KR102599866B1 - Manufacturing Method of Chestnut inner Shell Tea - Google Patents
Manufacturing Method of Chestnut inner Shell Tea Download PDFInfo
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- KR102599866B1 KR102599866B1 KR1020210113193A KR20210113193A KR102599866B1 KR 102599866 B1 KR102599866 B1 KR 102599866B1 KR 1020210113193 A KR1020210113193 A KR 1020210113193A KR 20210113193 A KR20210113193 A KR 20210113193A KR 102599866 B1 KR102599866 B1 KR 102599866B1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/12—Rolling or shredding tea leaves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/06—Treating tea before extraction; Preparations produced thereby
- A23F3/14—Tea preparations, e.g. using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/20—Removing unwanted substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/40—Tea flavour; Tea oil; Flavouring of tea or tea extract
- A23F3/405—Flavouring with flavours other than natural tea flavour or tea oil
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
- A23L2/382—Other non-alcoholic beverages fermented
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
- C12J1/04—Vinegar; Preparation or purification thereof from alcohol
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
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- A—HUMAN NECESSITIES
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- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/10—Drying, dehydrating
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/12—Electrical treatment, e.g. electrolysis, electrical field treatment, with or without heating effect
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
Abstract
본 발명은 율피차의 제조방법에 관한 것으로, 율피 100중량부를 2,450MHz의 마이크로파로 10분 동안 조사하는 단계(단계 1); 상기 마이크로파 처리된 율피를 1.5%(w/v) 농도의 자염수에 20~30℃에서 5~10분 동안 1차 침지하는 단계(단계 2); 상기 1차 침지된 율피를 아로니아식초에 20~30℃에서 1~3분 동안 2차 침지하는 단계(단계 3); 상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하는 단계(단계 4); 상기 1차 건조한 율피를 60℃에서 2시간 동안 2차 건조하는 단계(단계 5); 및 상기 2차 건조된 율피를 분쇄하여 율피분말을 제조하는 단계(단계 6); 를 포함하여 제조하는 것을 기술적 특징으로 하며, 쓴맛을 저감시킬 수 있는 장점이 있으며, 율피의 유용성분을 섭취할 수 있는 장점이 있다.
The present invention relates to a method of manufacturing Yulpi tea, comprising the steps of irradiating 100 parts by weight of Yulpi tea with a microwave of 2,450 MHz for 10 minutes (step 1); Primary immersion of the microwave-treated Yulpi in 1.5% (w/v) concentration of saline water at 20-30°C for 5-10 minutes (step 2); Secondary immersion of the primarily immersed Yulpi in aronia vinegar at 20-30°C for 1-3 minutes (step 3); Primary drying the secondarily immersed yulpi at 80°C for 1 hour (step 4); Secondary drying the first dried yulpi at 60°C for 2 hours (step 5); And grinding the secondary dried yulpi to produce yulpi powder (step 6); It has a technical feature of being manufactured including, and has the advantage of reducing the bitter taste and of being able to consume the useful components of Yulpi.
Description
본 발명은 율피차의 제조방법에 관한 것으로, 보다 상세하게는 쓴맛을 저감시킬 수 있으며, 율피의 유용성분을 섭취할 수 있는, 율피차의 제조방법에 관한 것이다.The present invention relates to a method of producing Yulpi tea, and more specifically, to a method of producing Yulpi tea that can reduce the bitter taste and consume the useful components of Yulpi tea.
밤나무(Castanea crenata Sieb. et Zucc)는 너도밤나무과(Fagaceae)에 속하는 낙엽활엽교목 중 하나로서, 9~10월에 견과류의 과실이 열리며, 주로 중국 및 일본 한국과 같은 아시아 지역에 분포되어 해발 700m 아래의 비교적 따뜻하고 해가 잘 드는 산기슭에 식재하고 있는 식물이다.Chestnut tree (Castanea crenata Sieb. et Zucc) is one of the deciduous broad-leaved trees belonging to the beech family (Fagaceae). It bears nuts in September and October, and is mainly distributed in Asian regions such as China, Japan, and Korea, up to 700m above sea level. This plant is planted at the foot of a relatively warm and sunny mountain below.
이와 같은 밤나무의 경우 그 열매를 식용으로 사용하던 것이 일반적이었으며, 이러한 밤 열매는 주로 전분질로 구성된 알맹이와, 이러한 알맹이를 둘러싸고 있는 두층의 껍질인 외피 및 내피로 이루어져 있어, 식용으로 사용하기 위해서는 비교적 씁쓸한 맛을 내는 외피 및 내피는 제거한 후 순수한 과육만을 식품으로 활용해왔다.In the case of chestnut trees like this, it was common to use the fruit for edible purposes. These chestnut fruits are composed of a kernel mainly composed of starch, and a two-layer shell (outer skin) and inner skin surrounding the kernel, so it must be relatively bitter to be used for food. The outer skin and inner skin, which provide flavor, have been removed and only the pure flesh has been used as food.
또한, 이러한 밤나무는 예로부터 그 과실을 율(栗), 잎을 율엽(栗葉), 꽃을 율화(栗花), 종자를 율자(栗子), 과실의 속껍질을 율피(栗皮)라고 하여 다양한 약재로 사용되어 왔으며, 한방에서는 주름살, 하혈, 지혈, 건위, 보신작용 및 칠독의 해독제로서의 효능이 있는 것으로 알려져 왔다.In addition, this type of chestnut tree has been called various types since ancient times, with its fruit called yul, its leaves called yul-yeop, its flowers yulhwa, its seeds called yulja, and the inner skin of the fruit called yulpi. It has been used as a medicinal herb, and in oriental medicine, it has been known to be effective as an antidote to wrinkles, bleeding, hemostasis, health, health, body health, and seven poisons.
특히, 밤 열매의 내피인 율피의 경우 tyrosinase 활성억제, 노화자동산화 억제, 멜라닌 생성 억제 등과 같은 기능이 있음이 밝혀짐에 따라, 밤 열매를 식품으로 활용하던 과정에서 제거 후 폐기되어 왔던 율피를 수거하여 미용팩이나 미백화장품의 원료로 활용하고 있다.In particular, as it has been discovered that Yulpi, the inner skin of chestnut fruit, has functions such as inhibiting tyrosinase activity, inhibiting auto-oxidation of aging, and inhibiting melanin production, the Yulpi, which had been removed and discarded during the process of using chestnut fruit as food, is being collected. Therefore, it is used as a raw material for beauty packs and whitening cosmetics.
또한, 율피의 경우 당질, 아미노산, 각종 무기질뿐만 아니라 최근 생리 활성물질로 각광을 받고 있는 Polyphenol성 tannin과, free radical 소거작용이 강하여 페암 등의 발생을 현저히 감소시키는 물질로 규명된 catechin이 다량 함유되어 있으며, 특히 율피 내에 함유된 각종 항암 및 항산화 기능을 갖는 유효성분으로 인하여 지방질의 산화를 막고 혈관벽의 손상을 감소시키며 혈액순환을 원활하게 해줄 뿐만 아니라 피로회복에도 좋은 것으로 알려짐에 따라 이를 이용한 각종 식품도 개발되고 있다.In addition, Yulpi contains a large amount of not only carbohydrates, amino acids, and various minerals, but also polyphenol tannin, which has recently been in the spotlight as a biologically active substance, and catechin, which has been identified as a substance that has a strong free radical scavenging effect and significantly reduces the occurrence of lung cancer. In particular, it is known that the active ingredients contained in Yulpi, which have various anti-cancer and antioxidant functions, prevent oxidation of lipids, reduce damage to blood vessel walls, facilitate blood circulation, and are good for fatigue recovery, so various foods using it are also produced. It is being developed.
