KR102605615B1 - Functional composition capable of both soil pest control and soil improvement - Google Patents

Functional composition capable of both soil pest control and soil improvement Download PDF

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KR102605615B1
KR102605615B1 KR1020200175770A KR20200175770A KR102605615B1 KR 102605615 B1 KR102605615 B1 KR 102605615B1 KR 1020200175770 A KR1020200175770 A KR 1020200175770A KR 20200175770 A KR20200175770 A KR 20200175770A KR 102605615 B1 KR102605615 B1 KR 102605615B1
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neem
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박매호
김창숙
김민정
김보빈
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주식회사 자연과 미래
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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    • AHUMAN NECESSITIES
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    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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    • AHUMAN NECESSITIES
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    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
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    • A01N65/03Algae
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/26Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/28Myrtaceae [Myrtle family], e.g. teatree or clove
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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    • C09K17/00Soil-conditioning materials or soil-stabilising materials
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Abstract

본 발명은 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것으로서, 더욱 상세하게는 약효증진제로 멀구슬 양명아주 회화나무 차나무에서 추출한 식물추출물, 님오일(Azadirachtin) 또는 님케익(neem-cake), 계피오일, 백운석, 동물부산물, 유황 등이 있으며, 바인더 또는 부형제로 전분(Starch), 글루코오스(Glucose), 규조토(Diatomite) 등을 검토 하여 제형화 하여 만들어 사용하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것이다.The present invention relates to a functional composition capable of controlling soil pests and improving soil at the same time, and more specifically, as a drug efficacy enhancer, plant extracts extracted from Neem, Yangmyeongju, P. china, and Camellia sinensis, neem oil (Azadirachtin), or neem-cake. , cinnamon oil, dolomite, animal by-products, sulfur, etc., and binders or excipients such as starch, glucose, and diatomite are reviewed and formulated to be used for soil pest control and soil improvement at the same time. It relates to possible functional compositions.

Description

토양해충방제와 토양개량이 동시에 가능한 기능성 조성물{Functional composition capable of both soil pest control and soil improvement}Functional composition capable of both soil pest control and soil improvement}

본 발명은 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것으로서, 더욱 상세하게는 약효증진제로 멀구슬 양명아주 회화나무 차나무에 추출한 식물추출물, 님오일(Azadirachtin) 또는 님케익(Neem-cake), 계피오일(Cinnam-aldehyde), 백운석, 동물부산물, 유황 등이 있으며, 바인더 또는 부형제로 전분(Starch), 글루코오스(Glucose), 규조토(Diatomite) 등을 검토하여 제형화하여 만들어 사용하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것이다.The present invention relates to a functional composition capable of controlling soil pests and improving soil at the same time, and more specifically, as a drug efficacy enhancer, plant extracts extracted from Neem, Yangmyeongju, P. china, and Camellia sinensis, neem oil (Azadirachtin), or neem-cake. , cinnamon oil (cinnam-aldehyde), dolomite, animal by-products, sulfur, etc., and starch, glucose, diatomite, etc. as binders or excipients are reviewed and formulated to control soil pests. It relates to a functional composition that can simultaneously improve and improve soil.

전세계적으로 광범위하게 분포하여 농작물에 피해를 주는 식물기생선충은 식물의 지상부에 피해를 주거나 토양에 서식하면서 식물의 뿌리에 피해를 준다. 여러 식물기생선충 중에서 가장 방제가 어렵고 큰 피해를 주는 것이 뿌리혹선충이다.Plant parasitic nematodes, which are widely distributed around the world and cause damage to crops, damage the above-ground parts of plants or damage the roots of plants while living in the soil. Among various plant parasitic nematodes, root-knot nematodes are the most difficult to control and cause the greatest damage.

이러한 뿌리혹선충의 방제법으로는 재배적방제, 물리적방제 그리고 화학적 방제가 있다. Control methods for these root-knot nematodes include cultural control, physical control, and chemical control.

재배적 방제에는 담수, 휴경, 건토, 깊이갈이, 객토, 벼 윤작 재배, 저항성 품종 등이 있으며, 물리적 방제에는 열처리(스팀, 건열, 온탕침법), 태양열 소독 등이 사용되며 화학적 방제에는 포스치아제이트(선충탄) 등의 화학 약제를 살포하여 뿌리혹선충을 방제하고 있다.Agronomic control includes freshwater, fallow, dry soil, deep plowing, fertilized soil, rice rotation, and resistant varieties. Physical control includes heat treatment (steam, dry heat, hot water immersion) and solar disinfection. Chemical control includes Poscia. Root-knot nematodes are controlled by spraying chemical agents such as jate (nematode charcoal).

이의 방제를 위하여 기생선충의 밀도의 증가로 인한 농작물의 수확량 감소를 억제하기 위한 토양소독제를 사용하게 되며, 주로 유기인계의 fosthiazate와 cadusafos 그리고, 밧사미드(유효성분: dazomet)등의 살선충제가 광범위하게 사용되고 있다. 이러한 화학합성농약은 최근에 저독성 농약으로 전환되는 경향이 매우 뚜렷하기는 하나 인체에 대하여 최소한 4급 독성을 나타내며, 토양에 잔류하다가 빗물과 함께 하천으로 유입되어 어류에 대한 3급 이상의 독성을 나타내는 물질이 대부분으로서, 이들의 사용은 최근의 소비자의 식생활 안전을 위협하는 문제점이 있었다.To control this, soil disinfectants are used to suppress the decrease in crop yield due to the increase in the density of parasitic nematodes, and a wide range of nematicides such as organophosphorus fosthiazate, cadusafos, and batsamide (active ingredient: dazomet) are used. It is being used extensively. Although these chemical synthetic pesticides have recently shown a clear tendency to be converted to low-toxicity pesticides, they exhibit at least grade 4 toxicity to the human body, and are substances that remain in the soil and flow into rivers with rainwater, showing grade 3 or higher toxicity to fish. In most cases, their use has had problems threatening the dietary safety of recent consumers.

물리적방제 [physical control]는 잡초나 병충해방제시 화학적, 생물학적 방제가 아닌 물리적 수단으로 병해충을 방제하는 방법으로 종묘소독과 토양소독하는 것이 있다.Physical control is a method of controlling pests using physical means rather than chemical or biological control when exterminating weeds or pests, and includes seedling disinfection and soil disinfection.

종묘소독(種苗消毒))은 종묘(種苗)의 전염병의 발생을 방지하기 위하여 실시하는 것이며, 온탕침법·냉수온탕침법·욕탕침법·태양열 이용법이 있으며 토양소독은 토양전염병의 발생을 방지하기 위하여 실시하는 밭의 표토를 긁어 모아서 거기에 가연제(可燃劑)를 놓고 태우거나 철판 위에 흙을 놓고 밑에서 가열하여 소독하는 소토(燒土)와, 보일러에서 나오는 고압 수증기를 파이프로 땅속에 분출시켜 독하는 증기소독(蒸氣消毒) 및 판흙 등 비교적 소량의 흙을 소독하기 위해 전열장치가 들어 있는 용기 안에 흙을 넣고 가열 살균하는 전기소독(電氣消毒)방법이다Seedling disinfection is carried out to prevent the occurrence of infectious diseases in seedlings. There are hot water acupuncture methods, cold water acupuncture methods, bath acupuncture methods, and solar heat use methods. Soil disinfection is performed to prevent the occurrence of soil infectious diseases. The topsoil of the field is scraped up and burned with a combustible agent, or the soil is placed on an iron plate and heated from below to disinfect it, and high-pressure steam from a boiler is sprayed into the ground through a pipe to poison it. To disinfect a relatively small amount of soil, such as steam sterilization and clay, it is an electric sterilization method in which soil is placed in a container containing an electric heating device and heated to sterilize it.

