KR19980084687A - Coating processing method of vehicle roof forge woven from polyester yarn - Google Patents

Coating processing method of vehicle roof forge woven from polyester yarn Download PDF

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KR19980084687A
KR19980084687A KR1019970020535A KR19970020535A KR19980084687A KR 19980084687 A KR19980084687 A KR 19980084687A KR 1019970020535 A KR1019970020535 A KR 1019970020535A KR 19970020535 A KR19970020535 A KR 19970020535A KR 19980084687 A KR19980084687 A KR 19980084687A
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flame retardant
weight
forge
parts
coating
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KR1019970020535A
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Korean (ko)
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KR100216962B1 (en
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김일경
양용주
신태철
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한형수
주식회사 새한
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/244—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons
    • D06M15/248—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons containing chlorine
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10—Repellency against liquids
    • D06M2200/12—Hydrophobic properties
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30—Flame or heat resistance, fire retardancy properties
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00—Physical properties
    • D10B2401/02—Moisture-responsive characteristics
    • D10B2401/021—Moisture-responsive characteristics hydrophobic
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2505/00—Industrial
    • D10B2505/12—Vehicles
    • D—TEXTILES; PAPER
    • D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2505/00—Industrial
    • D10B2505/18—Outdoor fabrics, e.g. tents, tarpaulins

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

본 발명은 폴리에스터 원사로 직성한 차량용 루프 포지의 코팅가공방법에 관한 것으로, 폴리에스터 원착사(Dope dyed yarn)를 원사로 사용하여 제직한 포지에 브롬계 방염제가 전체 조성물의 40 ~ 80중량부, 클로로화합물 10 ~ 35중량부, 염화파라핀 10 ~ 25중량부로 구성된 방염수지를 사용하여 두께 0.5 ~ 2.5mm로 1차 나이프 코팅하고 100 ~ 140℃에서 30 ~ 120초간 건조시킨 다음 그 위에 다시 방염수지를 두께 1.0 ~ 3.5mm로 도포하여 2차 나이프 코팅함을 특징으로 하며 이와 같이 하여 얻은 방염수지는 경량성이 부여될 뿐만 아니라 방염성이 우수하고 피코팅재와 기포간의 접착력이 우수하며 세탁 견뢰도가 뛰어나고 방수성, 발수성이 뛰어나 우천시에도 가벼워서 운반이 용이한 효과를 가진다.The present invention relates to a method for coating a vehicle roof forge woven with polyester yarn, wherein the bromine-based flame retardant is 40 to 80 parts by weight of the entire composition of the woven fabric using a polyester dyed yarn as a yarn. Using a flame retardant resin consisting of 10 to 35 parts by weight of chloro compound and 10 to 25 parts by weight of paraffin chloride, first knife coating to a thickness of 0.5 to 2.5 mm, dried at 100 to 140 ° C. for 30 to 120 seconds, and then again Is coated with a thickness of 1.0 ~ 3.5mm, characterized in that the second knife coating and the obtained flame-retardant resin is not only given light weight, but also excellent in flame retardancy, excellent adhesion between the coating material and the bubble, excellent washing fastness and waterproof It has excellent water repellency and is light even in rainy days, making it easy to carry.

Description

폴리에스터 원사로 직성한 차량용 루프 포지의 코팅가공방법Coating processing method of vehicle roof forge woven from polyester yarn

본 발명은 방염성이 우수한 차량용 경량 루프 포지의 코팅방법에 관한 것으로, 보다 상세하게는 폴리에스터 원사로 제직한 포지에 아크릴 바인더와 안료를 함유하는 브롬계 방염제와 염화파라핀 및 클로로 화합물로 이루어진 방염수지로서 건식 나이프 코팅법을 적용하여 방염성이 우수한 차량용 루프 포지를 제조하는 방법에 관한 것이다.The present invention relates to a coating method of a light-proof roof forge for automobiles having excellent flame retardancy, and more particularly, to a flame retardant made of a bromine flame retardant containing an acrylic binder and a pigment, a paraffin chloride and a chloro compound in a fabric woven with polyester yarn. It relates to a method of manufacturing a vehicle roof forge excellent in flame resistance by applying a dry knife coating method.

