropene process azeotropes with HF
FR2977584B1 (fr) * 2011-07-08 2014-12-05 Arkema France Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique
WO2013154059A1 (ja) * 2012-04-09 2013-10-17 旭硝子株式会社 共沸または共沸様組成物、および２，３，３，３－テトラフルオロプロペンまたはクロロメタンの製造方法
JP6011008B2 (ja) * 2012-04-27 2016-10-19 旭硝子株式会社 共沸または共沸様組成物、および２，３，３，３−テトラフルオロプロペンまたはヘキサフルオロプロペンの製造方法
FR3000093B1 (fr) * 2012-12-26 2015-07-17 Arkema France Composition azeotropique ou quasi-azeotropique de chloromethane
FR3000096B1 (fr) 2012-12-26 2015-02-20 Arkema France Composition comprenant du 2,3,3,3-tetrafluoropropene
FR3003565B1 (fr) * 2013-03-20 2018-06-29 Arkema France Composition comprenant hf et 2,3,3,3-tetrafluoropropene
FR3023286B1 (fr) * 2014-07-02 2018-02-16 Arkema France Procede de fabrication de tetrafluoropropene
EP3141587B1 (en) 2015-02-19 2019-05-08 Daikin Industries, Ltd. Composition containing mixture of fluorinated hydrocarbons, and method for producing same
GB2540427B (en) 2015-07-17 2017-07-19 Mexichem Fluor Sa De Cv Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf)
FR3046165B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene
JP2017122063A (ja) * 2016-01-06 2017-07-13 ダイキン工業株式会社 ２，３，３，３−テトラフルオロプロペンの製造方法
JP6485493B2 (ja) * 2017-06-16 2019-03-20 ダイキン工業株式会社 ペンタフルオロプロパンと水とを含む共沸又は共沸様組成物、並びにペンタフルオロプロパンの製造方法
FR3077572B1 (fr) * 2018-02-05 2021-10-08 Arkema France Composition azeotropique ou quasi-azeotropique ternaire comprenant hf, 2,3,3,3-tetrafluoropropene et 1,1,1,2,2,-pentafluoropropane.
EP3861083B1 (en) * 2018-10-04 2024-03-20 The Chemours Company FC, LLC Azeotropic composition of hfo-1234yf and ethane
JP6863489B2 (ja) * 2019-01-28 2021-04-21 ダイキン工業株式会社 １，２−ジフルオロエチレン又は１，１，２−トリフルオロエチレンと、フッ化水素とを含む共沸様組成物
CN114940888B (zh) * 2022-06-29 2023-02-28 珠海格力电器股份有限公司 制冷剂及其制备方法

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US4975156A (en) * 1989-05-04 1990-12-04 Atochem North America, Inc. Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof
IT1256631B (it) * 1992-12-10 1995-12-12 Ausimont Spa Procedimento per la separazione di hf da sue miscele con gli idroclorofluorcarburi 123 e/o 124
WO1999020585A1 (en) * 1997-10-17 1999-04-29 E.I. Du Pont De Nemours And Company Separating 1,1,1,3,3-pentafluoropropane from hydrogen fluoride
US6521803B1 (en) * 1998-12-18 2003-02-18 Solvay (Societe Anonyme) Method for separating a mixture comprising at least an hydrofluoroalkane and hydrogen fluoride, methods for preparing a hydrofluoroalkane and azeotropic compositions
WO2002059067A1 (en) * 2001-01-25 2002-08-01 Honeywell International, Inc. Process for the manufacture of fluorocarbons
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US7897823B2 (en) * 2004-10-29 2011-03-01 E. I. Du Pont De Nemours And Company Process for production of azeotrope compositions comprising hydrofluoroolefin and hydrogen fluoride and uses of said azeotrope compositions in separation processes
US20060116538A1 (en) * 2004-10-29 2006-06-01 Ralph Newton Miller Azeotrope compositions comprising 1,1,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7476771B2 (en) * 2005-11-01 2009-01-13 E.I. Du Pont De Nemours + Company Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7423188B2 (en) * 2005-11-01 2008-09-09 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising E-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7388117B2 (en) * 2005-11-01 2008-06-17 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7803975B2 (en) * 2006-07-13 2010-09-28 E.I. Du Pont De Nemours And Company Process for separating a fluoroolefin from HF by liquid-liquid extraction
GB0614927D0 (en) * 2006-07-27 2006-09-06 Ineos Fluor Holdings Ltd Separation process
JP5439177B2 (ja) * 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20140117682A (ko) * 2012-02-03 2014-10-07 아르끄마 프랑스 2,3,3,3-테트라플루오로프로펜 제조방법
CN104100687A (zh) * 2013-04-09 2014-10-15 喜来健株式会社 温热治疗仪用自动张力调节装置
KR20200098688A (ko) * 2018-01-08 2020-08-20 허니웰 인터내셔날 인코포레이티드 1234yf로의 244bb 탈염화수소화 동안 불순물의 형성을 감소시키는 시스템 및 방법

Also Published As

Publication number Publication date
KR20180031811A (ko) 2018-03-28
WO2009105512A1 (en) 2009-08-27
EP2247561B1 (en) 2014-03-26
MX2010009080A (es) 2010-09-07
KR101842380B1 (ko) 2018-03-26
CA2713086A1 (en) 2009-08-27
BRPI0906014A2 (pt) 2015-06-30
EP2247561A1 (en) 2010-11-10
KR101946378B1 (ko) 2019-02-12
KR20190016124A (ko) 2019-02-15
JP2011513227A (ja) 2011-04-28
CN101952230B (zh) 2015-07-22
ES2463670T3 (es) 2014-05-28
RU2010138783A (ru) 2012-03-27
RU2476416C2 (ru) 2013-02-27
KR20160120804A (ko) 2016-10-18
CN101952230A (zh) 2011-01-19

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