대한민국공개특허공보 제10-2009-0081987호(2009.07.29.)에는 율피 분말의 가공방법 및 그 가공된 분말을 이용한 율피차와 음료가 개시되어 있다.Korean Patent Publication No. 10-2009-0081987 (July 29, 2009) discloses a processing method for Yulpi powder and Yulpi tea and drinks using the processed powder.
상기 율피 분말을 이용한 율피차는 가공공정이 단순한 장점이 있지만, 율피의 쓴맛이 나는 단점이 있다.Yulpi tea using the Yulpi powder has the advantage of a simple processing process, but has the disadvantage of having a bitter taste of Yulpi.
본 발명의 목적은 쓴맛을 저감시킬 수 있는, 율피차의 제조방법을 제공하는 것이다. The purpose of the present invention is to provide a method for producing Yulpi tea, which can reduce bitterness.
본 발명의 다른 목적은 율피의 유용성분을 섭취할 수 있는, 율피차의 제조방법을 제공하는 것이다. Another object of the present invention is to provide a method for producing Yulpi tea, which can consume the useful components of Yulpi.
상기 목적을 달성하기 위하여 본 발명은 다음과 같은 수단을 제공한다.To achieve the above object, the present invention provides the following means.
본 발명은, 율피를 2,450MHz의 마이크로파로 10분 동안 조사하는 단계(단계 1); 상기 마이크로파 처리된 율피를 1.5%(w/v) 농도의 자염수에 20~30℃에서 5~10분 동안 1차 침지하는 단계(단계 2); 상기 1차 침지된 율피를 아로니아식초에 20~30℃에서 1~3분 동안 2차 침지하는 단계(단계 3); 상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하는 단계(단계 4); 상기 1차 건조한 율피를 60℃에서 2시간 동안 2차 건조하는 단계(단계 5); 및 상기 2차 건조된 율피를 분쇄하여 율피분말을 제조하는 단계(단계 6); 를 포함하는, 율피차의 제조방법을 제공한다.The present invention includes the steps of irradiating Yulpi with microwaves of 2,450 MHz for 10 minutes (step 1); Primary immersion of the microwave-treated Yulpi in 1.5% (w/v) concentration of saline water at 20-30°C for 5-10 minutes (step 2); Secondary immersion of the primarily immersed Yulpi in aronia vinegar at 20-30°C for 1-3 minutes (step 3); Primary drying the secondarily immersed yulpi at 80°C for 1 hour (step 4); Secondary drying the first dried yulpi at 60°C for 2 hours (step 5); And grinding the secondary dried yulpi to produce yulpi powder (step 6); It provides a manufacturing method of Yulpi tea, including.
상기 단계 3에서, 상기 아로니아식초의 제조방법은, 아로니아를 정제수에 20~30℃에서 1~2분 동안 침지하는 단계; 현미추출액 100중량부에 상기 침지한 아로니아 30~40중량부를 가하고 95~105℃에서 50~60분 동안 가열한 후에 여과하여 아로니아추출액을 수득하는 단계; 상기 아로니아추출액 100중량부에 액화효소 3~4중량부를 첨가하고 60℃에서 20~30분 동안 액화시키는 단계; 상기 액화된 아로니아추출액 100중량부에 당화효소 3~4중량부를 첨가하고 60℃에서 50~60분 동안 당화시키는 단계; 상기 당화된 아로니아추출액 100중량부에 효모 1~3중량부를 가하고 30~35℃에서 3~4일 동안 알코올 발효시켜 알코올발효액을 수득하는 단계; 상기 알코올발효액 100중량부에 초산균 1~5중량부를 가하고 30~35℃에서 10~13일 동안 초산 발효시켜 초산발효액을 제조하는 단계; 및 상기 초산발효액을 10~20℃에서 10~30일 동안 숙성시키는 단계; 를 포함하며, 상기 현미추출액은 정제수 100중량부에 현미 10~15중량부, 머위 1~5중량부, 우엉 1~5중량부 및 유근피 1~5중량부를 가하고 100~105℃에서 20~30분 동안 가열하여 제조한다.In step 3, the method for producing aronia vinegar includes immersing aronia in purified water at 20 to 30° C. for 1 to 2 minutes; Adding 30 to 40 parts by weight of the soaked aronia to 100 parts by weight of brown rice extract, heating at 95 to 105°C for 50 to 60 minutes, and then filtering to obtain an aronia extract; Adding 3 to 4 parts by weight of liquefaction enzyme to 100 parts by weight of the aronia extract and liquefying it at 60°C for 20 to 30 minutes; Adding 3 to 4 parts by weight of saccharification enzyme to 100 parts by weight of the liquefied aronia extract and saccharifying it at 60°C for 50 to 60 minutes; Adding 1 to 3 parts by weight of yeast to 100 parts by weight of the saccharified aronia extract and performing alcohol fermentation at 30 to 35° C. for 3 to 4 days to obtain an alcoholic fermentation broth; Preparing an acetic acid fermentation liquid by adding 1 to 5 parts by weight of acetic acid bacteria to 100 parts by weight of the alcoholic fermentation liquid and fermenting the acetic acid at 30 to 35° C. for 10 to 13 days; And maturing the acetic acid fermentation liquid at 10 to 20°C for 10 to 30 days; It includes, and the brown rice extract is prepared by adding 10 to 15 parts by weight of brown rice, 1 to 5 parts by butterbur, 1 to 5 parts by weight of burdock root, and 1 to 5 parts by weight of radish root bark to 100 parts by weight of purified water and steeping at 100 to 105°C for 20 to 30 minutes. It is prepared by heating for a while.
상기 단계 5 이후에 상기 2차 건조한 율피를 4~5㎏/㎠, 100~110℃에서 5~6분 동안 퍼핑하는 단계를 추가한다. After step 5, the step of puffing the secondary dried yulpi at 4 to 5 kg/cm2 and 100 to 110°C for 5 to 6 minutes is added.
