KR20050013386A - A method for producing ginseng tea bag using a method of extrusion process fabrication and the product thereof - Google Patents
A method for producing ginseng tea bag using a method of extrusion process fabrication and the product thereofInfo
- Publication number
- KR20050013386A KR20050013386A KR1020030052013A KR20030052013A KR20050013386A KR 20050013386 A KR20050013386 A KR 20050013386A KR 1020030052013 A KR1020030052013 A KR 1020030052013A KR 20030052013 A KR20030052013 A KR 20030052013A KR 20050013386 A KR20050013386 A KR 20050013386A
- Authority
- KR
- South Korea
- Prior art keywords
- ginseng
- tea
- extruded
- leaching
- drying
- Prior art date
Links
- 235000008434 ginseng Nutrition 0.000 title claims abstract description 158
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 title claims abstract description 157
- 235000003140 Panax quinquefolius Nutrition 0.000 title claims abstract description 157
- 244000269722 Thea sinensis Species 0.000 title claims abstract description 64
- 238000001125 extrusion Methods 0.000 title claims abstract description 40
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 241000208340 Araliaceae Species 0.000 title claims abstract 32
- 238000000034 method Methods 0.000 title claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 56
- 108090000790 Enzymes Proteins 0.000 claims abstract description 40
- 102000004190 Enzymes Human genes 0.000 claims abstract description 40
- 238000001035 drying Methods 0.000 claims abstract description 28
- 239000002245 particle Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 11
- 229920002472 Starch Polymers 0.000 claims abstract description 9
- 239000008107 starch Substances 0.000 claims abstract description 9
- 235000019698 starch Nutrition 0.000 claims abstract description 9
- 238000010298 pulverizing process Methods 0.000 claims abstract description 4
- 230000035622 drinking Effects 0.000 claims abstract description 3
- 238000002386 leaching Methods 0.000 claims description 54
- 238000002347 injection Methods 0.000 claims description 12
- 239000007924 injection Substances 0.000 claims description 12
- 230000000593 degrading effect Effects 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 7
- 235000021329 brown rice Nutrition 0.000 claims description 6
- 108010071289 Factor XIII Proteins 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 241000533293 Sesbania emerus Species 0.000 claims description 3
- 235000012438 extruded product Nutrition 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 235000019640 taste Nutrition 0.000 abstract description 6
- 239000000796 flavoring agent Substances 0.000 abstract description 5
- 235000019634 flavors Nutrition 0.000 abstract description 5
- 239000000835 fiber Substances 0.000 abstract 1
- 240000004371 Panax ginseng Species 0.000 description 126
- 235000013616 tea Nutrition 0.000 description 54
- 229940088598 enzyme Drugs 0.000 description 35
- 235000002789 Panax ginseng Nutrition 0.000 description 15
- 239000012153 distilled water Substances 0.000 description 15
- 238000011282 treatment Methods 0.000 description 15
- 238000002835 absorbance Methods 0.000 description 13
- 238000006911 enzymatic reaction Methods 0.000 description 13
- 239000001913 cellulose Substances 0.000 description 12
- 229920002678 cellulose Polymers 0.000 description 12
- 239000000047 product Substances 0.000 description 8
- 108010059892 Cellulase Proteins 0.000 description 7
- 229940106157 cellulase Drugs 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- 238000009826 distribution Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- 239000004480 active ingredient Substances 0.000 description 5
- 235000013353 coffee beverage Nutrition 0.000 description 5
- 230000002255 enzymatic effect Effects 0.000 description 5
- 239000000284 extract Substances 0.000 description 5
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- 238000012360 testing method Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 4
- 235000020710 ginseng extract Nutrition 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 238000001179 sorption measurement Methods 0.000 description 4
- 108010075550 termamyl Proteins 0.000 description 4
- 235000019658 bitter taste Nutrition 0.000 description 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
- 235000019606 astringent taste Nutrition 0.000 description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
- 210000004556 brain Anatomy 0.000 description 2
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- 235000013312 flour Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 229930182494 ginsenoside Natural products 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 239000008101 lactose Substances 0.000 description 2
- 239000011859 microparticle Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 150000007949 saponins Chemical class 0.000 description 2
- 235000017709 saponins Nutrition 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 208000022531 anorexia Diseases 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 206010061428 decreased appetite Diseases 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 201000006549 dyspepsia Diseases 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 235000015092 herbal tea Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000021539 instant coffee Nutrition 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
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- 235000019633 pungent taste Nutrition 0.000 description 1
- 229940125723 sedative agent Drugs 0.000 description 1
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- 238000004062 sedimentation Methods 0.000 description 1
- 235000019614 sour taste Nutrition 0.000 description 1
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- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/08—Oxidation; Fermentation
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/12—Rolling or shredding tea leaves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/163—Liquid or semi-liquid tea extract preparations, e.g. gels, liquid extracts in solid capsules
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P30/00—Shaping or working of foodstuffs characterised by the process or apparatus
- A23P30/20—Extruding
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2124—Ginseng
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/214—Tea
Abstract
Description
본 발명은 압출성형공정에 의하여 인삼 침출차를 제조하는 방법에 관한 것이다.The present invention relates to a method for manufacturing a ginseng leaching tea by an extrusion molding process.
일반적으로 인삼은 허약체질, 식욕부진, 소화불량, 설사의 치료약이면서 자양강장(滋養强壯), 강정(强精), 진정(鎭靜)제로 사용하며, 많은 사람들이 기호 식품으로 먹고 있는 실정이다.In general, ginseng is a medicine for weakness, anorexia, indigestion, diarrhea, nourishing tonic (,), Gangjeong (强 精), sedatives (많은), many people are eating as a favorite food.
이를 위한 종래의 인삼차에는 인삼의 추출액(엑기스)을 농축시켜 고형분으로 제조한 인삼차와, 인삼 엑기스와 부형제(포도당 또는 유당)를 혼합하여 과립 형태로 제조한 인삼차가 있는데, 현재 판매되고 있는 인삼차와 홍삼차는 대부분 추출차 형태로 개발되어 있다.Conventional ginseng teas for this purpose are ginseng teas prepared by concentrating the extract (extract) of ginseng and made into solids, and ginseng teas prepared by mixing ginseng extract and excipients (glucose or lactose) in granular form. Tea is mostly developed in the form of extract tea.
인스턴트커피를 제외한 동서양의 차류는 주로 침출차의 형태이다. 녹차를 비롯한 허브차의 대부분은 티백을 액상용매(물)에 넣어 맛, 향, 색과 유효성분을 침출시키는 침출차 형태의 제품이 대부분이다. 고려인삼은 세계적으로 효능이 잘 알려져 있지만 티백에 담가서 간편하게 음용할 수 있는 인삼침출차는 개발되어 있지 않다.East and west teas, except instant coffee, are mainly leached tea. Most herbal teas, including green tea, are most often in the form of leach teas, which leach tea bags into liquid solvents (water) to leach flavors, flavors, colors and active ingredients. Korean ginseng is well known around the world, but no ginseng leaching tea has been developed that can be easily dipped in tea bags.
