KR20100138933A - 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 - Google Patents

공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 Download PDF

Info

Publication number
KR20100138933A
KR20100138933A KR1020107020746A KR20107020746A KR20100138933A KR 20100138933 A KR20100138933 A KR 20100138933A KR 1020107020746 A KR1020107020746 A KR 1020107020746A KR 20107020746 A KR20107020746 A KR 20107020746A KR 20100138933 A KR20100138933 A KR 20100138933A
Authority
KR
South Korea
Prior art keywords
hfc
composition
distillation
entrainer
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
KR1020107020746A
Other languages
English (en)
Korean (ko)
Inventor
제프리 피. 크납
Original Assignee
이 아이 듀폰 디 네모아 앤드 캄파니
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 이 아이 듀폰 디 네모아 앤드 캄파니 filed Critical 이 아이 듀폰 디 네모아 앤드 캄파니
Publication of KR20100138933A publication Critical patent/KR20100138933A/ko
Ceased legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
KR1020107020746A 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법 Ceased KR20100138933A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US3035908P 2008-02-21 2008-02-21
US61/030,359 2008-02-21

Related Child Applications (1)

Application Number Title Priority Date Filing Date
KR1020167027807A Division KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

Publications (1)

Publication Number Publication Date
KR20100138933A true KR20100138933A (ko) 2010-12-31

Family

ID=40513940

Family Applications (4)

Application Number Title Priority Date Filing Date
KR1020107020746A Ceased KR20100138933A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020197003238A Ceased KR20190016124A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020167027807A Active KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020187007744A Active KR101946378B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

Family Applications After (3)

Application Number Title Priority Date Filing Date
KR1020197003238A Ceased KR20190016124A (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020167027807A Active KR101842380B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR1020187007744A Active KR101946378B1 (ko) 2008-02-21 2009-02-19 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법

Country Status (10)

Country Link
EP (1) EP2247561B1 (enExample)
JP (1) JP2011513227A (enExample)
KR (4) KR20100138933A (enExample)
CN (1) CN101952230B (enExample)
BR (1) BRPI0906014A2 (enExample)
CA (1) CA2713086A1 (enExample)
ES (1) ES2463670T3 (enExample)
MX (1) MX2010009080A (enExample)
RU (1) RU2476416C2 (enExample)
WO (1) WO2009105512A1 (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20140117682A (ko) * 2012-02-03 2014-10-07 아르끄마 프랑스 2,3,3,3-테트라플루오로프로펜 제조방법
CN104100687A (zh) * 2013-04-09 2014-10-15 喜来健株式会社 温热治疗仪用自动张力调节装置
KR20200098688A (ko) * 2018-01-08 2020-08-20 허니웰 인터내셔날 인코포레이티드 1234yf로의 244bb 탈염화수소화 동안 불순물의 형성을 감소시키는 시스템 및 방법