상기 단계 6 이후에 상기 율피분말 100중량부에 기호성 향상제 1~5중량부를 포함하는 단계를 추가하되, 상기 기호성 향상제는 감추출분말 50~60중량%, 배추출분말 20~30중량%, 고구마순발효분말 10~20중량% 및 스테비아발효분말 1~3중량%를 포함하며, 상기 감추출분말은 감 100중량부에 정제수 500~600중량부, 탈지분유 1~5중량부, 구연산 1~3중량부 및 이소말토올리고당 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열하고 여과한 감추출액을 동결건조한 후 분말화하여 수득하며, 상기 배추출분말은 배 100중량부에 정제수 500~600중량부, 루틴 1~5중량부 및 셀룰라아제 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열한 후 여과한 배추출액을 동결건조한 후 분말화하여 수득하며, 상기 고구마순발효분말의 제조방법은, 고구마순을 100~110℃에서 1~2시간 동안 증숙하는 단계; 상기 증숙된 고구마순을 10~15℃에서 1~2일 동안 숙성하는 단계; 상기 숙성된 고구마순 100중량부에 알룰로스 1~5중량부 및 진피추출액 40~50중량부를 가하고 1.2~1.6기압, 80~90℃에서 3~4시간 동안 추출하여 고구마순추출액을 수득하는 단계; 상기 고구마순추출액 100중량부에 복분자종균 1~5중량부, 프락토올리고당 1~5중량부 및 자일로스 1~5중량부를 가하고 20~24℃에서 12~14시간 동안 발효시킨 후 여과하여 고구마순발효액을 제조하는 단계; 및 상기 고구마순발효액을 동결건조한 후 분말화하는 단계; 를 포함하며, 상기 진피추출액은 진피 100중량부에 95%(v/v) 에탄올 500~600중량부를 가하고 25~27℃에서 24시간 동안 방치한 후 여과하여 제조하며, 상기 복분자종균의 제조방법은, 복분자 100g에 100㎖의 멸균수를 가하고 마쇄기로 분쇄한 다음 착즙한 후 여과하여 복분자 추출액을 제조하는 단계; 옥수수가루 및 갈락토오스를 중량비 1:1로 배합하여 배지를 제조하는 단계; 및 상기 배지 100중량부에 상기 복분자 추출액 50중량부를 가하고 20~22℃에서 20~22일 동안 발효시키는 단계; 를 포함하며, 상기 스테비아발효분말은 스테비아잎 100중량부에 정제수 500~550중량부를 가하고 95~105℃에서 30~40분 동안 가열한 후 여과한 스테비아잎추출액 100중량부에 블루베리발효액 5~10중량부를 가하고 20~24℃에서 24~26시간 동안 발효시킨 후 여과한 스테비아발효액을 동결건조한 후 분말화하여 제조하며, 상기 블루베리발효액은 블루베리착즙액 100중량부에 효모 1~5중량부를 가하고 20~24℃에서 48~50시간 동안 발효시켜 제조한다.After step 6, a step of including 1 to 5 parts by weight of a palatability improver per 100 parts by weight of the yulpi powder is added, wherein the palatability improver is 50 to 60% by weight of persimmon extract powder, 20 to 30% by weight of pear extract powder, and sweet potato sprouts. It contains 10-20% by weight of fermented powder and 1-3% by weight of fermented stevia powder, and the persimmon extract powder contains 500-600 parts by weight of purified water, 1-5 parts by weight of skim milk powder, and 1-3 parts by weight of citric acid per 100 parts by weight of persimmon. 1 to 3 parts by weight and isomaltooligosaccharide are added, heated at 90 to 95°C for 40 to 50 minutes, and the filtered persimmon extract is freeze-dried and powdered to obtain the pear extract powder. 600 parts by weight, 1 to 5 parts by weight of rutin, and 1 to 3 parts by weight of cellulase are added, heated at 90 to 95°C for 40 to 50 minutes, and the filtered pear extract is freeze-dried and powdered to obtain the sweet potato sprout powder. The manufacturing method includes steaming sweet potato shoots at 100-110°C for 1-2 hours; Aging the steamed sweet potato shoots at 10 to 15°C for 1 to 2 days; Adding 1 to 5 parts by weight of allulose and 40 to 50 parts by weight of dermis extract to 100 parts by weight of the aged sweet potato shoots and extracting at 1.2 to 1.6 atmospheres and 80 to 90°C for 3 to 4 hours to obtain a sweet potato shoot extract; To 100 parts by weight of the sweet potato shoot extract, 1 to 5 parts by weight of Bokbunja sprouts, 1 to 5 parts by weight of fructo-oligosaccharides and 1 to 5 parts by weight of xylose were added, fermented at 20 to 24°C for 12 to 14 hours, and then filtered to produce sweet potato shoots. Preparing a fermentation broth; And freeze-drying the fermented sweet potato shoot and then powdering it; It includes, and the dermal extract is prepared by adding 500 to 600 parts by weight of 95% (v/v) ethanol to 100 parts by weight of dermis, leaving it at 25 to 27°C for 24 hours, and then filtering. The method for producing the bokbunja spawn is , adding 100 ml of sterilized water to 100 g of bokbunja, crushing it with a grinder, squeezing juice, and filtering to prepare a bokbunja extract; Preparing a medium by mixing corn flour and galactose in a weight ratio of 1:1; And adding 50 parts by weight of the bokbunja extract to 100 parts by weight of the medium and fermenting at 20 to 22 ° C. for 20 to 22 days; The stevia fermented powder includes adding 500 to 550 parts by weight of purified water to 100 parts by weight of stevia leaves, heating at 95 to 105°C for 30 to 40 minutes, and adding 5 to 10 parts by weight of blueberry fermentation liquid to 100 parts by weight of filtered stevia leaf extract. It is manufactured by adding 1 part by weight and fermenting at 20-24°C for 24-26 hours, then filtering the stevia fermentation liquid, freeze-drying it, and powdering it. The blueberry fermentation liquid is prepared by adding 1-5 parts by weight of yeast to 100 parts by weight of blueberry juice. It is manufactured by fermenting at 20~24℃ for 48~50 hours.
본 발명에 따른 율피차의 제조방법은 쓴맛을 저감시킬 수 있는 장점이 있다The method for producing Yulpi tea according to the present invention has the advantage of reducing bitterness.
또한, 본 발명에 따른 율피차의 제조방법은 율피의 유용성분을 섭취할 수 있는 장점이 있다. In addition, the method for producing Yulpi tea according to the present invention has the advantage of being able to consume the useful components of Yulpi.
이하, 본 발명을 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail as follows.
먼저, 본 발명에 따른 율피차의 제조방법을 설명한다.First, the manufacturing method of Yulpi tea according to the present invention will be described.
본 발명의 율피차의 제조방법은,The method for producing Yulpi tea of the present invention is,
율피를 2,450MHz의 마이크로파로 10분 동안 조사하는 단계(단계 1);Irradiating Yulpi with microwaves at 2,450 MHz for 10 minutes (step 1);
상기 마이크로파 처리된 율피를 1.5%(w/v) 농도의 자염수에 20~30℃에서 5~10분 동안 1차 침지하는 단계(단계 2);Primary immersion of the microwave-treated Yulpi in 1.5% (w/v) concentration of saline water at 20-30°C for 5-10 minutes (step 2);
상기 1차 침지된 율피를 아로니아식초에 20~30℃에서 1~3분 동안 2차 침지하는 단계(단계 3);Secondary immersion of the primarily immersed Yulpi in aronia vinegar at 20-30°C for 1-3 minutes (step 3);
상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하는 단계(단계 4);Primary drying the secondarily immersed yulpi at 80°C for 1 hour (step 4);
상기 1차 건조한 율피를 60℃에서 2시간 동안 2차 건조하는 단계(단계 5); 및Secondary drying the first dried yulpi at 60°C for 2 hours (step 5); and
상기 2차 건조된 율피를 분쇄하여 율피분말을 제조하는 단계(단계 6);Grinding the secondary dried yulpi to produce yulpi powder (step 6);
를 포함한다.Includes.
본 발명은 율피를 마이크로파 처리한 후에 자염수 및 아로니아식초에 침지함으로써 율피의 쓴맛을 제거하는 장점이 있다.The present invention has the advantage of removing the bitter taste of yulpi by treating it with microwaves and then immersing it in saline water and aronia vinegar.