침출차 형태의 인삼차는 국내에서 대량생산되어 판매되는 제품은 없으며, 미국에서 건조인삼과 인삼추출액을 포함한 13가지 성분을 조합하여 Ginseng NRG Tea(Golden Remple of Oregon, Inc. Eugene, OR USA) 제품을 제조 판매하고 있으나, 분석 결과 인삼성분은 20% 였으며 인삼추출물이 대부분을 차지하는 추출차에 가까운 형태의 제품이었다.Ginseng tea in the form of leaching tea is not mass-produced and sold in Korea, and Ginseng NRG Tea (Golden Remple of Oregon, Inc. Eugene, OR USA) is manufactured by combining 13 ingredients including dry ginseng and ginseng extract in the United States. However, the analysis showed that the ginseng component was 20%, and the product was close to the extract tea that the ginseng extract occupies most.
본 발명은 상기한 바와 같은 종래의 문제점을 해결하기 위한 것으로, 인삼이 지니고 있는 본래의 약효 및 맛과 향을 그대로 유지한 채 간편하게 침출차의 형태로 만들어 마실 수 있는 인삼차의 제조 방법을 제공하는데 그 목적이 있다. 본 발명의 기술적 과제는 압출성형공정을 이용하여 인삼의 유효성분이 효과적으로 침출되는 인삼 침출차를 개발함으로써 달성하였다.The present invention is to solve the conventional problems as described above, to provide a manufacturing method of ginseng tea that can be easily made in the form of leach tea while maintaining the original medicinal efficacy and taste and aroma of ginseng as its purpose There is this. The technical problem of the present invention was achieved by developing a ginseng leaching car which effectively leaches ginseng using an extrusion molding process.
도 1은 압출성형공정과 셀룰라아제 처리가 침출속도에 미치는 영향을 실험한 결과를 나타내는 그래프이다.1 is a graph showing the results of experiments on the effect of the extrusion process and cellulase treatment on the leaching rate.
도 2는 압출성형공정과 효소처리가 액상용매에 대한 용해성 및 분산성에 미치는 영향을 나타내는 그림이다.2 is a diagram showing the effect of the extrusion molding process and enzyme treatment on the solubility and dispersibility of the liquid solvent.
본 발명은 압출성형공정에 의하여 인삼 침출차를 제조하는 방법에 관한 것이다.The present invention relates to a method for manufacturing a ginseng leaching tea by an extrusion molding process.
본 발명은 인삼을 파쇄하고 전분 분해효소 또는 섬유소 분해효소 중 하나를 처리하거나 두 가지 효소를 조합하여 처리하는 단계; 상기 효소처리된 인삼을 건조시켜 수분함량을 10~40%로 조절하는 단계; 상기 건조인삼을 쌍축 압출성형기에 투입하고 스크류 회전속도 100~350rpm, 사출구부위 온도 80∼130℃로 압출성형하는 단계; 및 상기 압출성형물을 건조, 분쇄하는 단계로 구성된다.The present invention comprises the steps of crushing ginseng and processing either starch or fibrinase or a combination of the two enzymes; Drying the enzyme-treated ginseng to adjust the water content to 10 to 40%; Inserting the dried ginseng into a twin screw extrusion machine and extruding the screw at a rotational speed of 100 to 350 rpm and an injection port temperature of 80 to 130 ° C .; And drying and pulverizing the extrudate.
이하, 본 발명의 구체적인 구성을 실시예를 통하여 상세히 설명하고자 하나, 본 발명의 권리범위가 이들 실시예에만 한정되는 것은 아니다.Hereinafter, one specific configuration of the present invention will be described in detail by way of examples, but the scope of the present invention is not limited only to these embodiments.
실시예 : 압출성형 인삼침출차의 제조방법Example: Method of manufacturing extrusion molded ginseng leaching tea
제 1 단계 : 효소반응 단계First step: enzyme reaction step
뇌두부위를 제거한 뒤 미근을 포함한 파쇄한 수삼(chopped ginseng)이나 뇌두부위와 미근과 세근부위를 제거하고 주근과 지근을 가진 주근수삼(main-root ginseng)으로 전처리하였다.After the brain head was removed, the chopped ginseng including the triceps was removed, or the brain head, the triceps, and the triceps were removed and pretreated with main-root ginseng with main and root muscles.
상기 파쇄수삼에 전분 분해효소인 Termamyl Supra(Novozymes, Denmark)를 인삼 1kg당 112.6㎕씩 100㎖의 증류수로 희석시킨 뒤 첨가하고 호바트믹서(LP-201, Taiwan)를 이용해 30분간 혼합하였다. 이것을 80℃ 건조기에서 1시간 30분 효소 반응시켰다.Starch degrading enzyme Termamyl Supra (Novozymes, Denmark) was added to the crushed ginseng with 112.6 μl of 100 g of distilled water per 1 kg of ginseng, followed by mixing for 30 minutes using a Hobart mixer (LP-201, Taiwan). This was enzymatically reacted for 1 hour and 30 minutes in an 80 degreeC drier.
상기 효소처리된 수삼에 전분 분해효소 AMG(Novozymes, Denmark)와 섬유소 분해효소 Celluclast 1.5 L FG(Novozymes, Denmark)을 각각 164㎕, 2.5㎕를 100㎖증류수에 희석시켜 첨가하고 30분간 혼합하였다. 이것을 60℃ 건조기에 넣고 45시간 동안 효소 반응시켰다.Starch degrading enzyme AMG (Novozymes, Denmark) and cellulose degrading enzyme Celluclast 1.5 L FG (Novozymes, Denmark) were respectively added to the enzyme treated ginseng, diluted with 100 ml distilled water, and mixed for 30 minutes. This was placed in a 60 ° C. drier and subjected to enzymatic reaction for 45 hours.
제 2 단계 : 건조 단계Second step: drying step
상기 제 1 단계에서 3가지 효소가 처리된 수삼을 건조온도 100℃에서 수분함량 20%로 건조시켰다. 상기 건조온도는 80~120℃, 수분함량은 10~40%에서 본 발명이 효과적으로 실시될 수 있다.Fresh ginseng treated with three enzymes in the first step was dried to a moisture content of 20% at a drying temperature of 100 ℃. The drying temperature is 80 ~ 120 ℃, moisture content can be effectively carried out the present invention at 10 to 40%.
상기 원료로는 수삼 이외에 백삼가루를 쓸 수 있는데, 수삼의 수분함량은 75-80% 정도이므로 수분함량을 감소시키는 건조과정이 필요하나, 백삼가루는 건조 단계를 필요로 하지 않는다.As the raw material, white ginseng powder can be used in addition to ginseng, and the moisture content of ginseng is about 75-80%, so a drying process is required to reduce moisture content, but white ginseng powder does not require a drying step.