종래에 일반적으로 사용하고 있는 방염가공 방법으로는 소재를 방염수지에 함침시켜 도포하는 함침법과 소재의 표면에 방염수지를 나이프(knife)로 도포하는 건식나이프 코팅법으로 구분된다.Flame retardant processing methods generally used in the prior art are classified into an impregnation method of impregnating and applying the material to the flame retardant resin and a dry knife coating method of applying the flame retardant resin to the surface of the material with a knife.

함침법에 있어서는 방염수지의 내부침투가 용이하고 도포량의 조절이 가능하나 방염수지의 점도 조절에 세심한 주의가 필요하며 건조 속도가 느려 생산성에 문제점이 있으며, 건식 나이프 코팅법에 있어서는 직물의 경사, 위사의 골과 골 사이의 균일한 코팅과 침투가 어려워 도포량의 한계가 있으며 이로 인해 방염성의 불량과 내구성이 떨어지는 단점이 있고, 원료수지를 혼합할 때 세심한 주의를 기울여야 하며, 고가의 원료를 사용하는 과정에서 교반이 잘못되어 일정하게 분산되지 않았을 때는 그 수지를 사용할 수 없게 작업상의 어려움이 있다. 그 뿐만 아니라 코팅을 위해서 나이프를 일정수준으로 맞추어서 가공함으로써 티끌 등 불순물로 인하여 불량율이 높고, 두껍게 코팅함으로써 원재료비가 비싸게 되며 가공속도가 느려 생산성의 한계가 있다.In the impregnation method, it is easy to penetrate the inside of the flame retardant resin and the amount of coating can be controlled, but it is necessary to pay close attention to the control of the viscosity of the flame retardant resin and there is a problem in productivity due to the slow drying speed. Uniform coating between the bones and bones is difficult to penetrate, which limits the amount of coating, which results in poor flame retardancy and poor durability, and requires careful attention when mixing the raw material resins and the process of using expensive raw materials. When the agitation is incorrect and the dispersion is not uniform, there is a difficulty in working so that the resin cannot be used. In addition, by processing the knife to a certain level for the coating process, the defect rate is high due to impurities such as dust, thick coating is expensive raw materials cost and processing speed is slow, there is a limit of productivity.

또한 종래의 차량용 루프 포지 및 천막지는 천연섬유인 면을 소재로 함으로 우천시 많은 양의 수분을 흡수하여 무게가 무거워지고 중량과중으로 운반상의 어려움이 따랐다.In addition, the conventional vehicle roof forge and tent are made of cotton made of natural fiber, so that it absorbs a large amount of moisture in rainy weather, resulting in heavy weight and difficulty in carrying heavy weight.

따라서 본 발명은 종래의 함침법에 의한 생산성의 저하를 개선하고, 건식 코팅법에 의한 방염성의 불량과 내구성의 불량을 완전 해결하며 중량 과중에 따른 문제점을 해소하기 위하여 예의 연구한 결과 수분율이 낮은 폴리에스터 원사로 제직된 포지를 소재로 하여 가공이 편리하고 경량성을 부여할 뿐아니라 방염효과가 큰 방염수지로써 코팅가공처리를 하여 방염성이 우수한 차량용 루프 포지 및 천막지를 개발하게 되어 본 발명을 완성하였다.Therefore, the present invention has been conducted to improve the decrease in productivity by the conventional impregnation method, to completely solve the flame retardancy and durability defects by the dry coating method and to solve the problems caused by heavy weight, low moisture content poly The fabric is made of polyester yarn, which is easy to process and gives light weight as well as the coating process with flame retardant resin with high flame-retardant effect. .

이하 본 발명을 상세하게 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail.