기소독은 특수한 시설이나 기계가 필요하고 전기소독(電氣消毒) 실험시예서 실시하는 것으로 토양소독은 토양살균제의 향상으로 실행되지 않는다. Injection poisoning requires special facilities or machines and is carried out in an electric disinfection experiment, so soil disinfection is not carried out due to the improvement of soil disinfectants.

학적방제는 화학물질(약제)을 사용하여 병해충이나 잡초와 같은 유해 생물을 방제하는 으로 방법으로, 효과가 확실하고 빠르지만 약해 발생의 염려가 있고 천적도 동시에 죽이는 문제점이 있다.Pesticide control is a method of controlling harmful organisms such as pests and weeds using chemicals (medicines). It is effective and fast, but there is a risk of causing damage and the problem of killing natural enemies at the same time.

본 발명의 배경이 되는 기술로는 특허공개 제2007-0035646호 "계피로부터 분리, 정제한 시나믹 알데히드를 함유하는 농업용 선충방제제 조성물"(특허문헌 1)이 있다. 상기 배경기술에서는 '계피(Cinnamomum cassia)를 분쇄한 후 중량의 5배인 70% 함수 알코올을 가하여 4-40℃에서 12시간 동안 추출한 후 여과한 여액을 함유하는 농업용 선충방제제'을 제안한다. 그러나 상기 배경기술은 본 발명과 같은 구성의 뿌리혹선충에 대해 살선충 효과를 가지는 용도에 대해서는 아직 개시된 바가 없다.The technology behind the present invention is Patent Publication No. 2007-0035646, “Agricultural nematode control composition containing cinnamon aldehyde isolated and purified from cinnamon” (Patent Document 1). The above background technology proposes 'an agricultural nematode control agent containing the filtrate obtained by pulverizing cinnamon (Cinnamomum cassia), adding 70% hydrous alcohol (5 times its weight), extracting it at 4-40°C for 12 hours, and then filtering it.' However, the above background technology has not yet disclosed a use having a nematicidal effect on root-knot nematodes with the same configuration as the present invention.

특허공개 제2007-0035646호 " 계피로부터 분리, 정제한 시나믹 알데히드를 함유하는농업용 선충방제제 조성물"Patent Publication No. 2007-0035646 “Agricultural nematode control composition containing cinnamon aldehyde isolated and purified from cinnamon”

본 발명은 상기와 같은 문제점을 해결하기 위한 것으로, 천연성분을 제형화 하여 만들어 토양해충방제와 토양개량이 동시에 가능하여 작물해충에 대한 방제가 효과적이며 대량생산이 가능하여 경제적인 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하는데 그 목적이 있다.The present invention is intended to solve the problems described above, and is made by formulating natural ingredients to enable soil pest control and soil improvement at the same time, so it is effective in controlling crop pests and can be mass-produced, making it economical for soil pest control and soil improvement. The purpose is to provide a functional composition that can be improved simultaneously.

본 발명은 규조토, 백운석, 님케익, 유황가루, 해조추출물, 옥수수전분 및 히카마박으로 이루어지는 파우더에, 생선부산물발효액, 식물성추출물, 님오일 및 계피오일을 혼합한 액상제를 혼합하여 파고자리파리에 사용하는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하고자 한다.The present invention is a powder made of diatomaceous earth, dolomite, neem cake, sulfur powder, seaweed extract, corn starch, and jicama meal, mixed with a liquid agent mixed with fermented fish by-products, vegetable extracts, neem oil, and cinnamon oil to kill Fargo flies. The aim is to provide a functional composition capable of controlling soil pests and improving soil at the same time, which is characterized by being used for.

또한, 파우더 100중량부를 기준으로 액상제 25~35중량부를 혼합하여 이루어지는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하고자 한다.In addition, the aim is to provide a functional composition capable of simultaneously controlling soil pests and improving the soil, which is made by mixing 25 to 35 parts by weight of a liquid agent based on 100 parts by weight of powder.

또한, 파우더는 백운석 29~43중량부, 규조토 23~27중량부, 님케익 12~16중량부, 해조추출물 1.5~2.5중량부, 유황가루 9~11중량부, 옥수수전분 9~11중량부 및 히카마박 2.5~3.5중량부를 혼합하여 이루어지는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하고자 한다.In addition, the powder contains 29 to 43 parts by weight of dolomite, 23 to 27 parts by weight of diatomaceous earth, 12 to 16 parts by weight of neem cake, 1.5 to 2.5 parts by weight of seaweed extract, 9 to 11 parts by weight of sulfur powder, 9 to 11 parts by weight of corn starch, and The aim is to provide a functional composition capable of controlling soil pests and improving soil at the same time, which is made by mixing 2.5 to 3.5 parts by weight of jicamabak.

또한, 식물추출물은 멀구슬 양명아주 회화나무 차나무 추출물인 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하고자 한다.In addition, the aim is to provide a functional composition capable of controlling soil pests and improving soil at the same time, characterized in that the plant extract is an extract of Neem, Yangmyeongju, Prickly pear, and Tea tree.

또한, 차나무는 차나무 종자를 세척하고 분쇄기로 분쇄한 후 용매를 혼합하고 추출한 후, 95중량% 주정을 혼합하여 감압농축하는 과정을 반복하여 농축하여 추출한 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물을 제공하고자 한다.In addition, tea tree is concentrated and extracted by repeating the process of washing tea tree seeds, pulverizing them with a grinder, mixing solvents, extracting, mixing 95% by weight alcohol and concentrating under reduced pressure, which is used for soil pest control and soil improvement at the same time. The aim is to provide a possible functional composition.

본 발명의 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물은 약효증진제로 멀구슬 양명아주 회화나무 차나무에서 추출한 식물성추출물, 님오일(Azadirachtin) 또는 님케익(Neem-cake), 계피오일(Cinnam-aldehyde), 백운석, 동물부산물, 유황 등이 있으며, 바인더 또는 부형제로 전분(Starch), 글루코오스(Glucose), 규조토(Diatomite) 등을 사용하는 토양해충방제와 토양개량이 동시에 가능하여 작물해충에 대한 방제가 효과적이며 대량생산이 가능하여 경제적인 매우 유용한 효과가 있다.The functional composition of the present invention capable of controlling soil pests and improving the soil at the same time is a drug efficacy enhancer that contains vegetable extracts extracted from Neem, Yangmyeong-Aju, Prickly pear, and Tea Tree, Neem oil (Azadirachtin) or Neem-cake, and Cinnam-aldehyde. ), dolomite, animal by-products, sulfur, etc., and soil pest control and soil improvement using starch, glucose, and diatomite as binders or excipients are possible at the same time, allowing control of crop pests. It is effective and can be mass-produced, so it has a very economical and useful effect.

아래에서 본 발명은 제시된 실시 예를 참조하여 상세하게 설명이 되지만 제시된 실시 예는 본 발명의 명확한 이해를 위한 예시적인 것으로 본 발명은 이에 제한되지 않는다. Below, the present invention will be described in detail with reference to the presented embodiments, but the presented embodiments are illustrative for a clear understanding of the present invention, and the present invention is not limited thereto.

이하 바람직한 실시예에 따라 본 발명의 기술적 구성을 상세히 설명하면 다음과 같다.Hereinafter, the technical configuration of the present invention will be described in detail according to preferred embodiments.

