KR20060128315A - Manufacturing method and composition of medical herbs soap for anti-acne - Google Patents

Manufacturing method and composition of medical herbs soap for anti-acne Download PDF

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KR20060128315A
KR20060128315A KR1020050049661A KR20050049661A KR20060128315A KR 20060128315 A KR20060128315 A KR 20060128315A KR 1020050049661 A KR1020050049661 A KR 1020050049661A KR 20050049661 A KR20050049661 A KR 20050049661A KR 20060128315 A KR20060128315 A KR 20060128315A
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soap
weight
composition
acne
ethyl alcohol
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김해숙
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김해숙
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14Shaping
    • C11D13/18Shaping by extrusion or pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

Provided is a composition for medicinal soap for preventing skin diseases such as acne and sebum over-secretion, which uses medicinal herbs having an effect of improving skin conditions while avoiding the use of a chemical sterilizing or antibacterial agent, and thus causes no side effect. The composition for medicinal soap comprises a Chinese medicinal herb extract obtained by the method comprising the steps of: mixing dried Houttuynia cordata Thunb leaves with the same amount of licorice powder; introducing the mixed Chinese medicinal herb powder into 20% ethyl alcohol solution containing 20% of ethyl alcohol and 80% of water and used in an amount corresponding to about 30 times of the weight of the mixed powder; stirring the solution for 5 minutes twice a day at about 20 deg.C for a period of 20 days; and collecting the supernatant. A soap base is mixed with the Chinese medicinal herb extract and then with tea tree oil, and the resultant mixture is formed into soap.

Description

한약재인 어성초와 감초 그리고 티트리 오일을 첨가란 여드름 피부질환 예방용 약용비누 제조방법 및 그 조성물{Manufacturing Method and Composition of Medical Herbs Soap for Anti-Acne}Manufacturing method and composition of herbal soap for preventing acne skin disease by adding Eochocho, licorice and tea tree oil, which are herbal medicines {Manufacturing Method and Composition of Medical Herbs Soap for Anti-Acne}

도 1은 발명의 구성의 설명순서1 is an explanation procedure of a configuration of the invention

종래 특허공개 1995-11598호, 특허공개 1995-14288호, 특허공개 2002-89269호 등에서 항균성 티트리 오일을 성분으로 하는 조성으로 여드름에 예방에 주안점으로 사용되었으며 한약 성분인 어성초, 감초 성분을 첨가한 특허공개 1993-2499호, 2004-83994호 등에 항균작용으로 복합 조성물을 사용하였다. 본 발명은 3가지 복합조성 티트리 오일, 어성초 그리고 감초들을 사용하여 여드름 피부의 예방 약용 비누 조성물을 발명하였다.It is a composition containing antimicrobial tea tree oil as a component in Patent Publication No. 1995-11598, Patent Publication No. 1995-14288, Patent Publication No. 2002-89269, etc. The composite composition was used for antimicrobial activity by patent publication 1993-2499, 2004-83994, etc. The present invention has invented a medicated soap composition for preventing acne skin using three complex tea tree oils, fish herb and licorice.

어성초, 감초 등의 한약재들을 용액 추출하여 비누제조 과정에 추출물을 첨가하고 압출, 성형과정에 티트리 오일을 첨가하여 약용비누를 만든 다음 후 피부 자극성 시험을 테스트하고 여드름 질환에 적합성을 조사한 것이다.After extracting herbal medicines such as Eochocho and Licorice, extract was added to soap manufacturing process, tea tree oil was added to extrusion and molding process to make medicated soap, and then tested for skin irritation test and examined for acne disease.

* 감초는 시베리아 동부와 중국 종 북부가 원산인 콩과 다년초로서 뿌리가 달기 때문에 감초라고 한다. 여러 가지 약효가 많아 한방약에 거의 포함되는 매우 중요한 생약이다. 해독작용과 함께 한방약의 맛을 순하게 하고 효력을 촉진하는 역할을 한다.Licorice is a soybean and perennial herb that is native to eastern Siberia and northern China. Many drugs are very important because they are almost included in herbal medicine. Along with detoxification, the effect of herbal medicines is to soften and promote the effect.