상기 단계 3에서, 상기 아로니아식초의 제조방법은,In step 3, the method for producing aronia vinegar is,
아로니아를 정제수에 20~30℃에서 1~2분 동안 침지하는 단계;Immersing aronia in purified water at 20-30°C for 1-2 minutes;
현미추출액 100중량부에 상기 침지한 아로니아 30~40중량부를 가하고 95~105℃에서 50~60분 동안 가열한 후에 여과하여 아로니아추출액을 수득하는 단계;Adding 30 to 40 parts by weight of the soaked aronia to 100 parts by weight of brown rice extract, heating at 95 to 105°C for 50 to 60 minutes, and then filtering to obtain an aronia extract;
상기 아로니아추출액 100중량부에 액화효소 3~4중량부를 첨가하고 60℃에서 20~30분 동안 액화시키는 단계;Adding 3 to 4 parts by weight of liquefaction enzyme to 100 parts by weight of the aronia extract and liquefying it at 60°C for 20 to 30 minutes;
상기 액화된 아로니아추출액 100중량부에 당화효소 3~4중량부를 첨가하고 60℃에서 50~60분 동안 당화시키는 단계;Adding 3 to 4 parts by weight of saccharification enzyme to 100 parts by weight of the liquefied aronia extract and saccharifying it at 60°C for 50 to 60 minutes;
상기 당화된 아로니아추출액 100중량부에 효모 1~3중량부를 가하고 30~35℃에서 3~4일 동안 알코올 발효시켜 알코올발효액을 수득하는 단계;Adding 1 to 3 parts by weight of yeast to 100 parts by weight of the saccharified aronia extract and performing alcohol fermentation at 30 to 35° C. for 3 to 4 days to obtain an alcoholic fermentation broth;
상기 알코올발효액 100중량부에 초산균 1~5중량부를 가하고 30~35℃에서 10~13일 동안 초산 발효시켜 초산발효액을 제조하는 단계; 및Preparing an acetic acid fermentation liquid by adding 1 to 5 parts by weight of acetic acid bacteria to 100 parts by weight of the alcoholic fermentation liquid and fermenting the acetic acid at 30 to 35° C. for 10 to 13 days; and
상기 초산발효액을 10~20℃에서 10~30일 동안 숙성시키는 단계;Aging the acetic acid fermentation liquid at 10 to 20°C for 10 to 30 days;
를 포함한다.Includes.
상기 현미추출액은 정제수 100중량부에 현미 10~15중량부, 머위 1~5중량부, 우엉 1~5중량부 및 유근피 1~5중량부를 가하고 100~105℃에서 20~30분 동안 가열하여 제조한다.The brown rice extract is prepared by adding 10 to 15 parts by weight of brown rice, 1 to 5 parts by butterbur, 1 to 5 parts by weight of burdock root, and 1 to 5 parts by weight of radish root bark to 100 parts by weight of purified water and heating at 100 to 105°C for 20 to 30 minutes. do.
본 발명은 상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하고, 60℃에서 2시간 동안 2차 건조함으로써, 율피의 유용성분의 파괴를 최소화할 수 있는 장점이 있다.The present invention has the advantage of minimizing the destruction of useful components of the yulpi by first drying the secondarily immersed yulpi at 80°C for 1 hour and secondly drying it at 60°C for 2 hours.
본 발명은 상기 단계 5 이후에 상기 2차 건조한 율피를 4~5㎏/㎠, 100~110℃에서 5~6분 동안 퍼핑하는 단계를 추가할 수 있다. The present invention may add the step of puffing the secondary dried yulpi at 4 to 5 kg/cm2 and 100 to 110°C for 5 to 6 minutes after step 5.
상기 2차 건조한 율피를 퍼핑함으로써 율피의 떫은 맛을 더욱 감소시킬 수 있는 장점이 있다.There is an advantage in that the astringent taste of the yulpi can be further reduced by puffing the secondary dried yulpi.
본 발명은 상기 단계 6 이후에 상기 율피분말 100중량부에 기호성 향상제 1~5중량부를 포함하는 단계를 추가할 수 있다.The present invention may add a step of including 1 to 5 parts by weight of a palatability improver per 100 parts by weight of the Yulpi powder after step 6.
상기 기호성 향상제는 감추출분말 50~60중량%, 배추출분말 20~30중량%, 고구마순발효분말 10~20중량% 및 스테비아발효분말 1~3중량%를 포함한다.The palatability improver includes 50-60% by weight of persimmon extract powder, 20-30% by weight of pear extract powder, 10-20% by weight of fermented sweet potato shoot powder, and 1-3% by weight of fermented stevia powder.
상기 감추출분말은 감 100중량부에 정제수 500~600중량부, 탈지분유 1~5중량부, 구연산 1~3중량부 및 이소말토올리고당 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열하고 여과한 감추출액을 동결건조한 후 분말화하여 수득한다. The persimmon extract powder is prepared by adding 500 to 600 parts by weight of purified water, 1 to 5 parts by weight of skim milk powder, 1 to 3 parts by weight of citric acid, and 1 to 3 parts by weight of isomaltooligosaccharide to 100 parts by weight of persimmon, and incubating at 90 to 95°C for 40 to 50 minutes. It is obtained by freeze-drying the persimmon extract that has been heated and filtered for a while, and then powdering it.
상기 배추출분말은 배 100중량부에 정제수 500~600중량부, 루틴 1~5중량부 및 셀룰라아제 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열한 후 여과한 배추출액을 동결건조한 후 분말화하여 수득한다. The pear extract powder is made by adding 500 to 600 parts by weight of purified water, 1 to 5 parts by weight of rutin, and 1 to 3 parts by weight of cellulase to 100 parts by weight of pears, heating at 90 to 95°C for 40 to 50 minutes, and then freezing the filtered pear extract. Obtained by drying and powdering.
상기 고구마순발효분말의 제조방법은,The method for producing the fermented sweet potato shoot powder is,
고구마순을 100~110℃에서 1~2시간 동안 증숙하는 단계;Steaming sweet potato shoots at 100-110°C for 1-2 hours;
상기 증숙된 고구마순을 10~15℃에서 1~2일 동안 숙성하는 단계;Aging the steamed sweet potato shoots at 10 to 15°C for 1 to 2 days;
상기 숙성된 고구마순 100중량부에 알룰로스 1~5중량부 및 진피추출액 40~50중량부를 가하고 1.2~1.6기압, 80~90℃에서 3~4시간 동안 추출하여 고구마순추출액을 수득하는 단계; Adding 1 to 5 parts by weight of allulose and 40 to 50 parts by weight of dermis extract to 100 parts by weight of the aged sweet potato shoots and extracting at 1.2 to 1.6 atmospheres and 80 to 90°C for 3 to 4 hours to obtain a sweet potato shoot extract;
상기 고구마순추출액 100중량부에 복분자종균 1~5중량부, 프락토올리고당 1~5중량부 및 자일로스 1~5중량부를 가하고 20~24℃에서 12~14시간 동안 발효시킨 후 여과하여 고구마순발효액을 제조하는 단계; 및To 100 parts by weight of the sweet potato shoot extract, 1 to 5 parts by weight of Bokbunja sprouts, 1 to 5 parts by weight of fructo-oligosaccharides and 1 to 5 parts by weight of xylose were added, fermented at 20 to 24°C for 12 to 14 hours, and then filtered to produce sweet potato shoots. Preparing a fermentation broth; and
상기 고구마순발효액을 동결건조한 후 분말화하는 단계;Freeze-drying the fermented sweet potato shoot and then powdering it;
를 포함한다.Includes.
상기 진피추출액은 진피 100중량부에 95%(v/v) 에탄올 500~600중량부를 가하고 25~27℃에서 24시간 동안 방치한 후 여과하여 제조한다.The dermal extract is prepared by adding 500 to 600 parts by weight of 95% (v/v) ethanol to 100 parts by weight of dermis, leaving it at 25 to 27°C for 24 hours, and then filtering.
