KR102654423B1 - cosmetic containing garlic fermented extract and manufacturing method thereof - Google Patents
cosmetic containing garlic fermented extract and manufacturing method thereof Download PDFInfo
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- KR102654423B1 KR102654423B1 KR1020160080585A KR20160080585A KR102654423B1 KR 102654423 B1 KR102654423 B1 KR 102654423B1 KR 1020160080585 A KR1020160080585 A KR 1020160080585A KR 20160080585 A KR20160080585 A KR 20160080585A KR 102654423 B1 KR102654423 B1 KR 102654423B1
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- 235000004611 garlic Nutrition 0.000 title claims abstract description 68
- 239000002537 cosmetic Substances 0.000 title claims abstract description 28
- 239000000284 extract Substances 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 244000245420 ail Species 0.000 title 1
- 240000002234 Allium sativum Species 0.000 claims abstract description 67
- 241000209094 Oryza Species 0.000 claims abstract description 19
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 19
- 235000009566 rice Nutrition 0.000 claims abstract description 19
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 16
- 239000006000 Garlic extract Substances 0.000 claims abstract description 14
- 235000020706 garlic extract Nutrition 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 239000012141 concentrate Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 241001148471 unidentified anaerobic bacterium Species 0.000 claims abstract description 5
- 244000063299 Bacillus subtilis Species 0.000 claims abstract description 4
- 235000014469 Bacillus subtilis Nutrition 0.000 claims abstract description 3
- 238000001035 drying Methods 0.000 claims abstract description 3
- 238000000227 grinding Methods 0.000 claims abstract description 3
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 claims description 13
- 238000000855 fermentation Methods 0.000 claims description 9
- 230000004151 fermentation Effects 0.000 claims description 9
- 230000006641 stabilisation Effects 0.000 claims 1
- 238000011105 stabilization Methods 0.000 claims 1
- 230000006872 improvement Effects 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 10
- 206010040880 Skin irritation Diseases 0.000 abstract description 9
- 231100000475 skin irritation Toxicity 0.000 abstract description 9
- 230000036556 skin irritation Effects 0.000 abstract description 9
- 230000002087 whitening effect Effects 0.000 abstract description 6
- 230000037303 wrinkles Effects 0.000 abstract description 6
- 239000004480 active ingredient Substances 0.000 abstract description 5
- 230000003712 anti-aging effect Effects 0.000 abstract description 4
- 239000006210 lotion Substances 0.000 description 9
- 235000019645 odor Nutrition 0.000 description 9
- 206010015150 Erythema Diseases 0.000 description 8
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 7
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 7
- 235000010081 allicin Nutrition 0.000 description 7
- 231100000321 erythema Toxicity 0.000 description 7
- 230000037394 skin elasticity Effects 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- NAXKFVIRJICPAO-LHNWDKRHSA-N [(1R,3S,4R,6R,7R,9S,10S,12R,13S,15S,16R,18S,19S,21S,22S,24S,25S,27S,28R,30R,31R,33S,34S,36R,37R,39R,40S,42R,44R,46S,48S,50R,52S,54S,56S)-46,48,50,52,54,56-hexakis(hydroxymethyl)-2,8,14,20,26,32,38,43,45,47,49,51,53,55-tetradecaoxa-5,11,17,23,29,35,41-heptathiapentadecacyclo[37.3.2.23,7.29,13.215,19.221,25.227,31.233,37.04,6.010,12.016,18.022,24.028,30.034,36.040,42]hexapentacontan-44-yl]methanol Chemical compound OC[C@H]1O[C@H]2O[C@H]3[C@H](CO)O[C@H](O[C@H]4[C@H](CO)O[C@H](O[C@@H]5[C@@H](CO)O[C@H](O[C@H]6[C@H](CO)O[C@H](O[C@H]7[C@H](CO)O[C@@H](O[C@H]8[C@H](CO)O[C@@H](O[C@@H]1[C@@H]1S[C@@H]21)[C@@H]1S[C@H]81)[C@H]1S[C@@H]71)[C@H]1S[C@H]61)[C@H]1S[C@@H]51)[C@H]1S[C@@H]41)[C@H]1S[C@H]31 NAXKFVIRJICPAO-LHNWDKRHSA-N 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 6
- 241000894006 Bacteria Species 0.000 description 5
- 102000004190 Enzymes Human genes 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 3
- 239000004310 lactic acid Substances 0.000 description 3
- 235000014655 lactic acid Nutrition 0.000 description 3
- 229910052711 selenium Inorganic materials 0.000 description 3
- 239000011669 selenium Substances 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 150000003464 sulfur compounds Chemical class 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229930003451 Vitamin B1 Natural products 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000012790 confirmation Methods 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 235000021109 kimchi Nutrition 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 235000019633 pungent taste Nutrition 0.000 description 2