제 3 단계 : 압출성형공정 단계Third step: extrusion process step
상기 제 2 단계에서 건조시킨 수삼을 쌍축 압출성형기에 투입하고, 수분함량 20%, 스크류 회전속도 300rpm, 사출구부위 온도 110℃로 압출성형하였다.The fresh ginseng dried in the second step was introduced into a twin screw extruder, and was extruded at a water content of 20%, a screw rotational speed of 300 rpm, and an injection port temperature of 110 ° C.
사용한 쌍축 압출성형기의 길이와 직경비(L/D ratio)는 25, 사출구직경 3.0mm, 원료투입속도 150g/min, 바렐온도분포 110/90/70℃로 하였으며, 스크루배열은 예비실험을 거처 사입부위는 피치가 큰 스크루, 사출구부위에는 인삼세포벽의 파열을 증가시키기 위하여 피치의 길이가 작은 스크루(high shear screw)를 배열하였으며 압출성형기 바렐내부에 인삼원료가 체류하는 시간을 증가시키기 위하여 역피치 스크루를 배열하였다.The length and diameter ratio (L / D ratio) of the used twin screw extruder was 25, the injection diameter was 3.0mm, the raw material feeding speed 150g / min, the barrel temperature distribution was 110/90/70 ℃, and the screw arrangement was preliminary tested. In the injection part, a screw with a large pitch is arranged at the injection hole, and a high pitch screw with a small pitch is arranged to increase the rupture of the ginseng cell wall.In order to increase the residence time of the ginseng raw material in the barrel of the extruder The pitch screw was arranged.
상기 압출성형공정은 수분함량 10~40%, 스크류 회전속도 100~350 rpm, 사출구부위 온도 80∼130℃에서 효과적으로 실시될 수 있다.The extrusion molding process may be effectively carried out at a water content of 10 to 40%, a screw rotational speed of 100 to 350 rpm, and an injection port temperature of 80 to 130 ° C.
제 4 단계 : 건조 및 분쇄 단계Fourth step: drying and grinding step
상기 제 3 단계의 압출성형물을 온도 80℃에서 15분 동안 건조시킨 다음, 압출성형물을 분쇄하여 입자 크기를 500㎛로 하였다.The extrudates of the third step were dried at a temperature of 80 ° C. for 15 minutes, and then the extrudate was pulverized to obtain a particle size of 500 μm.
상기 입자 크기는 200㎛-0.5㎜에서 본 발명이 효과적으로 실시될 수 있다.The particle size can be effectively carried out the present invention at 200 ㎛ -0.5mm.
상기와 같은 방법으로 얻어진 인삼 분말을 티백에 포장하여 침출차 제품으로 이용하거나, 원두커피 추출기에 침출하여 이용하였다.The ginseng powder obtained by the above method was packaged in a tea bag and used as a leach tea product, or leached in a coffee bean extractor.
또는 상기와 같은 방법으로 얻어진 압출성형 수삼이나 백삼은 액상용매(물)에 녹는 량이 크게 증가하였으므로 압출성형물을 마이크로분쇄기로 100㎛ 이하로 미세입자화하여 액상용매에 용해, 분산시킨 인삼차 또는 음료 시제품 제조에 이용하였다.Alternatively, the extruded ginseng or white ginseng obtained by the above method has greatly increased the amount of soluble in the liquid solvent (water). It was used for.
실험예 1 : 최적의 압출성형 공정변수Experimental Example 1 Optimal Extrusion Process Parameters
수삼을 야채파쇄기(화진전공, 서울)를 사용하여 파쇄한 다음, 건조시켜 수분함량 20, 25, 30%로 조절하고 스크루 회전속도 200, 300rpm에서 압출성형하였다. 이때 바렐온도분포는 110/90/70℃, 원료투입속도는 150g/min로 고정하였다.Fresh ginseng was crushed using a vegetable crusher (Hwajin Vacuum, Seoul), dried to adjust the moisture content to 20, 25, 30% and extruded at a screw rotation speed of 200, 300 rpm. At this time, the barrel temperature distribution was fixed at 110/90/70 ° C., and the raw material input speed was 150 g / min.
압출성형한 수삼을 분쇄하여 입자크기를 0.5㎜ 이하로 하고, 분말의 색도를 헌터 색도계(Hunter colorimeter)를 사용하여 측정하였다. 압출성형 수삼분말 3g을100㎖의 증류수에 20분 동안 분산시킨 후 12,000rpm에서 20분간 원심분리하여 당농도(Brix,%)를 측정하였으며 수용성지수(WSI)는 4,000rpm에서 20분간 원심분리한 상등액에 포함된 건물량과 시료함량의 비(%)로 표시하였으며 이것은 침출된 고형분의 량을 나타내는 지표가 될 수 있다. 갈색도(Browness)와 적색도(Redness)는 12,000rpm에서 20분간 원심분리한 상등액의 420과 520㎚ 파장에서 흡광도를 각각 나타내었다. 측정의 결과는 하기 표 1과 같다.The extruded ginseng was pulverized to a particle size of 0.5 mm or less, and the chromaticity of the powder was measured using a Hunter colorimeter. 3 g of extruded ginseng powder was dispersed in 100 ml of distilled water for 20 minutes and centrifuged at 12,000 rpm for 20 minutes to measure sugar concentration (Brix,%), and the water-soluble index (WSI) was centrifuged at 4,000 rpm for 20 minutes. It is expressed as the ratio of dry matter to sample content in% and can be an indicator of the amount of leached solids. Brownness and redness showed absorbance at 420 and 520 nm wavelengths of the supernatant centrifuged at 12,000 rpm for 20 minutes, respectively. The results of the measurements are shown in Table 1 below.
당농도(Brix), 수용성지수(WSI), 수분흡착도(WAI)는 수분함량과 스크루 회전속도에 따라 유의적으로 영향을 받지 않았다. 한편 갈색도와 적색도는 수분함량과 스크루 회전속도에 따라 유의적으로 영향을 받았다. 수분함량이 30%에서 20%로 감소함에 따라 갈색도는 1.62에서 2.32로 43% 증가하였으며 적색도는 0.58에서 1.07로 84% 증가하였다. 또한 스크루 회전속도를 200에서 300rpm으로 증가시킬 때 갈색도와 적색도가 유의적으로 증가하는 경향을 보였다. 갈색도와 적색도는 인삼과 홍삼의 중요한 유효성분인 사포닌과 사포닌 변형체인 진세노사이드(ginsenoside) 함량의 지표가 될 수 있으므로 수분함량 20%, 스크루 회전속도 300rpm에서 사포닌과 진세노사이드의 함량이 가장 높다고 할 수 있다. 결론적으로 수삼의 이용한 압출성형 침출차의 압출성형조건은 수분함량 20%, 스크루 회전속도 300rpm이 적당하다.Sugar concentration, water solubility index (WSI), and water adsorption (WAI) were not significantly affected by moisture content and screw rotation speed. On the other hand, brownness and redness were significantly affected by moisture content and screw rotation speed. As the water content decreased from 30% to 20%, the brownness increased by 43% from 1.62 to 2.32 and the redness increased by 84% from 0.58 to 1.07. In addition, brownness and redness tended to increase significantly when the screw rotation speed was increased from 200 to 300rpm. Brownness and redness can be an indicator of the content of saponins and ginsenosides, which are important active ingredients of ginseng and red ginseng, so saponins and ginsenosides are the highest at 20% moisture content and 300 rpm. can do. In conclusion, the extrusion condition of the extruded leaching vehicle using fresh ginseng is suitable for 20% water content and screw rotation speed of 300rpm.
