KR102628308B1 - 분자체 ssz-109의 합성 - Google Patents

분자체 ssz-109의 합성 Download PDF

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Publication number
KR102628308B1
KR102628308B1 KR1020207033418A KR20207033418A KR102628308B1 KR 102628308 B1 KR102628308 B1 KR 102628308B1 KR 1020207033418 A KR1020207033418 A KR 1020207033418A KR 20207033418 A KR20207033418 A KR 20207033418A KR 102628308 B1 KR102628308 B1 KR 102628308B1
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South Korea
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molecular sieve
ssz
reaction mixture
molar ratio
tetramethylhexane
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KR20210040830A (ko
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단 씨에
아데올라 플로렌스 오조
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셰브런 유.에스.에이.인크.
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing iron group metals, noble metals or copper
    • B01J29/74—Noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/86—Borosilicates; Aluminoborosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/30—Three-dimensional structures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
KR1020207033418A 2018-06-07 2019-04-26 분자체 ssz-109의 합성 Active KR102628308B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201862681759P 2018-06-07 2018-06-07
US62/681,759 2018-06-07
PCT/IB2019/053433 WO2019234517A1 (en) 2018-06-07 2019-04-26 Synthesis of molecular sieve ssz-109

Publications (2)

Publication Number Publication Date
KR20210040830A KR20210040830A (ko) 2021-04-14
KR102628308B1 true KR102628308B1 (ko) 2024-01-24

Family

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KR1020207033418A Active KR102628308B1 (ko) 2018-06-07 2019-04-26 분자체 ssz-109의 합성

Country Status (6)

Country Link
US (1) US10577252B2 (https=)
EP (1) EP3802425B1 (https=)
JP (1) JP7119128B2 (https=)
KR (1) KR102628308B1 (https=)
CN (1) CN112218826B (https=)
WO (1) WO2019234517A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023235692A1 (en) * 2022-05-31 2023-12-07 Chevron U.S.A. Inc. Molecular sieve boron ssz-121, its synthesis and use
US12544744B2 (en) 2022-05-31 2026-02-10 Chevron U.S.A. Inc. Molecular sieve boron SSZ-113
CN119233947A (zh) 2022-05-31 2024-12-31 雪佛龙美国公司 具有高酸度的分子筛SSZ-117x

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090076317A1 (en) 2007-09-18 2009-03-19 Wenyih Frank Lai Synthesis of high activity ZSM-48
WO2018197982A1 (en) 2017-04-28 2018-11-01 Chevron U.S.A. Inc. Molecular sieve ssz-109, its synthesis and use
WO2018229582A1 (en) 2017-06-12 2018-12-20 Chevron U.S.A. Inc. Molecular sieve ssz-111, its synthesis and use