본 발명은 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것으로서, 더욱 상세하게는 약효증진제로 님오일(Azadirachtin) 또는 님케익(Neem-cake), 멀구슬 양명아주 회화나무 차나무에서 추출한 식물성추출물, 계피오일(Cinnam-aldehyde), 백운석, 동물부산물, 유황 등이 있으며, 바인더 또는 부형제로 전분(Starch), 글루코오스(Glucose), 규조토(Diatomite) 등을 검토하여 제형화 하여 만들어 사용하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물에 관한 것이다.The present invention relates to a functional composition capable of controlling soil pests and improving soil at the same time, and more specifically, as a drug efficacy enhancer, neem oil (Azadirachtin) or neem-cake, and vegetable extracts extracted from Neem, Yangmyeongju, Prickly pear, and Tea tree. , cinnamon oil (cinnam-aldehyde), dolomite, animal by-products, sulfur, etc., and starch, glucose, diatomite, etc. as binders or excipients are reviewed and formulated as a soil pest control agent. It relates to a functional composition that can simultaneously improve and improve soil.

본 발명은 규조토, 백운석, 님케익, 유황가루, 해조류추출물, 옥수수전분 및 히카마박으로 이루어지는 파우더에, 생선부산물발효액, 식물성추출물, 님오일 및 계피오일을 혼합한 액상제를 혼합하여 사용하도록 한다.The present invention uses a liquid agent mixed with fermented fish by-products, vegetable extracts, neem oil, and cinnamon oil in a powder made of diatomaceous earth, dolomite, neem cake, sulfur powder, seaweed extract, corn starch, and jicama meal. .

규조토는 단세포 생물인 규조가 죽은 후 그 유해가 쌓여서 형성된 암석이나 퇴적물을 말한다. 대부분의 규조토는 백색을 띠며 약 3㎛ 이하 혹은 1mm 이상 크기의 입자를 가지기도 하지만 보통은 약 10-200㎛ 크기의 세립질 입자로 구성되어 있다. 건조된 규조토의 일반적인 화학조성은 실리카가 약 80-90%, 알루미나가 약 2-4%, 산화철이 약 0.5-2% 정도를 보인다.Diatomaceous earth refers to rocks or sediments formed by the remains of diatoms, single-celled organisms, after they die. Most diatomaceous earth is white and may have particles of about 3㎛ or less or more than 1mm, but usually consists of fine-grained particles of about 10-200㎛. The general chemical composition of dried diatomaceous earth is about 80-90% silica, about 2-4% alumina, and about 0.5-2% iron oxide.

농업에서 규조토는 살충제는 물론 고화방지제로도 사용된다. 일부 농부들은 가축들의 먹이가 굳지 않도록 규조토를 사용하고 수경 재배에서 증식 배지 역할을 하는 데 사용한다. 채소를 재배하는 데 있어서 규조토는 펄라이트(perlite), 버미큘라이트(vermiculite)와 같은 팽창성 점토와 같이 배수가 일어나는 동안에도 물과 영양분을 보존한 상태에서 산소의 순환을 높여주기 때문에 토양 개량제(soil conditioner)로 사용된다.In agriculture, diatomaceous earth is used not only as an insecticide but also as an anti-caking agent. Some farmers use diatomaceous earth to keep their livestock's food from hardening and to serve as a growth medium in hydroponic cultivation. In growing vegetables, diatomaceous earth, like expanded clays such as perlite and vermiculite, is used as a soil conditioner because it increases oxygen circulation while preserving water and nutrients even during drainage. It is used.

백운석 혹은 돌로마이트(dolomite)는 이 광물을 처음 기록한 프랑스 지질학자 돌로뮤에서 유래되었다. 백운석은‘흰 구름 같은 광물’을 뜻하며, 고화석으로도 불리며, 삼방정계에 속하는 광물로 화석성분은 CaMg(CO3)2이다. 탄산칼슘(CaCO3)과 탄산마그네슘(MgCO3) 이 1:1로 복탄산염을 이루고, 흰색, 회색 또는 분홍색, 노란색, 갈색, 녹색을 띤다. 투명 또는 반투명하고 유리 광택이 있는데 결정은 때로 진주 광택이 난다. Dolomite or dolomite is named after the French geologist Dolomew, who first described this mineral. Dolomite means 'white cloud-like mineral' and is also called a paleofossil. It is a mineral belonging to the trigonal system and its fossil component is CaMg(CO 3 ) 2 . Calcium carbonate (CaCO 3 ) and magnesium carbonate (MgCO 3 ) form a complex carbonate in a 1:1 ratio, and are colored white, gray, pink, yellow, brown, or green. They are transparent or translucent and have a glassy luster, and the crystals sometimes have a pearlescent luster.

농업분야 사용은 백운석을 28~10mesh 입도로 파쇄하여 비료용으로 사용되는 것을 석회고토 비료라 한다. 생석회, 소석회 비료와 마찬가지로 산성토양의 토질개량제로서 토양을 중화시켜주고 엽록소 생성(Mg) 등 영양 보충과 중금속 흡수 억제, 미생물 활동 촉진, 병해충 예방 등 농작물의 생산량 증대와 품질 향상, 농경지 보호 등의 효과가 있다.For use in the agricultural field, dolomite is crushed to a particle size of 28 to 10 mesh and used as fertilizer, which is called lime kaolin fertilizer. Like quick lime and slaked lime fertilizers, it is a soil conditioner for acidic soils and neutralizes the soil. It also supplements nutrients such as chlorophyll (Mg), inhibits heavy metal absorption, promotes microbial activity, prevents diseases and pests, increases crop production and improves quality, and protects farmland. There is.

유황은 인류가 작물로부터 발생하는 병해충을 방제하고자 사용한 천연물질 중의 하나이다. 유럽의 고서에 의하면 BC 9세기경, 호메로스(Homer)는 유황은 해충이 기피하는 물질이라고 서술하고 있다. 살균제로서 유황은 1800년대 프랑스에서 포도 흰가루병으로 인하여 포도주 생산량의 80중량부까지 감소하면서 포도 흰가루병을 방제하기 위하여 본격적으로 사용되기 시작하였고 1845년 미국으로 전해져 포도과원에 포도의 흰가루병뿐만 아니라 응애에도 방제효과가 있어 광범위하게 사용되게 되었다. Sulfur is one of the natural substances used by mankind to control diseases and pests arising from crops. According to an old European book, Homer, around the 9th century BC, described sulfur as a substance that pests avoid. Sulfur as a fungicide began to be used in earnest in France in the 1800s to control powdery mildew on grapes, as wine production decreased to 80 parts by weight due to powdery mildew on grapes. It was introduced to the United States in 1845, and was effective in controlling not only powdery mildew on grapes but also mites in grape orchards. It came to be used widely.

순수한 유황은 매우 안정하여 물에 녹지 않은 결정성 황색 고체이다. 인체에 직접적으로 투여될 경우 독성이 강하여 부작용을 초래할 수 있다고 보고되어 있다. 이러한 독성을 가졌음에도 불구하고 유황은 유기농자재로서 미국, 유럽, 우리나라 등지에서 사용이 허용되어 있다. 그리고 현재 우리나라에서도 친환경 유기농 병해충 방제목적으로 사용할 수 있는 친환경 유기농자재의 원료로 허용되어 있으며, 유황을 함유하고 있는 제품이 판매되고 있다.Pure sulfur is a crystalline yellow solid that is very stable and insoluble in water. It has been reported that when administered directly to the human body, it is highly toxic and may cause side effects. Despite its toxicity, sulfur is an organic material and is allowed to be used in the United States, Europe, and Korea. And currently, in Korea, it is permitted as a raw material for eco-friendly organic materials that can be used for eco-friendly organic pest control purposes, and products containing sulfur are sold.

국내에서는 분말유황을 토양에 직접 시비하였을 때 과채류와 마늘의 품질이 증진되거나 병방제 효과가 있다는 연구가 보고된 바 있다.In Korea, studies have reported that applying powdered sulfur directly to the soil improves the quality of fruits and vegetables and garlic or has a disease control effect.

