KR20030018038A - Method of inoganic Fireproof Paint and Fireproof Bond - Google Patents

Method of inoganic Fireproof Paint and Fireproof Bond Download PDF

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Publication number
KR20030018038A
KR20030018038A KR1020030008372A KR20030008372A KR20030018038A KR 20030018038 A KR20030018038 A KR 20030018038A KR 1020030008372 A KR1020030008372 A KR 1020030008372A KR 20030008372 A KR20030008372 A KR 20030008372A KR 20030018038 A KR20030018038 A KR 20030018038A
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South Korea
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adhesive
fire
flammable
retardant
paint
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KR1020030008372A
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Korean (ko)
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조성균
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조성균
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Priority to KR1020030008372A priority Critical patent/KR20030018038A/en
Publication of KR20030018038A publication Critical patent/KR20030018038A/en

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J1/00—Adhesives based on inorganic constituents
    • C09J1/02—Adhesives based on inorganic constituents containing water-soluble alkali silicates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks

Abstract

PURPOSE: A method for preparing an inorganic fireproof paint/adhesive is provided, wherein the inorganic fireproof paint/adhesive is applied to paper, plywood, wood, rock, cement or steel plate materials and shows the adhesive power by natural drying or drying at a temperature below 100 deg.C. CONSTITUTION: The method comprises the step of mixing sodium silicate as a ceramic binder, 10 wt% of borax or boric acid (H3BO3), and optionally a dye and preparing the mixture into an aqueous solution.

Description

무기 방화 페인트 겸 방화접착제 제조방법.{Method of inoganic Fireproof Paint and Fireproof Bond}Production method of inorganic fire retardant paint and fire retardant adhesive {Method of inoganic Fireproof Paint and Fireproof Bond}

본 발명의 방화페인트 기능은 가연성 소재로된 건축 내외장재, 가구 및 집기류 등의 노출된 표면에 스프레이나 붓으로 도포하여 자연 건조 시키면 방염처리가 되고 색상이 필요시에는 임의의 색소를 첨가시키면 도색 역할까지 할 수 있다. 화재 발생시 방염처리층은 열침해를 받어 부풀어 올라 단열 방화층을 형성하여 인화 발화접을 지연시키고 접착된 표면층은 가연성 소재에 함침 고착되어 있으므로 산소를 차단하여 가연성 소재가 불꽃 없이 탄화되어 소방기준치를 충분히 만족시킨다. 방화접착제의 기능중 면 접찹 경우는 가연성소재나 비가연성 소재의 동일 종류나 이질 종류 관계없이 접착면에 스프레이나 붓으로 도포하여 접착시켜 자연건조나 시간단축을 요할 시에는 방염, 반응온도 이하인 100도씨 이하 저온으로 건조시키면 완벽한 접착면을 갖고 화재 발생시 열 침해를 받으면 도포된 접착층이 부풀어 올라 단열 방화층을 형성하여 인화발화점을 지연시키고 양 접착면을 접착제와 함침 고착되어 소재에 산소를 차단시켜 불꽃없이 탄화된다.Fire-retardant paint function of the present invention is applied to the exposed surface, such as building interior and exterior materials, furniture, and household appliances made of combustible materials by spraying or brushing it to be dried naturally, it is flame-retardant treatment, if the color is required to add any pigment to the paint role can do. In the event of a fire, the flame-retardant layer undergoes thermal invasion and swells to form an insulating fire-proof layer, delaying ignition ignition, and the bonded surface layer is impregnated with a flammable material. Let's do it. In the case of the function of fire-retardant adhesive, if it is a cotton glue, it is applied to the adhesive surface by spray or brush regardless of the same kind or heterogeneous type of flammable material or non-flammable material. When dried at a low temperature below the seed, it has a perfect adhesive surface, and if it is invaded by heat in case of fire, the applied adhesive layer swells to form a thermal insulation fireproof layer, delays the flash point, and impregnates both adhesive surfaces with an adhesive to block oxygen to the material Without carbonization.

방화접착제의 기능중 가연성 비가연성 분말형의 소재(목재분, 종이분, 흙, 모래등)을 접착 고형화 시킬 경우 소정의 접착제를 임의의 소재와 배합 압축성형하여 자연건조나 100도씨 이하 저온으로 건조시키면 소재의 고유 물성을 유지하면서 견고한 고형체가 이루어진다.In case of flammable non-flammable powder type materials (wood flour, paper powder, soil, sand, etc.) among the functions of the fire retardant adhesive, certain adhesives are mixed with any material and compressed to form natural dry or low temperature below 100 degrees. Drying results in a solid solid that retains the material's inherent properties.

