KR102528157B1 - A Method for Preparing Liquid Eyelash Nutritional Supplements Containing a Large Amount of Black Beans and, the Liquid Nutritional Supplements for Eyelashes That is Produced through the Method - Google Patents

Abstract

The present invention contains a large amount of black beans, but further contains minerals and mixtures that can improve the health of eyelashes, continuously supplying nutrition to the eyelashes, while maintaining the proper length of the eyelashes and minimizing eyelash loss. It relates to a method for manufacturing an eyelash liquid nutrient containing a large amount of black beans, characterized in that it can improve the overall health of eyelashes, and an eyelash liquid nutrient prepared through the same.

Description

A method for preparing liquid eyelash nutritional supplements containing a large amount of black beans and, the Liquid Nutritional Supplements for Eyelashes That is Produced through the Method}

The present invention contains a large amount of black soybean, but further contains minerals and mixtures that can improve the health of eyelashes to continuously supply nutrients to eyelashes while maintaining an appropriate length of eyelashes and minimizing eyelash loss. It relates to a method for manufacturing an eyelash liquid nutrient containing a large amount of black beans, characterized in that it can improve the overall health of eyelashes, and an eyelash liquid nutrient prepared through the same.

Eyelashes, like hair in general, can change in condition depending on how you care for them. To take good care of your eyelashes, a healthy and balanced diet is essential, and you should eat at least five servings of raw vegetables and fruits high in vitamins C and E every day. However, it is not easy to consume raw vegetables and fruits with high vitamin C and E content every day, so the present inventors have prepared eyelash liquid nutritional supplements to make it easier to maintain eyelash health.

Republic of Korea Patent Publication 10-2019-0012602 Publication date (February 11, 2019)

In order to solve the above problem, the present invention

A first mixture containing a black bean extract, a second mixture containing a cabbage extract, a third mixture formed by grinding minerals, a fourth mixture containing a daylily flower extract, and a fifth mixture comprising a berry mixture By mixing the intermediate mixture with xanthan gum to form a final mixture, and stirring the emulsion on the final mixture, it is possible to maintain the proper length of eyelashes and minimize eyelash loss while maintaining eyelash health It is an object of the invention to provide a method for manufacturing eyelash liquid nutrients containing a large amount of black beans, characterized in that to maintain, and an eyelash liquid nutritional supplement prepared through this.

In order to solve the above problem, the present invention

90 to 95 wt% of a first mixture prepared by mixing one or two or more selected from black bean extract, brown rice extract, black sesame extract, walnut extract, black rice extract, pine nut extract, jujube extract, or wormwood extract; ,

Cabbage extract, orange extract, lemon extract, kiwi extract, broccoli extract, or spinach extract, and 1 to 3 wt% of a second mixture prepared by mixing two or more selected from among.

1 to 3 wt% of a third mixture formed by grinding cerium and biotite;

Daylily flower extract, acacia flower extract, aspen flower extract, gujeolcho flower extract, white peony flower extract, chicken cocoon flower extract, clown flower extract, wisteria flower extract, bush clover flower extract, rhododendron flower extract, thistle flower extract, cockroach extract, large 1 to 2 wt% of a fourth mixture prepared by mixing any one or two or more extracts selected from Gaksichi extract or Babobyeo,

Characterized in that it comprises an intermediate mixture prepared by mixing 1 to 2 wt% of a fifth mixture prepared by mixing any one or two or more selected from gooseberry extract, asahi berry extract, raspberry extract or maqui berry extract A liquid eyelash nutrition supplement containing a large amount of black beans is provided.

In addition, the present invention to solve the above problem,

Black bean extract 80 ~ 90 wt%, brown rice extract 1 ~ 3 wt%, black sesame extract 1 ~ 10 wt%, walnut extract 1 ~ 2 wt%, black rice extract 1 ~ 2 wt%, pine nut extract 1 ~ 2 wt%, 90 to 95 wt% of a first mixture prepared by mixing 1 to 2 wt% of jujube extract and 1 to 2 wt% of artemisia extract,

A second mixture 1 prepared by mixing 20 to 30 wt% of cabbage extract, 20 to 30 wt% of orange extract, 20 to 30 wt% of lemon extract, 10 to 20 wt% of kiwi extract, 10 to 20 wt% of broccoli extract, and 10 to 20 wt% of spinach extract ~ 3 wt%;

1 to 3 wt% of a third mixture formed by grinding cerium and biotite;

Daylily flower extract 1 ~ 5 wt%, acacia flower extract 1 ~ 5 wt%, japonica flower extract 1 ~ 5 wt%, gujeolcho flower extract 1 ~ 5 wt%, white peony flower extract 1 ~ 5 wt%, cockerel flower extract 1 ~ 5 wt%, clown flower extract 1 ~ 10 wt%, wisteria flower extract 1 ~ 10 wt%, bush clover flower extract 1 ~ 5 wt%, rhododendron flower extract 1 ~ 10 wt%, thistle flower extract 1 ~ 10 wt% 1 to 2 wt% of a fourth mixture prepared by mixing any one or two or more extracts selected from 1 to 10 wt% of cockroach extract, 1 to 15 wt% of chinensis extract, or 1 to 15 wt% of Foolia ,

Prepared by mixing 1 to 2 wt% of a fifth mixture prepared by mixing 5 to 40 wt% of gooseberry extract, 5 to 40 wt% of Asahi berry extract, 5 to 40 wt% of raspberry extract, and 5 to 40 wt% of maqui berry extract an intermediate mixture;

a final mixture prepared by mixing 90 to 99 wt% of the intermediate mixture and 1 to 10 wt% of xanthan gum at 25° C.;