한편, 백삼가루(수분함량 12%)를 수분함량(20, 25, 30%), 스크루 회전속도(200, 300rpm)를 달리하여 압출성형하고, 상기와 같은 방법으로 갈색도, 적색도 등을 측정한 결과, 백삼의 경우도 수삼과 마찬가지로 수분함량 20%, 스크루 회전속도 300rpm에서 유효성분의 함량이 높음을 확인하였다.Meanwhile, white ginseng powder (moisture content 12%) is extruded by varying water content (20, 25, 30%) and screw rotation speed (200, 300 rpm), and the brownness, redness, etc. are measured in the same manner as described above. As a result, in the case of white ginseng as well as ginseng, it was confirmed that the content of the active ingredient is high at 20% moisture content, screw rotation speed 300rpm.
실험예 2 : 압출성형 수삼의 입자크기와 현미첨가에 따른 침출특성Experimental Example 2 Leaching Characteristics of Extruded Fresh Ginseng by Particle Size and Brown Rice Addition
압출성형 공정변수인 스크루 회전속도 200rpm, 바렐 온도분포 110/80/70℃, 원료투입속도 150g/min를 고정시키고, 수분함량 20%에서 압출성형한 수삼, 수분함량 28%에서 압출성형한 수삼 및 현미를 30% 첨가하고 수분함량 28%에서 압출성형한 수삼 시료의 입자크기를 200-500㎛, 500-800㎛, 800㎛-1.0㎜로 각각 조절하여 80℃ 에서 3분간 침출한 침출액을 12,000rpm에서 10분간 원심분리한 다음, 파장 260, 420, 440, 500, 520㎚에서 상등액의 흡광도를 각각 측정하였다.The fresh ginseng extruded at 20% moisture content and fresh ginseng extruded at 20% moisture content by fixing the screw rotation speed 200rpm, barrel temperature distribution 110/80/70 ℃, raw material input speed 150g / min. 12,000rpm of the leaching solution leached at 80 ℃ for 3 minutes by adjusting the particle size of the fresh ginseng sample extruded at 30% water content and 28% moisture content to 200-500㎛, 500-800㎛, 800㎛-1.0㎜ After centrifugation for 10 minutes at, the absorbance of the supernatant was measured at wavelengths of 260, 420, 440, 500, and 520 nm, respectively.
수용성지수(WSI)와 수분흡착도(WAI)는 압출성형 수삼가루 3g을 증류수 25㎖에 넣고, 30℃ 항온 진탕기(SWB-10, Jeil Tech)에서 30분간 진탕교반한 뒤 4,000rpm에서 15분간 원심분리하여 상등액을 건조한 고형분과 시료무게의 비를 수용성지수로 표시하였다. 측정의 결과는 하기 표 2에 나타내었다.The water solubility index (WSI) and the water adsorption (WAI) were added to 3 g of extruded ginseng flour in 25 ml of distilled water, followed by shaking for 30 minutes in a 30 ° C constant temperature shaker (SWB-10, Jeil Tech), followed by 15 minutes at 4,000 rpm. The supernatant was centrifuged and the ratio of dry solids and sample weight was expressed in water solubility index. The results of the measurements are shown in Table 2 below.
수삼과 백삼의 압출성형물의 침출액과 마찬가지로 수분함량이 28%에서 20%로 감소할수록 260-520㎚ 파장에서 흡광도는 증가하는 경향을 보였다. 현미를 30% 첨가함에 따라 흡광도는 전반적으로 감소하였다. 한편, 현미를 첨가한 압출성형 인삼침출차는 인삼침출액의 농도는 약간 낮았지만 현미의 구수한 맛과 향 등의 품질을 보였다. 수용성지수도 흡광도와 동일하게 수분함량의 감소와 함께 증가하는 경향을나타내었다. 압출성형물의 입자크기를 200-500㎛, 500-800㎛, 800㎛-1.0㎜로 조절하였을 때 침출액의 흡광도는 입자크기의 감소와 함께 유의적으로 증가하는 경향을 나타내었다. 수용성지수도 흡광도와 마찬가지로 입자크기가 감소할수록 증가하는 경향을 보였다.As with the leachate of fresh ginseng and white ginseng, the absorbance tended to increase at 260-520nm as the water content decreased from 28% to 20%. The absorbance decreased overall with the addition of 30% brown rice. On the other hand, the extruded ginseng leaching tea added with brown rice showed a slightly lower concentration of ginseng leachate but the quality and taste of brown rice. The water solubility index also showed a tendency to increase with the decrease of water content, similar to the absorbance. When the particle size of the extrudate was adjusted to 200-500 μm, 500-800 μm, and 800 μm-1.0 mm, the absorbance of the leachate showed a tendency to increase significantly with the decrease of the particle size. The water solubility index also tended to increase with decreasing particle size.
실험예 3 : 압출성형공정 및 셀룰라아제 처리가 침출속도에 미치는 영향Experimental Example 3: Effect of Extrusion Molding Process and Cellulase Treatment on Leaching Rate
건조과정에서 셀룰라아제를 처리한 시료, 건조과정에서 셀룰라아제를 처리하고 압출성형한 시료, 건조과정에서 셀룰라아제를 처리하지 않고 압출성형한 시료, 압출성형공정에서 셀룰라아제를 처리한 시료에 대한 각각의 침출속도를 측정하여 압출성형공정과 셀룰라아제 처리가 침출속도에 미치는 영향을 살펴보았다.The leaching rates of the cellulase-treated samples in the drying process, the cellulase-treated and extruded samples in the drying process, the extruded samples without the cellulase in the drying process, and the cellulase-treated samples in the extrusion process were measured. Measurements were made to investigate the effects of extrusion and cellulase treatment on leaching rates.
원료수삼은 동진제약에서 5년 근 수삼을 구입하여 뇌두를 제거하고, 가정용 야채파쇄기(화진전공, 서울)로 30초간 파쇄하였다. 전처리에 사용한 효소는 최적 온도와 pH가 각각 50-60℃, 4.5-5.0인 Celluclast 1.5 L FG(Novozymes, Denmark)를 사용하였다. 건조처리 중 분산을 향상시키기 위하여 증류수로 희석시킨 0.1%의 효소용액을 혼합하였다.Raw ginseng was purchased for 5 years from Dongjin Pharm. The fresh ginseng was removed from the head, and was crushed for 30 seconds with a home vegetable crusher (Hwajin Electric, Seoul). The enzyme used for pretreatment was Celluclast 1.5 L FG (Novozymes, Denmark) with optimum temperature and pH of 50-60 ° C and 4.5-5.0, respectively. In order to improve dispersion during the drying treatment, 0.1% enzyme solution diluted with distilled water was mixed.