* 어성초는 메밀의 잎이 메밀의 잎과 비슷하고 약용식물이므로 약모밀이라고 부른다. 멸어성초라고 말하기도 한다. 응달진 숲 속에서 자라며 땅속줄기가 옆으로 길게 뻗고 가늘며 흰색이다. 줄기는 곧게 서고 높이가 20∼50cm이며 몇 개의 세로줄이 있고 털이 없으며 냄새가 난다. 잎은 어긋나고 넓은 달걀 모양의 심장모양이며 길이가 3∼8cm이고 끝이 뾰족하며 가장자리가 밋밋하고 떡잎이 잎자루 밑 부분에 붙어 있다. 한국(울릉도·안면도·거제도)·일본, 중국, 히말라야, 자바에 분포한다. * Eoseongcho is called buckwheat because buckwheat leaves are similar to buckwheat leaves and are medicinal plants. It is also called perish starch. It grows in a shady forest and its stem is long and thin and white. Stems stand straight, 20-50cm high, with several vertical lines, hairless, and smelly. Leaves are alternate, wide egg-shaped heart-shaped, 3-8cm long, pointed at the end, with flat edges, and the cotyledon is attached to the bottom of petiole. It is distributed in Korea (Ulleungdo, Anmyeondo, Geoje), Japan, China, Himalayas, and Java.

줄기와 잎에서 비린내가 나서 붙여진 이름이다. 중국의 본초강목에 어성초가 중금속의 독을 해독하는 작용이 있다고 기록하였고, 영남 채역록에도 어성초가 농소독 제로 나와있다.It's a fishy name on stems and leaves. Eoseongcho recorded the action of detoxification of heavy metals in Chinese herbal trees, and Eoseongcho was listed as an agricultural poison in the Yeongnam quarry.

* 티트리(Tea Tree) 나무는 학명으로 Melaleleuca Alternifolia이며 호주 원주민이 피부질환에 잎의 추출물을 사용하여 왔든 것으로 항균작용이 우수하여 이 나무의 수증기법으로 오일을 취하여 식물성 천연 항균성 오일로 화장품 및 의약품으로 많이 사용되고 있다.* Tea Tree is a scientific name Melaleleuca Alternifolia, and it is a natural antibacterial oil derived from oil using the water vapor method of this tree. It is used a lot.

도표 1에 따라 발명의 구성으로 With the composition of the invention according to Table 1

1. 약용 한약추출 액기스 만드는 방법은 먼저 말린 어성초잎, 가루인 감초뿌리들을 같은 무게 비율로 하여 이들 2가지 한약재 합한 무게의 약 30배의 20% 알코올용액(알코올 20%, 물 80%)에 넣어 하루에 2번씩 5분간 저어주면서 일상온도 약 20℃에서 20일 동안 실시한다. 20일 후 용액 윗부분만 사용한다.1. Method of making medicinal herb extract extract is to put dried Echo leaves and powdered licorice roots in the same weight ratio and put them in 20% alcohol solution (20% alcohol, 80% water) of 30 times the combined weight of these two herbs. Stir twice for 5 minutes twice a day for 20 days at 20 ℃. After 20 days, use only the top of the solution.

2. 약용 비누제조는 표1의 조성에 따라 2. Manufacture of medicated soap according to the composition of table 1

콩기름 Soybean oil 26.026.0 라우릴 산Lauryl Mountain 17.017.0 미리스틱 산Mystic acid 6.06.0 스테아릭 산Stearic acid 8.08.0 글리세린glycerin 4.04.0 바셀린vaseline 1.01.0 어성초, 감초액기스Eoseongcho, licorice extract 27.427.4 가성소다Caustic soda 9.69.6 100100

비누를 다음과 같은 방법으로 만든다.Make soap in the following way:

1) 큰 탱크에 먼저 지방산 라우릴산, 미리스틱산 그리고 스테아릭 산과 콩기름, 바세린, 글리세린을 혼합 한 다음 약 70-80℃에서 녹인다.1) In a large tank, first mix the fatty acid lauryl acid, mystic acid and stearic acid with soybean oil, petrolatum and glycerin, then dissolve at about 70-80 ℃.

2) 작은 탱크에서 용액 추출물에 가성소다를 녹인다.2) Dissolve caustic soda in solution extract in small tank.

3) 큰 탱크의 혼합액을 60℃로 유지하면서 작은 탱크의 혼합액을 서서히 혼합하여 저어 준다. 혼합한 다음 다시 80℃로 5분간 유지하고 온도를 실온으로 식힌 후 비누로 쓸 수 있을 정도로 말린다.3) While mixing the mixed liquid of the small tank, slowly stir and mix the mixed liquid of the small tank. After mixing, hold it again at 80 ° C for 5 minutes, cool the temperature to room temperature and dry it enough to use with soap.

4) 말린 비누에 티트리 오일을 혼합한 다음 압출 성형하여 약용비누를 완성한다.4) Mix tea tree oil with dried soap and then extrude to complete medicated soap.