A first composition prepared by mixing 60 to 80 wt% of distilled water, 10 to 30 wt% of glycerine, and 0.1 to 10 wt% of EDTA-2Na and completely dissolving by heating at 72 ° C. class,

Cyclomethicone 10 ~ 30 wt%, Cetearyl alcohol 8 ~ 25 wt%, Mineral oil 5 ~ 15 wt%, Grape seed oil 5 ~ 15 wt%, Cetearyl glucoside 5-15 wt%, sorbitan sesquioleate 3-11 wt%, polyoxyethylene alkyl ether 3-7 wt%, isopropyl Isopropyl myristate 1 ~ 5 wt%, Panthenol 1 ~ 5 wt%, Glyceryl stearate / PEG-300 stearate (PEG-300 stearate) 1 ~ 5 wt%, dimethicone A second composition prepared by mixing a mixture of 0.1 to 1 wt% of (Dimethiicone) and 0.1 to 1 wt% of Butylated Hydroxy Toluene (BHT) and completely dissolving the mixture by heating at 72° C.;

An emulsion formed by mixing the completely dissolved second composition into the completely dissolved first composition and stirring at 2600 to 3000 rpm for 15 to 20 minutes;

50 to 99.9 wt% of the emulsion is added to 0.1 to 50 wt% of the final mixture and stirred at 3900 to 4,000 rpm for 10 to 15 minutes to provide an eyelash liquid nutrient containing a large amount of black beans, characterized in that .

In addition, the present invention to solve the above problem,

After adding one or a mixture of two or more selected from black beans, brown rice, black sesame, walnuts, black rice, pine nuts, jujubes, or wormwood to purified water, the first mixture is maintained at 18 to 22 ° C. for 1 to 3 weeks Step (S1) of producing a;

After mixing any one or two selected from cabbage, orange, lemon, kiwi, broccoli, or spinach, drying with hot air and pulverizing to prepare a dried product, putting the pulverized dried product in ethanol and extracting under reflux to prepare an extract. Filtering the extract to prepare a second mixture (S2);

Preparing a third mixture formed by grinding cerium and biotite (S3);

A mixture of daylily flower, acacia flower, jasmine flower, gujeolcho flower, white peony flower, cockerel flower, clown flower, wisteria flower, bush clover flower, rhododendron flower, thistle flower, cockle, large horned rhizome, and barberry flower is suspended in distilled water. After reflux extraction and filtration, the filtrate was concentrated under reduced pressure and centrifuged at a rotation speed of 800 to 1,200 rpm for 30 to 40 minutes to obtain a supernatant, and heating and sterilizing to prepare a fourth mixture (S4);

One or two selected from gooseberry, asahi berry, raspberry, and maqui berry are mixed, hot air dried, and pulverized to prepare a dried product, and the pulverized dried product is put in ethanol and extracted under reflux to prepare an extract, and then the extract is prepared. Filtering to prepare a fifth mixture (S5);

Mixing the first mixture, the second mixture, the third mixture, the fourth mixture, and the fifth mixture to form an intermediate mixture (S6);

A step (S7) of preparing a final mixture by mixing the intermediate mixture and xanthan gum at 25 ° C;

Mixing distilled water, glycerine, and EDTA-2Na and heating at 72 ° C. to completely dissolve the first composition (S8);

Cyclomethicone , Cetearyl alcohol , Mineral oil , Grape seed oil , Cetearyl glucoside , Sorbitan sesquioleate , Polyoxyethylene alkyl ether, Isopropyl myristate, Panthenol, Glyceryl stearate/PEG-300 stearate, Dimethicone Mixing a mixture of (Dimethiicone) and Butylated Hydroxy Toluene (BHT) and completely dissolving it by heating at 72 ° C. to form a second composition (S9);

Forming an emulsion by adding the completely dissolved second composition to the completely dissolved first composition phase, mixing, and stirring at 2600 to 3000 rpm for 15 to 20 minutes (S10);

It provides a method for producing eyelash liquid nutrients containing a large amount of black beans, characterized in that it comprises the step (S11) of adding the emulsion to the final mixture and stirring at 3900 to 4,000 rpm for 10 to 15 minutes.

The present invention has the effect of improving the overall health of the eyelashes while maintaining the appropriate length of the eyelashes and minimizing the eyelash loss phenomenon while continuously supplying nutrition to the eyelashes.

Process chart according to the method for manufacturing eyelash liquid nutrients containing a large amount of black beans of the present invention.

The major difference between the present invention and the prior patent is that it is prepared as an eyelash liquid nutrient containing a large amount of black soybean containing as an active ingredient one or more extracts selected from the group consisting of black bean extract, cabbage extract, daylily extract, and gooseberry extract. am.

Hereinafter, a detailed description will be given.