종래의 차량용 루프 포지나 천막지는 소재로써 면사 10수 9합사를 사용할 경우 그 중량이 1020g/㎡ 이었으나, 본 발명은 폴리에스터 원착사(Dope-dyed) 20수 2합 내지 20수 9합으로 가연하여 제직함으로써 생지의 중량을 230 ~ 350g/㎡ 로 경량화시킬 수 있다.Conventional vehicle roof forge or tent paper was 1020 g / ㎡ when the cotton yarn 10 10 9 synthetic yarn is used as a material, but the present invention is flammable to 20 polyesters 2 to 20 polyester 9 composites (Dope-dyed) By weaving, the weight of the dough can be reduced to 230 to 350 g / m 2.

이와 같이 하여 얻은 생지포지를 온도 40 ~ 80℃, 압력 2.0 ~ 5.0톤으로 카렌더링 처리한 후 아크릴바인더와 안료를 함유하는 브롬계 방염제를 전체 조성물의 40 ~ 80중량부, 염화파라핀을 10 ~ 35중량부, 클로로 화합물을 10 ~ 25중량부로 구성된 방염수지를 건식나이프 코팅법을 이용하여 두께 0.5 ~ 2.5㎟로 코팅한 다음 110 ~ 140℃에서 30 ~ 120초간 건조시키고, 다시 2차 나이프 코팅으로 두께 1.0 ~ 3.5mm로 도포한 후 100 ~ 140℃로 30 ~ 120초간 건조한 다음 최종적으로 온도 40 ~ 80℃, 압력 2.0 ~ 5.0톤으로 카렌더링 처리를 실시한다.The raw paper pouch obtained as described above was calendered at a temperature of 40 to 80 ° C. and a pressure of 2.0 to 5.0 ton. Then, a brominated flame retardant containing an acrylic binder and a pigment was 40 to 80 parts by weight of the whole composition, and a paraffin chloride was 10 to 35 Parts by weight, chloro-compound flame retardant resin consisting of 10 to 25 parts by weight of the coating using a dry knife coating method 0.5 ~ 2.5 ㎜ thick and then dried at 110 ~ 140 ℃ for 30 ~ 120 seconds, and then the second knife coating thickness It is applied to 1.0 ~ 3.5mm, dried at 100 ~ 140 ℃ for 30 ~ 120 seconds, and finally calendered at a temperature of 40 ~ 80 ℃, pressure 2.0 ~ 5.0 tons.

이 경우 방염수지로 사용되는 브롬계 방염제는 헥사 브로모 시클로 도데칸(Hexabromo cyclododecane), 테트라 브로모 에탄(Tetrabromo ethan)을 사용하며 본 발명에서는 그린 토너(안료)와 아크릴 바인더가 자체내에 배합된 브롬계 방염제인 파라카본 그린 1852K(독일 쉘 자일라커 사 제품)을 사용한다. 또 방염수지는 상기 브롬계 방염제에 접착성과 방염성을 부여하기 위하여 염화비닐 클로라이드계의 클로로화합물을 첨가하여 여기에 염화파라핀을 10 ~ 25중량부 첨가하므로 피가공물의 방염도는 증가한다.In this case, the bromine flame retardant used as the flame retardant resin uses hexa bromo cyclododecane and tetrabromo ethanol. Paracarbon green 1852K (manufactured by German shell xilaker) is used. In addition, the flame retardant resin adds 10 to 25 parts by weight of vinyl chloride chloride-based chloro compound to impart adhesion and flame retardancy to the bromine flame retardant, thereby increasing the flame retardance of the workpiece.

그러나 방염수지는 상기 브롬계 방염제와 클로로 화합물이외에 유연성을 부과하기 위하여 염화파라핀을 전체 조성물의 10 ~ 25중량부 첨가하고 물을 사용하지 않으므로 방염수지의 농도가 높아 건식 나이프 코팅법에 알맞도록 구성된 방염수지인 것이다.However, since the flame retardant resin is added to 10 to 25 parts by weight of the total composition and water is not used to impart flexibility other than the bromine flame retardant and the chloro compound, the flame retardant has a high concentration of the flame retardant and is suitable for dry knife coating. It is a resin.

이하 본 발명을 실시예에 의거 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail with reference to Examples.