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8766020B2 (en) * 2008-07-31 2014-07-01 Honeywell International Inc. Process for producing 2,3,3,3-tetrafluoropropene
JP5439177B2 (ja) 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法
EP4328213A3 (en) * 2006-10-27 2024-04-03 Honeywell International Inc. A high purity 2,3,3,3-tetrafluoropropene
WO2011052559A1 (ja) * 2009-10-27 2011-05-05 昭和電工株式会社 フッ素含有化合物の精製方法
KR101458679B1 (ko) * 2009-11-10 2014-11-05 다이킨 고교 가부시키가이샤 2,3,3,3-테트라플루오로프로펜의 정제 방법
WO2011099604A2 (en) * 2010-02-12 2011-08-18 Daikin Industries, Ltd. Process for producing fluorine-containing alkene
WO2012011609A1 (en) 2010-07-23 2012-01-26 Daikin Industries, Ltd. Purification method of 2,3,3,3-tetrafluoropropene
US8518293B2 (en) 2010-09-03 2013-08-27 Honeywell International Inc. 1,3,3,3-tetrafluoropropene process azeotropes with HF
FR2977584B1 (fr) * 2011-07-08 2014-12-05 Arkema France Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique
WO2013154059A1 (ja) * 2012-04-09 2013-10-17 旭硝子株式会社 共沸または共沸様組成物、および２，３，３，３－テトラフルオロプロペンまたはクロロメタンの製造方法
JP6011008B2 (ja) * 2012-04-27 2016-10-19 旭硝子株式会社 共沸または共沸様組成物、および２，３，３，３−テトラフルオロプロペンまたはヘキサフルオロプロペンの製造方法
FR3000093B1 (fr) * 2012-12-26 2015-07-17 Arkema France Composition azeotropique ou quasi-azeotropique de chloromethane
FR3000096B1 (fr) 2012-12-26 2015-02-20 Arkema France Composition comprenant du 2,3,3,3-tetrafluoropropene
FR3003565B1 (fr) * 2013-03-20 2018-06-29 Arkema France Composition comprenant hf et 2,3,3,3-tetrafluoropropene
FR3023286B1 (fr) * 2014-07-02 2018-02-16 Arkema France Procede de fabrication de tetrafluoropropene
EP3141587B1 (en) 2015-02-19 2019-05-08 Daikin Industries, Ltd. Composition containing mixture of fluorinated hydrocarbons, and method for producing same
GB2540427B (en) 2015-07-17 2017-07-19 Mexichem Fluor Sa De Cv Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf)
FR3046165B1 (fr) * 2015-12-23 2019-12-13 Arkema France Procede de production et de purification du 2,3,3,3-tetrafluoro-1-propene
JP2017122063A (ja) * 2016-01-06 2017-07-13 ダイキン工業株式会社 ２，３，３，３−テトラフルオロプロペンの製造方法
JP6485493B2 (ja) * 2017-06-16 2019-03-20 ダイキン工業株式会社 ペンタフルオロプロパンと水とを含む共沸又は共沸様組成物、並びにペンタフルオロプロパンの製造方法
FR3077572B1 (fr) * 2018-02-05 2021-10-08 Arkema France Composition azeotropique ou quasi-azeotropique ternaire comprenant hf, 2,3,3,3-tetrafluoropropene et 1,1,1,2,2,-pentafluoropropane.
EP3861083B1 (en) * 2018-10-04 2024-03-20 The Chemours Company FC, LLC Azeotropic composition of hfo-1234yf and ethane
JP6863489B2 (ja) * 2019-01-28 2021-04-21 ダイキン工業株式会社 １，２−ジフルオロエチレン又は１，１，２−トリフルオロエチレンと、フッ化水素とを含む共沸様組成物
CN114940888B (zh) * 2022-06-29 2023-02-28 珠海格力电器股份有限公司 制冷剂及其制备方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53116314A (en) * 1977-03-19 1978-10-11 Mitsui Petrochem Ind Ltd Separation of acetic acid and water
US4975156A (en) * 1989-05-04 1990-12-04 Atochem North America, Inc. Process for the separation of hydrogen fluoride, 1,1-dichloro-1-fluoroethane and 1-chloro-1,1-difluoroethane from liquid mixtures thereof
IT1256631B (it) * 1992-12-10 1995-12-12 Ausimont Spa Procedimento per la separazione di hf da sue miscele con gli idroclorofluorcarburi 123 e/o 124
WO1999020585A1 (en) * 1997-10-17 1999-04-29 E.I. Du Pont De Nemours And Company Separating 1,1,1,3,3-pentafluoropropane from hydrogen fluoride
US6521803B1 (en) * 1998-12-18 2003-02-18 Solvay (Societe Anonyme) Method for separating a mixture comprising at least an hydrofluoroalkane and hydrogen fluoride, methods for preparing a hydrofluoroalkane and azeotropic compositions
WO2002059067A1 (en) * 2001-01-25 2002-08-01 Honeywell International, Inc. Process for the manufacture of fluorocarbons
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US7897823B2 (en) * 2004-10-29 2011-03-01 E. I. Du Pont De Nemours And Company Process for production of azeotrope compositions comprising hydrofluoroolefin and hydrogen fluoride and uses of said azeotrope compositions in separation processes
US20060116538A1 (en) * 2004-10-29 2006-06-01 Ralph Newton Miller Azeotrope compositions comprising 1,1,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7476771B2 (en) * 2005-11-01 2009-01-13 E.I. Du Pont De Nemours + Company Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7423188B2 (en) * 2005-11-01 2008-09-09 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising E-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US7388117B2 (en) * 2005-11-01 2008-06-17 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7803975B2 (en) * 2006-07-13 2010-09-28 E.I. Du Pont De Nemours And Company Process for separating a fluoroolefin from HF by liquid-liquid extraction
GB0614927D0 (en) * 2006-07-27 2006-09-06 Ineos Fluor Holdings Ltd Separation process
JP5439177B2 (ja) * 2006-08-24 2014-03-12 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 共沸蒸留によってフッ化水素からフルオロオレフィンを分離する方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20140117682A (ko) * 2012-02-03 2014-10-07 아르끄마 프랑스 2,3,3,3-테트라플루오로프로펜 제조방법
CN104100687A (zh) * 2013-04-09 2014-10-15 喜来健株式会社 温热治疗仪用自动张力调节装置
KR20200098688A (ko) * 2018-01-08 2020-08-20 허니웰 인터내셔날 인코포레이티드 1234yf로의 244bb 탈염화수소화 동안 불순물의 형성을 감소시키는 시스템 및 방법

