KR20100083448A - Manufacturing method for beauty product of eye cream using caviar extracton - Google Patents

Manufacturing method for beauty product of eye cream using caviar extracton Download PDF

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KR20100083448A
KR20100083448A KR1020090002825A KR20090002825A KR20100083448A KR 20100083448 A KR20100083448 A KR 20100083448A KR 1020090002825 A KR1020090002825 A KR 1020090002825A KR 20090002825 A KR20090002825 A KR 20090002825A KR 20100083448 A KR20100083448 A KR 20100083448A
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caviar
concentrate
extract
eye cream
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한상훈
이강섭
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한상훈
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y5/00—Nanobiotechnology or nanomedicine, e.g. protein engineering or drug delivery
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/413—Nanosized, i.e. having sizes below 100 nm

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  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Zoology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE: A cosmetic product for whitening using caviar extract is provided to improve storage property at room temperature and efficiency and to ensure anti-wrinkle and anti-aging. CONSTITUTION: A method for manufacturing a functional cosmetic product for whitening using caviar extract comprises: a step of adding caviar to solvent(propylene glycol) and extracting at 60°C(±5) for 4-6 hours; a step of maintaining at 30-50°C to concentrate; a step of preparing the concentrate in a nano-emulation form; a step of adding 70-75 weight%, 5-10 weight% of caviar concentrate liquid; 0.1-0.5 weight% of methyl paraben, 0.3-0.5 weight% of disodium EDTA, 1-1.5 weight% of butylenes glycol, 0.2-0.5 weight% of imidazolidinylurea, 2-3 weight% of glycerin, 0.2-0.4 weight% of carbomer, 1.5-2.0 weight% of glyceryl monostearylate, 2-4 weight% of triethanol amine, 1-2 weight% of beewax, and 0.2-0.6 weight% of dimethicone and emulsifying at 70-85°C; a step of mixing the ingredients; a step of filtering with stainless net; and a step of inputting to a bottle.

Description

캐비어 추출물을 이용한 아이크림의 제조 방법{Manufacturing method for beauty product of eye cream using Caviar extracton} Manufacturing method for beauty product of eye cream using Caviar extracton}

본 발명은 미백 기능성 화장품 및 그 제조방법에 관한 것으로, 특히, 캐비어 농축물을 5% 이상 함유하고 호호바오일, 로스힙오일, 스테아릭에씨드, 마카데미아닛오일, 스쿠알렌, 산화방지제, 토코페롤, 하이아루로닉에씨드, 키토산, 상피추출물 등 천연 추출물을 첨가하여 눈가에 탄력을 주는 아이크림의 제조 방법에 관한 것이다.The present invention relates to a whitening functional cosmetics and a method for producing the same, in particular, containing at least 5% caviar concentrate, jojoba oil, lozenges oil, stearic acid, macadamia nitrile oil, squalene, antioxidant, tocopherol, The present invention relates to a method for preparing eye cream that gives elasticity to the eyes by adding natural extracts such as hyaluronic acid, chitosan, and epidermal extract.

본 발명에 의하면 캐비어 추출물과 천연 추출물을 함유하여 피부에 적합한 수분과 영양을 공급하고, 복합 보습성분의 빠르고 지속적인 수분 공급효과로 유수분의 균형이 이루어진다. 또한 캐비어 추출물 중 단백질, 비타민 성분이 생체조직에 적합한 수분과 영양을 공급하므로 지친 피부에 활력을 주어 피부를 정상화시키는 효과를 가져 온다. According to the present invention, the caviar extract and natural extracts are provided to supply moisture and nutrition suitable for the skin, and the balance of oil and moisture is achieved by the fast and continuous water supply effect of the complex moisturizing ingredient. In addition, protein and vitamin components of caviar extract supply moisture and nutrients suitable for biological tissues, thereby rejuvenating tired skin and bringing the effect of normalizing the skin.

본 발명은 캐비어 농축물을 이용한 아이크림과 제조 방법에 관한 것이다. The present invention relates to an eye cream using a caviar concentrate and a method for manufacturing the same.

대한민국 특허 제 10-0475255(2005년 02월 25일)호에 수록한 바와 같이 철갑상어의 알인 캐비어에는 여러 아미노산이 안정적으로 구성되어 있어 세포 친화력이 우수한 것으로 나타나 있다. 또한 상기 특허에서는 캐비어 추출물을 나노좀의 형태로 사용하고 있으나, 본 발명에서는 캐비어의 생리 활성을 극대화시키기 위해 얻어진 추출물을 다시 감압농축하여 이를 고농축화(고형분 50% 이상)한 제품을 생산하였으며, 이를 다시 나노에멀젼 형태로 만들어 원료로 사용하게 된다. 또한 대한민국 특허 10-2008-0123765(2008년 12월 08일 출원)호에서 서술하고 있는바 동 기술을 사용하여 캐비어를 추출 및 농축하여 기본 원료로 사용하고 있음을 밝힌다. As described in Korean Patent No. 10-0475255 (February 25, 2005), the egg-in caviar of sturgeon has been shown to be excellent in cell affinity because of its stable amino acid composition. In addition, the patent uses caviar extract in the form of nanosomes, but in the present invention, the extract obtained in order to maximize the physiological activity of caviar under reduced pressure again to produce a highly concentrated product (more than 50% solids), It is made into a nanoemulsion form and used as a raw material. In addition, as described in the Republic of Korea Patent No. 10-2008-0123765 (December 08, 2008) issued by the same technology, caviar is extracted and concentrated to use as a basic raw material.