상기 복분자종균의 제조방법은,The manufacturing method of the bokbunja spawn is,
복분자 100g에 100㎖의 멸균수를 가하고 마쇄기로 분쇄한 다음 착즙한 후 여과하여 복분자 추출액을 제조하는 단계;Preparing a bokbunja extract by adding 100 ml of sterilized water to 100 g of bokbunja, grinding it with a grinder, squeezing juice, and then filtering;
옥수수가루 및 갈락토오스를 중량비 1:1로 배합하여 배지를 제조하는 단계; 및 Preparing a medium by mixing corn flour and galactose in a weight ratio of 1:1; and
상기 배지 100중량부에 상기 복분자 추출액 50중량부를 가하고 20~22℃에서 20~22일 동안 발효시키는 단계;Adding 50 parts by weight of the bokbunja extract to 100 parts by weight of the medium and fermenting at 20 to 22°C for 20 to 22 days;
를 포함한다.Includes.
상기 스테비아발효분말은 스테비아잎 100중량부에 정제수 500~550중량부를 가하고 95~105℃에서 30~40분 동안 가열한 후 여과한 스테비아잎추출액 100중량부에 블루베리발효액 5~10중량부를 가하고 20~24℃에서 24~26시간 동안 발효시킨 후 여과한 스테비아발효액을 동결건조한 후 분말화하여 제조한다.The stevia fermentation powder is prepared by adding 500 to 550 parts by weight of purified water to 100 parts by weight of stevia leaves, heating at 95 to 105°C for 30 to 40 minutes, and adding 5 to 10 parts by weight of blueberry fermentation liquid to 100 parts by weight of filtered stevia leaf extract. It is manufactured by fermenting at ~24°C for 24-26 hours, then filtering the stevia fermentation liquid, freeze-drying it, and powdering it.
상기 블루베리발효액은 블루베리착즙액 100중량부에 효모 1~5중량부를 가하고 20~24℃에서 48~50시간 동안 발효시킨 것을 사용한다.The blueberry fermentation liquid is prepared by adding 1 to 5 parts by weight of yeast to 100 parts by weight of blueberry juice and fermenting it at 20 to 24°C for 48 to 50 hours.
본 발명에 따른 율피차의 제조방법은 쓴맛을 저감시킬 수 있는 장점이 있다The method for producing Yulpi tea according to the present invention has the advantage of reducing bitterness.
또한, 본 발명에 따른 율피차의 제조방법은 율피의 유용성분을 섭취할 수 있는 장점이 있다. In addition, the method for producing Yulpi tea according to the present invention has the advantage of being able to consume the useful components of Yulpi.
이하, 실시 예를 통하여 본 발명의 구성 및 효과를 더욱 상세히 설명하고자 한다. 이들 실시 예는 오로지 본 발명을 예시하기 위한 것일 뿐 본 발명의 범위가 이들 실시 예에 의해 제한되는 것은 아니다. Hereinafter, the configuration and effects of the present invention will be described in more detail through examples. These examples are only for illustrating the present invention and the scope of the present invention is not limited by these examples.
율피를 2,450MHz의 마이크로파로 10분 동안 조사하였다. 상기 마이크로파 처리된 율피를 1.5%(w/v) 농도의 자염수에 25℃에서 5분 동안 1차 침지하였다. 상기 1차 침지된 율피를 아로니아식초에 25℃에서 2분 동안 2차 침지하였다. 상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하였다. 상기 1차 건조한 율피를 60℃에서 2시간 동안 2차 건조하였다. 상기 2차 건조된 율피를 분쇄기에서 입경이 2㎜가 되도록 분쇄하여 율피분말을 제조하였다. Yulpi was irradiated with microwaves at 2,450 MHz for 10 minutes. The microwave-treated yulpi was first immersed in saline water with a concentration of 1.5% (w/v) at 25°C for 5 minutes. The firstly immersed yulpi was secondarily immersed in aronia vinegar at 25°C for 2 minutes. The secondarily immersed yulpi was first dried at 80°C for 1 hour. The first dried Yulpi was secondarily dried at 60°C for 2 hours. The secondarily dried yulpi was pulverized in a grinder to have a particle size of 2 mm to prepare yulpi powder.
상기 아로니아식초는, 아로니아를 정제수에 25℃에서 1분 동안 침지하고, 현미추출액 100중량부에 상기 침지한 아로니아 30중량부를 가하고 105℃에서 60분 동안 가열한 후에 여과하여 아로니아추출액을 수득하고, 상기 아로니아추출액 100중량부에 액화효소 4중량부를 첨가하고 60℃에서 30분 동안 액화시키고, 상기 액화된 아로니아추출액 100중량부에 당화효소 4중량부를 첨가하고 60℃에서 60분 동안 당화시키고, 상기 당화된 아로니아추출액 100중량부에 효모 3중량부를 가하고 30℃에서 4일 동안 알코올 발효시켜 알코올발효액을 수득하고, 상기 알코올발효액 100중량부에 초산균 5중량부를 가하고 30℃에서 13일 동안 초산 발효시켜 초산발효액을 제조하고, 상기 초산발효액을 20℃에서 10일 동안 숙성시켜 제조하였다. 상기 현미추출액은 정제수 100중량부에 현미 15중량부, 머위 5중량부, 우엉 5중량부 및 유근피 5중량부를 가하고 105℃에서 20분 동안 가열하여 제조하였다.The aronia vinegar is made by immersing aronia in purified water at 25°C for 1 minute, adding 30 parts by weight of the soaked aronia to 100 parts by weight of brown rice extract, heating at 105°C for 60 minutes, and filtering to obtain an aronia extract. Obtained, 4 parts by weight of liquefaction enzyme was added to 100 parts by weight of the aronia extract and liquefied at 60°C for 30 minutes, and 4 parts by weight of saccharification enzyme was added to 100 parts by weight of the liquefied aronia extract and liquefied at 60°C for 60 minutes. After saccharification, 3 parts by weight of yeast were added to 100 parts by weight of the saccharified aronia extract and alcohol fermented at 30°C for 4 days to obtain an alcoholic fermentation liquid. 5 parts by weight of acetic acid bacteria were added to 100 parts by weight of the alcoholic fermentation liquid and fermented at 30°C for 13 days. An acetic acid fermentation liquid was prepared by fermenting acetic acid for 10 days, and the acetic acid fermentation liquid was aged at 20°C for 10 days. The brown rice extract was prepared by adding 15 parts by weight of brown rice, 5 parts by weight of butterbur, 5 parts by weight of burdock root, and 5 parts by weight of root bark to 100 parts by weight of purified water and heating at 105°C for 20 minutes.
실시예 1에서, 상기 2차 건조한 율피를 4㎏/㎠, 100℃에서 6분 동안 퍼핑한 것을 제외하고 나머지는 동일하게 하여 율피분말을 제조하였다.In Example 1, yulpi powder was prepared in the same manner except that the second dried yulpi was puffed at 4 kg/cm2 and 100°C for 6 minutes.
실시예 1에서 제조한 율피분말 100중량부에 기호성 향상제 3중량부를 혼합하였다. 상기 기호성 향상제는 감추출분말 60중량%, 배추출분말 25중량%, 고구마순발효분말 12중량% 및 스테비아발효분말 3중량%를 혼합하여 제조하였다.3 parts by weight of a palatability improver was mixed with 100 parts by weight of the Yulpi powder prepared in Example 1. The palatability improver was prepared by mixing 60% by weight of persimmon extract powder, 25% by weight of pear extract powder, 12% by weight of fermented sweet potato shoot powder, and 3% by weight of fermented stevia powder.
