KR20000054462A - Manufacturing method of mineral powder with high productivity - Google Patents

Manufacturing method of mineral powder with high productivity Download PDF

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Publication number
KR20000054462A
KR20000054462A KR1020000031236A KR20000031236A KR20000054462A KR 20000054462 A KR20000054462 A KR 20000054462A KR 1020000031236 A KR1020000031236 A KR 1020000031236A KR 20000031236 A KR20000031236 A KR 20000031236A KR 20000054462 A KR20000054462 A KR 20000054462A
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KR
South Korea
Prior art keywords
mineral powder
particles
water
fine particles
mineral
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KR1020000031236A
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Korean (ko)
Inventor
석미수
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석미수
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by 석미수 filed Critical 석미수
Priority to KR1020000031236A priority Critical patent/KR20000054462A/en
Publication of KR20000054462A publication Critical patent/KR20000054462A/en
Priority to KR10-2001-0007699A priority patent/KR100451574B1/en
Priority to DE10115941A priority patent/DE10115941B4/en
Priority to JP2001105149A priority patent/JP3631440B2/en
Priority to NO20011666A priority patent/NO20011666L/en
Priority to GB0108299A priority patent/GB2361007B/en
Priority to IT2001MI000715A priority patent/ITMI20010715A1/en
Priority to AU33405/01A priority patent/AU3340501A/en
Priority to SG200102256A priority patent/SG94807A1/en
Priority to SE0101185A priority patent/SE521257C2/en
Priority to CA002343500A priority patent/CA2343500A1/en
Priority to CNB011178612A priority patent/CN1164806C/en
Priority to FR0104613A priority patent/FR2807031A1/en
Priority to ES200100795A priority patent/ES2194579B1/en
Priority to MXPA01003456A priority patent/MXPA01003456A/en
Priority to BR0101313-0A priority patent/BR0101313A/en
Priority to US09/825,593 priority patent/US6669882B2/en
Priority to IDP20010296D priority patent/ID29741A/en
Priority to HK01108474A priority patent/HK1037695A1/en

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D1/00Treatment of filament-forming or like material
    • D01D1/02Preparation of spinning solutions

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Artificial Filaments (AREA)

Abstract

PURPOSE: A process of preparing mineral powder having excellent productivity by mixing mineral powder and water, removing foreign material using a first electromagnet, separating the second largest particles from smaller particles, removing smaller particles, adding a specified amount of water and passing through a filter membrane is provided which enables to produce fibers having excellent quality. CONSTITUTION: A process comprises the steps of precisely grinding a mixture of fine particles of mineral powder and water; removing iron scraps or foreign materials by an electromagnet; removing only smaller particles by separating smaller particles from the second largest particles and spinning raw fibers by adding 1 to 10% by a mineral composition of fine particles obtained from passing through a filter membrane in wet state,

Description

생산성이 우수한 광물 분말의 제조방법{.}Manufacturing method of mineral powder with high productivity {.}

본 발명은 광물 분말을 이용하여 화학수지와 혼합하여 원사를 방사할 때 광물 분말의 입자가 미세하며 균일하게 하고 이물질 또는 타 광물질을 제거함으로서 종래의 광물 분말을 화학수지와 혼합하여 방사함에 있어서 칩을 만드는 과정과 방사과정, 연신, 가연 등의 일련의 제조과정에서 문제시 되었던 사절, 마모, 생산성 등의 문제점을 해결하여 우수한 생산성과 사절, 부속의 마모가 없으며 원할한 생산 공정을 수행할 수 있도록 하기 위한 그 조성물의 제조 방법에 관한 것이다.According to the present invention, when the yarn is mixed with the chemical resin by using the mineral powder, the particles of the mineral powder are fine and uniform, and the foreign matter or other minerals are removed to remove the chips from the conventional mineral powder by mixing with the chemical resin. To solve the problems such as trimming, abrasion, and productivity that are a problem in the manufacturing process such as making process, spinning process, stretching process, and combustible product, it is possible to perform excellent production process without having excellent productivity, trimming, and wear of parts. To a process for the preparation of the composition.