- 239000002453 shampoo Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229960003495 thiamine Drugs 0.000 description 2
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 2
- 235000010374 vitamin B1 Nutrition 0.000 description 2
- 239000011691 vitamin B1 Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010009944 Colon cancer Diseases 0.000 description 1
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010016952 Food poisoning Diseases 0.000 description 1
- 208000019331 Foodborne disease Diseases 0.000 description 1
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 241000590002 Helicobacter pylori Species 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- IDIDJDIHTAOVLG-VKHMYHEASA-N S-methylcysteine Chemical compound CSC[C@H](N)C(O)=O IDIDJDIHTAOVLG-VKHMYHEASA-N 0.000 description 1
- 208000007107 Stomach Ulcer Diseases 0.000 description 1
- 229930003471 Vitamin B2 Natural products 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 235000001465 calcium Nutrition 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 208000029742 colonic neoplasm Diseases 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 229940029982 garlic powder Drugs 0.000 description 1
- 235000013922 glutamic acid Nutrition 0.000 description 1
- 239000004220 glutamic acid Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000000415 inactivating effect Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 201000007270 liver cancer Diseases 0.000 description 1
- 208000014018 liver neoplasm Diseases 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 229960001913 mecysteine Drugs 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 235000019654 spicy taste Nutrition 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 235000019164 vitamin B2 Nutrition 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 230000036642 wellbeing Effects 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
본 발명은 마늘의 발효 추출물을 함유한 화장품의 제조 방법에 관한 것으로, 이러한 방법은, 멸균 처리된 쌀겨 90-110 중량%, 물 1-3 중량%, 설탕 0.1-0.3중량%를 넣고 고초균이 접착하도록 교반하는 단계와, 상기 쌀겨 혼합물에 혐기성균이 발생하지 않도록 1일 2~4회의 교반을 통하여 70-75 시간 동안 75~85℃의 열을 유지시키는 단계와, 상기 단계를 거친 후 발열된 쌀겨를 안정화되도록 48시간 동안 60-65℃의 온도로 유지시키는 단계와, 상기한 60-65℃의 온도를 유지시키면서 효모를 첨가하고 쌀겨 속에 마늘을 안치시킨 후 48시간 동안 마늘을 1차 숙성시키는 단계와, 상기 1차 숙성된 마늘을 진공 쳄버에 넣고 30-35℃의 상온에서 3개월 동안 2차 숙성시키는 단계와, 상기 2차 숙성된 마늘에서 농축액을 추출하여 3-6℃에서 1개월간 3차 숙성시키는 단계와, 상기 3차 숙성된 마늘 농축액을 건조, 분말화 후 용매로 추출하여 마늘 발효 추출물을 얻는 단계, 및 상기 마늘 발효 추출물을 전체 중량에 대하여 0.1-2.0중량%를 포함하는 것을 특징으로 한다. 본 발명은 상기와 같은 제조 방법에 따라, 특정의 효모를 이용하여 마늘을 발효시킨 후 그 추출물을 이용한 화장품을 마련함으로써 마늘의 특이 취를 현저히 감소시키고, 높은 함량의 항노화 활성 성분을 제공하므로 피부 미백, 탄력 및 주름개선, 피부 자극완화 및 진정효과가 우수하여 상품성을 증대시킬 수 있는 효과가 발생한다.The present invention relates to a method for manufacturing cosmetics containing a fermented extract of garlic, in which 90-110% by weight of sterilized rice bran, 1-3% by weight of water, and 0.1-0.3% by weight of sugar are added and Bacillus subtilis adheres. A step of stirring to prevent the generation of anaerobic bacteria in the rice bran mixture, a step of maintaining heat at 75 to 85° C. for 70 to 75 hours through stirring 2 to 4 times a day to prevent the generation of anaerobic bacteria in the rice bran mixture, and the rice bran heated after the above steps. maintaining the temperature at 60-65°C for 48 hours to stabilize it, adding yeast while maintaining the above-mentioned temperature of 60-65°C, placing garlic in rice bran, and then primary maturing the garlic for 48 hours. A step of placing the firstly aged garlic in a vacuum chamber and secondly maturing it at room temperature of 30-35°C for 3 months, extracting a concentrate from the secondly aged garlic and thirdly maturing it at 3-6°C for one month. A step of maturing, drying and powdering the thirdly aged garlic concentrate and extracting it with a solvent to obtain a fermented garlic extract, and comprising 0.1-2.0% by weight of the fermented garlic extract based on the total weight. do. The present invention, according to the above manufacturing method, ferments garlic using a specific yeast and prepares cosmetics using the extract, thereby significantly reducing the specific odor of garlic and providing a high content of anti-aging active ingredients to protect the skin. It has excellent whitening, elasticity and wrinkle improvement, skin irritation relief, and soothing effects, which can increase marketability.