In the present invention, black bean extract 80 ~ 90 wt%, brown rice extract 1 ~ 3 wt%, black sesame extract 1 ~ 10 wt%, walnut extract 1 ~ 2 wt%, black rice extract 1 ~ 2 wt%, pine nut extract 1 ~ A first mixture prepared by mixing 2 wt%, 1 to 2 wt% of jujube extract, and 1 to 2 wt% of Artemisia extract,
Cabbage extract 20 ~ 30 wt%, orange extract 20 ~ 30 wt%, lemon extract 20 ~ 30 wt%, kiwi extract 10 ~ 20 wt%, broccoli extract 10 ~ 20 wt% and spinach extract 10 ~ 20 wt% With the second mixture prepared,
A third mixture formed by grinding 10 to 50 wt% of cerium and 50 to 90 wt% of biotite;
Daylily flower extract 1 ~ 5 wt%, acacia flower extract 1 ~ 5 wt%, japonica flower extract 1 ~ 5 wt%, gujeolcho flower extract 1 ~ 5 wt%, white peony flower extract 1 ~ 5 wt%, cockerel flower extract 1 ~ 5 wt%, clown flower extract 1 ~ 10 wt%, wisteria flower extract 1 ~ 10 wt%, bush clover flower extract 1 ~ 5 wt%, rhododendron flower extract 1 ~ 10 wt%, thistle flower extract 1 ~ 10 wt% , A fourth mixture prepared by mixing 1 to 10 wt% of cockroach extract, 1 to 15 wt% of Great Barbecue extract and 1 to 15 wt% extract of Baboon,
A fifth mixture prepared by mixing 5 to 40 wt% of gooseberry extract, 5 to 40 wt% of Asahi berry extract, 5 to 40 wt% of raspberry extract, and 5 to 40 wt% of maqui berry extract,
An intermediate mixture was prepared by mixing 94 wt% of the first mixture, 2 wt% of the second mixture, 2 wt% of the third mixture, 1 wt% of the fourth mixture, and 1 wt% of the fifth mixture,
A final mixture prepared by mixing 90 to 99 wt% of the intermediate mixture and 1 to 10 wt% of xanthan gum at 25 ° C.

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In addition, the liquid nutrient described below is an eyelash liquid nutrient containing a large amount of black soybean of the present invention.

Hereinafter, details of the components including the first mixture will be described.

The first mixture is prepared by mixing any one or two or more selected from black bean extract, brown rice extract, black sesame extract, walnut extract, black rice extract, pine nut extract, jujube extract, or wormwood extract.

Also, prior to the explanation, the eyelashes are moist. Protein, vitamins, vitamin B, and minerals must be supplied to achieve healthy and shiny eyelashes and to improve the phenomenon of eyelashes escaping from the skin.

[Composition of the first mixture]

The black bean extract includes 80 to 90 wt% based on the total weight of the first mixture. The reason why the soybeans contain a lot of soybeans is that black soybeans not only create a protective layer on eyelashes through lecithin, but also supply nutrients. In addition, the black soybean contains nutrients such as lipid, vitamin B1, vitamin B2, and vitamin E as well as high-quality protein, and also contains cysteine, which is an essential component for hair growth, so that eyelashes can be lubricated.

The brown rice extract includes 1 to 3 wt% based on the total weight of the first mixture. The brown rice contains 15.5% moisture, 7.4% protein, 3.0% lipid, 71.8% sugar, 1.0% fiber, 1.3% ash, and 0.54 mg of vitamin B1 in 100 g, which accounts for most of the sugar (starch) and slows down insulin secretion. It can improve the phenomenon that the eyelashes are separated from the skin, that is, being pulled out.

The black sesame extract contains 1 to 10 wt% based on the total weight of the first mixture, and black sesame contains a lot of keratin, so it has the effect of improving the phenomenon of eyelashes separating from the skin and at the same time keeping the eyelashes shiny. can

The walnut extract includes 1 to 2 wt% based on the total weight of the first mixture. Among nuts, it has a unique protein taste, and is rich in biotin, a complex of omega 3 fatty acids, vitamin E, and vitamin B, which has the effect of making eyelashes healthy.

The black rice extract contains 1 to 2 wt% of the total weight of the first mixture, is rich in anthocyanin, can strengthen the immunity of eyelashes, and contains a large amount of minerals important for eyelash health.

The pine nut extract contains 1 ~ 2 wt% of the first mixture by weight, and is rich in minerals, unsaturated fatty acids, vitamin B, and vitamin E, so that nutrients can be delivered evenly to the scalp and strengthen the eyelashes by strengthening the hair roots of the eyelashes. .

The jujube extract contains 1 to 2 wt% of the first mixture by weight, and the jujube contains a large amount of vitamin B2, vitamin C, vitamin E, protein, vitamin A and beta-carotene to smoothly supply the eyelashes with nutrients. This can make your eyelashes healthy.

The wormwood extract contains 1 to 2 wt% based on the total weight of the first mixture. The wormwood is very beneficial for hair health because it is rich in vitamin A and vitamin C.

Thus, the first mixture contains 80 to 90 wt% of black bean extract, 1 to 3 wt% of brown rice extract, 1 to 10 wt% of black sesame extract, 1 to 2 wt% of walnut extract, 1 to 2 wt% of black rice extract, It is prepared by mixing 1 to 2 wt% of pine nut extract, 1 to 2 wt% of jujube extract, and 1 to 2 wt% of artemisia extract,

More specifically, the first mixture is black bean extract 90wt%, brown rice extract 1 wt%, black sesame extract 2wt%, walnut extract 1 wt%, black rice extract 2 wt%, pine nut extract 2 wt%, jujube extract It is preferably prepared by mixing 1 wt% and 1 wt% of Artemisia extract.

also. The first mixture contains 90 to 95 wt%, more preferably 95 wt%, based on the total weight of the intermediate mixture.

If the first mixture is less than 90 wt% relative to the total weight of the intermediate mixture, the effect of improving eyelashes may be reduced, and if it exceeds 95 wt%, the content of other components is reduced accordingly, which is not preferable.

Hereinafter, details of the components including the second mixture will be described.

The second mixture is prepared by mixing any one or two or more selected from cabbage extract, orange extract, lemon extract, kiwi extract, broccoli extract, or spinach extract.

[Composition of the second mixture]

The cabbage extract contains 20 to 30 wt% of the total weight of the second mixture, and the cabbage supplies rich fiber and dietary fiber to the eyelash hair roots, and the cabbage contains vitamin U and vitamin K at the same time and affects dry eyelashes. Cabbage, which has a strong sulfur component, can prevent oxidation of eyelashes and improve the health of eyelashes and hair during the changing seasons.