수삼 중량의 0.001%기준 셀루클라스트(Celluclast) 희석액을 호바트믹서(LP-201, Taiwan)를 이용해 30분간 혼합한 파쇄수삼 및 증류수를 가한 파쇄수삼(대조군)을 다음과 같은 건조조건으로 동일하게 건조하였다. 건조온도 60℃의 열풍건조기(SM-60, Jongro Industrial Co.)에서 5시간 효소반응 시킨 후 80℃에서 건조하여 수분함량을 15% 이하로 조절하였다.Dry crushed ginseng (control group) mixed with dilution of Celluclast based on 0.001% of ginseng weight for 30 minutes using Hobart mixer (LP-201, Taiwan) and dried crushed ginseng (control group) under the same drying conditions as follows. It was. After enzymatic reaction for 5 hours in a hot air dryer (SM-60, Jongro Industrial Co.) at a drying temperature of 60 ℃ and dried at 80 ℃ to control the water content to less than 15%.
스크루 직경은 31mm이고, L/D ratio는 25:1인 자체 제작한 실험용 쌍축압출성형기를 이용하여 효소처리한 건조파쇄수삼과 효소를 가하지 않은 건조파쇄수삼을 압출성형하였다. 원료사입량은 179.16g/min, 수분함량은 20%로 맞추고, 사출구의 직경은 3mm, 스크루 회전속도는 300rpm으로 고정하였다. 바렐 온도분포는 효소처리 건조수삼은 107/124/77℃ (바렐 순서 1/2/3)과 107/115/77℃, 증류수를 첨가한 대조구는 117/123/82℃에서 압출성형한 압출물을 열풍건조기 온도 80℃ 4시간 건조하여 UD mill(3010-030, UDY Co. USA)을 이용해서 분쇄하여 인삼침출차 적성을 검토하였다.The dried shredded ginseng and the enzyme-treated dry shredded ginseng were extruded using a self-experimental twin screw extruder with a screw diameter of 31 mm and an L / D ratio of 25: 1. The raw material injection amount was set at 179.16 g / min, the water content was set at 20%, the diameter of the injection hole was 3 mm, and the screw rotation speed was fixed at 300 rpm. Barrel temperature distribution is extruded at 107/124/77 ℃ for enzyme-treated dry water (1/2/3 barrel order) and 107/115/77 ℃ and 117/123/82 ℃ for control. Was dried for 4 hours at 80 ° C. in a hot air dryer, and ground using a UD mill (3010-030, UDY Co. USA) to examine the ginseng leachability.
수용성지수(WSI)와 수분흡착도(WAI)는 압출성형수삼가루 3g을 증류수 25㎖에 넣고, 30℃ 항온 진탕기(SWB-10, JEIO TECH)에서 30분간 진탕교반한 뒤 4,000rpm에서 15분간 원심분리하였다.The water solubility index (WSI) and the water adsorption (WAI) were mixed with 3 g of extruded ginseng flour in 25 ml of distilled water and stirred for 30 minutes in a 30 ° C constant temperature shaker (SWB-10, JEIO TECH), followed by 15 minutes at 4,000 rpm. Centrifuged.
압출성형수삼가루의 침출 패턴 분석은 시료 3g을 5.5cm x 4.5cm의 티백에 포장한 다음 침출반응기(TW-SM, Wooju Scientific Co. Korea)에서 60℃의 증류수 500㎖과 티백을 넣고, 임펠러 회전속도 100rpm으로 2, 4, 6, 8, 10, 15분 동안 침출시킨 침출액 10㎖을 채취하였다. 채취한 침출액을 12,000rpm에서 15분 동안 원심분리한 상등액을 여과(Whatman No.1)한 여액을 스펙트로포토미터(TU-1800pc, Human Co. Colorado, USA)를 사용하여 흡광도(파장 420, 440, 500, 520㎚)를 각각 측정하였다. 그 결과는 하기 표 3과 같다.For the leaching pattern analysis of the extruded water powder, 3g of sample was packed in a 5.5cm x 4.5cm teabag, and 500ml of 60 ° C distilled water and teabag were placed in a leaching reactor (TW-SM, Wooju Scientific Co. Korea), and the impeller was rotated. 10 ml of the leachate leached for 2, 4, 6, 8, 10, and 15 minutes was collected at a speed of 100 rpm. The supernatant was centrifuged at 12,000 rpm for 15 minutes and the supernatant was filtered (Whatman No. 1). The filtrate was absorbed by using a spectrophotometer (TU-1800pc, Human Co. Colorado, USA) (wavelengths 420, 440, 500 and 520 nm) were measured, respectively. The results are shown in Table 3 below.
압출성형 수삼시료를 티백에 담아 침출시켰을 때 440㎚에서 흡광도(갈색도)의 측정을 통한 침출속도상수(release rate constant)는 효소처리와 압출성형공정을 통해 8배정도 증가하였다. 즉 효소처리 수삼건조물의 0.0209min-1/2에서 압출성형공정을 통하여 0.1627min-1/2로 증가하는 경향을 보였다. 이것은 수삼을 셀룰로오스(cellulose) 분해효소인 셀루클라스트(Celluclast)로 처리하여 압출성형할 경우, 효과적으로 인삼침출차에 적합한 3분에서 5분 이내에 인삼의 맛과 유효성분을 침출시킬 수가 있음을 의미한다.When extruded fresh ginseng samples were leached into tea bags, the release rate constant through measurement of absorbance (brown) at 440 nm was increased by 8 times through enzymatic treatment and extrusion process. That is tended to increase in 0.1627min -1/2 throughout the extrusion process from 0.0209min -1/2 of the enzyme-treated fresh ginseng dry product. This means that when ginseng is extruded by treating with cellulose degrading enzyme, Celluclast, it can effectively leach ginseng flavors and active ingredients within 3 to 5 minutes suitable for ginseng leaching tea.
동일한 압출성형조건에서 압출성형공정을 할 때, 건조과정에 셀루클라스트를 파쇄수삼에 반응시키는 경우(B)와 건조한 파쇄수삼을 압출성형할 때 압출성형기 바렐내부로 셀루클라스트 희석액을 주입시키는 경우(D)로 효소를 처리하였는데 건조전처리 과정에 효소를 처리한 압출성형물의 수용성지수와 침출속도상수가 유의적으로 높았다.When the extrusion process is performed under the same extrusion molding conditions, when cellulose cellulose is reacted with crushed ginseng during drying (B) and when cellulose cellulose diluent is injected into the extruder barrel when extruded dry crushed ginseng The enzyme was treated with (D), but the solubility index and leaching rate constant of the extruded extruded product were significantly higher.