화제 발생시 고온으로 상승하여 인화발화점을 지나도 망상형태로 혼합결합되어 있어 단열방화층으로 되며 산소의 차단으로 고형체를 유지하면서 탄화되어 화염 차단 효과를 얻는다.When the fire is generated, it rises to a high temperature and is mixed in a mesh form even after passing through the flash point, so that it becomes a heat-insulating fireproof layer and is carbonized while maintaining a solid body by blocking oxygen to obtain a flame blocking effect.

상기와 같이 본 발명품은 무기소재로 이루어져 그 자체만으로도 방염 역활을 할 수 있고 용재가 물(H2O) 이므로 화재의 위험이 없고 냄새가 없어 친 환경적이다.As described above, the present invention is made of an inorganic material and can act as a flame retardant by itself, and since the solvent is water (H 2 O), there is no risk of fire and no smell, which is environmentally friendly.

표면도포나 접착작업이 간편하고 방염기능, 접착기능, 도색기능등 다기능을 갖는 장점이 있고 소재 자체가 저가이므로 대중적으로 사용될 수 있는 개발품이다.It is a development product that can be widely used because it has the advantages of simple surface coating and adhesive work, multi-function such as flame retardant function, adhesive function, and painting function.

종래 제품은 많이 개발되어 있으나 제품소재가 대다수 유무기 혼합형이고 용제가 가연성 신너이므로 사용상 화재의 위험이 있고 유해성 냄새가 나기 때문에 비환경적이고 고가이다.Conventional products have been developed a lot, but since most of the product materials are organic-inorganic mixed type and the solvent is a flammable thinner, there is a risk of fire in use and it is non-environmental and expensive because of the harmful smell.

본 발명은 무기물 수성 바인더를 기조로 하고 무기물인 방염제 및 필요시 임의 색소를 혼합교반하여 수용액 상태로 제조되어 물(H2O)로 희석할 수 있고 스프레이나 붓으로 가연성 소재에 도포하고 자연건조하면 소방기준에 적합한 방염기능을 수행할 수 있고 방염접착제의 기능중 면접착의 경우는 가연성 소재나 비가연성 소재의 동일 종류나 이질 종류 관계없이 접착면에 스프레이나 붓으로 도포하여 접착시켜 자연건조나 100도씨 이하 저온으로 건조시키면 완벽한 접착면을 갖고 화재 발생시 열침해를 받으면 도포된 접착층이 부풀어 올라 단열방화층을 형성하고 양접착면을 접착제와 함침 고착되어 소재에 산소를 차단시켜 불꽃 없이 탄화되어 방염작용을 한다.The present invention is based on an inorganic aqueous binder, and mixed with an inorganic flame retardant and optional pigment if necessary, prepared in the form of an aqueous solution can be diluted with water (H 2 O) and applied to a combustible material with a spray or a brush and dried naturally It is possible to perform fire-resistance function that meets the standard of fire-fighting, and in case of surface adhesion among the functions of flame-retardant adhesive, it is applied by spraying or brushing on the adhesive surface irrespective of the same kind or heterogeneous type of flammable material or non-flammable material. If the temperature is lower than the seed, it has a perfect adhesive surface, and if it is thermally invaded in the event of a fire, the applied adhesive layer swells to form a heat insulation fireproof layer, and both adhesive surfaces are impregnated with an adhesive to block oxygen in the material to be carbonized without flame to be flame-retarded. Do it.

방화 접착제의 기능 중 가연성, 비가연성 분말형의 소재(목재분, 종이분, 흙, 모래 등)을 소정의 형태로 접착고형화 시킬 경우 소정의 접착제와 임의의 소재를 배합하여 압축성형하고 건조시키면 견고한 고형체가 형성되며 열 침해시 단열 및 산소 차단 효과가 있어 강도 있는 고형체를 유지하면서 탄화된다.In case of flammable and non-flammable powder material (wood powder, paper powder, soil, sand, etc.) in the form of adhesive, solidified by compression molding and drying by mixing the specific adhesive and any material. Solids are formed, and they have a thermal insulation and oxygen blocking effect during heat invasion and are carbonized while maintaining a solid solid.

도색이 필요시에는 색소를 첨가 사용하면 방염, 발색 기능을 동시에 수행한다.When painting is required, the addition of pigments can be used for flame retardant and color development functions.