The orange extract contains 20 to 30 wt% of the total weight of the second mixture, and the orange is basically rich in vitamin C, so it plays an important role in strengthening the eyelash hair roots.

The lemon extract contains 20 to 30 wt% of the total weight of the second mixture and, like the orange, is basically rich in vitamin C and plays an important role in strengthening the eyelash hair roots. In addition to the lemon, folic acid, B complex As an important source of vitamins and essential minerals, all of these nutrients support the body's functions. The lemon is very good for the eyelashes, and it plays a role in making the hair roots healthy by adjusting the natural acidity of the hair roots of the eyelashes and cleaning dead cells.

The kiwi extract contains 10 to 20 wt% of the total weight of the second mixture, and the kiwi contains omega 3, zinc, magnesium, etc. that supply moisture to the hair, and in particular, the minerals contained in kiwi improve blood circulation of the hair roots. It can be promoted to improve the separation of eyelashes from the skin.

The broccoli extract contains 10 to 20 wt% of the total weight of the second mixture, and the broccoli contains a component called sulforaphane to increase the production of enzymes that protect the hair roots, strengthen the hair roots, and activate blood circulation in the hair roots of the eyelashes. do

The spinach extract contains 10 to 20 wt% of the total weight of the second mixture, and the spinach is rich in vitamin a and can improve eyelash health by preventing the eyelashes from drying out.

Thus, the second mixture contains 20 to 30 wt% of cabbage extract, 20 to 30 wt% of orange extract, 20 to 30 wt% of lemon extract, 10 to 20 wt% of kiwi extract, 10 to 20 wt% of broccoli extract, and 10 to 20 wt% of spinach extract. It is prepared by mixing 20 wt%,

More preferably, it is prepared by mixing cabbage extract 20 wt%, orange extract 20 wt%, lemon extract 30 wt%, kiwi extract 10 wt%, broccoli extract 10 wt% and spinach extract 10 wt%.

The second mixture is preferably added in an amount of 1 to 3 wt%, more preferably 2 wt%, based on the total weight of the intermediate mixture.

If the second mixture is less than 1 wt% relative to the total weight of the intermediate mixture, the effect on the proposed eyelashes is insignificant, and if it exceeds 3 wt%, the content of other components is reduced accordingly, which is not preferable.

Hereinafter, details of the components including the third mixture will be given.

The third mixture is formed by grinding 10 to 50 wt% of cerium and 50 to 90 wt% of biotite.

[Composition of the third mixture]

Cerium is a mineral that is a raw material for lanthanide elements, and is a rare earth element that is abundant and easy to use. It can be used without increasing the purity, so the application field is wide. Among various rare earth elements, it is common, but it is produced in large quantities in other element extraction processes and is widely used.

Cerium is a chemical element with atomic number 58, symbol Ce, and is a ductile, silvery-white metal. It also changes color easily when exposed to air and is soft enough to be cut with a knife. It is the second element of the lanthanide family and has a predominantly +3 oxidation state, but it can also have a stable +4 oxidation state depending on the substance.

Cerium is processed into 15 ~ 25㎛ powder and used, and cerium contains 10 ~ 50 wt% of the total weight of the third mixture. Increases ATP (Adenosine Triphosphate) component and promotes protein expression, which is helpful for hair growth and hair growth. It has an effect on, and also has an excellent property of attracting substances to remove activated oxygen, that is, it can prevent eyelashes from escaping.

Biotite is a stone of life with a higher far-infrared ray emissivity (93-94%) than ocher and elvan, and a germanium content of up to 36ppm, and has the effect of removing carcinogens.

Biotite is a silicate mineral belonging to the common mica family. Abundant in metamorphic, pegmite, granite and other intrusive igneous rocks. The external color is black, brownish black, greenish black, etc., and the streak color is white. The cleavage is complete on the underside. The hardness is about 2.5 to 3.0 on the Mohs hardness scale.

biotite It is processed into powder of 15 ~ 25㎛ and contains 50 ~ 90 wt% of the total weight of the third mixture, and the biotite activates metabolism to help blood circulation to the hair roots and play a role in making eyelashes healthy .

In addition, the third mixture preferably contains 1 to 3 wt% based on the total weight of the intermediate mixture, more preferably 1 wt% based on the total weight of the intermediate mixture.

If the third mixture is less than 1 wt%, the effective effect of the mineral is not properly exerted, and if the third mixture exceeds 3 wt%, the liquid nutrient is diluted and is preferably used in a limited range.

Hereinafter, details of the components including the fourth mixture will be given.

The fourth mixture is a daylily flower extract, an acacia flower extract, a sturgeon flower extract, a gujeolcho flower extract, a white peony flower extract, a chicken cocoa flower extract, a clown flower extract, a wisteria flower extract, a bush clover flower extract, a lily flower extract, a thistle flower extract, It is prepared by mixing any one or two or more extracts selected from the cockroach extract, the great horned chinensis extract, and the barnacle.

[Composition of the 4th mixture]

The daylily flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, and the fragrance of the daylily flower relaxes the muscles of the body to relieve stress and refresh the mood. Daylily (fragrant plantain, 玉簪花) is a perennial plant of the monocotyledonous lily lily family, and is also called jade hairpin flower and baekhakseok.