결론적으로, 압출성형을 통해 침출속도는 현저히 증가하며, 효소인 셀루클라스트를 처리할 경우 침출속도는 더욱 증가하며, 셀루클라스트를 압출성형 전처리건조과정에서 반응시키는 경우가 압출성형시 압출성형기 바렐내부로 직접 셀루클라스트를 반응시키는 경우보다 침출속도가 높음을 확인하였다.In conclusion, the leaching rate is significantly increased through extrusion molding, and the leaching rate is increased when the enzyme cellulose blast is treated. It was confirmed that the leaching rate is higher than the case of directly reacting cellulose blast inside.
실험예 4 : 섬유소분해효소 및 전분분해효소 처리가 침출속도에 미치는 영향Experimental Example 4 Effect of Fibrinase and Starch Enzyme Treatment on Leaching Rate
침출속도를 더욱 증가시키기 위한 방안으로 셀루클라스트와 함께 전분분해효소인 Termamyl?Supra와 AMG를 파쇄수삼의 건조전처리 동안에 첨가하여 압출성형하는 경우 침출속도를 비교하였다.In order to further increase the leaching rate, the leaching rate was compared in the case of extrusion molding by adding starch degrading enzymes Termamyl®Supra and AMG together with cellulose blast during dry pretreatment of crushed ginseng.
동진제약에서 구입한 5년근 수삼의 뇌두를 제거하고 가정용파쇄기로 30초간 파쇄하였다. 파쇄한 수삼건조는 두 가지 방법을 사용하였는데, 3가지 효소를 첨가한 것과 효소를 첨가하지 않고 증류수를 첨가한 것으로 나누었다.The head of five-year-old ginseng from Dongjin Pharm was removed and crushed for 30 seconds with a domestic crusher. The dried ginseng was divided into two methods, divided into three enzymes and distilled water without enzymes.
활성온도와 pH가 각각 90-95℃, 5-6인 Termamyl Supra(Novozymes, Denmark)를 인삼 1kg당 112.6㎕의 효소를 100㎖의 증류수로 희석시킨 뒤 호바트믹서(LP-201, Taiwan)를 이용해 30분간 혼합하였다. 잘 혼합된 시료를 80℃ 건조기에서 1시간 30분 효소 반응과 호화시켰다.Termamyl Supra (Novozymes, Denmark), whose activity temperature and pH are 90-95 ° C and 5-6, respectively, was diluted 112.6 μl of enzyme per kg of ginseng with 100 ml of distilled water and then Hobart mixer (LP-201, Taiwan). Mix for 30 minutes. The well mixed sample was enzymatically subjected to enzymatic reaction for 1 hour and 30 minutes at 80 DEG C.
여기에 활성온도와 pH가 각각 60-63℃, 4-4.5인 AMG(Novozymes, Denmark)와 활성온도와 pH가 각각 50-60℃, 4.5-5인 Celluclast 1.5 L FG(Novozymes, Denmark)을 각각 164㎕과 2.5㎕를 100㎖ 증류수에 희석시켜 30분간 혼합하였다. 두 가지 효소를 혼합한 파쇄수삼을 60℃의 건조기에 넣고 45시간 동안 효소 반응과 압출성형 조건에 알맞게 건조시킨 효소처리와 함께 건조된 시료를 조제하였다. 또한 3가지 효소대신에 중류수를 첨가하여 건조한 파쇄수삼을 대조구로 하여 비교하였다.AMG (Novozymes, Denmark) at 60-63 ° C and 4-4.5, respectively, and Celluclast 1.5 L FG (Novozymes, Denmark) at 50-60 ° C and 4.5-5, respectively. 164 μl and 2.5 μl were diluted in 100 ml distilled water and mixed for 30 minutes. The crushed ginseng mixed with the two enzymes was put in a dryer at 60 ° C., and a dried sample was prepared with the enzyme treatment dried for 45 hours according to the enzyme reaction and the extrusion molding conditions. In addition, dried crushed ginseng was added as a control by adding midstream water instead of three enzymes.
건조한 효소처리하여 건조한 파쇄 수삼의 사입량은 180g/min, 수분함량은 20%, 사출구의 직경은 3mm, 스크루 회전속도는 300rpm으로 고정하였다. 또한 바렐의 온도분포는110/100/84℃ (바렐순서 1/2/3)로 조절하여 압출성형을 하였다. 압출성형한 수삼을 열풍건조기에서 80℃, 4시간 건조하여 입지크기 200-500㎛로 분쇄하여 압출성형 침출차시료로 하였다.Dry enzymatic treatment of dried crushed ginseng was fixed at 180g / min, water content 20%, diameter of injection hole 3mm, screw rotation speed at 300rpm. In addition, the temperature distribution of the barrel was adjusted to 110/100/84 ° C. (barrel order 1/2/3) to perform extrusion molding. The extruded ginseng was dried at 80 ° C. for 4 hours in a hot air dryer, and ground to a size of 200-500 μm to obtain an extruded leaching sample.
파쇄한 수삼의 건조 전처리과정에 3가지 효소를 반응시켜 압출성형한 침출차시료의 수용성지수(WSI), 수분흡착도(WAI)와 침출패턴 분석하여 침출속도상수(k)를 계산하였다. 수용성지수(WSI)는 시료 3g과 증류수 25㎖에 넣고, 30℃ 항온 진탕기(SWB-10, JEIO TECH)에서 30분간 교반한 뒤 원심분리(4000rpm, 15min)하여 상등에 포함된 고형분함량에 대한 시료의 비로 나타내었다.The leach rate constant (k) was calculated by analyzing three enzymes in the dry pretreatment of crushed fresh ginseng by analyzing the water-soluble index (WSI), water adsorption degree (WAI) and leaching pattern of the extruded leaching tea samples. The water-soluble index (WSI) was added to 3 g of sample and 25 ml of distilled water, stirred for 30 minutes in a 30 ° C constant temperature shaker (SWB-10, JEIO TECH), followed by centrifugation (4000rpm, 15min) for the solid content contained in the upper portion. Shown as the ratio of the samples.
침출패턴 시료 3g을 5.5cm x 4.5cm의 티백에 담아서 반응기(TW-SM, Wooju Scientific Co. Korea)에 60℃ 증류수 500㎖과 티백을 넣고, 페달의 회전속도 100rpm에서 침출시간 2, 4, 6, 8, 10, 15 분마다 각각 10㎖의 침출액을 채취해서 원심분리(12000rpm, 15min)한 다음 여과(Whatman No.1)하였다. 여액을 스펙트로포토미터(TU-1800pc, Human Co. CO, USA)로 파장 420, 440, 500, 520㎚에서 각각 흡광도를 측정하였다. 그 결과는 하기의 표 4와 같다.3g of the leaching pattern sample was placed in a 5.5cm x 4.5cm teabag, and 500ml of 60 ° C distilled water and teabag were put into a reactor (TW-SM, Wooju Scientific Co. Korea), and leaching time 2, 4, 6 at the rotation speed of the pedal at 100rpm. 10 ml of leachate was collected every 8, 10 and 15 minutes, and then centrifuged (12000 rpm, 15 min) and filtered (Whatman No. 1). The filtrate was measured for absorbance at wavelengths 420, 440, 500 and 520 nm, respectively, using a spectrophotometer (TU-1800pc, Human Co. CO, USA). The results are shown in Table 4 below.