본 발명은 고농도 나모에멀젼 캐비어 추출물을 이용한 아이크림과 그 제조 방법에 관한 것이다. The present invention relates to an eye cream using a high concentration namo emulsion caviar extract and a preparation method thereof.

본 발명에서는 종래의 캐비어 추출물을 그대로 사용한 것에서 벗어나 캐비어 추출물을 감압식 방법으로 농축시켜 이를 에멀젼화 한 후 화장품의 원료로 사용하게 되는 것 또한 포함하게 된다. 캐비어 추출물은 고형분이 30% 미만일 경우 상온에서 보존하기 어렵고 쉽게 상할 수 있다. 이를 극복하기 위해 고형분이 50% 이상 되도록 감압 농축하게 되는데 이때 캐비어의 성분이 파괴되지 않도록 하기 위해 저온(30-60℃)에서 농축하게 된다. 또한 본 발명에서는 상기에서 얻어진 고농축 나모에멀젼 캐비어 추출물을 이용하여 눈가에 영양분을 공급하는 아이크림을 만들게 되는데, 캐비어 성분의 활성화를 높이기 위해 유용한 천연 추출물을 첨가하게 된다. 예를 들면, 호호바오일, 로스힙오일, 스테아릭에씨드, 마카데미아닛오일, 스쿠알렌, 산화방지제, 토코페롤, 하이아루로닉에씨드, 키토산, 상피추출물을 첨가하여 캐비어 단독 제품보다 눈가 세포에 대한 생리활성을 더욱 높이는 효과를 볼 수 있다.In the present invention, away from using the conventional caviar extract as it is to include the caviar extract is concentrated in a pressure-sensitive method and then emulsified it to be used as a raw material of cosmetics. Caviar extract is difficult to preserve at room temperature when the solid content is less than 30% and may easily perish. In order to overcome this, the solid content is concentrated under reduced pressure to 50% or more. At this time, the concentration of the caviar is concentrated at low temperature (30-60 ° C.) so as not to be destroyed. In the present invention, using the highly concentrated namoemulsion caviar extract obtained above to make the eye cream to supply nourishment to the eyes, a natural extract useful to increase the activation of the caviar component is added. For example, jojoba oil, lozenges oil, stearic acid, macadamia nut oil, squalene, antioxidants, tocopherols, hyaluronic acid, chitosan, and epidermal extracts are added to eye cells rather than caviar alone. You can see the effect of further enhancing the biological activity.

본 발명에 사용되는 기초 원료인 캐비어는 상온에서 보관시 쉽게 그 성질이 변할 수 있으므로 캐비어를 추출하여 감압식 농축기에서 30-50℃를 유지하며 고형분이 50% 이상 되도록 농축하게 된다. 이로써 원료의 성질을 변형시키지 않고 상온 에서도 변질이 되지 않는 고농축 나노 에멀젼 캐비어를 얻었고, 이것을 원료로 아이크림을 만든다. 본 발명에 따르면 화장품의 조성 및 생산 과정은 다음과 같다. Caviar, which is a basic raw material used in the present invention, can easily change its properties when stored at room temperature, so that the caviar is extracted and maintained at 30-50 ° C. in a pressure-sensitive concentrator and concentrated to 50% or more solids. This resulted in a highly concentrated nano emulsion caviar that does not alter the properties of the raw material and does not deteriorate even at room temperature. According to the present invention, the composition and production process of the cosmetics are as follows.