상기 감추출분말은 감 100중량부에 정제수 600중량부, 탈지분유 5중량부, 구연산 3중량부 및 이소말토올리고당 3중량부를 가하고 95℃에서 50분 동안 가열하고 여과한 감추출액을 동결건조한 후 분말화하여 수득하였다.The persimmon extract powder is prepared by adding 600 parts by weight of purified water, 5 parts by weight of skim milk powder, 3 parts by weight of citric acid, and 3 parts by weight of isomaltooligosaccharide to 100 parts by weight of persimmon, heating at 95°C for 50 minutes, and freeze-drying the filtered persimmon extract to form a powder. It was obtained by mixing.
상기 배추출분말은 배 100중량부에 정제수 600중량부, 루틴 5중량부 및 셀룰라아제 3중량부를 가하고 95℃에서 50분 동안 가열한 후 여과한 배추출액을 동결건조한 후 분말화하여 수득하였다. The pear extract powder was obtained by adding 600 parts by weight of purified water, 5 parts by weight of rutin, and 3 parts by weight of cellulase to 100 parts by weight of pears, heating at 95°C for 50 minutes, lyophilizing the filtered pear extract, and then powdering it.
상기 고구마순발효분말은, 고구마순을 100℃에서 1시간 동안 증숙하고, 상기 증숙된 고구마순을 15℃에서 2일 동안 숙성하고, 상기 숙성된 고구마순 100중량부에 알룰로스 5중량부 및 진피추출액 50중량부를 가하고 1.2기압, 90℃에서 3시간 동안 추출하여 고구마순추출액을 수득하고, 상기 고구마순추출액 100중량부에 복분자종균 5중량부, 프락토올리고당 5중량부 및 자일로스 5중량부를 가하고 24℃에서 12시간 동안 발효시킨 후 여과하여 고구마순발효액을 제조하고, 상기 고구마순발효액을 동결건조한 후 분말화하여 제조하였다. The sweet potato shoot fermented powder is made by steaming sweet potato shoots at 100°C for 1 hour, maturing the steamed sweet potato shoots at 15°C for 2 days, and adding 5 parts by weight of allulose and dermis to 100 parts by weight of the aged sweet potato shoots. 50 parts by weight of the extract was added and extracted at 1.2 atm and 90°C for 3 hours to obtain a sweet potato shoot extract. To 100 parts by weight of the sweet potato shoot extract, 5 parts by weight of Bokbunja spores, 5 parts by weight of fructo-oligosaccharides and 5 parts by weight of xylose were added. Fermentation was performed at 24°C for 12 hours and then filtered to prepare a sweet potato shoot fermentation liquid. The sweet potato shoot fermentation liquid was freeze-dried and then powdered.
상기 진피추출액은 진피 100중량부에 95%(v/v) 에탄올 600중량부를 가하고 25℃에서 24시간 동안 방치한 후 여과하여 제조하였다.The dermal extract was prepared by adding 600 parts by weight of 95% (v/v) ethanol to 100 parts by weight of dermis, leaving it at 25°C for 24 hours, and then filtering.
상기 복분자종균은, 복분자 100g에 100㎖의 멸균수를 가하고 마쇄기로 분쇄한 다음 착즙한 후 여과하여 복분자 추출액을 제조하고, 옥수수가루 및 갈락토오스를 중량비 1:1로 배합하여 배지를 제조하고, 상기 배지 100중량부에 상기 복분자 추출액 50중량부를 가하고 22℃에서 20일 동안 발효시켜 제조하였다. The Bokbunja spawn was prepared by adding 100 ml of sterilized water to 100 g of Bokbunja, pulverizing it with a grinder, extracting juice, and then filtering to prepare Bokbunja extract, and mixing corn flour and galactose in a weight ratio of 1:1 to prepare a medium, and the medium It was prepared by adding 50 parts by weight of the bokbunja extract to 100 parts by weight and fermenting at 22°C for 20 days.
상기 스테비아발효분말은 스테비아잎 100중량부에 정제수 500중량부를 가하고 105℃에서 40분 동안 가열한 후 여과한 스테비아잎추출액 100중량부에 블루베리발효액 10중량부를 가하고 24℃에서 24시간 동안 발효시킨 후 여과한 스테비아발효액을 동결건조한 후 분말화하여 제조하였다.The stevia fermentation powder is prepared by adding 500 parts by weight of purified water to 100 parts by weight of stevia leaves, heating at 105°C for 40 minutes, adding 10 parts by weight of blueberry fermentation liquid to 100 parts by weight of filtered stevia leaf extract, and fermenting at 24°C for 24 hours. It was manufactured by freeze-drying the filtered stevia fermentation liquid and powdering it.
상기 블루베리발효액은 블루베리착즙액 100중량부에 효모 5중량부를 가하고 20℃에서 50시간 동안 발효시켜 제조하였다.The blueberry fermentation liquid was prepared by adding 5 parts by weight of yeast to 100 parts by weight of blueberry juice and fermenting at 20°C for 50 hours.
[비교예 1][Comparative Example 1]
밤 열매로부터 분리된 율피를 깨끗한 물에 세척하고 건조기에서 50℃의 온도 하에 3시간 건조한 후, 바로 냉각기에 투입하여 -10℃에서 3시간 동안 동결건조한 다음, 상기 동결건조된 율피를 분쇄기에서 입경이 2~3㎜이 되도록 분쇄하고, 상기 율피 분쇄물을 볶음솥에서 150℃의 온도로 45분 가량 열처리하여 율피 분말을 제조하였다.The yulpi separated from the chestnut fruit is washed in clean water, dried in a dryer at a temperature of 50°C for 3 hours, immediately put into a cooler and freeze-dried at -10°C for 3 hours, and then the freeze-dried yulpi is crushed in a grinder to reduce particle size. It was pulverized to 2-3 mm, and the pulverized Yulpi powder was heat-treated in a stir-fry pot at a temperature of 150°C for about 45 minutes to prepare Yulpi powder.
[실험예 1][Experimental Example 1]
상기 실시예 1 내지 3 및 비교예 1에서 제조한 율피분말을 80℃의 온수 100㎖에 2g씩 3분간 우려낸 후 남녀성인 20명에게 시음을 시킨 다음, 색, 향, 맛 및 전반적 기호도에 대한 9점 척도법으로 관능검사를 실시하여 평균값을 표 1에 나타냈다.The Yulpi powder prepared in Examples 1 to 3 and Comparative Example 1 was steeped in 100 ml of hot water at 80°C for 3 minutes each, and then tasted by 20 male and female adults, and then tested for color, aroma, taste and overall preference. A sensory test was conducted using the point scale method, and the average values are shown in Table 1.
향: 율피가 용출된 차의 향이 구수하고 고소한 향이 진할수록 강도가 큰 것으로 하고, 탄내가 나거나 풋냄새가 날수록 강도가 작은 것으로 하였다.
맛: 율피가 용출된 차의 맛이 구수하고 고소한 맛이 진할수록 강도가 큰 것으로 하고, 탄맛이나 떫은 맛이 진할수록 강도가 작은 것으로 하였다.Color: The turbidity of the tea from which Yulpi was eluted was observed, and if it was clear without fine particles, the intensity was considered high. If there was a lot of powder and the turbidity was high, the intensity was considered low.