히카마(Pachyrhizus erosus, Yam bean)는 콩과의 덩굴식물로 ‘멕시칸 감자, ‘멕시칸 순무’‘콩감자’라고 불리며 멕시코가 원산지다. 표면은 노란색이며 껍질이 쉽게 벗겨진다. 속은 배나 감자와 비슷한 크림색이다. 단맛이 나고 식감이 아삭아삭하다. 맛이 ‘고소한 사과’같다는 표현이 있다. 뿌리를 제외한 줄기나 잎, 종자 등은 살충제로 이용한다. 잎과 줄기에 독성이 있어서 병충해에 강해 어디서도 잘 자란다. Jicama ( Pachyrhizus erosus , Yam bean) is a vine of the legume family and is called ‘Mexican potato,’ ‘Mexican turnip,’ or ‘bean potato.’ It is native to Mexico. The surface is yellow and the peel peels off easily. The inside is cream-colored, similar to a pear or potato. It has a sweet taste and a crunchy texture. There is an expression that the taste is like ‘a savory apple.’ Except for the roots, stems, leaves, and seeds are used as pesticides. The leaves and stems are toxic, so it is resistant to pests and diseases and grows well anywhere.

히카마에는 로테논이라는 살충 성분이 들어 있다. 로테논은 무색의 결정으로, 화학식 C23 H22 O6. 녹는점 163℃이다. 물에는 거의 녹지 않고, 아세톤·클로로폼 등에 녹는다. 식물성 살충제로서, 특히 오이 고자리파리류에 대해 특효가 있다. 사람과 가축에 대한 독성은 적다. 제품에 사용되는 히카마잎과 종자를 50℃에서 400 bar로 15min 동안 초임계 추출 시 로테논의 함량은 약 1%였다.Jicama contains an insecticidal ingredient called rotenone. Rotenone is a colorless crystal with the chemical formula C23 H22 O6. The melting point is 163℃. It is almost insoluble in water, but dissolves in acetone, chloroform, etc. As a vegetable pesticide, it is particularly effective against cucumber fern flies. It has low toxicity to humans and livestock. When the jicama leaves and seeds used in the product were supercritically extracted at 50°C and 400 bar for 15 minutes, the rotenone content was about 1%.

히카마 잎 추출물은 Chrysomya bezziana 파리 유충 구더기에 살충 효과가 있었으며 종자추출물 혹은 종자추출물의 살충성분에는 흰줄기 모기 유충과 목화진딧물, 박각시나방, 배추 좀 나방 등에 살충효과가 있으므로 농업분야에 널리 사용가능하다.Jicama leaf extract has an insecticidal effect on Chrysomya bezziana fly larvae and maggots, and the seed extract or insecticidal components of the seed extract have an insecticidal effect on white-stalked mosquito larvae, cotton aphids, white-tailed moths, and cabbage moths, so they can be widely used in the agricultural field. .

히카마(Pachyrhizus erosus, Yam bean) 박(cake)은 수율을 높이기 위하여 히카마 종자를 분쇄하여 헥산을 히카마 종자의 20배수 넣은 후 실온에서 24시간 동안 추출하여 형성하도록 할 수 있다.To increase yield, jicama ( Pachyrhizus erosus , Yam bean) cake can be formed by crushing jicama seeds, adding 20 times the amount of hexane as jicama seeds, and then extracting at room temperature for 24 hours.

해조추출물은 다양한 해조를 원료로 하여 제조 과정이나 제조 후 제품에 어떤 화학적 과정이나 화합물을 첨가하지 않은 천연제품을 사용하도록 한다.Seaweed extract is made from various seaweeds and is a natural product that does not add any chemical processes or compounds to the product during or after manufacturing.

이와 같은 해조추출물은 식물의 천연 생장촉진제이면서 천연 유기농자재로 사용될 수 있고, 1차, 2차 영양분의 강력한 원료 및 여러 가지 생리활성제로 구성되며, 본 발명에서는 해조추출물을 분말화한 제품을 사용하도록 한다.Such seaweed extract is a natural growth promoter of plants and can be used as a natural organic material, and is composed of powerful raw materials of primary and secondary nutrients and various bioactive agents. In the present invention, a product made by powdering seaweed extract is used. do.

본 발명에서는 님케익을 파우더로 사용한다.In the present invention, neem cake is used as a powder.

님(Neem)은 멀구슬나무과(Meliaceae)로 학명은 Azadirachta indica 이다.Neem is a member of the neem family (Meliaceae) and its scientific name is Azadirachta indica .

반 상록교목으로 아열대 및 열대지방에서 많이 자라는데 그 50중량부 이상이 인도에 서식하고 있다. 2~3월 흰 꽃이 피며, 꽃이 지고 난 후 달리는 녹색 열매는 7~8월이 되면 노랗게 익어 새들이 즐겨 찾는다. 건조에 강하며 내염성도 높다. 열매는 식용 가능하며 민간 약재로도 이용한다.It is a semi-evergreen tree that grows widely in subtropical and tropical regions, and more than 50 parts by weight of it is found in India. White flowers bloom in February and March, and the green fruits that grow after the flowers ripen turn yellow in July and August, making them a favorite among birds. It is resistant to drying and has high salt resistance. The fruit is edible and is also used as a folk medicine.

님나무 껍질은 차갑고 쓰며 수렴성이 있으며, 독을 없애고, 피를 맑게 한다. 열매에서 추출하는 님오일은 특유의 향이 있으며 식용으로는 사용되지 않는다.Neem tree bark is cold, bitter, and astringent, removes poison, and purifies the blood. Neem oil extracted from the fruit has a unique scent and is not used for food.

열매는 쓴맛이 있고, 치질약, 구충제로 사용된다. 씨 역시 그 맛은 쓰고 구충제로 사용되며, 해독작용이 있다. 씨에서는 45중량부의 오일이 추출되는데 마늘, 유황과 비슷한 냄새가 나는 쓴맛의 오일로서 지방산이 풍부하며 비타민 E, 필수 아미노산 등이 들어 있다.The fruit has a bitter taste and is used as a hemorrhoid medicine and anthelmintic. The seeds are also bitter in taste, used as an insect repellent, and have a detoxifying effect. 45 parts by weight of oil is extracted from the seeds. It is a bitter oil with an odor similar to garlic and sulfur, and is rich in fatty acids and contains vitamin E and essential amino acids.

님케익의 주요성분인 아자디라크틴(azadirachtin)은 곤충의 성장, 생식에 영향을 미쳐 생물농약으로 유용하게 사용되고 있다.Azadirachtin, the main ingredient in neem cake, affects the growth and reproduction of insects and is useful as a biological pesticide.

특히, 원료에 광물(백운석, 규조토 등)이 많이 함유될 경우 제형화가 되지 않거나 쉽게 부스러져 부형제로 천연성분인 옥수수전분을 사용하여 제형화가 가능하도록 하였다.In particular, if the raw materials contain a lot of minerals (dolomite, diatomaceous earth, etc.), they cannot be formulated or easily break down, so corn starch, a natural ingredient, was used as an excipient to enable formulation.

본 발명에서 액상제로는 생선부산물발효액, 식물추출물, 님오일 및 계피오일을 혼합하여 형성한다.In the present invention, the liquid agent is formed by mixing fish by-product fermentation liquid, plant extract, neem oil, and cinnamon oil.

생선부산물은 수산가공업의 부산물로서 식용으로서는 적합하지 못한 부위를 모은 것으로 어종에 따라 영양소 함량 등이 차이가 나지만 양질의 단백질함유량이 35~75% 수준으로 높고 라이신, 메티오닌, 트립토판, 트레오닌 등의 아미노산이 풍부하며 비타민 B군도 풍부하다.Fish by-products are by-products of the seafood processing industry and are a collection of parts that are unsuitable for human consumption. The nutrient content varies depending on the fish species, but the content of high-quality protein is high at around 35-75% and amino acids such as lysine, methionine, tryptophan, and threonine. It is rich in vitamin B group.