Description
본 발명은 마늘의 발효 추출물을 함유한 화장품 및 그 제조방법에 관한 것으로서, 더욱 상세하게는 특정의 효모를 이용하여 마늘을 발효시킨 후 그 추출물을 이용한 화장품을 마련함으로써 마늘의 특이 취를 현저히 감소시키고, 높은 함량의 항노화 활성 성분을 제공하므로 피부 미백, 탄력 및 주름개선, 피부 자극완화 및 진정효과가 우수하여 상품성을 증대시킬 수 있는 마늘의 발효 추출물을 함유한 화장품 및 그 제조방법에 관한 것이다.The present invention relates to cosmetics containing a fermented extract of garlic and a method for manufacturing the same. More specifically, the present invention relates to fermenting garlic using a specific yeast and then preparing a cosmetic using the extract to significantly reduce the specific odor of garlic. It relates to cosmetics containing fermented extracts of garlic that provide a high content of anti-aging active ingredients and thus have excellent skin whitening, elasticity and wrinkle improvement, skin irritation relief, and soothing effects, thereby increasing marketability, and their manufacturing methods.
일반적으로 마늘(garlic)은 중앙아시아가 원산인 백합과(白合科)에 속하는 식물이며, 대한민국을 비롯하여 중국, 일본 등 극동(極東)에서 많이 재배되고 있으며 그 효능이 과학적으로 밝혀져 웰빙 식품으로 인정받고 있다.In general, garlic is a plant belonging to the Liliaceae family, which is native to Central Asia. It is widely cultivated in the Far East, including Korea, China, and Japan, and its efficacy has been scientifically revealed and it is recognized as a well-being food. I'm receiving it.
이러한 마늘은 주요 성분으로서 탄수화물 20%, 단백질 3.3%, 지방 0.4%, 섬유질 0.92%, 회분 13.4%를 함유하며, 그 밖에 비타민 B1, 비타민 B2, 비타민 C, 글루탐산(glutamic acid), 칼슘, 철, 인, 아연, 셀레늄, 알리신 등 다양한 영양소가 함유되어 있다.Garlic's main ingredients include 20% carbohydrates, 3.3% protein, 0.4% fat, 0.92% fiber, and 13.4% ash. In addition, it contains vitamin B1, vitamin B2, vitamin C, glutamic acid, calcium, iron, It contains various nutrients such as phosphorus, zinc, selenium, and allicin.
그리고 마늘의 대표적인 성분은 알린(allin)이라는 유황화합물인데 알린은 아무런 향이 없지만 마늘 조직이 상하는 순간 알린은 조직 안에 있던 알리나제라는 효소와 작용해 자기방어물질인 알리신(allicin)이 된다.And the representative ingredient of garlic is a sulfur compound called allin. Allin has no scent, but as soon as garlic tissue is damaged, allin interacts with an enzyme called allinase within the tissue to become allicin, a self-defense substance.
상기한 알리신은 매운맛과 동시에 독한 냄새를 풍기지만 강력한 살균, 항균 작용을 하여 식중독균을 죽이고 위궤양을 유발하는 헬리코박터 파이로리균까지 죽이는 효과가 있다.The above-mentioned allicin has a spicy taste and a strong odor, but has a strong sterilizing and antibacterial effect, killing food poisoning bacteria and Helicobacter pylori bacteria that cause gastric ulcers.
또한 알리신은 소화를 돕고 면역력도 높이며, 콜레스테롤 수치를 낮출 뿐만 아니라 비타민 B1과 결합하면 알리티아민으로 변하여 피로 회복에 도움을 준다. In addition, allicin not only aids digestion, increases immunity, and lowers cholesterol levels, but also turns into allitiamine when combined with vitamin B1, helping to relieve fatigue.
그리고 마늘에는 알리신 외에 다양한 유황화합물질이 들어 있는데 예컨대 메틸시스테인(methylcysteine)은 간암과 대장암을 억제한다고 알려져있으며 이러한 유황화합물질은 활성산소를 제거하는 항산화 작용도 한다.In addition to allicin, garlic contains various sulfur compounds. For example, methylcysteine is known to inhibit liver cancer and colon cancer, and these sulfur compounds also have an antioxidant effect by removing free radicals.
