KR20000006939A - Antimicrobial Soap Composition Containing Xanthorrhizol - Google Patents

Antimicrobial Soap Composition Containing Xanthorrhizol Download PDF

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KR20000006939A
KR20000006939A KR1019990050486A KR19990050486A KR20000006939A KR 20000006939 A KR20000006939 A KR 20000006939A KR 1019990050486 A KR1019990050486 A KR 1019990050486A KR 19990050486 A KR19990050486 A KR 19990050486A KR 20000006939 A KR20000006939 A KR 20000006939A
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soap
antimicrobial
skin
soap composition
antibacterial
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KR1019990050486A
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Korean (ko)
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황재관
심재석
공태욱
이금기
변유량
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황재관
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Priority to KR1019990050486A priority Critical patent/KR20000006939A/en
Publication of KR20000006939A publication Critical patent/KR20000006939A/en
Priority to PCT/KR2000/000432 priority patent/WO2000067711A1/en
Priority to US10/312,134 priority patent/US6696404B1/en
Priority to AU46176/00A priority patent/AU4617600A/en

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74—Biological properties of particular ingredients

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Emergency Medicine (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

PURPOSE: An antibacterial soap composition including xanthorrhizol represented by formula 1 is provided which takes antibacterial action for microbes causing dermatitis. CONSTITUTION: The antibacterial soap composition including xanthorrhizol represented by formula 1 is obtained by adding 0.001-5.0 wt% of xanthorrhizol to general soap.

Description

잔소리졸을 포함하는 항균 비누 조성물{Antimicrobial Soap Composition Containing Xanthorrhizol}Antimicrobial soap composition containing a nagging sol {Antimicrobial Soap Composition Containing Xanthorrhizol}

본 발명은 피부염증 유발원인균들에 대해 항균활성을 가진 물질을 함유한 항균 비누 조성물에 관한 것이다.The present invention relates to an antibacterial soap composition containing a substance having an antimicrobial activity against the causes causing dermatitis.

보다 상세하게는 여드름, 무좀, 가려움증, 습진 등의 각종 피부 염증을 유발하는 대표적인 병원성 균주인 프로피오니박테리움 아크네스(Propionibacterium acnes), 캔디다 알비칸스(Candida albicans), 스태필로코커스 아우레우스(Staphylococcus aureus)와 스태필로코커스 에피더미스(Staphylococcus epidermis)에 대하여 우수한 항균활성을 가지는 물질을 함유하여 항균작용이 향상된 비누 조성물에 관한 것이다.More specifically, the typical pathogenic strains that cause various skin inflammations such as acne, athlete's foot, itching and eczema, Propionibacterium acnes, Candida albicans, Staphylococcus aureus, Staphylococcus Aureus) and Staphylococcus epidermis (Staphylococcus epidermis) relates to a soap composition with improved antibacterial activity by containing a substance having excellent antimicrobial activity.

일반적으로 피부는 피지선에서 피지가 모공을 통해서 분비되어 피부 표면으로 수분이 증발되는 것을 억제하여 피부의 탄력을 유지하게 된다. 그러나 피부상피 세포의 비정상적인 각화에 의하여 모공이 막히고 피지가 피부표면으로 배출되지 않으면 피지가 모공 내에 뭉쳐있게 되고 여기에 병원성균들이 침입하게 되면 염증이 생기게 된다. 피부표면에서 피지가 잘 배출되더라도 세정 후 시간이 흐르면 공기중의 병원성균들이 피부 표면에 증식하여 피지를 부패시킴으로서 피부에서 악취가 나고, 피부를 자주 세정하면 피지성분이 제거되어 각질층이 연화되어 피부가 건조하고 거칠어지는 문제점이 있다(참조 : Mazzaglia G., et al., J. Antimicrob. Chemother., 41:259∼266, 1998).In general, the skin is secreted from the sebaceous glands through the pores to inhibit the evaporation of moisture to the skin surface to maintain the elasticity of the skin. However, if the pores are blocked by abnormal keratinization of skin epithelial cells, and sebum is not discharged to the skin surface, sebum will clump together in the pores, and pathogens invade it, causing inflammation. Even if the sebum is well discharged from the surface of the skin, time passes after the cleaning, the pathogenic bacteria in the air multiply on the surface of the skin and decay the sebum, causing odors from the skin. There is a problem of drying and roughness (Mazzaglia G., et al., J. Antimicrob. Chemother., 41: 259-266, 1998).