본 발명에서 식물성추출물은 멀구슬, 양명아주, 회화나무, 정향, 차나무 등 다양한 천연유래 식물추출물을 사용할 수 있으며, 특히, 식물추출물로 차나무 추출물을 사용하도록 할 수 있다.In the present invention, a variety of naturally derived plant extracts such as neem, columbine, prickly pear tree, clove, and tea tree can be used as the vegetable extract. In particular, tea tree extract can be used as the plant extract.

차나무는 상록의 활엽관목으로서, 학명은 Camellia sinensis이다 Camellia는 동백나무속을 뜻한다. 한국에서는 주로 녹차로 이용되는 Camellia sinensis var. sinensis이 전라도, 경상도, 제주도에서 재배되고 있다. 홍차용으로 주로 이용되는 Camellia sinensis var. assamica은 인도, 스리랑카 등지에서 재배된다. Tea tree is an evergreen broad-leaved shrub. Its scientific name is Camellia sinensis . Camellia refers to the genus Camellia. Camellia sinensis var., which is mainly used as green tea in Korea. sinensis is cultivated in Jeolla-do, Gyeongsang-do, and Jeju-do. Camellia sinensis var. mainly used for black tea. assamica is cultivated in places such as India and Sri Lanka.

아열대 상록 관목으로 환경에 따라 작은 교목으로 자라기도 한다. 수확의 편의를 위해 1미터 내외 높이로 다듬는다. 가지가 많이 갈라진다. 1년생 가지는 흰색이며 잔털이 있고, 2년생 가지는 회갈색이며 털이 없다. 잎은 보통 어긋나며 피침상 장타원형으로 표면은 녹색의 엽맥이 들어갔고 뒷면은 회녹색으로 맥이 튀어나왔으며 양면에 털이 없다. 꽃은 10-11월에 피고 지름 3-5cm로서 흰색이며 향기가 있고 1-3개가 액생하거나 가지 끝에 달린다. 열매는 이듬해의 가을에 익으며 종자는 둥글고 단단하다. It is a subtropical evergreen shrub that can grow into a small tree depending on the environment. For convenience of harvesting, trim them to a height of about 1 meter. The branches diverge a lot. First-year branches are white and have fine hairs, and second-year branches are grey-brown and hairless. The leaves are usually alternate, lanceolate, and oval in shape, with green veins on the surface and grey-green veins on the back, with no hairs on both sides. Flowers bloom in October-November, are 3-5cm in diameter, are white, fragrant, and 1-3 are axillary or hang at the ends of branches. The fruit ripens in the fall of the following year, and the seeds are round and hard.

차나무의 종자는 화장품과 식용으로도 이용되며, 씨앗에서 짜낸 기름은 비료나 가축의 사료로도 쓰이고 비누의 대용으로 쓴다.The seeds of the tea tree are also used for cosmetics and edible purposes, and the oil squeezed from the seeds is also used as fertilizer or livestock feed and as a substitute for soap.

차나무 추출물은 차나무 종자를 세척하고 분쇄기로 분쇄한 후 용매를 혼합하고 추출한 후, 95중량 % 주정을 혼합하여 감압농축하는 과정을 반복하여 농축하여 추출하도록 한다.The tea tree extract is concentrated and extracted by repeating the process of washing the tea tree seeds, pulverizing them with a grinder, mixing solvents, extracting, mixing with 95% by weight alcohol and concentrating under reduced pressure.

차나무 종자 100g을 기준으로 분쇄기로 분쇄한 후, 분쇄시료의 20배수 용매를 분쇄시료가 든 flask에 넣는다. 이후, 각 시료를 추출온도 50℃로 세팅되어 있는 shaker에 넣고 over night 동안 추출한다 추출과정을 마무리하고 gauze와 filter paper를 사용하여 각시료 여과 과정을 진행한다. After pulverizing 100g of tea tree seeds with a grinder, add 20 times the amount of solvent as the pulverized sample into the flask containing the pulverized sample. Afterwards, each sample is placed in a shaker set at an extraction temperature of 50°C and extracted over night. The extraction process is completed and each sample is filtered using gauze and filter paper.

멀구슬(Melia azedarach)은 멀구슬나무(Melia azedarach)는 멀구슬나무과(科 Meliaceae)에 속하는 낙엽교목으로 수피(樹皮)가 잘게 갈라지며 가지 끝에 잎이 달려있다. 열대와 아열대에 지역에 분포하는 식물로 나무껍질 및 뿌리껍질에는 주로 네고리형 트리테르페노이드, 플라본 안트라퀴논 등의 성분을 함유되어 껍질, 열매, 씨 잎에는 구충, 항균, 항바이러스 등의 작용을 한다고 알려져 있고 둥근 난형으로 양명아주는 전초에서 독특한 냄새가 난다.Neem (Melia azedarach) is a deciduous tree belonging to the neem family (Meliaceae). The bark is finely divided and leaves hang at the ends of branches. It is a plant distributed in tropical and subtropical regions. Its bark and root bark mainly contain ingredients such as four-cyclic triterpenoids and flavone anthraquinones, and its bark, fruits, seeds, and leaves have anti-parasitic, antibacterial, and antiviral effects. It is known to have a round oval shape and has a unique odor from its seedlings.

회화나무(Sophora japonica)는 콩과에 속하는 낙엽활엽교목으로 소지는 녹색이고 자르면 냄새가 난다. 잎은 소엽으로 된 우상복엽이다. 꽃은 8월에 피고 황백색이며 원추화서(圓錐花序 원뿔 모양의 꽃)이고, 열매는 잘록잘록한 꼬투리며, 길이 5~8cm 정도로 10월에 익는다. 토심이 깊고 비옥한 곳을 좋아하나 물기가 적어도 잘 살고 병충해에도 강하다.Sophora japonica is a deciduous broad-leaved tree belonging to the legume family. Its branches are green and emit an odor when cut. The leaves are pinnately compound with leaflets. The flowers bloom in August and are yellow-white, cone-shaped flowers. The fruits are narrow pods, about 5 to 8 cm long, and ripen in October. It likes deep, fertile soil, but thrives even when it is not wet and is resistant to pests and diseases.

양명아주(Chenopodium ambrosioides)는 명아주과의 일년초로 줄기는 가지를 많이 치고, 위쪽에 성긴 털이 있으며, 꽃은 6~10월 사이에 핀다. 잎은 장 타원상 피침형으로 어긋나고 가장자리에 크기가 다른 톱니가 있으며, 엽병은 짧고 뒷면은 담황색 선점이 있다. 열매는 포과이며, 종자는 흑갈색의 둥근 난형으로 양명아주는 전초에서 독특한 냄새가 난다. Chenopodium ambrosioides is an annual plant in the Chenopodium family. The stem has many branches, has sparse hairs on the upper part, and flowers bloom between June and October. The leaves are long, oval-lanceolate, alternate, have teeth of different sizes on the edges, and the petioles are short and have light yellow lines on the back. The fruit is a porpoise, and the seeds are dark brown, round, ovate, and the seedlings of Yangmyeong-Aju have a unique smell.

상기 멀구슬나무, 회화나무 및 양명아주를 혼합하여 사용하면, 각각의 추출물을 단독으로 사용하였을 때보다 우수한 살충효과를 발휘함이 확인되었다It was confirmed that when the neem tree, prickly pear tree, and columbine extract were used in a mixture, a superior insecticidal effect was achieved compared to when each extract was used alone.