아울러 마늘은 토양에 있는 셀레늄을 흡수, 저장하며 셀레늄 역시 암을 예방하는 것으로 알려진 무기질이다(파워푸드 슈퍼푸드, 2010.12.11, 푸른행복).In addition, garlic absorbs and stores selenium in the soil, and selenium is also a mineral known to prevent cancer (Power Food Superfood, December 11, 2010, Blue Happiness).
그러나 이와 같은 마늘의 우수한 기능성이 밝혀지고 있지만, 마늘의 특성상 가공이 쉽지 않아, 조미료나 건강기능식품과 같은 제한적인 분야에 사용되어 왔으며, 그 사용량도 제한적이었다.However, although the excellent functionality of garlic has been revealed, due to the nature of garlic, it is not easy to process, so it has been used in limited fields such as seasonings and health functional foods, and the amount of use has also been limited.
즉, 마늘의 독한 냄새와 자극적인 맛으로 인하여 그 뛰어난 효능에도 불구하고 그 이용에 있어 상당한 제약을 받고 있는데 특히 알리신은 항균작용이 있기 때문에 마늘을 마쇄하여 발효시키는 것이 어려워 널리 이용되지못하고 있다.In other words, due to the strong smell and pungent taste of garlic, despite its excellent efficacy, there are significant restrictions in its use. In particular, because allicin has an antibacterial effect, it is difficult to grind and ferment garlic, making it not widely used.
이에 따라, 발효균의 활성을 저해하는 성분의 생성을 가열처리에 의하여 억제함으로써 발효하거나, 마늘을 고온의 수증기로 멸균처리 및 효소 불활성화 처리를 하여 추출, 여과하여 냄새를 제거하고자 하는 시도가 있었으나 열처리 공정에 의하여 마늘의 유용한 활성성분들이 파괴되거나 감소하여 효과가 저하되는 문제점을 내포하고 있었다.Accordingly, there have been attempts to ferment garlic by suppressing the production of components that inhibit the activity of fermenting bacteria through heat treatment, or to remove odors by extracting and filtering garlic by sterilizing garlic with high-temperature steam and inactivating enzymes, but heat treatment There was a problem that the useful active ingredients of garlic were destroyed or reduced by the process, reducing its effectiveness.
따라서 본 발명은 상기한 사정을 감안하여 이루어진 것으로, 본 발명의 목적은 특정의 효모를 이용하여 마늘을 발효시킨 후 그 추출물을 이용한 화장품을 마련함으로써 마늘의 특이 취를 현저히 감소시키고, 높은 함량의 항노화 활성 성분을 제공하므로 피부 미백, 탄력 및 주름개선, 피부 자극완화 및 진정효과가 우수하여 상품성을 증대시킬 수 있는 마늘의 발효 추출물을 함유한 화장품 및 그 제조방법을 제공하는 데 있다.Therefore, the present invention was made in consideration of the above circumstances, and the purpose of the present invention is to significantly reduce the specific odor of garlic by fermenting garlic using a specific yeast and then providing cosmetics using the extract, and to produce a high content of garlic. The aim is to provide cosmetics containing fermented extracts of garlic that can increase marketability by providing anti-aging active ingredients, thereby improving skin whitening, improving elasticity and wrinkles, relieving skin irritation, and soothing the skin, and a method for manufacturing the same.