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ212070A (en) * 1984-05-30 1988-04-29 Mobil Oil Corp Crystalline metallophosphoaluminate, prouction thereof, and use as a catalyst
US5268161A (en) * 1992-10-09 1993-12-07 Chevron Research And Technology Company Process for preparing molecular sieves using a 1,3,3,8,8-pentamethyl-3-azoniabicyclo [3.2.1] octane template
JP3322308B2 (ja) * 1999-09-28 2002-09-09 財団法人 化学技術戦略推進機構 ゼオライトの合成方法
EP1088780A3 (de) * 1999-10-01 2002-09-04 Heidelberger Druckmaschinen Aktiengesellschaft Vorrichtung zum wahlweisen Verschleissen von Blasöffnungen in Bedruckstoff führenden Leiteinrichtungen oder Stangen von Rotationsdruckmaschinen
US7157075B1 (en) * 2005-08-30 2007-01-02 Chevron U.S.A. Inc. Process for preparing MTT zeolites using nitrogen-containing organic compounds
US7754187B2 (en) * 2005-10-31 2010-07-13 Exxonmobil Chemical Patents Inc. Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins
WO2009055216A2 (en) * 2007-10-26 2009-04-30 Exxonmobil Chemical Patents Inc. Method of preparing a molecular sieve composition
FR2925479B1 (fr) * 2007-12-19 2010-01-08 Inst Francais Du Petrole Procede de preparation d'une zeolithe de type structural ith
US8500991B2 (en) * 2008-12-16 2013-08-06 Exxonmobil Research And Engineering Company High activity MTT framework type molecular sieves
CN104271508B (zh) * 2012-05-08 2016-12-14 埃克森美孚化学专利公司 沸石zsm‑18、其合成与其用途
EP2676728A1 (en) * 2012-06-18 2013-12-25 ExxonMobil Chemical Patents Inc. Synthesis of crystalline molecular sieves having the EUO framework type
US9725327B2 (en) * 2012-11-28 2017-08-08 Exxonmobil Chemical Patents Inc. MFI with unusual morphology
SG11201508120QA (en) * 2013-04-02 2015-10-29 Exxonmobil Res & Eng Co Emm-25 molecular sieve material, its synthesis and use
US9296620B2 (en) * 2013-08-09 2016-03-29 Chevron U.S.A. Inc. Preparation of high-silica cha-type molecular sieves using a mixed template
US9266744B2 (en) * 2013-10-10 2016-02-23 Chevron U.S.A. Inc. Synthesis of borosilicate ton-framework type molecular sieves
US9259720B2 (en) * 2014-06-04 2016-02-16 Chevron U.S.A. Inc. Method for making molecular sieve SSZ-100
US9193600B1 (en) * 2014-06-04 2015-11-24 Chevron U. S. A. Inc. Method for making molecular sieve SSZ-99
US9617163B2 (en) * 2014-10-10 2017-04-11 Chevron U.S.A. Inc. Method for making EUO framework type molecular sieves
KR102284567B1 (ko) * 2014-10-24 2021-08-03 셰브런 유.에스.에이.인크. 분자체 ssz-102 및 이의 합성
SG10202006503RA (en) * 2015-08-27 2020-08-28 Chevron Usa Inc Molecular sieve ssz-91, methods for preparing ssz-91, and uses for ssz-91
US9822012B2 (en) * 2016-04-12 2017-11-21 Chevron U.S.A. Inc. Molecular sieve Al-SSZ-63 composition of matter and synthesis thereof
WO2017204867A1 (en) * 2016-05-26 2017-11-30 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-63
CN106350832B (zh) * 2016-08-26 2018-04-10 肯特催化材料股份有限公司 分子筛模板剂高纯度氢氧化六甲双铵水溶液的制备方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090076317A1 (en) 2007-09-18 2009-03-19 Wenyih Frank Lai Synthesis of high activity ZSM-48
WO2018197982A1 (en) 2017-04-28 2018-11-01 Chevron U.S.A. Inc. Molecular sieve ssz-109, its synthesis and use
US20180312408A1 (en) 2017-04-28 2018-11-01 Chevron U.S.A. Inc. Molecular sieve ssz-109, its synthesis and use
US10214427B2 (en) 2017-04-28 2019-02-26 Chevron U.S.A. Inc. Molecular sieve SSZ-109, its synthesis and use
WO2018229582A1 (en) 2017-06-12 2018-12-20 Chevron U.S.A. Inc. Molecular sieve ssz-111, its synthesis and use
US10221074B2 (en) 2017-06-12 2019-03-05 Chevron U.S.A. Inc. Molecular sieve SSZ-111, its synthesis and use

Also Published As

Publication number Publication date
WO2019234517A1 (en) 2019-12-12
EP3802425B1 (en) 2022-02-23
JP7119128B2 (ja) 2022-08-16
KR20210040830A (ko) 2021-04-14
JP2021525701A (ja) 2021-09-27
CN112218826A (zh) 2021-01-12
WO2019234517A9 (en) 2020-10-15
US20190375648A1 (en) 2019-12-12
CN112218826B (zh) 2023-05-26
US10577252B2 (en) 2020-03-03
EP3802425A1 (en) 2021-04-14

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