3가지 효소처리를 하여 압출성형한 시료의 침출율이 가장 높았으며 침출속도상수(k)는 0.1754min-1/2로 효소를 처리하지 않은 시료의 0.01824min-1/2보다 10배 정도 증가하였다. 파쇄수삼의 건조과정 중 3가지 효소의 처리에 의하여 수용성지수는 43.2%에서 48.8%로 5.6% 증가하였다. 압출성형공정을 통하여 10%가량 수용성지수가 증가하였다. 또한 침출속도상수는 건조과정중 효소처리를 통해 2배 증가하였으며 압출성형을 통해 측정한 파장에서 흡광도는 10배 정도 증가하는 경향을 보였다.The leaching rate of the samples extruded by three enzyme treatments was the highest, and the leaching rate constant (k) was 0.1754min -1/2, which was 10 times higher than 0.01824min -1/2 of the samples without enzyme treatment. . The water solubility index increased by 5.6% from 43.2% to 48.8% by treatment of three enzymes during the drying process of shredded ginseng. The water solubility index increased by about 10% through the extrusion process. In addition, the leaching rate constant increased twice by enzymatic treatment during the drying process, and the absorbance tended to increase about 10 times at the wavelength measured by extrusion molding.
실험예 5 : 압출성형 인삼침출차 제품의 관능검사Experimental Example 5 Sensory Evaluation of Extruded Ginseng Extraction Products
압출성형공법과 효소반응으로 개발한 인삼침출차의 품질을 평가하기 위하여 식품공학과 남학생 6명, 여학생 8명을 대상으로 관능검사를 실시하였다. 시료는 건조과정 동안 Termamyl Supra?, AMG 및 Celluclast를 파쇄수삼에 반응시켜서 건조한 파쇄수삼을 수분함량 20%, 사출구의 직경 3mm, 스크루 회전속도 300rpm, 바렐의 온도분포 110/100/84℃ (바렐순서 1/2/3)로 조절하여 압출성형한 수삼을 열풍건조기에서 80℃, 4시간 건조하여 입지크기 200-500㎛로 분쇄하여 압출성형 침출차 시제품으로 하였다. 관능검사에서는 시제품의 품질특성은 분말의 색과 향기, 침출액의 색, 향, 맛을 용어의 선정과 함께 시중에서 판매되는 추출형 홍삼정차(고려인삼창, 농협)와 품질비교를 하였다.In order to evaluate the quality of ginseng leaching tea developed by extrusion and enzymatic reaction, sensory tests were conducted on 6 male and 8 female students. The sample was reacted with Termamyl Supra®, AMG and Celluclast to crushed ginseng during the drying process to make the dried crushed ginseng water content 20%, diameter of injection hole 3mm, screw rotation speed 300rpm, barrel distribution 110/100/84 ℃ (barrel 1/2 g) extruded ginseng was dried at 80 ° C. for 4 hours in a hot air dryer, and ground to 200-500 μm in size. In the sensory test, the quality characteristics of the prototypes were compared with those of commercially available red ginseng tea (Korea ginseng chang, Nonghyup) with the selection of terms for the color and aroma of the powder and the color, aroma and taste of the leachate.
관능검사용 시료는 홍삼정차 1백(3g)을 80℃ 증류수 80㎖에 녹인 홍삼정차시료와 80℃의 증류수 80㎖에 압출성형 침출차시제품 5g을 담은 티백을 5분 동안 침출시킨 침출액을 시료로 하여 관능검사를 하였다.Samples for sensory test were red ginseng tea samples containing 100 g of red ginseng tea in 80 ml of distilled water at 80 ° C, and a leachate obtained by leaching a tea bag containing 5 g of an extruded leach tea product in 80 ml of distilled water at 80 ° C for 5 minutes. Sensory evaluation was performed.
홍삼정차의 용액과 압출성형 인삼침출차 시제품과 침출액의 색, 맛, 향에 대한 용어의 빈도는 하기의 표 5와 같다.The frequency of terms for the color, taste and aroma of the red ginseng tea solution and the extruded ginseng leach tea prototype and the leach solution are shown in Table 5 below.
압출성형 침출차는 쓴맛이 홍삼전차보다 높았다. 이것은 압출성형 침출차 제품과 비교하여 홍삼정차는 홍삼추출액과 포도당과 유당이 첨가되어 원료의 조성의 차이에 기인하는 것으로 판단되었다.The extruded leaching tea had a bitter taste higher than the red ginseng tank. This is because red ginseng tea was added to red ginseng extract, glucose and lactose compared to the extruded leach tea products.
압출성형 인삼침출차의 경우 단맛과 구수한 맛이 홍삼정차보다 높았다. 또한쓴맛과 떫은맛은 홍삼정차보다 낮게 나타났다. 그러므로 전체적인 기호도는 압출성형 인삼침출차가 홍삼정차보다 높게 나타났다.In the case of extruded ginseng leaching tea, the sweet and sour taste was higher than the red ginseng tea. Bitter and astringent tastes were lower than those of red ginseng tea. Therefore, the overall acceptability of extruded ginseng leaching tea was higher than that of red ginseng tea.
실험예 6 : 가정용 원두커피 추출기용 인삼침출차의 침출율 조사Experimental Example 6: Investigation of leaching rate of ginseng leaching tea for home bean coffee extractor
압출성형수삼을 이용하여 티백 형태의 침출차 이외에 가정용 원두커피 추출기에 침출하여 손쉽게 음용할 수 있는 인삼차를 제조할 수 있는지 여부를 알아보기 위하여, 침출율에 대한 실험을 수행하였다.In order to find out whether the ginseng tea can be easily prepared by leaching it in domestic coffee bean extractor in addition to the tea bag type leaching tea using the extruded ginseng, an experiment on the leaching rate was performed.