Also Published As

Publication number Publication date
KR20180031811A (ko) 2018-03-28
WO2009105512A1 (en) 2009-08-27
EP2247561B1 (en) 2014-03-26
MX2010009080A (es) 2010-09-07
KR101842380B1 (ko) 2018-03-26
CA2713086A1 (en) 2009-08-27
BRPI0906014A2 (pt) 2015-06-30
EP2247561A1 (en) 2010-11-10
KR101946378B1 (ko) 2019-02-12
KR20190016124A (ko) 2019-02-15
JP2011513227A (ja) 2011-04-28
CN101952230B (zh) 2015-07-22
ES2463670T3 (es) 2014-05-28
RU2010138783A (ru) 2012-03-27
RU2476416C2 (ru) 2013-02-27
KR20160120804A (ko) 2016-10-18
CN101952230A (zh) 2011-01-19

Similar Documents

Publication Publication Date Title
KR101946378B1 (ko) 공비 증류에 의한 플루오르화수소로부터의 2,3,3,3-테트라플루오로프로펜의 분리 방법
KR102136117B1 (ko) 공비 증류에 의한 플루오르화수소로부터의 1,3,3,3-테트라플루오로프로펜의 분리 방법
KR102035526B1 (ko) 3,3,3-트라이플루오로프로펜 및 플루오르화수소를 포함하는 공비 조성물 및 이의 분리방법
HK1153186A (en) Processes for separation of 2,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation
HK1153188A (en) Processes for separation of 1,3,3,3-tetrafluoropropene from hydrogen fluoride by azeotropic distillation
HK1152029A (en) Azeotrope compositions comprising 3,3,3-trifluoropropene and hydrogen fluoride and processes for separation thereof

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20100916

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20140206

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20150804

Patent event code: PE09021S01D

E601 Decision to refuse application
PE0601 Decision on rejection of patent

Patent event date: 20160608

Comment text: Decision to Refuse Application

Patent event code: PE06012S01D

Patent event date: 20150804

Comment text: Notification of reason for refusal

Patent event code: PE06011S01I

J201 Request for trial against refusal decision
PJ0201 Trial against decision of rejection

Patent event date: 20160906

Comment text: Request for Trial against Decision on Refusal

Patent event code: PJ02012R01D

Patent event date: 20160608

Comment text: Decision to Refuse Application

Patent event code: PJ02011S01I

Appeal kind category: Appeal against decision to decline refusal

Appeal identifier: 2016101005240

Request date: 20160906

A107 Divisional application of patent
PA0104 Divisional application for international application

Comment text: Divisional Application for International Patent

Patent event code: PA01041R01D

Patent event date: 20161006

J121 Written withdrawal of request for trial
PC1202 Submission of document of withdrawal before decision of registration

Comment text: [Withdrawal of Procedure relating to Patent, etc.] Withdrawal (Abandonment)

Patent event code: PC12021R01D

Patent event date: 20161010

PJ1201 Withdrawal of trial

Patent event code: PJ12011R01D

Patent event date: 20161010

Comment text: Written Withdrawal of Request for Trial

Appeal identifier: 2016101005240

Request date: 20160906

Appeal kind category: Appeal against decision to decline refusal

Decision date: 20161010

WITB Written withdrawal of application