3. 피부 자극성 검사 3. Skin irritation test

상기 제조된 비누로 100g 비누로 성인 남녀 30명에게 온수의 물로서 얼굴에 세수한 후 3분 후 자극시험을 하고 2차 실험은 30분 후 자극 테스트하였으며 3차 실험은 매일 아침, 저녁 2회 실시하여 10일 후에 자극시험, 4차 실험은 매일 아침, 저녁 2회 30일 후 자극시험을 실시하였다.After washing the face with hot water water to 30 adult men and women with 100g soap, the stimulation test after 3 minutes and the second test was a stimulation test after 30 minutes, the third experiment was carried out twice every morning and evening After 10 days, the stimulation test, the fourth experiment was performed every morning, evening, 30 days after the stimulation test.

표2는 피부 반응에 따른 반응치를 반응기준으로 나타내었다.Table 2 shows the response value according to the skin response as a response standard.

반 응reaction 반 응 치Reaction 반응기준Response criteria 00 0.00.0 무반응No response ++ 0.50.5 희미한 홍반Faint erythema ++++ 1.01.0 경계가 뚜렷한 약한 홍반Weak erythema with clear borders ++++++ 2.02.0 뚜렷한 홍반Distinct erythema ++++++++ 3.03.0 수포water blister

* 피부 반응도 산출 공식은 = 반응치 X 반응 사람 수 * The formula for calculating skin responsiveness is = response value X number of people responding

* 평균 반응도 = (1차 반응치 x 반응 수 + 2차 반응치 x 반응 수 + 3차 반응치 x 반응 수 + 4차 반응치 x 반응 수) / 종합 반응 참가자 수* Average Responsiveness = (1st Response x Responses + 2nd Response x Responses + 3rd Response x Responses + 4th Response x Responses) / Total Response Participants

평균 반응도을 계산하여 표3의 평균반응에 따른 판정기준을 산정하여 표4의 판정기준에 따라 자극의 정도를 나타내었다.The average reactivity was calculated to determine the criterion according to the average response in Table 3, and the degree of stimulation was indicated according to the criterion in Table 4.

자극성 반응의 평균 반응도에 따른 판정기준Criteria according to average responsiveness of stimulus response 피부 평균 반응도Skin responsiveness 판정기준Criteria 0 ~ 0.490 to 0.49 무자극Non-irritating 0.5 ~ 0.990.5 to 0.99 경 자극Carotid stimulation 1.0 ~ 1.991.0 to 1.99 중 자극Stimulation 2.0 ~ 32.0 to 3 강 자극River stimulation

반응도(자극성 피부반응):Reactivity (Irritation Skin Response): 반 응reaction 반응치Response 1차 실험 반 응자 수Primary Experiment Responders 2차 실험 반 응자 수Secondary experiment responders 3차 실험 반 응자 수3rd experiment responders 4차 실험 반 응자 수4th experiment responders 평균반응도Average reactivity 00 0.00.0 30명30 persons 30명30 persons 29명29 people 29명29 people 00 ++ 0.50.5 00 00 1One 1One 0.0080.008 ++++ 1.01.0 00 00 00 00 00 ++++++ 2.02.0 00 00 00 00 00 ++++++++ 3.03.0 00 00 00 00 00

표3의 평균 판정기준에 따른 반응도(표4) 결과에 의해 According to the result of responsiveness (Table 4) according to the average criterion of Table 3

평균반응도 값이 최고 0.008 이하이므로 피부 무자극이었다.As the average reactivity value was less than 0.008, it was not skin irritant.

4. 여드름 피부 패널시험4. Acne skin panel test

상기 비누제품 100g 으로 남, 여 여드름 질환 30명을 대상으로 실사용 평가 테스트를 하였다. 사용기간은 4주이며 아침과 저녁에 2회 걸쳐 실시하였으며 그 결과를 표5에 나타낸다.The soap product 100g male and female acne disease 30 people were tested for practical evaluation. The period of use is four weeks and was conducted twice in the morning and evening. The results are shown in Table 5.

* 5포인트 스케일** 5-point scale *

5: 매우 좋다 4: 좋다 3: 보통 2: 나쁨 1: 매우 나쁨5: very good 4: good 3: moderate 2: bad 1: very bad

여드름 트러블 해소 패널시험 결과Acne Trouble Relief Panel Test Results 시험항목Test Items 포인트 크기Point size 판정수Judgment Count 여드름 피부질환 해소   Relieves acne skin disease 55 2020 44 55 33 44 22 1One 1One 00 평균Average 4.384.38

평균값이 4.38이므로 여드름 피부에 효과가 있음으로 나타났다.The mean value is 4.38, which is effective for acne skin.