The acacia flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, and contains an ingredient called acacetin, which has anti-inflammatory and anti-cancer effects. In the case of acacia, the moisture content of acacia petals is 86.60%, and when dried, crude protein is 24.55%, crude is 8.51%, total sugar is 30.97%, and ascorbic acid is about 16%, tannic acid (tannicacid) is known to be relatively high in sugar, protein and ascorbic acid (ascorbicacid) content of about 15%

The extract of the blackberry flower contains 1 to 5 wt% based on the total weight of the fourth mixture, and is good for arthritis, neuralgia, and customary arthritis. Sytrax japonica (Sytrax japonica Sib. et Zucc.) is a deciduous tree belonging to the Zuccaceae family, reaching a height of 10 m, and the leaves are alternate and long oval or diamond-shaped. The peel of the fruit of the japonica tree contains an ingredient called egosaponin, and the seeds contain various types of glycerides, fatty oils, and egonol.

The gujeolcho flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, and has been used as a household medicine to drink when women have cold hands and feet or cold after childbirth in oriental medicine and private practice. It is known to be warm, has strong analgesic and anti-inflammatory properties, and is effective in treating high blood pressure and gastrointestinal diseases. Studies on the physiological activity of Gujeolcho mainly have reports on antibacterial substances, and other studies are insignificant. Gujeolcho shows high total polyphenol content and total flavonoid content in flowers. It has high antioxidant activity. It has great potential as a natural antioxidant.

The peony flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, and is known to have antibacterial effects, protective effects against liver toxicity, anticancer effects, and immune function enhancing effects, and a representative component is peonyflorin (paeoniflorin). ), paeonol, and paeonin. In particular, it has been reported that peonyflorin exerts a significant effect on UV-induced DNA destruction in human skin tissue and prevention of facial wrinkles, and plasmarenin activity (PRA) protects normal cells against oxidative stress. It is known to be able to do it, so it is expected to have effects such as preventing skin aging, but there is no direct study on the effect on skin whitening and wrinkles.

The chrysanthemum flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, has been used for diabetes as a folk remedy, and recently inhibited α-glucosidase, an intestinal glycolysis digestive enzyme, It has been reported that it has a hypoglycemic effect that lowers the concentration of glucose in the blood. Commelinin, a flavonoid, has been reported in petals of chicken ileum. It is believed that the synthesis of chicken ileum extract is inhibited due to the loss of protease activity through inhibition of the expression and process of proteins required for the enzyme pathway related to synthesis. Therefore, it was confirmed that there is a whitening effect by inhibiting the enzyme involved in the synthetic pathway of chicken ileum grass.

The clown flower extract contains 1 to 10 wt% based on the total weight of the fourth mixture, and is known to treat wind action and muscle and skeletal pain as folk remedies.

The wisteria flower extract contains 1 to 10 wt% of the total weight of the fourth mixture, and the wisteria flower relieves muscle pain and is very effective against uterine cancer and stomach cancer in women. Also, wisteria flower extract has potential as a natural antioxidant.

The bush clover flower extract contains 1 to 5 wt% of the total weight of the fourth mixture, and is used in the private sector as a treatment for skin fungi and as a diuretic. Quercetin, kaempferol, trifolin, isoquercitrin, orientin, isoorientin, etc. have been reported as components of Hagi, but there are few studies on their pharmacological action. am. Hsagi flower extract exhibits antioxidant and anti-inflammatory effects, and is effective in skin beauty as it is shown to reduce melanin production in B16/F10 cells.

The rhubarb flower extract contains 1 to 10 wt% of the total weight of the fourth mixture, and is used in the private sector to strengthen the lungs, prevent cough and asthma, and quench thirst. It is also effective when the mother gives birth to a child and milk does not come out. It protects the heart, clears the mind, helps blood vessels, and controls lack of energy and lethargy. In particular, it relieves neuralgia, rheumatism, and atopy.

The thistle flower extract contains 1 to 10 wt% of the total weight of the fourth mixture, and is known to have hemostatic and antibacterial effects, and is widely used in folk medicine and herbal medicine prescription. In particular, thistle flower root is used for the treatment of rheumatism in Japan. Thistle flower extract has been confirmed to have an antidepressant action and has been reported to be effective in depression as it can also reduce activity due to depression.

The cockroach extract contains 1 to 10 wt% based on the total weight of the fourth mixture, and the cockroach is an annual plant of the Asteraceae family. Distributed in East Asia, Europe and North America. In the Korean Peninsula, it is an indigenous plant as an alien species.

The extract of Rhododendron japonica contains 1 to 15 wt% based on the total weight of the fourth mixture, and the Rhododendron japonica is a perennial plant of the Asteraceae family. It is also called thorns, some somnamul, and pungmoguk, and has a great effect on strengthening the body's immunity.

Or, the idiot extract contains 1 to 15 wt% of the extract relative to the total weight of the fourth mixture, and the annual grass of the idiot plant family. The height is 40~80cm, and the leaves are alternate and have petioles. It is similar to Yeokkyun, but has hairs on the stem, black dots on the leaves, and no spicy taste. From June to September, the pink flower blooms as a spike inflorescence, and the fruit is an achene. It grows near the water and is distributed in Korea, Japan, China, and Indonesia.

The fourth mixture contains 1 to 5 wt% of daylily flower extract, 1 to 5 wt% of acacia flower extract, 1 to 5 wt% of stelae flower extract, 1 to 5 wt% of Gujeolcho flower extract, 1 to 5 wt% of white peony flower extract, 1 ~ 5 wt% of chicken cocoa flower extract, 1 ~ 10 wt% of clown flower extract, 1 ~ 10 wt% of wisteria flower extract, 1 ~ 5 wt% of Hsagi flower extract, 1 ~ 10 wt% of lichen flower extract, 1 ~ 10 wt% of thistle flower extract It is prepared by mixing ~ 10 wt%, 1 ~ 10 wt% of cockroach extract, 1 ~ 15 wt% of Great hornbill extract, and 1 ~ 15 wt% of Pooja extract.