이러한 상기 목적은 본 발명에 의해 달성되며, 본 발명의 일면에 따라, 마늘의 발효 추출물을 함유한 화장품의 제조방법은, 멸균 처리된 쌀겨 90-110 중량%, 물 1-3 중량%, 설탕 0.1-0.3중량%를 넣고 고초균(바실러스 서브틸러스)이 접착하도록 교반하는 단계와, 상기 쌀겨 혼합물에 혐기성균이 발생하지 않도록 1일 2~4회의 교반을 통하여 70-75 시간 동안 75~85℃의 열을 유지시키는 단계와, 상기 단계를 거친 후 발열된 쌀겨를 안정화되도록 48시간 동안 60-65℃의 온도로 유지시키는 단계와, 상기한 60-65℃의 온도를 유지시키면서 효모를 첨가하고 쌀겨 속에 마늘을 안치시킨 후 48시간 동안 마늘을 1차 숙성시키는 단계와, 상기 1차 숙성된 마늘을 진공 쳄버에 넣고 30-35℃의 상온에서 3개월 동안 2차 숙성시키는 단계와, 상기 2차 숙성된 마늘에서 농축액을 추출하여 3-6℃에서 1개월간 3차 숙성시키는 단계와, 상기 3차 숙성된 마늘 농축액을 건조, 분말화 후 용매로 추출하여 마늘 발효 추출물을 얻는 단계, 및 상기 마늘 발효 추출물을 전체 중량에 대하여 0.1-2.0중량%를 포함하는 것을 특징으로 한다.This above object is achieved by the present invention, and according to one aspect of the present invention, a method for producing a cosmetic containing a fermented extract of garlic includes 90-110% by weight of sterilized rice bran, 1-3% by weight of water, and 0.1% by weight of sugar. Adding -0.3% by weight and stirring to allow Bacillus subtilis to adhere, and stirring 2 to 4 times a day to prevent anaerobic bacteria from forming in the rice bran mixture, at a temperature of 75 to 85°C for 70 to 75 hours. maintaining the heat, maintaining the temperature of 60-65°C for 48 hours to stabilize the rice bran heated after the above steps, adding yeast while maintaining the temperature of 60-65°C, and adding yeast to the rice bran. A step of primary maturing the garlic for 48 hours after placing the garlic, placing the primary aged garlic in a vacuum chamber and secondary maturing the garlic for 3 months at room temperature of 30-35°C, and secondary maturing the garlic for 48 hours. Extracting the concentrate from garlic and thirdly maturing it at 3-6°C for one month; drying and powdering the thirdly aged garlic concentrate and extracting it with a solvent to obtain a garlic fermentation extract; and the garlic fermentation extract It is characterized in that it contains 0.1-2.0% by weight based on the total weight.
이때 상기 효모는 야생 효모나 사카로마이세스 세레비제인 것이 바람직하다.At this time, the yeast is preferably wild yeast or Saccharomyces cerevisiae.
본 발명의 다른 일면에 따라, 상기한 제조 방법에 의해 제조된 마늘 발효 추출물은 화장품 조성물 전체 중량에 대하여 0.1~2중량% 함유되는데 이러한 화장품은 피부 미백, 피부탄력개선, 피부주름개선, 피부자극완화 및 피부진정용 화장품에 사용될 수 있을 뿐만 아니라 화장수, 크림, 에센스, 클렌징 폼, 클렌징 워터, 팩, 바디 로션, 바디 오일, 바디 젤, 샴푸, 린스, 헤어 컨디셔너, 헤어 젤, 파운데이션, 립스틱, 마스카라 또는 메이크업 베이스의 제형으로 제조될 수 있다는 것을 당업자는 용이하게 알 수 있을 것이다.According to another aspect of the present invention, the fermented garlic extract prepared by the above-described production method contains 0.1 to 2% by weight based on the total weight of the cosmetic composition, and these cosmetics have skin whitening, skin elasticity improvement, skin wrinkle improvement, and skin irritation relief. and skin soothing cosmetics, as well as lotion, cream, essence, cleansing foam, cleansing water, pack, body lotion, body oil, body gel, shampoo, rinse, hair conditioner, hair gel, foundation, lipstick, mascara or Those skilled in the art will easily know that it can be manufactured into a makeup base formulation.
본 발명은 상기와 같은 제조 방법에 따라, 특정의 효모를 이용하여 마늘을 발효시킨 후 그 추출물을 이용한 화장품을 마련함으로써 마늘의 특이 취를 현저히 감소시키고, 높은 함량의 항노화 활성 성분을 제공하므로 피부 미백, 탄력 및 주름개선, 피부 자극완화 및 진정효과가 우수하여 상품성을 증대시킬 수 있는 효과가 발생한다.The present invention, according to the above manufacturing method, ferments garlic using a specific yeast and prepares cosmetics using the extract, thereby significantly reducing the specific odor of garlic and providing a high content of anti-aging active ingredients to protect the skin. It has excellent whitening, elasticity and wrinkle improvement, skin irritation relief, and soothing effects, which can increase marketability.
이하, 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 본 발명을 용이하게 실시할 수 있을 정도로 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail so that a person skilled in the art can easily practice the present invention.
우선적으로 다음과 같은 방법으로 마늘 발효 추출물을 제조한다.First, prepare the garlic fermentation extract by the following method.
1. 멸균처리된 쌀겨100g에 물 1g과 설탕0.1g을 넣고 고초균(바실러스 서브틸러스)이 접착하도록 교반하여 80℃의 열을 발생시키고 이후 쌀겨에 혐기성균이 발생하지 않도록 1일 3회의 교반을 통하여 72시간 열을 유지한다.1. Add 1g of water and 0.1g of sugar to 100g of sterilized rice bran and stir to allow Bacillus subtilus to adhere to generate heat of 80℃. Afterwards, stir 3 times a day to prevent anaerobic bacteria from forming in the rice bran. Maintains heat for 72 hours.