광물 분말이 첨가된 화학섬유에 있어서 문제점이었던 설비를 마모시키는 주된 원인은 금속광물의 결정형(벽개모양)이 피라미드상, 주상, 능면체상, 육면체상, 팔면체상, 십이면체상 등의 다변화로 이루어진 특징으로 인하여 불규칙적으로 원사 표층에 나와 있어 마찰에 의한 쇠붙이는 마모됨은 물론이고 방사 설비가 고가이므로, 그 동안 정상적인 생산을 하기에는 불가능하여 실패를 거듭하였다. 또한 방사시에는 사절 발생이 빈번하여 방사가 어려웠고 정상적인 사질의 원사를 생산할수 없었다. 그러므로 광물 분말을 첨가한 합성섬유가 정상적으로 생산이 이루어 질수 있도록 하기 위해서는 섬유 표층면이 미끄러워야 하므로 결정형이 탁상 또는 판상, 비늘상 이며, 기능이 있는 필로규산염 광물(층상구조형), 파이로필라이트, 캐올리나이트(사문석)군, 몬모릴로나이트군, 녹니석군, 백운모군, 흑운모군 등의 광물 분말을 조성하여 화학수지에 첨가함으로써 정상적인 사질의 원사를 생산할 수 있는 발명을 하여 본 발명자가 한국 특허 출원 번호10-2000-0017775호를 출원 한 바와 같이 생산성이 좋은 필로규산염 광물이라도 타 광물질과 이물질이 포함되어 있으므로 이러한 물질들을 제거 시킴으로서 광물의 입자를 미세분으로 균일하게 조성할 수 있으며 생산성이 우수한 광물 분말을 조성하여 화학수지에 첨가함으로서 생산성이 우수하고 사질이 좋은 원사를 생산할 수 있도록 하기 위함이 본 발명의 목적이 있다.The main cause of wear of the equipment, which was a problem in chemical fiber added with mineral powder, is that the crystalline form of the metal mineral (cleft) is made up of a variety of pyramidal, columnar, rhombohedral, hexahedral, octahedral, and dodecahedral forms. Due to the characteristic of irregularities on the surface of the yarn, the wear of the metal is not only worn out by friction, but also the spinning equipment is expensive. In addition, it was difficult to spin due to frequent trimming during spinning and could not produce normal yarn. Therefore, the surface of the fiber must be slippery in order for the synthetic fiber added with the mineral powder to be produced normally, so the crystal form is tabletop, plate-like or scale-like, and the functional phyllosilicate mineral (layered structure), pyrophyllite, The inventors of the present invention can produce a yarn of normal sand by forming a mineral powder such as kaolinite (serpentine) group, montmorillonite group, chlorite group, dolomite group, biotite group and adding to chemical resin. As filed with -2000-0017775, even the highly productive phyllosilicate minerals contain other minerals and foreign substances, so that these particles can be removed to uniformly form the particles of minerals and produce mineral powders with high productivity. Added to chemical resins for high productivity and good quality To be able to produce yarn in order are the object of the present invention.

이에따라 본 발명은 상기 문제점을 해결하기 위하여 인체에 유익하고 기능효과가 있는 천연 광물 또는 인공 합성 광물 그룹에서 선택된 1종 이상의 광물을 광물질에 따라 500℃∼1,200℃ 범위내에서 소성시키는 과정과 1차 325메시 이상으로 분쇄기에 의하여 분쇄하고 2차 반복하여 정밀 밀링 하여 분쇄하는 것과 또는 다른 분쇄 방법에 의하여 미립자의 광물 분말 입경이 방사시 원사 섬도의 ⅓이하가 되게하여야 하며, 특히 3데니어 이하의 원사 방사에는 1미크론 이하가 바람직하다.Accordingly, in order to solve the above problems, the present invention provides a process for calcining at least one mineral selected from the group of natural minerals or artificial synthetic minerals beneficial and functional to the human body within the range of 500 ° C. to 1,200 ° C. according to minerals. The particle size of the mineral powder of the fine particles should be less than or equal to the yarn fineness during spinning, by grinding by a grinder over a mesh, followed by precision milling by second repetition, or by other grinding methods, and especially for yarn spinning of 3 denier or less. 1 micron or less is preferable.