More specifically, the fourth mixture contains 5 wt% of daylily flower extract, 5 wt% of acacia flower extract, 5 wt% of japonica flower extract, 5 wt% of Gujeolcho flower extract, 5 wt% of white peony flower extract, and 5 wt% of chrysanthemum flower extract. %, clown flower extract 10 wt%, wisteria flower extract 10 wt%, bush clover flower extract 5 wt%, rhododendron flower extract 10 wt%, thistle flower extract 10 wt%, cockle extract 10 wt%, chinensis extract 1 wt% % and 14 wt% of turmeric extract.

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The fourth mixture contains 1 to 2 wt%, more preferably 1 wt%, based on the total weight of the intermediate mixture.

If the fourth mixture is less than 1 wt%, the content of the component is too insignificant, and if it exceeds 2 wt%, it may cause irritation around the eyelashes, so it is preferable to use it in a limited range.

Hereinafter, details of the components including the fifth mixture will be given.

A fifth mixture is prepared by mixing the diane gooseberry extract, the asahi berry extract, the raspberry extract, and the maqui berry extract.

[Composition of the fifth mixture]

The gooseberry extract contains 5 to 40 wt% based on the total weight of the fifth mixture, and the gooseberry is a fruit of a gooseberry tree belonging to the Currant family. In addition to purple egg-shaped fine hair, there are round and smooth types of light green, yellow, and white. Gooseberries have very low calories (30 kcal or 125 kJ per 100 g), low sugar content, and are rich in potassium, vitamin C, and minerals. With the active ingredients presented above, it is possible to keep the eyelashes healthy.

The Asahi berry extract contains 5 to 40 wt% of the total weight of the fifth mixture, and the Asahi berry contains antioxidants, vitamins A, C, E, K, minerals, amino acids, and essential fatty acids in the Asahi berry to make healthy eyelashes. , It slows down the phenomenon of eyelash splitting. It also contains omega-3 fatty acids that increase the protein level of your eyelashes.

The raspberry extract contains 5 to 40 wt% of the total weight of the fifth mixture, the raspberry contains vitamin C and folic acid, and the amount of vitamin C contained in 100 g of the raspberry is equal to the amount contained in a normal-sized tangerine. helps keep you healthy.

Maqui berry extract contains 5 ~ 40 wt% of the total weight of the 5th mixture, and Maqui berry is rich in various vitamins, calcium, iron, and potassium. In addition, it is rich in anthocyanin, a type of polyphenol. there is. It also has an anti-inflammatory effect, so it plays a role in catching harmful substances in the hair roots.

A fifth mixture is prepared by mixing 5 to 40 wt% of gooseberry extract, 5 to 40 wt% of Asahi berry extract, 5 to 40 wt% of raspberry extract, and 5 to 40 wt% of maqui berry extract.

More preferably, the fifth mixture is prepared by mixing 40 wt% of gooseberry extract, 40 wt% of asahi berry extract, 10 wt% of raspberry extract, and 10 wt% of maqui berry extract.

In addition, the fifth mixture includes 1 to 2 wt% based on the total weight of the intermediate mixture, and more preferably, the fifth mixture includes 2 wt% based on the total weight of the intermediate mixture.

If the liquid nutrient is less than 1wt%, it may be difficult to express the effect of maintaining the health of eyelashes, and if it exceeds 2wt%, it is an economic loss because there is no significant effect thereof.

[intermediate mixture]

The intermediate mixture includes a first mixture, a second mixture, a third mixture, a fourth mixture, and a fifth mixture, specifically, 94 wt% of the first mixture, 2 wt% of the second mixture, 2 wt% of the third mixture, It is prepared by mixing 1 wt% of the fourth mixture and 1 wt% of the fifth mixture.

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[emulsion]

The emulsion was prepared by mixing 60 to 80 wt% of distilled water, 10 to 30 wt% of glycerine, and 0.1 to 10 wt% of EDTA-2Na and heating at 72 ° C. to completely dissolve the composition A first composition to be,

Cyclomethicone 10 ~ 30 wt%, Cetearyl alcohol 8 ~ 25 wt%, Mineral oil 5 ~ 15 wt%, Grape seed oil 5 ~ 15 wt%, Cetearyl glucoside 5-15 wt%, sorbitan sesquioleate 3-11 wt%, polyoxyethylene alkyl ether 3-7 wt%, isopropyl Isopropyl myristate 1 ~ 5 wt%, Panthenol 1 ~ 5 wt%, Glyceryl stearate / PEG-300 stearate (PEG-300 stearate) 1 ~ 5 wt%, dimethicone A second composition prepared by mixing a mixture of 0.1 to 1 wt% of (Dimethiicone) and 0.1 to 1 wt% of Butylated Hydroxy Toluene (BHT) and completely dissolving the mixture by heating at 72° C.;

The completely dissolved second composition is added to the completely dissolved first composition and mixed, and stirred at 2600 to 3000 rpm for 15 to 20 minutes.

Let's briefly look at the compositions included in the emulsion.

The glycerin is a drug used for purposes such as enema, lubrication, and moisturizing. The single agent is used as an enema and lubricant, and the complex agent is used in the form of liquid, eye drops, and injections for frostbite, dry eye syndrome, and volume reduction during surgery.

The EDTA-2Na is commonly used as a stabilizer in the manufacture of cosmetics.

The cyclomethicone (Cyclomethicone) is a kind of silicone oil having oil characteristics as a silicon compound. It is mainly used as a hair conditioning agent and skin softener, and is one of the ingredients that improve application properties.

The cetiayl alcohol The cetiayl alcohol has an effect of improving poor spreadability.