2. 72시간 경과 후 발열된 쌀겨를 안정시키고 이후 48시간을 유지시켜 쌀겨의 온도를 60℃ 까지 내린다.2. After 72 hours, stabilize the heated rice bran and maintain it for 48 hours to lower the temperature of the rice bran to 60℃.
3. 사카로마이세스 세레비제(Saccharomyces cerevisiae)인 효모를 첨가하여 60℃의 온도를 유지시키고 쌀겨 속에 마늘을 안치시킨 후 48시간 동안 마늘을 숙성시킨다.3. Saccharomyces cerevisiae yeast is added to maintain the temperature at 60°C, the garlic is placed in the rice bran, and the garlic is aged for 48 hours.
4. 숙성된 마늘을 진공 챔버에 넣고 30℃의 상온에서 3개월간 숙성시킨다.4. Place the aged garlic in a vacuum chamber and mature for 3 months at room temperature of 30℃.
이때 장시간 숙성시키는 방법은 김치에 유산균이 발생하도록 하는 방법과 유사한데 효모가 활동하여 발생시킨 효소를 먹이로 활성하는 유산균을 이용하는 방법으로 전통적인 장류의 제조 방법에 따른데 착안하여 연구한 것이다.At this time, the method of long-term maturation is similar to the method of producing lactic acid bacteria in kimchi. It is a method of using lactic acid bacteria that feed on enzymes produced by yeast, and was studied based on the traditional method of producing soybean paste.
이러한 방법으로 얻어진 유산균은 김치에서와 같이 마늘을 발효시킴으로써 마늘의 냄새를 감소시키고 알리신의 매운맛을 현저히 감소시킨다.The lactic acid bacteria obtained in this way reduce the odor of garlic and significantly reduce the pungency of allicin by fermenting garlic as in kimchi.
5. 마늘의 추출물을 5℃에서 1개월간 숙성시킨다.5. Ripen the garlic extract at 5℃ for 1 month.
6. 상기 숙성된 마늘을 건조, 분말화한 후 용매로 추출한다.6. The aged garlic is dried, powdered, and extracted with a solvent.
이때 상기 마늘 발효 추출물은 화장품 원료로 제조하기 위해 추출하는데 통상의 용매 추출에 사용되는 용매를 사용할 수 있다.At this time, the garlic fermentation extract can be extracted to manufacture cosmetic raw materials using a solvent used in conventional solvent extraction.
예컨대 상기 분말을 2~10배(중량)의 50~90% 메탄올에 용해시킨 다음, 여과하여 얻어진 여과액을 감압 하에서 농축하여 마늘 발효추출물을 얻는데 본 발명에서는 10g의 추출물 분말에 70% 메탄올을 사용하였다.For example, the powder is dissolved in 2 to 10 times (by weight) 50 to 90% methanol, then filtered, and the obtained filtrate is concentrated under reduced pressure to obtain a garlic fermentation extract. In the present invention, 70% methanol is used for 10 g of extract powder. did.
그리고 상기 마늘 발효 추출물은 화장품 조성물 전체 중량에 대하여 0.1~2중량% 함유되는데 이러한 화장품은 피부 미백, 피부탄력개선, 피부주름개선, 피부자극완화 및 피부진정용 화장품에 사용될 수 있을 뿐만 아니라 화장수, 크림, 에센스, 클렌징 폼, 클렌징 워터, 팩, 바디 로션, 바디 오일, 바디 젤, 샴푸, 린스, 헤어 컨디셔너, 헤어 젤, 파운데이션, 립스틱, 마스카라 또는 메이크업 베이스의 제형으로 제조될 수 있다는 것을 당업자는 용이하게 알 수 있을 것이다.In addition, the garlic fermentation extract contains 0.1 to 2% by weight based on the total weight of the cosmetic composition. These cosmetics can be used in cosmetics for skin whitening, skin elasticity improvement, skin wrinkle improvement, skin irritation relief, and skin soothing, as well as lotion and cream. Those skilled in the art will easily know that it can be prepared in the form of essence, cleansing foam, cleansing water, pack, body lotion, body oil, body gel, shampoo, rinse, hair conditioner, hair gel, foundation, lipstick, mascara or makeup base. You will find out.