이와같은 분쇄 공정 과정을 거치면서 습식에서 광물 분말과 물을 혼합하여 전자석을 설비에 부착 시킴으로서 쇠붙이 및 이물질을 제거할 수 있고 다음 단계에서 비중법에 의하여 크기가 큰 입자와 비중이 작은 입자를 선별한 후 미분말의 입자만을 분리 수거한 후 일정량의 물을 더 첨가하여 특수 부직포등의 휠타막을 통과시켜 얻어진 미립자의 광물 분말은 기능효과 또는 방사성 또는 생산성이 우수하며 원사의 사질 또한 우수하였다.Through this crushing process, the mineral powder and water are mixed in the wet process to attach the electromagnet to the equipment to remove the metal and foreign matters. In the next step, the large and small specific gravity particles are selected by the specific gravity method. After collecting and separating only the fine powder particles, the mineral powder of the fine particles obtained by passing through a filter film such as a special nonwoven fabric by adding a certain amount of water was excellent in functional effect, radioactivity or productivity, and yarn quality was also excellent.

이하 본 발명은 실시예를 통하여 보다 상세히 설명한다. 하기 실시예는 본 발명을 이에 한정하는 것은 아니며, 단지 구체적인 예시를 보여주기 위한 것이다.Hereinafter, the present invention will be described in more detail with reference to Examples. The following examples are not intended to limit the invention to this, only to illustrate specific examples.

(실시 예 1)(Example 1)

광물 분말의 미세분과 물을 일정량으로 혼합하여 습식 상태에서 정밀 분쇄하는 과정에 있어 설비에 전자석을 부착 시킴으로서 쇠붙이 및 이물질을 제거한 후 비중법에 의하여 크기가 큰 입자와 작은 입자를 분리시켜 작은 미분말의 입자만을 분리 수거한 후 일정량의 물을 더 첨가하여 휠타막을 통과 시킴으로서 얻어진 입자가 균일하고 이물질이 제거된 방사성이 우수한 광물 분말 미세분을 조성하였다.In the process of precision grinding in the wet state by mixing the fine powder of mineral powder and water in a predetermined amount, the electromagnet is attached to the equipment to remove the metal and foreign matter, and then the large and small particles are separated by the specific gravity method to separate the small fine particles. After separating and collecting the bay, a certain amount of water was further added to pass through the filter film, thereby forming a fine powder of fine mineral powder having excellent radioactivity with uniform particles and foreign substances removed.

본 발명은 광물 분말을 화학 수지와 혼합하여 원사를 생산함에 있어서 발생되는 문제점들을 해결하고 광물 분말의 이물질과 큰입자를 제거할 수 있어서 생산성이 우수하고 원사의 사질이 우수한 원사를 생산할 수 있는 섬유를 생산할 수 있는 광물 분말이 포함된 조성물을 제공해 준다.The present invention solves the problems caused by mixing the mineral powder with the chemical resin to produce the yarn and can remove the foreign matter and large particles of the mineral powder to produce a fiber that can produce a yarn with excellent productivity and excellent yarn quality It provides a composition containing a mineral powder that can be produced.

Claims (1)

a) 광물 분말의 미립자를 물과 혼합하여 습식에서 정밀 분쇄하는 단계와,a) mixing the fine particles of the mineral powder with water to precisely grind in wet, b) 정밀 분쇄하는 과정에 있어서 설비에 전자석을 부착 시킴으로서 쇠붙이 및 이물질을 제거하는 단계와,b) removing the metal parts and foreign substances by attaching electromagnets to the equipment in the process of precision grinding; c) 습식에서 비중법에 의하여 큰입자와 작은 입자를 분리시켜 미립자의 작은 입자만을 문리 수거하는 단계와,c) separating the large particles and the small particles by wet gravity method and collecting only small particles of the fine particles; d) 습식에서 휠타막을 사용하여 휠타막을 통과 시켜서 얻어진 미립자의 광물 분말 조성물 1∼10중량%를 첨가하여 원사를 방사하는 것을 특징으로 하는 합성 섬유용 광물 분말 조성물 및 그 제조방법.d) 1 to 10% by weight of the mineral powder composition of the fine particles obtained by passing through the filter film using a filter film in a wet manner, and spinning the yarn.
KR1020000031236A 2000-04-04 2000-06-07 Manufacturing method of mineral powder with high productivity KR20000054462A (en)