The mineral oil can be obtained by a combination of acid treatment and hydrogenation, by hydrogenation, or by intensively treating petroleum together with fuming sulfuric acid and sulfuric acid to obtain a highly refined petroleum-based mineral oil composed of a combination of hydrocarbons.

The grapeseed oil is oil made by pressing the seeds of grapes. It is made using seeds that are produced as a by-product of winemaking.

The sorbitan sesquioleate serves to help stabilize the emulsion and improve moisturizing power for components that do not mix with each other.

The isopropyl myristate is a compound used as a binder, fragrance, and skin softener. Isopropyl myristate is a compound of isopropanol and myristic acid. Absorbs well through the skin.

The panthenol is an alcohol derivative of pantothenic acid, a type of vitamin B. When panthenol enters the body, it is called pantothenic acid and is converted into vitamin B5, which is helpful for skin regeneration.

The glyceryl stearate is a type of hydrophobic surfactant, which stabilizes cosmetics so that they are not separated into an oil phase and an aqueous phase, and at the same time prevents freezing.

Butylated Hydroxy Toluene (BHT) is a phenolic compound antioxidant having polyphenols among antioxidants that prevent rancidity of fat.

Hereinafter, the final mixture will be reviewed.

[Final mixture]

A final mixture is prepared by mixing 97 to 99 wt% of the intermediate mixture and 1 to 3 wt% of xanthan gum at 25°C.

Most preferably, a final mixture is prepared by mixing 97 wt% of the intermediate mixture and 3 wt% of xanthan gum at 25°C.

Xanthan gum, a natural thickener, obtained by pure culture and fermentation of carbohydrates using Xanthomonas campestris, a causative bacterium of leaf disease of cabbage, is purified, dried, and pulverized in isopropyl alcohol. It is a mixture composed of sodium, potassium and calcium salts of north and glucuronic acid.

It has excellent heat resistance, and in particular, if there is glacial acetic acid or citric acid, the viscosity decrease is small even when heated. Natural thickeners such as xanthan gum decrease in viscosity when acidic or alkaline substances coexist, but xanthan gum does not decrease in viscosity due to pH and is stable within the pH range of 2 to 13. Xanthan gum has good viscosity compared to other thickeners, and the viscosity gradually increases with concentration.

If the intermediate mixture is less than 97 wt%, the effect of improving eyelashes may be insignificant, and if it is more than 99 wt%, the content of xanthan gum is reduced accordingly, which is not preferable.

Xanthan gum (Xanthan gum) less than 1wt% can cause viscosity control or decrease in usability, and if it exceeds 3 wt%, it is too thick, so it is preferable to use a limited range.

It is completed by adding 50 to 99.9 wt% of the emulsion to 0.1 to 50 wt% of the final mixture and stirring at 3900 to 4,000 rpm for 10 to 15 minutes.

Hereinafter, a detailed description of the step-by-step manufacturing method will be described.

[Step of preparing the first mixture (S1)]

After adding one or a mixture of two or more selected from black beans, brown rice, black sesame, walnuts, black rice, pine nuts, jujubes, or wormwood to purified water, the first mixture is maintained at 18 to 22 ° C. for 1 to 3 weeks to manufacture

more specifically. After adding one or a mixture of two or more selected from black bean extract, brown rice extract, black sesame extract, walnut extract, black rice extract, pine nut extract, jujube extract or wormwood extract to purified water, 1 to 1 at 18 to 22 ° C. It is characterized in that it is prepared by using a method in which the active ingredients of the raw material come out with purified water by maintaining for 3 weeks.

[Preparing the second mixture (S2)]

After mixing any one or two selected from cabbage, orange, lemon, kiwi, broccoli, or spinach, drying with hot air and pulverizing to prepare a dried product, putting the pulverized dried product in ethanol and extracting under reflux to prepare an extract. It is prepared by filtering the extract,

More specifically, one or two selected from cabbage, orange, lemon, kiwi, broccoli, or spinach are mixed and dried in hot air at 60 to 100 ° C. for 3 to 5 days, and the dried product is pulverized to prepare a pulverized dried product And, the pulverized dried product is put in ethanol 2 to 4 times for 2 to 4 hours, extracted under reflux to prepare an extract, and then the extract is prepared by filtering.

[Preparing a third mixture formed by pulverizing cerium and biotite (S3)]

The cerium is prepared by firstly making cerium powder by firing cerium powder at a temperature of 600 to 1000 ° C through a solid phase reaction grinding method, and mechanically pulverizing the cerium powder, and the biotite is prepared by putting the biotite ore into an ore crusher. and pulverized to prepare biotite powder.

A third mixture is prepared by mixing the pulverized cerium powder and biotite.

[Step of preparing a fourth mixture (S4)]

Daylily flower, acacia flower, japonica flower, gujeolcho flower, white peony flower, cockerel flower, clown flower, wisteria flower, bush clover flower, rhododendron flower, thistle flower, cockroach, large hornbill, or baboon, or A mixture of the two is suspended in distilled water, extracted under reflux, filtered, and the filtrate is concentrated under reduced pressure and centrifuged at a rotational speed of 800 to 1,200 rpm for 30 to 40 minutes to obtain a supernatant, which is prepared by heating and sterilizing.

[Step of preparing a fifth mixture (S5)]

Any one or two selected from gooseberry, asahi berry, raspberry and maqui berry are mixed, hot-air dried, and pulverized to prepare a dried product, and the pulverized dried product is put in ethanol and extracted under reflux to prepare an extract, and then the extract is prepared by filtration

More specifically, any one or two selected from gooseberry, asahi berry, raspberry, and maqui berry are mixed and dried in hot air at 60 to 100 ° C. for 3 to 5 days, and the dried product is pulverized to prepare a pulverized dried product, The pulverized dry matter is put in ethanol 2 to 4 times for 2 to 4 hours, extracted under reflux to prepare an extract, and then the extract is prepared by filtering.