정제수 70-75중량%과 캐비어 농축액 5-10중량%에 메칠파라벤 0.1-0.5중량%, 디소디움에이디티에이 0.3-0.5중량%, 부틸렌글리콜 1-1.5중량%, 이미다졸리디닐우레아 0.2-0.5중량%, 글리세린 2-3중량%, 카보머 0.2-0.4중량%, 글리세릴모노스테아레이트 1.5-2.0중량%, 트리에탄올아민 2-4중량%, 밀납 1-2중량%, 디메치곤 0.2-0.6중량%을 각각 혼합하여 70-85℃에서 가열하여 유화시키는 1단계와, 호호바오일, 로스힙오일, 스테아릭에씨드, 마카데미아닛오일, 스쿠알렌, 산화방지제, 토코페롤, 하이아루로닉에씨드, 키토산, 상피추출물 등을 각각 2-5중량%를 1단계에서 얻어진 혼합물에 첨가하여 호모믹서로 유화시키는 2단계, 2단계에서 얻어진 아이크림을 100-200메쉬의 스테인래스 망으로 여과하는 3단계 그리고 병에 주입하는 4단계로 이루어진다. 70-75% by weight of purified water and 5-10% by weight of caviar concentrate, 0.1-0.5% by weight of methyl paraben, 0.3-0.5% by weight of disodium ED, 1-1.5% by weight of butylene glycol, and 0.2-0.5 imidazolidinyl urea % By weight, 2-3% by weight glycerin, 0.2-0.4% by weight carbomer, 1.5-2.0% by weight glyceryl monostearate, 2-4% by weight triethanolamine, 1-2% by weight beeswax, 0.2-0.6% by weight dimethicone %, Each of which is mixed and heated at 70-85 ° C. to emulsify, jojoba oil, lozen hip oil, stearic acid, macadamia nitrile oil, squalene, antioxidant, tocopherol, hyaluronic acid, 2 steps of adding 2-5% by weight of chitosan and epidermal extract, respectively, to the mixture obtained in step 1 and emulsifying with a homomixer, 3 steps of filtering the eye cream obtained in step 2 with 100-200 mesh stained glass net, and There are four steps to inject into the bottle.

본 발명에 따라 캐비어를 고농축 나노에멀젼 형태로 만들면 기존의 일반적인 캐비어 추출물과 비교하여 상온에서도 보관이 용이하며 적은 양으로 더 많은 효과를 볼 수 있다. 또한 본 발명에 의한 아이크림은 캐비어의 성분은 물론 천연 추출물을 다량 함유하여 눈가의 수분 유지와 주름살의 방지, 피부노화의 지연등의 효과가 있다.When the caviar is made into a highly concentrated nanoemulsion form according to the present invention, it is easier to store at room temperature and more effective in a smaller amount compared to conventional general caviar extracts. In addition, the eye cream according to the present invention contains a large amount of natural extracts as well as components of the caviar, there is an effect such as maintaining the moisture around the eyes, preventing wrinkles, delaying skin aging.

본 발명은 캐비어 추출물을 한 단계 더 농축시킨 고농축 나노에멀젼 형태의 캐비어 원료를 먼저 구하고 이를 영양공급용 젤 형태의 화장품을 만들고자 하는데 있다. 캐비어 추출물은 캐비어를 용매(프로필렌 글라이콜)에 넣어 60℃(±5)에서 4-6시간 동안 순환 추출하며 얻어진 추출물을 감압식 농축기에서 30-50℃를 유지하며 고형분이 50% 이상 되도록 농축하게 된다. 이상에서 얻어진 나노에멀젼 형태의 고농축액을 준비하고, 정제수 70-75중량%과 캐비어 농축액 5-10중량%에 메칠파라벤 0.1-0.5중량%, 디소디움에이디티에이 0.3-0.5중량%, 부틸렌글리콜 1-1.5중량%, 이미다졸리디닐우레아 0.2-0.5중량%, 글리세린 2-3중량%, 카보머 0.2-0.4중량%, 글리세릴모노스테아레이트 1.5-2.0중량%, 트리에탄올아민 2-4중량%, 밀납 1-2중량%, 디메치곤 0.2-0.6중량%을 각각 혼합하여 70-85℃에서 가열하여 유화시키는 1단계와, 호호바오일, 로스힙오일, 스테아릭에씨드, 마카데미아닛오일, 스쿠알렌, 산화방지제, 토코페롤, 하이아루로닉에씨드, 키토산, 상피추출물 등을 각각 2-5중량%를 1단계에서 얻어진 혼합물에 첨가하여 호모믹서로 유화시키는 2단계, 2단계에서 얻어진 아이크림을 100-200메쉬의 스테인래스 망으로 여과하는 3단계 그리고 병에 주입하는 4단계로 이루어진다.The present invention is to obtain a caviar raw material in the form of high-concentration nanoemulsion in which the caviar extract is further concentrated, and to make cosmetics in the form of gel for nutrition. Caviar extract is circulated extraction of caviar in a solvent (propylene glycol) at 60 ℃ (± 5) for 4-6 hours, and the resulting extract is maintained at 30-50 ℃ in a vacuum condenser and concentrated to more than 50% solids do. To prepare a high-concentration liquid obtained in the form of nanoemulsion obtained above, 0.1-0.5% by weight of methyl paraben, 0.3-0.5% by weight of disodium ID, butylene glycol 1 in 70-75% by weight of purified water and 5-10% by weight of caviar concentrate -1.5% by weight, 0.2-0.5% by weight imidazolidinylurea, 2-3% by weight glycerin, 0.2-0.4% by weight carbomer, 1.5-2.0% by weight glyceryl monostearate, 2-4% by weight triethanolamine, 1 step of emulsification by mixing 1-2% by weight of beeswax and 0.2-0.6% by weight of dimethicone, and heating at 70-85 ° C., jojoba oil, lozen hip oil, stearic acid, macadamia nitrile oil and squalene 2, 5% by weight of an antioxidant, tocopherol, hyaluronic acid, chitosan, and epidermal extract, respectively, were added to the mixture obtained in step 1 to emulsify with a homomixer. -3 stages of filtration with 200 mesh stainless steel mesh and bottle There are four steps.