비누는 통상적으로 다음의 방법에 의해서 만들어진다. 즉, 유지와 야자유를 적당량 배합하여 60∼70℃로 가열 용해한 후, 80∼90℃의 수산화나트륨을 첨가하여 비누화반응을 실시하고, 상층에 뜬 비누로부터 하층에 가라앉는 비누와 반응의 부산물인 물, 비반응 수산화나트륨, 글리세린층 등을 분리제거 한 다음, 비누속에 있는 잔류글리세린과 수산화나트륨 등을 진한 소금물을 통상 2∼3회 가하여 제거하여 통상의 비누층을 얻고, 이를 건조하여 수분함량 13% 내외의 비누를 제조하고, 이와 같이 제조된 비누에 산화방지제, 보색제, 항료 등을 배합하여 성형제조한다.Soap is usually made by the following method. That is, a proper amount of oil and palm oil is mixed and melted by heating to 60-70 ° C, followed by saponification reaction by adding sodium hydroxide at 80-90 ° C. , Remove and remove the unreacted sodium hydroxide, glycerin layer, and then remove the remaining glycerin and sodium hydroxide in the soap 2 ~ 3 times to obtain a normal soap layer, and dried to obtain a moisture content of 13% Soap inside and outside is prepared, and the soap thus prepared is blended with an antioxidant, a complementary agent, a pharmaceutical, and the like to form and manufacture.

이와 같이 제조된 비누는 피부의 때나 노폐물을 제거하는데는 어느 정도 효과적이나 과도한 세정작용에 의해 피부의 향상성을 유지시키는 피지 등이 필요 이상으로 제거되어 피부를 손상시키고, 피부의 염증을 유발하는 병원성균들에 대해서 만족할 만한 효과를 얻지 못했다.Soap manufactured in this way is somewhat effective in removing dirt and wastes of the skin, but the sebum that maintains the improvement of the skin by excessive cleaning action is removed more than necessary to damage the skin and cause inflammation of the skin. No satisfactory effect was obtained for sex bacteria.

이러한 결점을 보완하기 위해서 여러 가지 영양성분을 첨가하거나 각종 식물추출물을 첨가하여 항균효과 및 피부 보호작용을 향상시키려는 방법들이 제안되어 왔으나 아직까지 항균효과가 개선되면서 피부에 자극을 주지 않고 지속성이 높은 항균 비누는 많이 개발되어 있지 못한 실정이다.In order to make up for the shortcomings, methods have been proposed to improve the antimicrobial effect and skin protection effect by adding various nutrients or various plant extracts. However, the antimicrobial effect has been improved. Soap is not developed much.

따라서 약용식물 등의 천연물로부터 피부에 자극을 주지 않으면서 피부 염증을 유발하는 균들에 대해 우수한 항균활성을 갖는 안전성이 높은 물질을 주성분으로 하는 새로운 항균 비누의 개발이 필요하다.Therefore, there is a need for the development of a new antibacterial soap based on a high-safety substance with excellent antimicrobial activity against bacteria that cause skin inflammation from natural products such as medicinal plants.

따라서 본 발명은 피부 염증의 원인이 되는 대표적인 미생물인 프로피오니박테리움 아크네스, 캔디다 알비칸스, 스태필로코커스 에피더미스, 스태필로코커스 아우레우스에 대해 강력한 항균활성을 나타내는 잔소리졸(xanthorrhizol)을 포함하여 항균작용을 함으로써 피부 보호 작용이 개선된 항균 비누 조성물을 제공하는 것을 목적으로 한다.Therefore, the present invention provides a xanthorrhizol that exhibits strong antibacterial activity against propionibacterium acnes, Candida albicans, Staphylococcus epidermis, Staphylococcus aureus, which are representative microorganisms that cause skin inflammation. It is an object of the present invention to provide an antibacterial soap composition having an antibacterial effect by improving skin protection.

상기의 목적을 달성하기 위한 본 발명은 피부 염증 유발균에 대한 항균활성을 가진 물질인 잔소리졸에 그 특징이 있다.The present invention for achieving the above object is characterized by the nagging sol is a substance having an antimicrobial activity against the skin inflammatory bacteria.

또한 본 발명은 항균활성 물질인 잔소리졸을 함유하는 항균 비누에 그 특징이 있다.In addition, the present invention is characterized by an antibacterial soap containing a naxoli sol which is an antimicrobial active material.

본 발명의 항균활성 물질인 잔소리졸은 커큐마 잔소리자(Curcuma xanthorrhiza)로부터 분리하였고, 잔소리졸의 분리 방법은 한국특허출원(등록번호) 10-1999-0016507과 10-1999-0044406에 상세하게 기재되어 있다.The antimicrobial active substance of the present invention, naxoli sol was isolated from Curcuma xanthorrhiza, and the method of separation of naxoli sol is described in detail in Korean Patent Application Nos. 10-1999-0016507 and 10-1999-0044406. It is.