[Step of forming an intermediate mixture (S6)]

The first mixture, the second mixture, the third mixture, the fourth mixture and the fifth mixture are mixed to prepare an intermediate mixture.

[Step of forming the final mixture (S7)]

A final mixture is prepared by mixing the intermediate mixture and xanthan gum at 25°C.

[Composition of the first composition (S8)]

As a step for preparing the emulsion, distilled water (Water), glycerine (Glycerine), and EDTA-2Na are mixed and heated at 72 ° C. to form the first composition while completely dissolving.

[Composing a second composition (S9)]

As a step for preparing the emulsion, Cyclomethicone, Cetearyl alcohol, Mineral oil, Grape seed oil, Cetearyl glucoside, Sorbitan Sorbitan sesquioleate, Polyoxyethylene alkyl ether, Isopropyl myristate, Panthenol, Glyceryl stearate/PEG-300 stearate ( A mixture of PEG-300 stearate), dimethicone, and butylhydroxytoluene (BHT) was mixed and heated at 72° C. to completely dissolve it to form a second composition.

[Forming an emulsion (S10)]

The completely dissolved second composition is added to the completely dissolved first composition phase, mixed, and stirred at 2600 to 3000 rpm for 15 to 20 minutes to form an emulsion.

[Step of adding emulsion to the final mixture and stirring (S11)]

Put the emulsion on the final mixture and stir for 10 to 15 minutes at 3900 to 4,000 rpm.

The completed eyelash liquid nutrient can be applied to the eyebrows, and in the case of men, it can be applied to the sideburn hairline.

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The present invention can improve the overall health of the eyelashes while maintaining the proper length of the eyelashes and minimizing eyelash loss while continuously supplying nutrients to the eyelashes, and thus has great industrial applicability.

Claims (7)

delete delete delete delete delete Black bean extract 80 ~ 90 wt%, brown rice extract 1 ~ 3 wt%, black sesame extract 1 ~ 10 wt%, walnut extract 1 ~ 2 wt%, black rice extract 1 ~ 2 wt%, pine nut extract 1 ~ 2 wt% A first mixture prepared by mixing 1 to 2 wt% of jujube extract and 1 to 2 wt% of artemisia extract,
Cabbage extract 20 ~ 30 wt%, orange extract 20 ~ 30 wt%, lemon extract 20 ~ 30 wt%, kiwi extract 10 ~ 20 wt%, broccoli extract 10 ~ 20 wt% and spinach extract 10 ~ 20 wt% With the second mixture prepared,
A third mixture formed by grinding 10 to 50 wt% of cerium and 50 to 90 wt% of biotite;
Daylily flower extract 1 ~ 5 wt%, acacia flower extract 1 ~ 5 wt%, japonica flower extract 1 ~ 5 wt%, gujeolcho flower extract 1 ~ 5 wt%, white peony flower extract 1 ~ 5 wt%, cockerel flower extract 1 ~ 5 wt%, clown flower extract 1 ~ 10 wt%, wisteria flower extract 1 ~ 10 wt%, bush clover flower extract 1 ~ 5 wt%, rhododendron flower extract 1 ~ 10 wt%, thistle flower extract 1 ~ 10 wt% , A fourth mixture prepared by mixing 1 to 10 wt% of cockroach extract, 1 to 15 wt% of Great Barbecue extract and 1 to 15 wt% extract of Baboon,
A fifth mixture prepared by mixing 5 to 40 wt% of gooseberry extract, 5 to 40 wt% of Asahi berry extract, 5 to 40 wt% of raspberry extract, and 5 to 40 wt% of maqui berry extract,

An intermediate mixture was prepared by mixing 94 wt% of the first mixture, 2 wt% of the second mixture, 2 wt% of the third mixture, 1 wt% of the fourth mixture, and 1 wt% of the fifth mixture,
a final mixture prepared by mixing 90 to 99 wt% of the intermediate mixture and 1 to 10 wt% of xanthan gum at 25° C.;

A first composition prepared by mixing 60 to 80 wt% of distilled water, 10 to 30 wt% of glycerine, and 0.1 to 10 wt% of EDTA-2Na and completely dissolving by heating at 72 ° C. class,
Cyclomethicone 10 ~ 30 wt%, Cetearyl alcohol 8 ~ 25 wt%, Mineral oil 5 ~ 15 wt%, Grape seed oil 5 ~ 15 wt%, Cetearyl glucoside 5-15 wt%, sorbitan sesquioleate 3-11 wt%, polyoxyethylene alkyl ether 3-7 wt%, isopropyl Isopropyl myristate 1 ~ 5 wt%, Panthenol 1 ~ 5 wt%, Glyceryl stearate / PEG-300 stearate (PEG-300 stearate) 1 ~ 5 wt%, dimethicone A second composition prepared by mixing a mixture of 0.1 to 1 wt% of (Dimethiicone) and 0.1 to 1 wt% of Butylated Hydroxy Toluene (BHT) and completely dissolving the mixture by heating at 72° C.;
An emulsion formed by mixing the completely dissolved second composition into the completely dissolved first composition and stirring at 2600 to 3000 rpm for 15 to 20 minutes;

An eyelash liquid nutrient containing black beans, characterized in that prepared by adding 50 to 99.9 wt% of the emulsion to 0.1 to 50 wt% of the final mixture and stirring for 10 to 15 minutes at 3900 to 4,000 rpm






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