상기와 같이 소방기준에 적합하고 사용이 간편하고 안정성이 있고 환경친화적이며 복합기능을 수행한다.As above, it meets the firefighting standards, is simple to use, stable, environmentally friendly, and performs a combination of functions.

도1은 본 발명의 무기방화 페인트 겸 방화접착제 중 방화페인트를 가연성소재의 노출된 표면에 도포된 도막층과 가연성 소재 상층부에 흡수된 흡수층의 단면도1 is a cross-sectional view of an absorbing layer absorbed by a coating layer coated on the exposed surface of a combustible material and an upper portion of the combustible material in the inorganic fire-retardant paint and fire-retardant adhesive of the present invention;

도2는 도1에서 방화페인트 도막층이 열을 받어 부풀어 오른 변형된 방화벽층과 가연성소재 표면에 흡수된 흡수층의 탄화된 부위의 단면도.FIG. 2 is a cross-sectional view of the carbonized portion of the deformed firewall layer and the absorbent layer absorbed on the flammable material surface in FIG.

도3은 본 발명의 무기방화페인트겸 방화 접착제중 방화 접착제로 접착한 단면도.Figure 3 is a cross-sectional view of the inorganic fire-retardant paint and fire-retardant adhesive of the present invention bonded with a fire-retardant adhesive.

도4는 도3의 접착층이 열 침해로 부풀어 올라 변형된 방화벽 층.FIG. 4 is a firewall layer in which the adhesive layer of FIG. 3 is inflated due to heat intrusion. FIG.

도5는 방화 접착제중 분쇄된 유무기 분말 재료를 방화접착제와 배합하여 접착 고형화 시킨 제품의 단면도.5 is a cross-sectional view of a product in which the solidified organic-inorganic powder material in the fire prevention adhesive is combined with the fire prevention adhesive to solidify the adhesive.

도6은 도5의 고형화된 제품이 열 침해를 받아 탄화되어도 견고한 형태를 유지한 상태의 단면도.FIG. 6 is a cross-sectional view of the solidified product of FIG. 5 in a state in which a solid form is maintained even when carbonized under heat intrusion; FIG.

[도면의 주요부분에 대한 부호의 설명][Explanation of symbols on the main parts of the drawings]

1. 가연성 소재 2. 가연성소재 표면에 도포 된 방화페인트 층 3. 가연성 소재 표면에 방화 페인트가 흡수된 층 4. (2)의 방화 페인트층이 열 침해를 받어부풀어 오른 변형된 상태의 층 5. (3)의 흡수층이 열 침해를 받어 탄화된 층1. Flammable material 2. Fire-retardant paint layer applied on the surface of flammable material 3. Layer where fire-resistant paint is absorbed on the surface of flammable material 4. Deformed layer in which the fire-resistant paint layer of (2) is swollen by heat invasion 5. Absorbent layer of (3) is heat invaded and carbonized layer

6. 접착소재(가연성 미 비가연성) 7. 무기방화 접착제로 접착된 단면층6. Adhesive material (non-flammable, non-flammable) 7. Single layer bonded with inorganic fireproof adhesive

8. (7)이 열 침해를 받어 부풀어 오른 변형된 상태의 층 9. 유무기 분말형태의 소재를 무기방화 접착제로 접착된 고형체의 단면도 10. (9)의 고형체가 열 침해를 받어 탄화된 상태의 탄화된 고형체.8. Deformed layer swelled due to heat invasion (7) 9. Cross-sectional view of solid body in which inorganic-inorganic powder-like material is bonded with an inorganic fireproof adhesive 10. Solids in (9) are thermally invaded and carbonized Carbonized solids in the sealed state.

본 발명의 구성은 접착 기능을 하는 규산소다(NaO·nSiO2·xH2O)를 기조로한 세라믹 바인더에 방염기능을 하는 붕산(H3BO3)이나 유사기능을 하는 붕사(Na2B4O7·10H2O)를 규산소다 대비 10% 내외, 발색이 필요시 임의의 색소를 첨가 혼합교반하여 수용액으로 제조한 무기 방화페인트 겸 방화 접착제를 필요시 용제인 물(H2O)로 적절히 희석하여 방염을 필요로 하는 경우에는 가연성 소재(벽지, 합판,목재, 가구류 등)에 스프레이 혹은 붓으로 도포하여 자연 건조시키면 도1에서와 같이 가연성 소재(1) 표면에 유리상의 도표면(2)이 형성되고 가연성소재(1) 상단층에 접착제가 흡수된 층(3)이 형성된다.The composition of the present invention is boric acid (H 3 BO 3 ) or flame retardant boric acid (Na 2 B 4 ) to the flame retardant function in a ceramic binder based on sodium silicate (NaO · nSiO 2 · xH 2 O) to the adhesive function O 7 · 10H 2 O) is about 10% compared to sodium silicate, and any color is mixed and stirred if necessary to develop an inorganic fire-retardant paint and fire-retardant adhesive prepared as an aqueous solution with water (H 2 O) as needed. If dilution is required for flame retardant, spray or brush on flammable material (wall paper, plywood, wood, furniture, etc.) and dry it naturally. Is formed and a layer 3 on which the adhesive is absorbed is formed on the upper layer of the combustible material 1.