아래 실시예는 본 발명을 제한하려는 것은 아니다. 또 실시예에서 부는 중량부를 나타낸다.The following examples are not intended to limit the invention. In the examples, parts represent parts by weight.

[실시예 1]Example 1

폴리에스터 원착사 20수 5합으로 가연한 방적사를 경, 위사로 하여 평직으로 제직한 생지를 온도 40℃ 압력 5.0톤으로 카렌더링하고 아크릴 바인더와 안료를 함유하는 브롬계 방염제인 파라카본 그린 1852K(독일 쉘 자일라커 사 제품)를 전체 조성물에 대해서 80부, 염화비닐클로라이드계의 클로로 화합물 10부와 염화파라핀 10부로 구성된 방염수지를 그 표면에 도포하되 1차 나이프 코팅으로 두께가 1.0mm 되게 도포층을 형성한 다음 100℃ × 120초간 건조시키고 다시 나이프 코팅으로 두께가 1.5mm 되도록 도포층을 형성한 후 100℃ × 120초간 건조시키고 40℃ × 5.0톤의 조건으로 카렌더링 처리를 하여 차량용 루프 포지를 완성하였다.Paracarbon Green 1852K, a brominated flame retardant containing acrylic binder and pigments, with a polyester weaving yarn composed of 20 polyester yarns, 5 polyester yarns, and light weft yarns. Germany Xylucker Co., Ltd.) was applied to the surface of the composition, 80 parts, 10 parts of vinyl chloride-based chloro compounds and 10 parts of chlorinated paraffins on the surface thereof, with a first knife coating to a thickness of 1.0 mm. And then dried for 100 ℃ × 120 seconds, and again to form a coating layer to the thickness of 1.5mm by knife coating, and then dried for 100 ℃ × 120 seconds and subjected to a calendering treatment under conditions of 40 ℃ × 5.0 tons Completed.

이 차량포지의 물성 측정결과는 방염도 잔영시간 2초, 탄화길이 8.0cm이고 발수도 측정결과는 80이었으며 포지의 무게 측정결과는 410g/㎡ 로서 면을 소재로 한 천막지보다 약 절반 정도로 가벼워 경량화 효과를 거둘 수 있었다.The properties of this vehicle forge were 2 seconds of flame retardancy, carbonization length of 8.0cm, and water repellency of 80. The weight of the forge was 410g / m2, which is about half lighter than cotton tent. It worked.

[실시예 2]Example 2

폴리에스터 필라멘트 (150/2)를 원사로 하여 직성한 생지를 카렌더링하고 브롬계 방염제인 파라카본 그린 1852K가 전체 조성물에 대해 40부, 염화파라핀 25부, 클로로 화합물 35부로 구성된 방염수지를 1차 나이프 코팅층의 두께를 2.0mm로 도포한 후 140℃ × 30초간 건조시킨 다음 다시 2차 나이프 코팅층의 두께를 3.0mm로 도포하고 140℃ × 30초간 건조시킨 후 80℃ × 2.0톤의 조건으로 카렌더링 처리를 하여 텐트포지를 완성하였다.The raw material which was knitted with polyester filament (150/2) as a yarn was calendered, and the flame retardant resin composed of 40 parts of bromine flame retardant Paracarbon Green 1852K, 25 parts of paraffin chloride and 35 parts of chloro compound was primary. After coating the thickness of the knife coating layer to 2.0mm and dried for 140 ℃ × 30 seconds, and then again the thickness of the second knife coating layer to 3.0mm and dried for 140 ℃ × 30 seconds and then calendering under the conditions of 80 ℃ × 2.0 tons The treatment completed the tentforge.

이 텐트 포지의 물성측정결과는 방염도 잔영시간 2초이며 탄화길이 8.0으로 우수하며 발수도 측정결과는 85이며 포지의 무게측정결과는 375g/㎡ 으로 면을 소재로 한 경우 보다 절반이상 가벼워 경량화를 기할 수 있다.The physical properties of this tent forge are 2 seconds of flame retardancy, excellent carbonization length of 8.0, water repellency measurement of 85, and the weight of the forge is 375g / m2, which is more than half lighter than cotton. It can be done.