상기의 항균활성물질인 잔소리졸을 함유한 항균 비누에 대하여 설명한다.The antimicrobial soap containing the naxorisol which is the said antimicrobial active substance is demonstrated.

본 발명의 항균 비누는 통상적인 미용 비누베이스의 주성분으로 사용되는 유지, 야자유, 팜유, 글리세린 등에 향료, 색소, 산화방지제, 보습제 등을 혼합하여 통상적인 제조방법으로 제조하였다.Antibacterial soap of the present invention was prepared by a conventional manufacturing method by mixing fragrances, pigments, antioxidants, moisturizers and the like to the fats and oils, palm oil, palm oil, glycerin used as the main component of a conventional cosmetic soap base.

상기와 같은 통상적인 미용 비누 조성성분에 항균활성을 가진 항균제로 본 발명의 잔소리졸을 첨가하여 항균 비누를 제조한다.The antimicrobial soap of the present invention is added as an antimicrobial agent having antimicrobial activity to the conventional cosmetic soap composition as described above to prepare an antibacterial soap.

이때 첨가되는 잔소리졸의 함량은 전체 비누 조성 성분의 0.001-5.0중량%로 하는 것이 바람직하다. 이는 0.001중량% 미만으로 첨가하는 경우에는 항균 및 소독작용이 미약하여 습진, 가려움증, 기미, 여드름 등을 제거하는 효과가 낮아지고, 5.0중량%를 초과하여 첨가하는 경우에는 상승효과가 낮아 경제적이지 못하고 오히려 기본적인 비누베이스의 양이 감소하여 세정력이 저하된다.At this time, the content of the naxazole sol is preferably set to 0.001-5.0% by weight of the total soap composition components. It is less effective to remove eczema, itching, blemishes, acne, etc. when the addition is less than 0.001% by weight, and the synergistic effect is not economical because it is less than 5.0% by weight. Rather, the amount of basic soap base is reduced, degrading the cleaning power.

이하 실시예 및 실험예를 통하여 본 발명을 상세하게 설명한다. 그러나 다음의 실시예 및 실험예 들은 본 발명을 예시하는 것으로 본 발명의 범위를 한정하는 것은 아니다.Hereinafter, the present invention will be described in detail with reference to Examples and Experimental Examples. However, the following Examples and Experimental Examples illustrate the present invention and do not limit the scope of the present invention.

또한 하기 실시예 및 실험예들에서 특별히 부피%임을 명시하지 않은 %는 중량%를 나타낸다.In addition, in the following Examples and Experimental Examples,% not specified as% by weight indicates weight%.

(실시예 1-5)(Example 1-5)

본 발명의 잔소리졸을 이용하여 실시예 1-5의 조성을 지니는 항균 비누를 제조하였다.An antibacterial soap having a composition of Example 1-5 was prepared using the nagging sol of the present invention.

0.001, 0.01, 0.1, 1.0, 5.0중량% 농도의 잔소리졸을 기본적인 비누베이스와 고르게 혼합한 후 향료, 색소 등을 넣어 통상적인 비누의 제조 방법에 따라 항균 비누 조성물을 제조하였다.The antimicrobial soap composition was prepared according to a conventional soap production method by mixing the nagging sol concentration of 0.001, 0.01, 0.1, 1.0, 5.0% by weight evenly with the basic soap base, and then added flavorings, pigments and the like.

(실험예 1)Experimental Example 1

잔소리졸을 함유한 항균 비누 조성물의 항균활성Antimicrobial Activity of Antimicrobial Soap Composition Containing Nagging Sol

4 ㎖의 배지에 실시예 1-5에서 제조한 항균 비누 조성물을 잔소리졸 함량이 각각 0.001, 0.01, 0.1, 1.0, 5.0중량%가 되도록 첨가한 후에 피부염증 유발균들을 함유하는 1 ㎖ 액을 첨가하고 48시간 배양한 후 생균수를 측정하여 항균활성을 구하였다. 이때 잔소리졸을 넣지 않은 대조군과 항균력을 비교하였으며, 그 결과를 하기 표 2에 나타내었다.To the 4 ml medium, the antibacterial soap composition prepared in Example 1-5 was added so that the content of nagging sol was 0.001, 0.01, 0.1, 1.0 and 5.0 wt%, respectively, and then 1 ml liquid containing dermatitis-inducing bacteria was added. After 48 hours of incubation, the number of viable cells was measured to determine the antimicrobial activity. The antimicrobial activity was compared with the control group without the nagging sol, and the results are shown in Table 2 below.