방화 접착제 기능 중 면 접착을 할 경우에는 가연성 소재, 불연성 소재 도 3의(6) 즉 종이류, 목재류, 석재류, 시멘트 류, 철판류 등의 소재에 방화 접착제를 도포하여 동종류나 이종류 간에 접착시키면 접착층(7)이 형성되며 자연건조나 속건을 요할 시에는 열 반응 이하 온도인 100도씨 이하 저온으로 건조하면 완벽한 접착력을 갖는다.In case of surface bonding among the fire retardant adhesives, flammable and non-flammable materials are applied to the same or different types by applying a fire retardant to a material such as paper, wood, stone, cement, iron plate, etc. of FIG. 3 (6). When the adhesive layer 7 is formed, when it is required to dry naturally or fast-drying, the adhesive layer 7 has a perfect adhesive strength when dried at a low temperature below 100 ° C, which is a temperature below the thermal reaction.

방화접착제 기능 중 분말형을 고형화 시에는 소재 도5(목재류 분쇄분, 종이류분, 흙, 모래 등) 중 소정의 방화 접착제를 첨가 배합하여 압축 성형하고 자연건조나 저온 건조시키면 물성의 변화 없이 견고한 고형체가 제조된다.When solidifying the powder form among the fire-resistant adhesives, a certain fire-resistant adhesive is added and blended in the material Figure 5 (wood, crushed, paper, soil, sand, etc.), and it is compressed and formed by natural drying or low temperature drying. Shapes are made.

발색 기능이 필요시 색소를 첨가한 방화 페인트를 소재에 도포하면 방염기능과 색상도료의 기능을 동시에 얻는다.When color development is needed, the fire prevention paints with pigments are applied to the material to obtain the functions of flame retardant and color paint.

본 발명의 방염작용은 무기방화페인트로 형성된 도포층 (2)은 화재 발생시 150도씨 내외에서부터 온도가 상승함에 따라 붕산은 피로붕산(H2B4O7)과 유리상태로 변형하면서 거품상태로 부풀어 오른 단열 방화층 도2의 (4)이 만들어저 가연성소재 (1)에 인화 착화점을 지연시키며 온도 상승에 따라 발화되지 않은 것은 가연성소재 표면과 가연성소재 상단부(3)에 방화페인트 흡수층(5)이 유리(glass)상태로 고착되어 산소를 차단시켜 발화하지 않고 탄화가 이루어지므로 소방기능을 충분히 만족시킨다.Flame-retardant action of the present invention is the coating layer (2) formed of an inorganic fire-resistant paint as the temperature rises from about 150 degrees when the fire occurs boric acid is transformed into a pyroboric acid (H 2 B 4 O 7 ) and a glass state in a foam state Puffed Insulation Fire Protection Layer FIG. 2 (4) is made to delay the ignition point of the combustible material (1) and not ignite as the temperature rises, the fire resistant paint absorbing layer (5) on the surface of the combustible material and the upper part of the combustible material It is fixed in this glass (glass) state and blocks oxygen so that carbonization is performed without ignition so that the fire fighting function is sufficiently satisfied.

방화접착제 중 면접착의 효과는 화재 발생시 도3의 (7) 접착층이 화재로 인해 과열이 되면 상기 기술한 바와 같이 거품상태로 부풀어 오른 단열방화층 도4의 (8)이 형성되고 소재(6)의 접착면은 유리상태로 고착되어 산소 차단으로 발화되지 않고 탄화가되어 방염 작용을 하고 방화 접착제로 접착하고 접착한 소재 표면에 방화 페인트로 도포하면 방화효과는 배가되며 극대화된다.The effect of surface adhesion among the fireproof adhesives is that when the fire occurs, the adhesive layer of FIG. 3 (7) is overheated due to the fire. The adhesive surface is fixed in the glass state and is not fired by the oxygen barrier, but is carbonized to act as a flame retardant. The fire protection effect is doubled and maximized when it is applied with fire protection paint on the surface of the bonded material.