멀구슬나무 회화나무 명아주의 잎, 줄기 및/또는 뿌리를 세척하고 건조하여 분쇄하여 동일한 량으로 넣고 유기용매를 1 : 10 내지 1 : 40의 중량비율로 혼합하여 48시간 이상 상온에서 추출하여 여과한 후 여과액을 진공감압 농축기를 이용하여 완전농축하고 동결건조기에서 건조시켜 추출물(crude extract)을 얻는다.Wash, dry and grind the leaves, stems and/or roots of Neem and Prickly pear tree pigweed in equal amounts, mix with organic solvent in a weight ratio of 1:10 to 1:40, extract and filter at room temperature for more than 48 hours. Afterwards, the filtrate is completely concentrated using a vacuum concentrator and dried in a freeze dryer to obtain a crude extract.

멀구슬 회화나무 명아주 식물의 추출물을 제조하기 위한 유기용매로는 메탄올, 에탄올, 디클로로메탄, 헥산 또는 이들의 혼합물을 사용할 수 있으며, 바람직하기로는 메탄올 또는 에탄올을 사용한다.The organic solvent for preparing the extract of the Neem plant or Pigweed plant can be methanol, ethanol, dichloromethane, hexane or a mixture thereof, preferably methanol or ethanol.

생성부산물발효액 및 식물추출물에 님오일과 계피오일의 식물성오일을 투입비율대로 투입하여 24시간 정도 충분히 교반하여 주고, 충분히 교반이 이루어진 액상제 혼합물을 상술한 파우더에 투입하여 교반을 진행하도록 하고, 이후 성형기를 이용하여 일정 형태로 제형하고 건조하도록 한다. Vegetable oils such as neem oil and cinnamon oil are added to the by-product fermentation liquid and plant extract according to the input ratio and stirred sufficiently for about 24 hours. The sufficiently stirred liquid mixture is added to the above-mentioned powder and stirred, and then Form it into a certain shape using a molding machine and dry it.

본 발명에서는 바람직하게는 파우더 100중량부를 기준으로 액상제 25~35중량부를 혼합하도록 하는데, 액상제가 25중량부 미만으로 혼합시에는 제형이 이루어지지 않고 잘 부스러지며, 35중량부를 초과하여 혼합시에는 건조가 느리고 제형의 경도가 떨어질 뿐만 아니라 경제성이 떨어지기 때문에, 액상제 25~35중량부를 혼합하도록 하는 것이 바람직하다.In the present invention, it is preferable to mix 25 to 35 parts by weight of liquid agent based on 100 parts by weight of powder. When mixed with less than 25 parts by weight of liquid agent, the formulation does not form and crumbles easily, and when mixed with more than 35 parts by weight, the liquid agent is mixed. Since drying is slow, the hardness of the formulation is low, and economic feasibility is low, it is preferable to mix 25 to 35 parts by weight of the liquid agent.

파우더는 백운석 29~43중량부, 규조토 23~27중량부, 님케익 12~16중량부, 해조추출물 1.5~2.5중량부, 유황가루 9~11중량부, 옥수수전분 9~11중량부 및 히카마박 2.5~3.5중량부를 혼합하는 것이 바람직하다.The powder contains 29 to 43 parts by weight of dolomite, 23 to 27 parts by weight of diatomaceous earth, 12 to 16 parts by weight of neem cake, 1.5 to 2.5 parts by weight of seaweed extract, 9 to 11 parts by weight of sulfur powder, 9 to 11 parts by weight of corn starch, and jicama. It is preferable to mix 2.5 to 3.5 parts by weight of foil.

규조토와 백운석은 백운석 43중량부, 규조토27중량부 보다 많이 넣으면 제형화가 어렵고 백운석을 29중량부, 규조토를 23중량부보다 적게 넣으면 경제성이 떨어진다. Diatomaceous earth and dolomite are difficult to formulate if more than 43 parts by weight of dolomite and 27 parts by weight of diatomaceous earth are added, and economic feasibility is poor if less than 29 parts by weight of dolomite and 23 parts by weight of diatomaceous earth are added.

님케익 12~16중량부, 유황가루 9~11중량부, 히카마박 2.8~3.5중량부는 살충효과 증진을 위한 혼합하는 것으로 일정량보다 적으면 살충효과가 떨어지고 많이 넣으면 경제성이 떨어진다.12 to 16 parts by weight of neem cake, 9 to 11 parts by weight of sulfur powder, and 2.8 to 3.5 parts by weight of jicama bag are mixed to enhance the insecticidal effect. If the amount is less than a certain amount, the insecticidal effect decreases, and if added in large amounts, it becomes less economical.

옥수수 전분 9~11중량부은 부형제로서 적게 넣으면 쉽게 부서지고 많게 넣을 경우 분해가 잘되지 않는다.9 to 11 parts by weight of corn starch is an excipient. If a small amount is added, it breaks easily, and if a large amount is added, it does not decompose easily.

<실험예 1><Experimental Example 1>

상추비효실험Lettuce effectiveness experiment

토양개량 및 생육자재 시제품이 상추 생육 및 수확량에 미치는 영향을 알아보기 위하여 다음과 같이 실험하였다.To determine the effect of soil improvement and growth material prototypes on lettuce growth and yield, the following experiment was conducted.

- 시험 작물 : 상추- Test crop: lettuce

- 사용약제 : 무처리, 실험구 (NF-D)- Chemicals used: untreated, experimental group (NF-D)

- 개요 및 재배방법 : 상추 종자를 20cm ×60cm 포트에 5kg의 흙을 넣고 시제품 10g 씩 토양 혼화 처리한 후 20cm 간격으로 상추 모종을 정식하였음.- Overview and cultivation method: Lettuce seeds were placed in a 20cm

- 구체적인 처리내용- Specific processing details

시험약제Test drug 주원료main ingredient 처리방법Processing method 무처리구Non-processed area 실험구(NF-D)Experimental district (NF-D) powder: 규조토 25중량부+ 백운석 35중량부+ 님케?? 15중량부+ 해조추출물 2중량부+ 유황가루 10중량부+ 옥수수전분 10중량부+ 히카마박 3중량부
liquid: 파우더 100중량부를 기준으로 생산부산물발효액10중량부 + 식물추출물 10중량부 + 님오일 5중량부+ 계피오일 5중량부
powder: 25 parts by weight of diatomaceous earth + 35 parts by weight of dolomite + Nimke?? 15 parts by weight + 2 parts by weight seaweed extract + 10 parts by weight sulfur powder + 10 parts by weight corn starch + 3 parts by weight jicama meal
liquid: Based on 100 parts by weight of powder, 10 parts by weight of fermentation liquid by-product + 10 parts by weight of plant extract + 5 parts by weight of neem oil + 5 parts by weight of cinnamon oil
토양 혼화 처리Soil mixing treatment

- 조사항목- Survey items

구 분division 조 사 항 목Investigation items 조사횟수Number of investigations 조 사 방 법Investigation method 비효시험Ineffectiveness test ○ 생육조사
- 최대엽장, 최대엽폭, 엽수, 엽록소함량
○ Growth survey
- Maximum leaf length, maximum leaf width, number of leaves, chlorophyll content
2회 Episode 2 정식 30일, 37일 후 구당 3잎에 대한 생육 및 수량조사함Growth and quantity survey of 3 leaves per plot 30 and 37 days after planting
○ 수량 및 품질조사
- 지상부생체중
○ Quantity and quality survey
- Above-ground living weight
○ 수확량 조사○ Yield survey 정식 30일, 37일 후 구당 전주에 대한 수량을 조사함After 30 and 37 days of official establishment, the quantity of electric poles per district was surveyed.