본 발명은 약용비누 조성에 일반적으로 많이 쓰는 한약재 감초, 어성초의 해독성분 2가지를 성분과 티트리 오일을 첨가하여 화학적으로 합성된 살균 또는 항균성 물질을 첨가함으로써 여러 가지 부작용을 발생시켰던 종래의 비누제품과 달리 피부자극에 안전하며 부작용없이 여드름 피부질환에 사용될 수 있다. The present invention is a conventional soap product that caused various side effects by adding chemically synthesized bactericidal or antimicrobial substances by adding two components of detoxification ingredients of medicinal herbs licorice and eoseongcho commonly used in medicated soap composition Unlike, it is safe for skin irritation and can be used for acne skin disease without side effects.

Claims (2)

말린 어성초잎, 감초가루 등을 같은 무게 비율로 하여 2가지 한약재 합한 무게의 약 30배의 20% 에틸 알코올용액(에틸 알코올 20%, 물 80%)에 넣어 하루에 2번씩 5분간 저어주면서 일상온도 약 20℃에서 20일 동안 실시한다. 20일 후 용액 윗부분만 사용하는 한약 추출물 만드는 방법과 조성비율.Dried fish leaf, licorice powder, etc. in the same weight ratio and added to 20% ethyl alcohol solution (20% ethyl alcohol, 80% water), about 30 times the weight of the two herbs, stirring twice a day for 5 minutes 20 days at about 20 ℃. After 20 days, the method and composition ratio of herbal extract using only the upper part of the solution. 큰 탱크에 먼저 라우릴 산(17.0중량%), 밀리스틱산(6.0중량%), 밀리스틱산(8.0중량%), 식물성 기름(26.0중량%), 글리세린(4.0중량%), 바셀린(1.0중량%)을 혼합 한 다음 약 70∼80℃로 녹이고, 작은 탱크에서 한약 추출물(27.4중량%)에 가성소다(9.6중량%)을 녹인 후 약 25℃ 정도로 온도를 유지한다. 큰 탱크의 혼합액을 60℃로 유지하면서 작은 탱크의 혼합액을 서서히 혼합하면서 저어준 후, 온도를 80℃로 5분간 유지한 다음 실온에서 식힌 후 비누로 쓸 수 있을 정도로 말린 다음 성형 건조하여 티트리 오일을 첨가하여 성형 압출하는 약용비누 제조방법과 위 조성비율.First, in a large tank, lauryl acid (17.0% by weight), mystic acid (6.0% by weight), mystic acid (8.0%), vegetable oil (26.0% by weight), glycerin (4.0% by weight), petroleum jelly (1.0% by weight) %) Is mixed and dissolved at about 70 ~ 80 ℃, caustic soda (9.6wt%) is dissolved in Chinese medicine extract (27.4wt%) in small tank and maintained at about 25 ℃. Stir the mixture of the small tank while stirring the mixture of the small tank while maintaining the mixture at a large tank at 60 ° C.Then, hold the temperature at 80 ° C for 5 minutes, cool it at room temperature, dry it with a soap and dry it by molding, and then tea tree oil. Medicinal soap manufacturing method and the composition ratio of the molding by extrusion molding.
KR1020050049661A 2005-06-10 2005-06-10 Manufacturing method and composition of medical herbs soap for anti-acne KR20060128315A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101128361B1 (en) * 2012-01-09 2012-03-23 조봉주 Natural soap using of tea oil and manufacturing method for the same
US20120135093A1 (en) * 2009-07-14 2012-05-31 Soonchunhyand University Industry Academy Cooperation Foundation Soap composition for treating acne containing absolute ginseng essential oil
CN110591842A (en) * 2019-09-30 2019-12-20 广州香枝化妆品有限公司 Plant handmade soap capable of removing mites and acnes and preparation method thereof
KR20210051840A (en) 2019-10-31 2021-05-10 전순호 Laundry Soap Having Vegetable Property
CN117064822A (en) * 2023-10-16 2023-11-17 广州市中通生化制品有限公司 Plant acne-removing composition, plant acne-removing patch and preparation method of plant acne-removing composition

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120135093A1 (en) * 2009-07-14 2012-05-31 Soonchunhyand University Industry Academy Cooperation Foundation Soap composition for treating acne containing absolute ginseng essential oil
KR101128361B1 (en) * 2012-01-09 2012-03-23 조봉주 Natural soap using of tea oil and manufacturing method for the same
CN110591842A (en) * 2019-09-30 2019-12-20 广州香枝化妆品有限公司 Plant handmade soap capable of removing mites and acnes and preparation method thereof
KR20210051840A (en) 2019-10-31 2021-05-10 전순호 Laundry Soap Having Vegetable Property
CN117064822A (en) * 2023-10-16 2023-11-17 广州市中通生化制品有限公司 Plant acne-removing composition, plant acne-removing patch and preparation method of plant acne-removing composition
CN117064822B (en) * 2023-10-16 2023-12-12 广州市中通生化制品有限公司 Plant acne-removing composition, plant acne-removing patch and preparation method of plant acne-removing composition

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