효소를 반응시키지 않은 건조수삼(A), 3가지 효소로 반응시킨 건조수삼(B), 효소를 반응시키지 않은 건조수삼을 압출성형한 시료(C), 3가지 효소로 반응시킨 건조수삼을 압출성형한 시료(D) 각 3g을 커피여과지 위에 담아 증류수 200㎖이 여과지를 통과하면서 인삼이 침출되는데 걸리는 시간, 커피여과지를 통과하여 침출된 고형분량, 침출된 인삼침출액의 흡광도를 파장 420㎚, 440㎚, 500㎚, 520㎚에서 각각 측정하였다. 그 결과는 하기 표 6과 같다.Extruded dry ginseng (A) without enzyme reaction, dried ginseng (B) reacted with three enzymes, sample (C) extruded dry ginseng without enzyme reaction, and dry ginseng reacted with three enzymes 3 g of each sample (D) was placed on a coffee filter paper, and the time required for 200 g of distilled water to leach ginseng as it passed through the filter paper, the amount of solids leached through the coffee filter paper, and the absorbance of the leached ginseng leachate were 420 nm and 440 nm. It measured at 500 nm, 520 nm, respectively. The results are shown in Table 6 below.
압출성형과 효소처리에 의해 여과지로 인삼추출액이 통과하는데 걸리는 시간이 단축되었으며 여과지를 통과한 고형분량, 흡광도가 유의적으로 증가하였다.Extrusion and enzymatic treatment shortened the time taken for the ginseng extract to pass through the filter paper, and the amount of solids and absorbance through the filter paper were significantly increased.
따라서, 티백 형태의 인삼침출차뿐만 아니라, 인삼침출용 여과지나 가정용 커피추출기와 유사한 인삼침출용 추출기로 침출시켜 음용하는 형태의 인삼차 제조가 가능함을 알 수 있다.Accordingly, it can be seen that ginseng tea of the ginseng leach tea, as well as ginseng leaching filter paper or ginseng leaching extractor similar to domestic coffee extractor can be produced by drinking ginseng tea.
실험예 7 : 압출성형수삼의 미세입자화를 통한 용해성 및 분산성 실험Experimental Example 7: Solubility and dispersibility test through microparticles of extruded ginseng
80℃에서 5시간 건조한 수삼(A), 건조한 수삼을 수분함량 25%, 사출구부위 온도 110℃, 스크루 회전속도 250 rpm에서 압출성형한 시료(B), 건조전처리 동안 섬유소 분해효소, 전분 분해효소를 처리하여 압출성형한 시료(압출성형조건은 B와 동일) (C)를 각각 건조하여 실험용 미세입자분쇄기를 사용하여 입자크기를 100㎛ 이하로 미세입자화하여 액상용매에 용해하여 분산시켰을 때 수용성지수(용해성) 및 분산성을 측정하였다.Fresh ginseng (A) dried at 80 ° C for 5 hours, 25% water content of dried ginseng, 110 ° C of injection hole temperature, sample extruded at 250 rpm of screw rotation speed, fibrinase, starch degrading enzyme during drying pretreatment Samples extruded by extruding (extrusion molding conditions are the same as B), each dried (C), and then used in an experimental microparticle crusher to make a particle size of 100 μm or less and dissolved and dispersed in a liquid solvent. Index (soluble) and dispersibility were measured.
그 결과, 건조수삼의 수용성지수 24.7%와 비교하여 압출성형한 시료의 수용성지수는 36.7%, 효소처리 압출성형한 시료는 42.2%로 크게 증가하였다.As a result, the water-soluble index of the extruded sample increased to 36.7% and that of the enzyme-treated extruded sample to 42.2%, compared to the water-soluble index of 24.7% of the dried ginseng.
분산성은 각 시료의 분산성을 비교하기 위하여 0.5g의 시료를 시험관에 담아 20㎖의 물에 분산시켰으며, 그 결과는 도 2에 나타내었다. 분산 후 2분 후 건조한 수삼(A-2)는 액상과 침전된 층의 구별이 나타나기 시작하였으나, 압출성형한 시료(B-2), 섬유소 분해효소, 전분 분해효소를 처리하여 압출성형한 시료(C-2)는 침전층의 구별이 뚜렷하지 않았다. 또한 8분에 건조한 수삼(A-8)는 침전층의 구별이 뚜렷하였으나 압출성형한 시료(B-8), 건조전처리 동안 효소를 처리하여 압출성형한 시료(C-8)는 분상정도가 양호하였다(도 2 참조).Dispersibility In order to compare the dispersibility of each sample, 0.5g of sample was placed in a test tube and dispersed in 20ml of water, and the result is shown in FIG. After 2 minutes of dispersion, the dried ginseng (A-2) began to distinguish between the liquid phase and the precipitated layer. However, the extruded sample (B-2), fibrinase, and starch degrading enzyme were treated to extrude ( C-2) did not distinguish distinctive layers. In addition, the fresh ginseng (A-8) dried at 8 minutes was clearly distinguished from the sedimentation layer, but the extruded sample (B-8) and the extruded sample (C-8) processed by the enzyme during the drying pretreatment had a good degree of phase separation. (See FIG. 2).
그러므로, 건조수삼 또는 백삼가루를 압출성형하거나 효소처리하여 압출성형한 인삼압출성형물을 미세입자화함으로써 액상용매에 용해 또는 분산시켜 음용하는 인삼차 제품을 제조할 수 있음을 확인하였다.Therefore, it was confirmed that ginseng tea products can be prepared by dissolving or dispersing the dried ginseng or white ginseng powder by dissolving or dispersing the extruded ginseng extrudate by enzymatic treatment.
본 발명은 압출성형공정에 의하여 인삼 침출차를 제조하는 방법에 관한 것으로, 압출성형공정에 의하여 단시간에 효과적으로 인삼 유효성분의 침출을 가능하게 할 뿐만 아니라 관능적으로도 우수한 인삼 침출차 형태의 제품을 제공하므로 이는 식품 산업상 매우 유용한 발명인 것이다.The present invention relates to a method for manufacturing a ginseng leaching tea by an extrusion molding process, which not only enables the leaching of effective ginseng active ingredients in a short time by the extrusion molding process, but also provides a product of a sensory excellent ginseng leaching tea form. It is a very useful invention in the food industry.
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KR100841656B1 (en) * | 2005-09-05 | 2008-07-02 | 유정상 | Manufacturing process of soluble components for ginseng |
KR100907497B1 (en) * | 2007-07-19 | 2009-07-13 | 한국식품연구원 | A manufacturing method of tea for using a extrusion molding |
KR100908014B1 (en) * | 2007-10-10 | 2009-07-16 | 주식회사농심 | Method for preparing red ginseng extract through injection molding |
KR20180082798A (en) * | 2017-01-11 | 2018-07-19 | 씨지에프주식회사 | Manufacturing method of gland containing saponin |
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KR100841656B1 (en) * | 2005-09-05 | 2008-07-02 | 유정상 | Manufacturing process of soluble components for ginseng |
KR100907497B1 (en) * | 2007-07-19 | 2009-07-13 | 한국식품연구원 | A manufacturing method of tea for using a extrusion molding |
KR100908014B1 (en) * | 2007-10-10 | 2009-07-16 | 주식회사농심 | Method for preparing red ginseng extract through injection molding |
KR20180082798A (en) * | 2017-01-11 | 2018-07-19 | 씨지에프주식회사 | Manufacturing method of gland containing saponin |
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