상기한 바와 같이 제조한 차량용 포지 및 천막지는 수분율이 낮은 폴리에스터 필라멘트사 또는 스펀사를 원사로 사용하였으므로 경량성을 부여할 뿐만 아니라, 방염성이 우수하고 피코팅재와 기포간의 접착력이 우수하여 세탁 견뢰가 뛰어나며 방수성, 발수성이 뛰어나 우천시에도 가벼워서 운반이 용이한 효과를 가진다.Vehicle forge and tent paper manufactured as described above are made of polyester filament yarn or spun yarn having a low moisture content as a yarn, which not only imparts lightness, but also has excellent flame retardancy and excellent adhesion between the coating material and the air bubble, thereby ensuring fast washing. Excellent waterproof and water-repellent, it is light even in rainy days, so it is easy to carry.

Claims (3)

폴리에스터 원착사(Dope-dyed yarn)를 경, 위사로 하여 제직한 생지포지를 아크릴 바인더와 안료를 함유하는 브롬계 방염제가 전체 조성물의 40 ~ 80중량부, 클로로 화합물 10 ~ 35중량부, 염화파라핀 10 ~ 25중량부로 구성된 방염수지를 사용하여 두께 0.5 ~ 2.5mm로 1차 나이프 코팅하고 100 ~ 140℃에서 30 ~ 120초간 건조시킨 다음, 그 위에 다시 방염수지를 두께 1.0 ~ 3.5mm로 도포하여 2차 나이프 코팅함을 특징으로 하는 차량용 루프 포지의 코팅가공방법.The brominated flame retardant containing acrylic binder and pigment is made of a polyester paper weaving yarn made of a polyester-dyed yarn with a light and weft yarn, and 40 to 80 parts by weight of the total composition, 10 to 35 parts by weight of a chloro compound, and chloride Using a flame retardant resin composed of 10 to 25 parts by weight of paraffin, the first knife is coated with a thickness of 0.5 to 2.5 mm, dried at 100 to 140 ° C. for 30 to 120 seconds, and then the flame retardant resin is applied again to a thickness of 1.0 to 3.5 mm. Coating process of the vehicle roof forge, characterized in that the second knife coating. 청구항 1에 있어서,The method according to claim 1, 브롬계 방염제는 헥사 브로모 시클로도데칸(Hexabromo cyclododecane), 테트라 브로모 에탄(Tetrabromo ethan)을 사용함을 특징으로 하는 차량용 루프 포지의 코팅가공방법.Bromine-based flame retardant coating method of a vehicle roof forge, characterized in that the use of hexa bromo cyclododecane (Hexabromo cyclododecane), tetrabromo ethanol (Tetrabromo ethan). 청구항 1에 있어서,The method according to claim 1, 클로로 화합물은 염화비닐클로라이드계 화합물을 사용함을 특징으로 하는 차량용 루프 포지의 코팅가공방법.Chlorine compound is a vinyl chloride chloride-based compound, characterized in that the coating process of the vehicle roof forge.
KR1019970020535A 1997-05-24 1997-05-24 Coating finish method of car's loop fabrics weaved polyester dope dyed yarn KR100216962B1 (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010003533A (en) * 1999-06-23 2001-01-15 염상모 Project of infraredray filter
KR100443467B1 (en) * 2002-05-07 2004-08-09 손권웅 Method of Check Pattern Fabric Using Non-Dyeing Warp and the Check Pattern Fabric

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104088153B (en) * 2014-06-25 2016-09-14 浙江金汇特材料有限公司 A kind of manufacture method of multi-functional industry cloth
KR102161382B1 (en) * 2019-07-23 2020-09-29 박몽룡 Cushion type breathable mat

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010003533A (en) * 1999-06-23 2001-01-15 염상모 Project of infraredray filter
KR100443467B1 (en) * 2002-05-07 2004-08-09 손권웅 Method of Check Pattern Fabric Using Non-Dyeing Warp and the Check Pattern Fabric

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