상기 표 2의 결과에서 알 수 있는 바와 같이, 본 발명에 따른 실시예의 항균 비누 조성물은 잔소리졸을 첨가함으로써 잔소리졸을 첨가하지 않은 대조군과 비교하였을때 피부염증 유발균에 대한 항균활성이 매우 높았다.As can be seen from the results of Table 2, the antimicrobial soap composition of the embodiment according to the present invention had a very high antimicrobial activity against the dermatitis-inducing bacteria as compared to the control group without adding the naxazole sol by adding the naxoli sol.

상기와 같이 본 발명의 잔소리졸은 천연물로부터 분리한 성분이어서 부작용을 최소화할 수 있다. 또한 일반적으로 사용할 수 있는 농도에서 프로피오니박테리움 아크네스, 캔디다 알비칸스, 스태필로코커스 아우레우스 및 스태필로코커스 에피더미스 등의 피부 염증 유발균들에 대한 항균 효과가 높아 통상적으로 사용하는 비누에 본 발명의 잔소리졸을 첨가하였을 때 항균효과가 상승하였다.As described above, the nagging sol of the present invention is a component separated from natural products, thereby minimizing side effects. In addition, soaps commonly used due to high antibacterial effects against skin irritants such as propionibacterium acnes, candida albicans, staphylococcus aureus, and staphylococcus epidermis at the concentrations that can be generally used. When the nagging sol of the present invention was added to the antibacterial effect was increased.

따라서 본 발명의 잔소리졸은 천연물로서 이를 함유한 항균 비누 조성물은 피부에 자극을 주거나 부작용을 일으키지 않으면서 가려움증, 여드름, 습진, 염증 및 무좀 등의 피부 질환에 대한 예방 및 치료에 우수한 효과를 나타낸다.Therefore, the nagging sol of the present invention is a natural product, and the antimicrobial soap composition containing the same shows an excellent effect on the prevention and treatment of skin diseases such as itching, acne, eczema, inflammation and athlete's foot without irritating or causing side effects on the skin.

Claims (2)

하기 화학식Ⅰ의 잔소리졸을 함유하는 항균 비누 조성물.An antibacterial soap composition containing a naxoli sol of formula (I): 제 1항에 있어서 잔소리졸을 0.001-5.0중량%의 함량으로 함유하는 항균 비누 조성물.The antibacterial soap composition according to claim 1, which contains a naxoli sol in an amount of 0.001-5.0% by weight.
KR1019990050486A 1999-05-08 1999-11-13 Antimicrobial Soap Composition Containing Xanthorrhizol KR20000006939A (en)

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KR1019990050486A KR20000006939A (en) 1999-11-13 1999-11-13 Antimicrobial Soap Composition Containing Xanthorrhizol
PCT/KR2000/000432 WO2000067711A1 (en) 1999-05-08 2000-05-08 A process for preparing xanthorrizol from curcuma xanthorriza roxb. and novel uses of the same
US10/312,134 US6696404B1 (en) 1999-05-08 2000-05-08 Antibacterial composition having xanthorrizol
AU46176/00A AU4617600A (en) 1999-05-08 2000-05-08 A process for preparing xanthorrizol from LTiGTcurcuma xanthorrizaLT/iGT roxb. and novel uses of the same

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KR20030069391A (en) * 2002-02-20 2003-08-27 주식회사 엘지생활건강 Cosmetic compositions with anti-bacterial agents against body malodor

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JPH07149628A (en) * 1993-11-30 1995-06-13 Suntory Ltd Improver for lipid metabolism
JPH0920635A (en) * 1995-07-04 1997-01-21 Shiseido Co Ltd Whitening skin preparation for external use
JPH09111282A (en) * 1995-10-17 1997-04-28 Maruzen Pharmaceut Co Ltd Bisabolane type sesquiterpene composition and its production
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Publication number Priority date Publication date Assignee Title
US5210538A (en) * 1990-09-26 1993-05-11 Kikusui Electronics Corporation Glitch detection circuit and method
JPH07149628A (en) * 1993-11-30 1995-06-13 Suntory Ltd Improver for lipid metabolism
JPH0920635A (en) * 1995-07-04 1997-01-21 Shiseido Co Ltd Whitening skin preparation for external use
JPH09111282A (en) * 1995-10-17 1997-04-28 Maruzen Pharmaceut Co Ltd Bisabolane type sesquiterpene composition and its production
WO2000067711A1 (en) * 1999-05-08 2000-11-16 Hwang, Jae-Kwan A process for preparing xanthorrizol from curcuma xanthorriza roxb. and novel uses of the same

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000054644A (en) * 2000-06-15 2000-09-05 황재관 Anti-cavity food composition comprising naxazole
KR20030069391A (en) * 2002-02-20 2003-08-27 주식회사 엘지생활건강 Cosmetic compositions with anti-bacterial agents against body malodor

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