(시험 결과 1)(Test Result 1)

가. 결과go. result

○ 상추 생육과 품질에 대한 효과(정식 30일 후)○ Effect on lettuce growth and quality (30 days after planting)

시험약제Test drug 엽록소함량
(SPAD)
Chlorophyll content
(SPAD)
최대엽장
(㎝)
Maximum leaf length
(cm)
최대엽폭
(㎝)
maximum leaf width
(cm)
엽수
(매/주)
ground game
(every week)
실 험 구
(NF-D)
experiment sphere
(NF-D)
53.453.4 16.516.5 9.79.7 55
무 처 리 구untreated sphere 50.550.5 14.514.5 8.48.4 55

○ 수량 및 수량구성요소(정식 30일 후) ○ Quantity and quantity components (30 days after formalization)

시험약제Test drug 지상부생체중
(g/주)
above-ground body weight
(g/week)
수확량
(g/구)
yield
(g/gu)
수확 증감율
(%)
Yield increase/decrease rate
(%)
실 험 구
(NF-D)
experiment sphere
(NF-D)
4.74.7 7070 4040
무 처 리 구untreated sphere 3.33.3 5050 --

나. 결과 요약me. Summary of Results

- 상추의 생육조사결과 30일 후 처리구는 무처리구 대비 초장최대엽장 최대엽폭에서 증가하는 경향을 보였으며 엽록소 함량 역시 높은 경향을 보였음- As a result of the lettuce growth investigation, after 30 days, the treated group showed an increase in the maximum leaf length and maximum leaf width compared to the untreated group, and the chlorophyll content also tended to be higher.

- 상추의 구당 수확량에서는 NF-D 처리구가 무처리구 대비 40% 증가하여 가장 많은 수확량을 보였으며 다른 처리구에서도 무처리구 대비 수확량이 증가하였음- In terms of lettuce yield per lot, the NF-D treatment group showed the highest yield with a 40% increase compared to the untreated group, and the yield in other treatments also increased compared to the untreated group.

(시험 결과 2)(Test Result 2)

가. 결과go. result

○ 상추 생육과 품질에 대한 효과(정식 37일 후)○ Effect on lettuce growth and quality (37 days after planting)

시험약제Test drug 엽록소함량
(SPAD)
Chlorophyll content
(SPAD)
최대엽장
(㎝)
Maximum leaf length
(cm)
최대엽폭
(㎝)
maximum leaf width
(cm)
엽수
(매/주)
ground game
(every week)
실 험 구
(NF-D)
experiment sphere
(NF-D)
40.240.2 17.817.8 9.99.9 1616
무 처 리 구untreated sphere 43.843.8 16.716.7 9.89.8 1616

○ 수량 및 수량구성요소(정식 37일 후) ○ Quantity and quantity components (37 days after formalization)

시험약제Test drug 지상부생체중
(g/주)
above-ground body weight
(g/week)
수확량
(g/구)
yield
(g/gu)
수확 증감율
(%)
Yield increase/decrease rate
(%)
실 험 구
(NF-D)
experiment sphere
(NF-D)
4.14.1 7070 7.77.7
무 처 리 구untreated sphere 4.04.0 6565 --

나. 결과 요약me. Summary of Results

- 상추의 생육조사결과 37일 후 처리구는 무처리구 대비 초장최대엽장 최대엽폭에서 증가하는 경향을 보였으며 엽록소 함량 역시 높은 경향을 보였음- As a result of the lettuce growth investigation, after 37 days, the treated group showed an increase in the maximum leaf length and maximum leaf width compared to the untreated group, and the chlorophyll content also tended to be higher.

- 상추의 구당 수확량에서는 NF-D의 수확량은 7.7% 증가하였음- In the yield per head of lettuce, the yield of NF-D increased by 7.7%.

- 37일 동안 작물생육 이상 및 외관상 나타난 비해 증상은 없었음 - There were no symptoms compared to crop growth abnormalities or appearance for 37 days.

다. 고찰all. Review

- 30일 37일 비교 및 비교 시험 결과 NF-D가 상추의 생육과 수량증가에서 가장 우수한 효과를 나타내었으며 모든 처리구에서 비해가 없었으므로 NF-D가 토양개량제로서 적절하다고 사료됨 - As a result of the 30- and 37-day comparison and comparison test, NF-D showed the best effect on the growth and yield increase of lettuce, and there was no comparison in all treatments, so NF-D is considered appropriate as a soil conditioner.

<실험예 2> <Experimental Example 2>

토양개량 및 생육자재 시제품이 쪽파 생육 및 수확량에 미치는 영향을 알아보기 위하여 다음과 같이 실험하였다.To determine the effect of soil improvement and growth material prototypes on chive growth and yield, the following experiment was conducted.

- 실험 작물 : 쪽파- Experimental crop: chives

- 사용약제 : 무처리, 대조구, 실험구(NF-D)- Chemicals used: untreated, control group, experimental group (NF-D)

- 개요 및 재배방법 : 쪽파 모종을 36.5cm ×64cm 포트에 18kg의 흙을 넣고 실험구Ⅰ(시제품) 17g과 대조구 10g씩 토양 혼화 처리한 후 10cm 간격으로 쪽파 모종을 정식하였음 - Overview and cultivation method: 18kg of soil was placed in a 36.5cm

- 주원료 투입비율 - Main raw material input ratio

시험약제Test drug 주원료main ingredient 처리방법Processing method 무처리구Non-processed area - - 실험구
(NF-D)
Experimental district
(NF-D)
powder: 규조토 25중량부+ 백운석 35중량부+ 님케?? 15중량부+ 해조추출물 2중량부+ 유황가루 10중량부+ 옥수수전분 10중량부+ 히카마박 3중량부
liquid: 파우더 100중량부를 기준으로 생산부산물발효액10중량부 + 식물추출물 10중량부 + 님오일 5중량부+ 계피오일 5중량부
powder: 25 parts by weight of diatomaceous earth + 35 parts by weight of dolomite + Nimke?? 15 parts by weight + 2 parts by weight seaweed extract + 10 parts by weight sulfur powder + 10 parts by weight corn starch + 3 parts by weight jicama meal
liquid: Based on 100 parts by weight of powder, 10 parts by weight of fermentation liquid by-product + 10 parts by weight of plant extract + 5 parts by weight of neem oil + 5 parts by weight of cinnamon oil
토양 혼화 처리Soil mixing treatment

- 조사항목- Survey items

구 분division 조 사 항 목Investigation items 조사횟수Number of investigations 조 사 방 법Investigation method 비효시험Ineffectiveness test ○ 생육조사
- 최대엽장, 근장
○ Growth survey
- Maximum leaf length, root length
1회 1 time 정식 34일 후 구당 쪽파 대한 생육 및 수량조사함34 days after planting, the growth and quantity of chives per district were investigated.
○ 수량 및 품질조사
- 지상하부생체중
○ Quantity and quality survey
- Live weight below ground

가. 결과go. result

○ 쪽파 생육과 수량에 대한 효과(정식 34일 후)○ Effect on chive growth and yield (34 days after planting)

시험약제Test drug 최대엽장
(㎝)
Maximum leaf length
(cm)
최대근장
(㎝)
Maximum length
(cm)
생체중
(g)
live weight
(g)
무 처 구What to do 25.125.1 15.915.9 60.9660.96 실 험 구
(NF-D)
experiment sphere
(NF-D)
27.627.6 19.819.8 81.3081.30

나. 결과 요약me. Summary of Results

쪽파의 생육조사결과 34일 후 실험구Ⅰ는 무처리구 대비 생체중이 32.9% 증가하였고 최대엽장 및 최대근장은 각각 10.0%, 24.5% 증가율을 보였음.As a result of the growth investigation of chives, after 34 days, experimental group I showed a 32.9% increase in live weight compared to the untreated group, and a 10.0% and 24.5% increase in maximum leaf length and maximum root length, respectively.