[실시예][Example]
이하, 하기의 실시예들을 통하여 본 발명을 상세하게 설명하지만, 본 발명이 이 예들에 의하여 한정되는 것은 아니며 화장품 효과를 위해 아래와 같이 실시하였다.Hereinafter, the present invention will be described in detail through the following examples, but the present invention is not limited to these examples and was carried out as follows for cosmetic effects.
실시예 1 : 마늘 발효 추출물의 제조Example 1: Preparation of garlic fermentation extract
시험예 1: 관능평가Test Example 1: Sensory evaluation
성인 남녀 20명을 대상으로 상기 실시예에서 제조된 마늘 발효 분말로부터 마늘의 특이 취가 나는지에 대하여 관능평가를 실시하였다. 그 결과를 표 1에 나타내었다.A sensory evaluation was conducted on 20 adult men and women to determine whether the fermented garlic powder prepared in the above example had a specific garlic odor. The results are shown in Table 1.
<특이 취 관능 평가><Special odor sensory evaluation>
0 (전혀 냄새가 나지 않았다) ~ 5(매우 심한 마늘 냄새가 났다)0 (there was no smell at all) to 5 (there was a very strong garlic smell)
상기 표 1 에서 확인되는 바와 같이, 본 발명의 실시예에서 제조된 마늘 발효 추출물은 마늘의 특이 취가 현저히 제거된 것을 알 수 있다.As can be seen in Table 1, the garlic fermentation extract prepared in Examples of the present invention had the specific garlic odor significantly removed.
실시예 2~3 : 마늘 발효 추출물을 함유하는 로션의 제조Examples 2-3: Preparation of lotion containing fermented garlic extract
마늘 발효 추출물(실시예 1)을 함유한 로션을 하기의 표 2의 조성 및 함량으로 통상의 방법에 따라 제조하였다.A lotion containing fermented garlic extract (Example 1) was prepared according to a conventional method with the composition and content shown in Table 2 below.
시험예 2: 피부 탄력개선 효과 확인Test Example 2: Confirmation of skin elasticity improvement effect
20~30대 남녀 10명을 대상으로 본 발명에 따른 마늘 발효 추출물을 함유한 화장료와 함유되지 않는 화장료를 매일 아침, 저녁으로 1주일 간 사용하게 하고 피부탄력개선 정도를 평가하게 하였다. 그 결과를 하기 표 3에 나타내었다.Ten men and women in their 20s and 30s were asked to use cosmetics containing and not containing fermented garlic extract according to the present invention every morning and evening for one week, and the degree of improvement in skin elasticity was evaluated. The results are shown in Table 3 below.
<피부 탄력개선 정도 평가><Evaluation of skin elasticity improvement>
0 (효과가 전혀 없다) ~ 5(피부 탄력이 매우 개선되었다.)0 (no effect at all) ~ 5 (skin elasticity is greatly improved.)
상기 표 3에서 확인되는 바와 같이, 본 발명 마늘 발효 추출물을 함유하는 실시예 2, 3의 로션 조성물은 상기 추출물을 함유하지 않은 비교예 1에 비해 피부 탄력개선 효과가 우수하였다.As confirmed in Table 3, the lotion compositions of Examples 2 and 3 containing the fermented garlic extract of the present invention had an excellent skin elasticity improvement effect compared to Comparative Example 1 which did not contain the extract.
시험예 3: 피부 진정 효과 확인Test Example 3: Confirmation of skin soothing effect
현재 피부 알레르기 증상이 없는 20~30대 남녀 10명을 대상으로 하완의 안쪽 부위에 테입 스트리핑 법(Tape Stripping Method)을 통한 피부자극을 유발한 후, 본 발명에 따른 마늘 발효 추출물을 함유한 화장료와 함유되지 않는 화장료를 도포하여 유발된 자극이 진정되는 정도를 상대평가 하였다. 먼저 하완의 안쪽 부위 두 곳에 일반 스카치 테이프로 30회 테이핑을 하여 피부 홍반을 유발하였다. 홍반 유발된 후, 본 발명에 따른 마늘 발효 추출물을 함유한 화장료를 도포하였으며, 본 발명에 따른 마늘 발효 추출물을 함유하지 않은 화장료를 도포하였다. 도포 후 3시간 후 피부 진정 정도를 평가하였다. 그 결과를 하기 표 4에 나타내었다.After inducing skin irritation through the tape stripping method on the inner part of the lower arm of 10 men and women in their 20s and 30s who do not currently have skin allergy symptoms, the cosmetic containing the fermented garlic extract according to the present invention and A relative evaluation was made of the degree to which irritation caused by applying cosmetics that did not contain the substance was calmed down. First, skin erythema was induced by taping two inner parts of the lower arm 30 times with regular scotch tape. After erythema was induced, a cosmetic containing the fermented garlic extract according to the present invention was applied, and a cosmetic not containing the fermented garlic extract according to the present invention was applied. The degree of skin soothing was evaluated 3 hours after application. The results are shown in Table 4 below.