Priority Applications (19)

Application Number Priority Date Filing Date Title
KR1020000031236A KR20000054462A (en) 2000-06-07 2000-06-07 Manufacturing method of mineral powder with high productivity
KR10-2001-0007699A KR100451574B1 (en) 2000-04-04 2001-02-16 Method of producing fiber having mineral powder and fiber produced therefrom
DE10115941A DE10115941B4 (en) 2000-04-04 2001-03-30 Process for the production of fibers with functional mineral powder and fibers made therefrom
NO20011666A NO20011666L (en) 2000-04-04 2001-04-03 Process for producing fibers having functional mineral powder and fiber prepared therefrom
SG200102256A SG94807A1 (en) 2000-04-04 2001-04-03 Method of producing fiber having functional mineral powder and fiber produced therefrom
CA002343500A CA2343500A1 (en) 2000-04-04 2001-04-03 Method of producing fiber having functional mineral powder and fiber produced therefrom
GB0108299A GB2361007B (en) 2000-04-04 2001-04-03 Method of producing fiber having functional mineral powder and fiber produced therefrom
IT2001MI000715A ITMI20010715A1 (en) 2000-04-04 2001-04-03 METHOD FOR THE PRODUCTION OF A FIBER WITH FUNCTIONAL MINERAL POWDERS AND FIBER PRODUCED BY THESE
AU33405/01A AU3340501A (en) 2000-04-04 2001-04-03 Method of producing fiber having functional mineral powder and fiber produced therefrom
JP2001105149A JP3631440B2 (en) 2000-04-04 2001-04-03 Manufacturing method of fiber added with mineral powder and fiber manufactured therefrom
SE0101185A SE521257C2 (en) 2000-04-04 2001-04-03 Method for producing fiber with functional mineral powder, as well as fiber made from it
CNB011178612A CN1164806C (en) 2000-04-04 2001-04-04 Manufacture of fibre containing functional mineral powder and fibre prepared by the same
IDP20010296D ID29741A (en) 2000-04-04 2001-04-04 METHOD OF MAKING FIBER THAT CONTAINS FUNCTIONAL MINERAL POWDERS AND THE FIBER PRODUCED
FR0104613A FR2807031A1 (en) 2000-04-04 2001-04-04 PROCESS FOR THE PREPARATION OF FIBER CONTAINING FUNCTIONAL MINERAL POWDER AND FIBER PREPARED THEREFROM
ES200100795A ES2194579B1 (en) 2000-04-04 2001-04-04 FIBER PRODUCTION METHOD THAT HAS FUNCTIONAL MINERAL POWDER AND FIBER PRODUCED FROM THE SAME.
MXPA01003456A MXPA01003456A (en) 2000-04-04 2001-04-04 Method of producing fiber having functional mineral powder and fiber produced therefrom.
BR0101313-0A BR0101313A (en) 2000-04-04 2001-04-04 Process for producing fiber having functional mineral powder and fiber produced through it
US09/825,593 US6669882B2 (en) 2000-04-04 2001-04-04 Process of making fiber having functional mineral powder
HK01108474A HK1037695A1 (en) 2000-04-04 2001-12-03 Method of producing fiber having functional mineral powder and fiber produced therefrom.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020000031236A KR20000054462A (en) 2000-06-07 2000-06-07 Manufacturing method of mineral powder with high productivity

Publications (1)

Publication Number Publication Date
KR20000054462A true KR20000054462A (en) 2000-09-05

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KR1020000031236A KR20000054462A (en) 2000-04-04 2000-06-07 Manufacturing method of mineral powder with high productivity

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100407220B1 (en) * 2000-03-20 2003-11-28 (주)성신텍스타일 method for manufacturing of functional fiber clay and mica as base material
KR100422478B1 (en) * 2001-03-02 2004-03-11 주식회사 휴비스 Polyester fiber containing illite

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100407220B1 (en) * 2000-03-20 2003-11-28 (주)성신텍스타일 method for manufacturing of functional fiber clay and mica as base material
KR100422478B1 (en) * 2001-03-02 2004-03-11 주식회사 휴비스 Polyester fiber containing illite

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