방화 접착제 기능 중 분말 고형화시의 효과는 압축성형된 고형체도5가 열침해를 받으면 단열 및 산소 차단효과가 있어 강도 있는 탄화 고형체가 되므로 방화 효과가 있다.The effect of powder solidification during the fire prevention adhesive function is the fire protection effect because the compressed molded solid figure 5 is thermally infiltrated and has an oxygen blocking effect, resulting in a strong carbonized solid.

이와 같은 구성으로 된 무기 방화 페인트 겸 방화 접착제는 무기물로 구성되어 방염효과가 탁월하고 용제는 물(H2O)로 사용하므로 사용 시 화제 위험이 없고 냄새가 없어 환경친화적이고, 방화접착제로 소재를 필요 용도에 붙이고 붙인 소재 전면에 방염처리를 하면 방염효과가 배가되어 탁월하다.Inorganic fire retardant paint and fire retardant adhesive composed of such a composition is composed of inorganic material and has excellent flame retardant effect and solvent is used as water (H 2 O). The flame retardant effect is doubled and excellent when the flame retardant treatment is applied to the entire surface of the material attached to the required use.

필요시 발색도료 역할을 겸하여 2중의 효과를 얻는, 다기능 제품이고 특히 구성소재가 저렴하여 사용함에 비용이 절감된다.If necessary, it is a multifunctional product that doubles the role of coloring paint, and in particular, the material is cheaper, and the cost is reduced.

Claims (4)

규산소다(NaO·nSiO2·xH2O)를 바인더로, 방염기능을 하는 붕산(H3BO3)이나 유사기능을 하는 붕사(Na2B4O7·10 H2O)를 규산소다 대비 10% 내외 발색이 필요시 색소를 첨가 혼합교반하여 수용액으로 제조한 무기방화 페인트 겸 방화 접착제.Sodium silicate (NaO · nSiO 2 · xH 2 O) is used as a binder, and boric acid (H 3 BO 3 ) that functions as a flame retardant or borax (Na 2 B 4 O 7 · 10 H 2 O) that functions similarly to sodium silicate. Inorganic fire retardant paint and fire retardant adhesive prepared as an aqueous solution by mixing and stirring the pigment when 10% color development is required. 제1항에 있어서The method of claim 1 가연성 및 비가연성 소재(벽지류, 합판류, 목재류, 가구류, 인테리어류, 철재류)의 방염 및 단열 코팅제.Flame retardant and thermal insulation coatings for flammable and non-combustible materials (wall paper, plywood, wood, furniture, interiors, steel). 제1항에서In claim 1 가연성 및 비가연성의 판 및 형재(벽지류, 합판류, 목재류, 가구류, 인테리어류, 철재류, 석재류, 시멘트 제품류)의 면접착제.Surface adhesives for flammable and non-flammable plates and profiles (wall paper, plywood, wood, furniture, interiors, iron, stone, cement products). 제1항에서In claim 1 분해된 유기물 및 무기물(분쇄된 목재 및 종이류, 토양류등)의 고형체 제조 접착제.Adhesives for making solids from decomposed organics and inorganics (crushed wood and paper, soils, etc.).
KR1020030008372A 2003-02-10 2003-02-10 Method of inoganic Fireproof Paint and Fireproof Bond KR20030018038A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100696874B1 (en) * 2003-11-28 2007-03-20 윤욱열 Composition for action of resist-fire and fire-extinguishing
US7560041B2 (en) 2003-11-28 2009-07-14 Wook Yeal Yoon Composition for action of resist-fire and fire-extinguishing
CN112830748A (en) * 2021-01-19 2021-05-25 北京慕成防火绝热特种材料有限公司 Preparation method of intrinsic hydrophobic non-intumescent steel structure fireproof coating

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100696874B1 (en) * 2003-11-28 2007-03-20 윤욱열 Composition for action of resist-fire and fire-extinguishing
US7560041B2 (en) 2003-11-28 2009-07-14 Wook Yeal Yoon Composition for action of resist-fire and fire-extinguishing
CN112830748A (en) * 2021-01-19 2021-05-25 北京慕成防火绝热特种材料有限公司 Preparation method of intrinsic hydrophobic non-intumescent steel structure fireproof coating

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