<피부자극정도(홍반) 평가><Skin irritation level (erythema) evaluation>
0(무반응) 1(매우 경미한 홍반흔적) 2(희미한 또는 가벼운 홍반) 0 (no response) 1 (very slight traces of erythema) 2 (dim or light erythema)
3(경계가 뚜렷하나 약한 홍반) 4(뚜렷한 홍반) 5(심한 홍반)3 (clear border but mild erythema) 4 (clear erythema) 5 (severe erythema)
상기 표 4에서 확인되는 바와 같이, 본 발명 마늘 발효 추출물을 함유하는 실시예 2 및 3의 로션 조성물은 상기 추출물을 함유하지 않은 비교예 1의 로션 조성물에 비해 피부자극완화 효과가 우수하였다.As confirmed in Table 4, the lotion compositions of Examples 2 and 3 containing the fermented garlic extract of the present invention had an excellent skin irritation alleviating effect compared to the lotion composition of Comparative Example 1 which did not contain the extract.
본 발명은 기재된 실시예에 따른 마늘의 발효 추출물을 포함하는 화장품의 제조방법에 한정되는 것은 아니고, 본 발명의 사상 및 범위를 벗어나지 않고 다양하게 수정 및 변형할 수 있음은 이 기술의 분야에서 통상의 지식을 가진 자에게 자명하다. 따라서 그러한 변형예 또는 수정예들은 본 발명의 특허청구범위에 속한다 해야 할 것이다.The present invention is not limited to the method for producing cosmetics containing fermented garlic extract according to the described embodiments, and various modifications and variations can be made without departing from the spirit and scope of the present invention as is known in the art. It is self-evident to those with knowledge. Therefore, it should be said that such variations or modifications fall within the scope of the patent claims of the present invention.
Claims (3)
쌀겨 100 중량부를 기준으로, 물 0.9 내지 3.3중량부, 설탕 0.1 내지 0.3중량부를 넣고 고초균(바실러스 서브틸리스)이 접착하도록 교반하는 단계;
상기 쌀겨 혼합물에 혐기성균이 발생하지 않도록 1일 2~4회의 교반을 통하여 70-75 시간 동안 75~85℃의 열을 유지시키는 단계;
상기 단계를 거친 후 발열된 쌀겨를 안정화되도록 48시간 동안 60-65℃의 온도로 유지시키는 단계;
상기 안정화 후 쌀겨에 효모를 첨가하고 쌀겨 속에 마늘을 안치시킨 후 48시간 동안 마늘을 1차 숙성시키는 단계;
상기 1차 숙성된 마늘을 진공 쳄버에 넣고 30-35℃의 실온에서 3개월 동안 2차 숙성시키는 단계;
상기 2차 숙성된 마늘에서 농축액을 추출하여 3-6℃에서 1개월간 3차 숙성시키는 단계;
상기 3차 숙성된 마늘 농축액을 건조, 분말화 후 용매로 추출하여 마늘 발효 추출물을 얻는 단계; 및
상기 마늘 발효 추출물을 전체 중량에 대하여 0.1-2.0중량%를 포함하는 것을 특징으로 하는 마늘의 발효 추출물을 함유한 화장품의 제조방법.In the manufacturing method of cosmetics containing fermented extract of garlic,
Based on 100 parts by weight of rice bran, adding 0.9 to 3.3 parts by weight of water and 0.1 to 0.3 parts by weight of sugar and stirring to allow Bacillus subtilis to adhere;
Maintaining heat at 75-85°C for 70-75 hours by stirring 2-4 times a day to prevent anaerobic bacteria from forming in the rice bran mixture;
Maintaining the heated rice bran at a temperature of 60-65°C for 48 hours to stabilize it after going through the above steps;
After the stabilization, adding yeast to the rice bran, placing the garlic in the rice bran, and then first maturing the garlic for 48 hours;
Putting the firstly aged garlic into a vacuum chamber and secondly maturing it at room temperature of 30-35°C for 3 months;
Extracting the concentrate from the secondary aged garlic and thirdly maturing it at 3-6°C for 1 month;
Obtaining a garlic fermentation extract by drying and powdering the thirdly aged garlic concentrate and extracting it with a solvent; and
A method for producing a cosmetic containing a fermented extract of garlic, characterized in that it contains 0.1-2.0% by weight of the fermented garlic extract based on the total weight.
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