Claims (1)

캐비어를 용매(프로필렌 글라이콜)에 넣어 60℃(±5)에서 4-6시간 동안 순환 추출하며 얻어진 추출물을 감압식 농축기에서 30-50℃를 유지하며 고형분이 50% 이상 되도록 농축하여 얻어진 나노에멀젼 형태의 고농축액을 준비하고, 정제수 70-75중량%과 캐비어 농축액 5-10중량%에 메칠파라벤 0.1-0.5중량%, 디소디움에이디티에이 0.3-0.5중량%, 부틸렌글리콜 1-1.5중량%, 이미다졸리디닐우레아 0.2-0.5중량%, 글리세린 2-3중량%, 카보머 0.2-0.4중량%, 글리세릴모노스테아레이트 1.5-2.0중량%, 트리에탄올아민 2-4중량%, 밀납 1-2중량%, 디메치곤 0.2-0.6중량%을 각각 혼합하여 70-85℃에서 가열하여 유화시키는 1단계와, 호호바오일, 로스힙오일, 스테아릭에씨드, 마카데미아닛오일, 스쿠알렌, 산화방지제, 토코페롤, 하이아루로닉에씨드, 키토산, 상피추출물 등을 각각 2-5중량%를 1단계에서 얻어진 혼합물에 첨가하여 호모믹서로 유화시키는 2단계, 2단계에서 얻어진 아이크림을 100-200메쉬의 스테인래스 망으로 여과하는 3단계 그리고 병에 주입하는 4단계로 이루어지는 아이 크림의 제조에 관한 것을 특징으로 함.Nanoemulsion obtained by circulating extraction of caviar in solvent (propylene glycol) for 4-6 hours at 60 ° C (± 5), maintaining the extract at 30-50 ° C in a vacuum condenser and concentrating it to 50% or more solids. Prepare a high concentrate in the form of, 70-75% by weight of purified water and 5-10% by weight of caviar concentrate 0.1-0.5% by weight of methyl paraben, 0.3-0.5% by weight of sodium disodium, 1-1.5% by weight of butylene glycol, 0.2-0.5% by weight of imidazolidinyl urea, 2-3% by weight of glycerin, 0.2-0.4% by weight of carbomer, 1.5-2.0% by weight of glyceryl monostearate, 2-4% by weight of triethanolamine, 1-2% of beeswax %, Dimethicone 0.2-0.6% by weight, and the first step of emulsification by heating at 70-85 ℃, jojoba oil, lozenges oil, stearic acid, macadamia nitrile oil, squalene, antioxidant, tocopherol , 2-5% by weight of hyaluronic acid, chitosan, epidermal extract, etc. The preparation of the eye cream comprising two steps of adding to the mixture obtained in the above step and emulsifying with a homomixer, three steps of filtering the eye cream obtained in the second step with a 100-200 mesh stained glass net and injecting it into the bottle. Characterized.
KR1020090002825A 2009-01-14 2009-01-14 Manufacturing method for beauty product of eye cream using caviar extracton KR20100083448A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104958231A (en) * 2015-06-29 2015-10-07 济南正骐生物科技有限公司 Black eye removing eye cream
CN106109387A (en) * 2016-08-24 2016-11-16 秦艳红 One is dispelled black eye eye cream
CN106137925A (en) * 2016-08-24 2016-11-23 秦艳红 A kind of defying age eye cream
CN112675108A (en) * 2020-12-31 2021-04-20 北京日光旭升精细化工技术研究所 Moisturizing, relieving and anti-wrinkle eye cream and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104958231A (en) * 2015-06-29 2015-10-07 济南正骐生物科技有限公司 Black eye removing eye cream
CN106109387A (en) * 2016-08-24 2016-11-16 秦艳红 One is dispelled black eye eye cream
CN106137925A (en) * 2016-08-24 2016-11-23 秦艳红 A kind of defying age eye cream
CN112675108A (en) * 2020-12-31 2021-04-20 北京日光旭升精细化工技术研究所 Moisturizing, relieving and anti-wrinkle eye cream and preparation method thereof

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