<실험예 3> <Experimental Example 3>

파 고자리파리에 대한 시제품의 살충효과를 알아보기 위하여 다음 과같이 실험하였다.To determine the insecticidal effect of the prototype on green onion flies, the following experiment was conducted.

- 시험 작물 : 쪽파- Test crop: chives

- 사용약제 : 무처리, 실험구(NF-D)- Chemicals used: untreated, experimental group (NF-D)

- 개요 및 재배방법 : 쪽파 모종을 36.5cm ×64cm 포트에 18kg의 흙을 넣고 실험구 (시제품) 17g과 대조구 10g씩 토양 혼화 처리한 후 10cm 간격으로 쪽파 모종을 정식하였음 - Overview and cultivation method: 18kg of soil was placed in a 36.5cm

- 파 고자리파리의 무처리 평균 피해주율이 12.8%로 약효 검증을 하기에 충분하였음- The average untreated damage rate of green onion fly was 12.8%, which was sufficient to verify the drug’s efficacy.

- 주원료 투입비율 - Main raw material input ratio

시험약제Test drug 주원료main ingredient 처리방법Processing method 무처리구No treatment - - 실험구
(NF-D)
Experimental district
(NF-D)
powder: 규조토 25중량부+ 백운석 35중량부+ 님케?? 15중량부+ 해조추출물 2중량부+ 유황가루 10중량부+ 옥수수전분 10중량부+ 히카마박 3중량부
liquid: 파우더 100중량부를 기준으로 생산부산물발효액10중량부 + 식물추출물 10중량부 + 님오일 5중량부+ 계피오일 5중량부
powder: 25 parts by weight of diatomaceous earth + 35 parts by weight of dolomite + Nimke?? 15 parts by weight + 2 parts by weight seaweed extract + 10 parts by weight sulfur powder + 10 parts by weight corn starch + 3 parts by weight jicama meal
liquid: Based on 100 parts by weight of powder, 10 parts by weight of fermentation liquid by-product + 10 parts by weight of plant extract + 5 parts by weight of neem oil + 5 parts by weight of cinnamon oil
토양 혼화 처리Soil mixing treatment

- 조사방법 - Research method

구분division 조사항목Survey items 조사횟수Number of investigations 조사방법Research method 약효medicinal effect 피해주율 Damage rate 1회 1 time 약제처리 28일 후 구당 전주(200주 )에 대한 피해주수 조사Survey on the number of damaged plants per district (200 plants) after 28 days of chemical treatment

가. 결과go. result

○ 파 고자리파리에 대한 약제방제 효과(약제처리 후 28일 차) ○ Effect of chemical control on green onion fly (28th day after chemical treatment)

시험약제Test drug 피해주율(%)Damage rate (%) 유의차
(DMRT)
significant difference
(DMRT)
방제가
(%)
pest control
(%)
Ⅰ반복ⅠRepeat Ⅱ반복ⅡRepeat Ⅲ반복ⅢRepeat 평 균average 실험구(NF-D)Experimental district (NF-D) 7.5 7.5 5.5 5.5 6.0 6.0 6.3 6.3 aa 50.8 50.8 무 처 리Untreated 15.0 15.0 12.0 12.0 11.5 11.5 12.8 12.8 aa -- C.V.(%)C.V.(%) -------------------------------------------------------- (7.4)(7.4)

나. 결과 요약me. Summary of Results

- 실험구의 방제가는 50.8% 무처리구 대비 우수한 방제가를 보였음 - The control value of the experimental group was 50.8%, showing an excellent control value compared to the untreated group.

상기와 같은 본 발명의 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물은 약효증진제로 멀구슬 양명아주 회화나무차나무에서 추출한 추출물(Tea saponin), 님오일(Azadirachtin) 또는 님케익(Neem-cake), 계피오일(Cinnam-aldehyde), 백운석, 동물부산물, 유황 등이있으며, 바인더 또는 부형제로 전분(Starch), 글루코오스(Glucose), 규조토(Diatomite) 등을 사용하는 토양해충방제와 토양개량이 동시에 가능하여 작물해충에 대한 방제가 효과적이며 대량생산이 가능하여 경제적인 매우 유용한 효과가 있다.The functional composition of the present invention capable of simultaneously controlling soil pests and improving soil as described above includes tea saponin, neem oil (Azadirachtin) or neem cake as a drug efficacy enhancer, Cinnam-aldehyde, dolomite, animal by-products, sulfur, etc. are included, and soil pest control and soil improvement are possible at the same time by using starch, glucose, and diatomite as binders or excipients. It is effective in controlling crop pests and can be mass-produced, so it has a very useful economic effect.

지금까지 본 발명은 제시된 실시 예를 참조하여 상세하게 설명이 되었지만 이 분야에서 통상의 지식을 가진 자는 제시된 실시 예를 참조하여 본 발명의 기술적 사상을 벗어나지 않는 범위에서 다양한 변형 및 수정 발명을 만들 수 있을 것이다. 본 발명은 이와 같은 변형 및 수정 발명에 의하여 제한되지 않으며 다만 아래에 첨부된 청구범위에 의하여 제한된다. So far, the present invention has been described in detail with reference to the presented embodiments, but those skilled in the art can make various variations and modifications without departing from the technical spirit of the present invention with reference to the presented embodiments. will be. The present invention is not limited by such variations and modifications, but is limited by the claims appended below.

Claims (5)

규조토, 백운석, 님케익, 유황가루, 해조류추출물, 옥수수전분 및 히카마박으로 이루어지는 파우더에, 생선부산물발효액, 차나무추출물, 님오일 및 계피오일을 혼합한 액상제를 혼합하여 파고자리파리에 사용하는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물.A powder made of diatomaceous earth, dolomite, neem cake, sulfur powder, seaweed extract, corn starch, and jicama meal is mixed with a liquid agent mixed with fermented fish by-products, tea tree extract, neem oil, and cinnamon oil to be used against phagocytos flies. A functional composition capable of simultaneously controlling soil pests and improving soil. 청구항 1에 있어서,
파우더 100중량부를 기준으로 액상제 25~35중량부를 혼합하여 이루어지는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물.
In claim 1,
A functional composition capable of controlling soil pests and improving soil at the same time, characterized by mixing 25 to 35 parts by weight of liquid agent based on 100 parts by weight of powder.
청구항 1에 있어서,
파우더는 백운석 29~43중량부, 규조토 23~27중량부, 님케익 12~16중량부, 해조추출물 1.5~2.5중량부, 유황가루 9~11중량부, 옥수수전분 9~11중량부 및 히카마박 2.5~3.5중량부를 혼합하여 이루어지는 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물.
In claim 1,
The powder contains 29 to 43 parts by weight of dolomite, 23 to 27 parts by weight of diatomaceous earth, 12 to 16 parts by weight of neem cake, 1.5 to 2.5 parts by weight of seaweed extract, 9 to 11 parts by weight of sulfur powder, 9 to 11 parts by weight of corn starch, and jicama. A functional composition capable of controlling soil pests and improving soil at the same time, characterized by mixing 2.5 to 3.5 parts by weight of pak.
삭제delete 청구항 1에 있어서,
차나무추출물은 차나무 종자를 세척하고 분쇄기로 분쇄한 후 용매를 혼합하고 추출한 후, 95중량% 주정을 혼합하여 감압농축하는 과정을 반복하여 농축하여 추출한 것을 특징으로 하는 토양해충방제와 토양개량이 동시에 가능한 기능성 조성물.





In claim 1,
Tea tree extract is a product capable of controlling soil pests and improving soil at the same time, which is characterized by being concentrated and extracted by repeatedly washing tea tree seeds, pulverizing them with a grinder, mixing solvents, extracting, then mixing 95% by weight alcohol and concentrating under reduced pressure. Functional composition.





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