Fragrance: The stronger and more savory the aroma of the tea from which Yulpi extract is, the greater the intensity. The stronger the burnt or green smell, the lower the intensity.
Taste: The more savory and savory the taste of the tea from which Yulpi was extracted, the greater the intensity, and the stronger the burnt or astringent taste, the lower the intensity.
표 1에서 나타난 바와 같이, 실시예 1 내지 3의 율피차는 비교예 1의 율피차에 비하여 떫은 맛 제거 효과가 우수한 것을 알 수 있다.As shown in Table 1, it can be seen that the Yulpi tea of Examples 1 to 3 has an excellent astringent taste removal effect compared to the Yulpi tea of Comparative Example 1.
[실험예 2][Experimental Example 2]
상기 실시예 1 내지 3 및 비교예 1에서 제조한 율피분말 0.1g을 채취하여 80℃의 온수 100㎖에 넣고 30분간 교반 침출 후 여과한 다음, 상기 여과액을 시료로 하여 하기와 같은 방법으로 총 페놀 화합물 및 플라보노이드 화합물의 함량을 측정하여 하기 표 2에 나타내었다.0.1 g of Yulpi powder prepared in Examples 1 to 3 and Comparative Example 1 was collected, placed in 100 ml of hot water at 80°C, stirred and leached for 30 minutes, and then filtered. The filtrate was used as a sample and the total was obtained in the following manner. The contents of phenol compounds and flavonoid compounds were measured and shown in Table 2 below.
- 총 페놀화합물 분석-- Analysis of total phenolic compounds -
율피의 열수 추출액 0.1㎖에 증류수 3㎖, 0.016M 포타슘 페리시아나이드(K3Fe(CN)6) 1㎖, 0.01M 삼염화철(FeCl3/0.1N HCl)용액 1㎖를 넣고 혼합한 후 15분간 방치하고, 안정제(H2O : 1% gum arabic : 85% phosphoric acid = 3 : 1 : 1, v/v/v) 5㎖ 첨가한 후 700㎚에서 흡광도를 측정하였으며, 몰식자산(gallic acid)으로 작성한 검량곡선으로 함량을 환산하였다.Add 3 mL of distilled water, 1 mL of 0.016M potassium ferricyanide (K 3 Fe(CN) 6 ), and 1 mL of 0.01M iron trichloride (FeCl 3 /0.1N HCl) solution to 0.1 mL of Yulpi's hot water extract and mix for 15 minutes. After leaving for a minute, 5 ml of stabilizer (H 2 O: 1% gum arabic: 85% phosphoric acid = 3: 1: 1, v/v/v) was added, and the absorbance was measured at 700 nm. Gallic acid The content was converted using a calibration curve prepared by .
-총 플라보노이드 화합물 분석--Total flavonoid compound analysis-
율피의 열수 추출액 1㎖에 diethylene glycol 10㎖, 1N NaOH 1㎖를 넣고 진탕한 후 37℃에서 1시간 방치하여 420㎚에서 흡광도를 측정하였으며, naringin으로 작성한 검량곡선에 준하여 함량을 환산하였다.10 ml of diethylene glycol and 1 ml of 1N NaOH were added to 1 ml of the hot water extract of Yulpi, shaken, left at 37°C for 1 hour, and the absorbance was measured at 420 nm. The content was converted according to the calibration curve prepared with naringin.
(㎎/100g)phenolic compounds
(mg/100g)
(㎎/100g)flavonoid compounds
(mg/100g)
표 2에 나타난 바와 같이, 실시예 1 내지 3의 율피분말은 비교예 1의 율피분말에 비하여 총 페놀 및 플라보노이드 화합물이 더 많이 함유되어 있는 것을 알 수 있다.As shown in Table 2, it can be seen that the Yulpi powder of Examples 1 to 3 contains more total phenol and flavonoid compounds than the Yulpi powder of Comparative Example 1.
Claims (4)
상기 마이크로파 처리된 율피를 1.5%(w/v) 농도의 자염수에 20~30℃에서 5~10분 동안 1차 침지하는 단계(단계 2);
상기 1차 침지된 율피를 아로니아식초에 20~30℃에서 1~3분 동안 2차 침지하는 단계(단계 3);
상기 2차 침지된 율피를 80℃에서 1시간 동안 1차 건조하는 단계(단계 4);
상기 1차 건조한 율피를 60℃에서 2시간 동안 2차 건조하는 단계(단계 5); 및
상기 2차 건조된 율피를 분쇄하여 율피분말을 제조하는 단계(단계 6);
를 포함하는,
율피차의 제조방법.
Irradiating Yulpi with microwaves at 2,450 MHz for 10 minutes (step 1);
Primary immersion of the microwave-treated Yulpi in 1.5% (w/v) concentration of saline water at 20-30°C for 5-10 minutes (step 2);
Secondary immersion of the primarily immersed Yulpi in aronia vinegar at 20-30°C for 1-3 minutes (step 3);
Primary drying the secondarily immersed yulpi at 80°C for 1 hour (step 4);
Secondary drying the first dried yulpi at 60°C for 2 hours (step 5); and
Grinding the secondary dried yulpi to produce yulpi powder (step 6);
Including,
How to make Yulpi tea.
상기 아로니아식초의 제조방법은,
아로니아를 정제수에 20~30℃에서 1~2분 동안 침지하는 단계;
현미추출액 100중량부에 상기 침지한 아로니아 30~40중량부를 가하고 95~105℃에서 50~60분 동안 가열한 후에 여과하여 아로니아추출액을 수득하는 단계;
상기 아로니아추출액 100중량부에 액화효소 3~4중량부를 첨가하고 60℃에서 20~30분 동안 액화시키는 단계;
상기 액화된 아로니아추출액 100중량부에 당화효소 3~4중량부를 첨가하고 60℃에서 50~60분 동안 당화시키는 단계;
상기 당화된 아로니아추출액 100중량부에 효모 1~3중량부를 가하고 30~35℃에서 3~4일 동안 알코올 발효시켜 알코올발효액을 수득하는 단계;
상기 알코올발효액 100중량부에 초산균 1~5중량부를 가하고 30~35℃에서 10~13일 동안 초산 발효시켜 초산발효액을 제조하는 단계; 및
상기 초산발효액을 10~20℃에서 10~30일 동안 숙성시키는 단계;
를 포함하며,
상기 현미추출액은 정제수 100중량부에 현미 10~15중량부, 머위 1~5중량부, 우엉 1~5중량부 및 유근피 1~5중량부를 가하고 100~105℃에서 20~30분 동안 가열하여 제조하는,
율피차의 제조방법.
The method of claim 1, wherein in step 3,
The method for producing the aronia vinegar is,
Immersing aronia in purified water at 20-30°C for 1-2 minutes;
Adding 30 to 40 parts by weight of the soaked aronia to 100 parts by weight of brown rice extract, heating at 95 to 105°C for 50 to 60 minutes, and then filtering to obtain an aronia extract;
Adding 3 to 4 parts by weight of liquefaction enzyme to 100 parts by weight of the aronia extract and liquefying it at 60°C for 20 to 30 minutes;
Adding 3 to 4 parts by weight of saccharification enzyme to 100 parts by weight of the liquefied aronia extract and saccharifying it at 60°C for 50 to 60 minutes;
Adding 1 to 3 parts by weight of yeast to 100 parts by weight of the saccharified aronia extract and performing alcohol fermentation at 30 to 35° C. for 3 to 4 days to obtain an alcoholic fermentation broth;
Preparing an acetic acid fermentation liquid by adding 1 to 5 parts by weight of acetic acid bacteria to 100 parts by weight of the alcoholic fermentation liquid and fermenting the acetic acid at 30 to 35° C. for 10 to 13 days; and
Aging the acetic acid fermentation liquid at 10 to 20°C for 10 to 30 days;
Includes,
The brown rice extract is prepared by adding 10 to 15 parts by weight of brown rice, 1 to 5 parts by butterbur, 1 to 5 parts by weight of burdock root, and 1 to 5 parts by weight of radish root bark to 100 parts by weight of purified water and heating at 100 to 105°C for 20 to 30 minutes. doing,
How to make Yulpi tea.
상기 단계 5 이후에 상기 2차 건조한 율피를 4~5㎏/㎠, 100~110℃에서 5~6분 동안 퍼핑하는 단계를 추가하는,
율피차의 제조방법.
According to clause 1,
After step 5, adding the step of puffing the secondary dried yulpi at 4 to 5 kg/cm2 and 100 to 110°C for 5 to 6 minutes,
How to make Yulpi tea.
상기 단계 6 이후에 상기 율피분말 100중량부에 기호성 향상제 1~5중량부를 포함하는 단계를 추가하되,
상기 기호성 향상제는 감추출분말 50~60중량%, 배추출분말 20~30중량%, 고구마순발효분말 10~20중량% 및 스테비아발효분말 1~3중량%를 포함하며,
상기 감추출분말은 감 100중량부에 정제수 500~600중량부, 탈지분유 1~5중량부, 구연산 1~3중량부 및 이소말토올리고당 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열하고 여과한 감추출액을 동결건조한 후 분말화하여 수득하며,
상기 배추출분말은 배 100중량부에 정제수 500~600중량부, 루틴 1~5중량부 및 셀룰라아제 1~3중량부를 가하고 90~95℃에서 40~50분 동안 가열한 후 여과한 배추출액을 동결건조한 후 분말화하여 수득하며,
상기 고구마순발효분말의 제조방법은,
고구마순을 100~110℃에서 1~2시간 동안 증숙하는 단계;
상기 증숙된 고구마순을 10~15℃에서 1~2일 동안 숙성하는 단계;
상기 숙성된 고구마순 100중량부에 알룰로스 1~5중량부 및 진피추출액 40~50중량부를 가하고 1.2~1.6기압, 80~90℃에서 3~4시간 동안 추출하여 고구마순추출액을 수득하는 단계;
상기 고구마순추출액 100중량부에 복분자종균 1~5중량부, 프락토올리고당 1~5중량부 및 자일로스 1~5중량부를 가하고 20~24℃에서 12~14시간 동안 발효시킨 후 여과하여 고구마순발효액을 제조하는 단계; 및
상기 고구마순발효액을 동결건조한 후 분말화하는 단계;
를 포함하며,
상기 진피추출액은 진피 100중량부에 95%(v/v) 에탄올 500~600중량부를 가하고 25~27℃에서 24시간 동안 방치한 후 여과하여 제조하며,
상기 복분자종균의 제조방법은,
복분자 100g에 100㎖의 멸균수를 가하고 마쇄기로 분쇄한 다음 착즙한 후 여과하여 복분자 추출액을 제조하는 단계;
옥수수가루 및 갈락토오스를 중량비 1:1로 배합하여 배지를 제조하는 단계; 및
상기 배지 100중량부에 상기 복분자 추출액 50중량부를 가하고 20~22℃에서 20~22일 동안 발효시키는 단계;
를 포함하며,
상기 스테비아발효분말은 스테비아잎 100중량부에 정제수 500~550중량부를 가하고 95~105℃에서 30~40분 동안 가열한 후 여과한 스테비아잎추출액 100중량부에 블루베리발효액 5~10중량부를 가하고 20~24℃에서 24~26시간 동안 발효시킨 후 여과한 스테비아발효액을 동결건조한 후 분말화하여 제조하며,
상기 블루베리발효액은 블루베리착즙액 100중량부에 효모 1~5중량부를 가하고 20~24℃에서 48~50시간 동안 발효시켜 제조하는,
율피차의 제조방법. According to clause 1,
After step 6, a step of including 1 to 5 parts by weight of a palatability improver per 100 parts by weight of the Yulpi powder is added,
The palatability improver includes 50-60% by weight of persimmon extract powder, 20-30% by weight of pear extract powder, 10-20% by weight of fermented sweet potato shoot powder, and 1-3% by weight of fermented stevia powder,
The persimmon extract powder is prepared by adding 500 to 600 parts by weight of purified water, 1 to 5 parts by weight of skim milk powder, 1 to 3 parts by weight of citric acid, and 1 to 3 parts by weight of isomaltooligosaccharide to 100 parts by weight of persimmon, and incubating at 90 to 95°C for 40 to 50 minutes. It is obtained by freeze-drying the heated and filtered persimmon extract and powdering it.
The pear extract powder is made by adding 500 to 600 parts by weight of purified water, 1 to 5 parts by weight of rutin, and 1 to 3 parts by weight of cellulase to 100 parts by weight of pears, heating at 90 to 95°C for 40 to 50 minutes, and then freezing the filtered pear extract. Obtained by drying and powdering,
The manufacturing method of the sweet potato sprout fermented powder is,
Steaming sweet potato shoots at 100-110°C for 1-2 hours;
Aging the steamed sweet potato shoots at 10 to 15°C for 1 to 2 days;
Adding 1 to 5 parts by weight of allulose and 40 to 50 parts by weight of dermis extract to 100 parts by weight of the aged sweet potato shoots and extracting at 1.2 to 1.6 atmospheres and 80 to 90°C for 3 to 4 hours to obtain a sweet potato shoot extract;
To 100 parts by weight of the sweet potato shoot extract, 1 to 5 parts by weight of Bokbunja sprouts, 1 to 5 parts by weight of fructo-oligosaccharides and 1 to 5 parts by weight of xylose were added, fermented at 20 to 24°C for 12 to 14 hours, and then filtered to produce sweet potato shoots. Preparing a fermentation broth; and
Freeze-drying the fermented sweet potato shoot and then powdering it;
Includes,
The dermal extract is prepared by adding 500 to 600 parts by weight of 95% (v/v) ethanol to 100 parts by weight of dermis, leaving it at 25 to 27°C for 24 hours, and then filtering.
The manufacturing method of the bokbunja spawn is,
Preparing a bokbunja extract by adding 100 ml of sterilized water to 100 g of bokbunja, grinding it with a grinder, squeezing juice, and then filtering;
Preparing a medium by mixing corn flour and galactose in a weight ratio of 1:1; and
Adding 50 parts by weight of the bokbunja extract to 100 parts by weight of the medium and fermenting at 20 to 22°C for 20 to 22 days;
Includes,
The stevia fermentation powder is prepared by adding 500 to 550 parts by weight of purified water to 100 parts by weight of stevia leaves, heating at 95 to 105°C for 30 to 40 minutes, and adding 5 to 10 parts by weight of blueberry fermentation liquid to 100 parts by weight of filtered stevia leaf extract. It is manufactured by fermenting at ~24℃ for 24~26 hours, then filtering the stevia fermentation liquid, freeze-drying it, and powdering it.
The blueberry fermentation liquid is manufactured by adding 1 to 5 parts by weight of yeast to 100 parts by weight of blueberry juice and fermenting for 48 to 50 hours at 20 to 24 ° C.
How to make Yulpi tea.
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