KR102501405B1 - A cosmetic composition having lasting moisturizing effects and a method for manufacturing the same - Google Patents
A cosmetic composition having lasting moisturizing effects and a method for manufacturing the same Download PDFInfo
- Publication number
- KR102501405B1 KR102501405B1 KR1020220131443A KR20220131443A KR102501405B1 KR 102501405 B1 KR102501405 B1 KR 102501405B1 KR 1020220131443 A KR1020220131443 A KR 1020220131443A KR 20220131443 A KR20220131443 A KR 20220131443A KR 102501405 B1 KR102501405 B1 KR 102501405B1
- Authority
- KR
- South Korea
- Prior art keywords
- oil
- cosmetic composition
- cream
- soap
- lotion
- Prior art date
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 104
- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 230000003020 moisturizing effect Effects 0.000 title abstract description 44
- 230000002045 lasting effect Effects 0.000 title abstract 3
- 238000000034 method Methods 0.000 title description 10
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
Description
본 발명은 지속적인 보습 효과를 가지는 화장료 조성물 및 이의 제조방법에 관한 것으로, 구체적으로는 고형 오일, 비휘발성 에스테르계 오일, 및 금속 산화물을 포함하고, 지속적인 보습 효과를 가지는 컨실러 조성물 및 이의 제조방법에 관한 것이다.The present invention relates to a cosmetic composition having a sustained moisturizing effect and a method for producing the same, and more specifically, to a concealer composition containing a solid oil, a non-volatile ester-based oil, and a metal oxide and having a continuous moisturizing effect, and a method for producing the same. will be.
피부의 결점을 가리기 위해 사용하는 컨실러 조성물은 다량의 금속산화물과 휘발성 물질을 주요성분으로 포함하여, 금속산화물이 피부에 고루 도포될 수 있도록 개발되었다. 따라서 종래의 컨실러 조성물은 다량의 휘발성 오일을 포함하는 것이 일반적인데, 이는 피부의 오일 잔여감을 해결하고 제형이 피부에 밀착되는 효과를 높여 커버력이 개선되는 효과가 있으나, 휘발되는 성질에 의하여 시간이 경과되면 피부에 건조함을 야기하고 금속산화물을 포함하는 화장료 조성물이 갈라지는 문제점이 있었다. 이러한 문제의 해결을 위해 최근 오일 성분을 보습력을 가지는 비휘발성 오일로 대체하고자 하는 노력이 있었으나, 비휘발성 오일을 주성분으로 이용할 경우 화장료 조성물의 피부 부착력이 저하되는 문제점이 발생하였다.Concealer compositions used to cover skin imperfections contain a large amount of metal oxides and volatile substances as main components, and have been developed so that metal oxides can be evenly applied to the skin. Therefore, conventional concealer compositions generally contain a large amount of volatile oil, which has the effect of improving the coverage by solving the oil residue on the skin and increasing the effect of the formulation adhering to the skin. When it does, there is a problem in that it causes dryness on the skin and the cosmetic composition containing the metal oxide is cracked. In order to solve this problem, efforts have recently been made to replace oil components with non-volatile oils having moisturizing power, but when non-volatile oils are used as a main component, the skin adhesion of the cosmetic composition is lowered.
이러한 종래 기술의 문제점을 해결하기 위하여, 본 발명자들은 각고의 노력을 지속한 끝에 비휘발성 오일의 흐름성을 제어하면서, 동시에 우수한 보습력을 가지는 컨실러용 화장료 조성물을 개발하기에 이르렀다. 따라서 본 발명은 지속적인 보습 효과를 가지는 화장료 조성물, 및 이의 제조방법에 관한 것으로서, 보다 상세하게는 고형 오일로 하이드로제네이티드 식물성 오일, 비휘발성 에스테르계 오일로 헥실라우레이트, 및 금속산화물을 특정 성분비로 함유하여 지속적인 보습 효과를 가지는 유중 수형 에멀젼 화장료 조성물 및 이의 제조방법에 관한 것이다. 종래 문제점을 현저히 개선한 본 발명의 화장료 조성물은 미용 분야에서 크게 이용될 것으로 기대된다.In order to solve these problems of the prior art, the present inventors have developed a cosmetic composition for concealer having excellent moisturizing power while controlling the flowability of non-volatile oil at the end of continuous efforts. Therefore, the present invention relates to a cosmetic composition having a sustained moisturizing effect, and a method for producing the same, and more particularly, to a solid oil containing hydrogenated vegetable oil, a non-volatile ester-based oil such as hexyllaurate, and a metal oxide in a specific component ratio. It relates to a water-in-oil emulsion cosmetic composition having a continuous moisturizing effect and a method for preparing the same. The cosmetic composition of the present invention, which significantly improves the conventional problems, is expected to be greatly used in the cosmetic field.
본 발명의 목적은 금속산화물의 피부 부착력을 저해하지 않으면서 지속적인 보습력을 갖는 유중수형 에멀젼 화장료 조성물, 및 이의 제조방법을 제공하고자 하는 것이다.An object of the present invention is to provide a water-in-oil type emulsion cosmetic composition having continuous moisturizing power without impairing the skin adhesion of metal oxide, and a method for preparing the same.
이를 위해, 본 발명은 고형 오일, 비휘발성 에스테르계 오일, 및 금속산화물을 포함하는 화장료 조성물, 및 이의 제조방법을 제공한다.To this end, the present invention provides a cosmetic composition comprising a solid oil, a non-volatile ester-based oil, and a metal oxide, and a method for preparing the same.
보다 바람직하게는 본 발명은 고형 오일로 하이드로제네이티드 식물성 오일, 비휘발성 에스테르계 오일로 헥실라우레이트, 및 금속산화물을 특정 성분비로 함유하여 지속적인 보습 효과를 가지는 유중 수형 에멀젼 화장료 조성물, 및 이의 제조방법을 제공한다.More preferably, the present invention is a water-in-oil emulsion cosmetic composition containing hydrogenated vegetable oil as a solid oil, hexylaurate as a non-volatile ester oil, and a metal oxide in a specific component ratio to have a continuous moisturizing effect, and a method for producing the same provides
그러나 본 발명이 이루고자 하는 기술적 과제는 이상에서 언급한 과제에 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업계에서 통상의 지식을 가진 자에게 명확하게 이해될 수 있을 것이다.However, the technical problem to be achieved by the present invention is not limited to the above-mentioned problems, and other problems not mentioned will be clearly understood by those skilled in the art from the following description.
이하, 본원에 기재된 다양한 구체예가 도면을 참조로 기재된다. 하기 설명에서, 본 발명의 완전한 이해를 위해서, 다양한 특이적 상세사항, 예컨대, 특이적 형태, 조성물 및 공정 등이 기재되어 있다. 그러나, 특정의 구체예는 이들 특이적 상세 사항 중 하나 이상 없이, 또는 다른 공지된 방법 및 형태와 함께 실행될 수 있다. 다른 예에서, 공지된 공정 및 제조 기술은 본 발명을 불필요하게 모호하게 하지 않게 하기 위해서, 특정의 상세사항으로 기재되지 않는다. "한 가지 구체예" 또는 "구체예"에 대한 본 명세서 전체를 통한 참조는 구체예와 결부되어 기재된 특별한 특징, 형태, 조성 또는 특성이 본 발명의 하나 이상의 구체예에 포함됨을 의미한다. 따라서, 본 명세서 전체에 걸친 다양한 위치에서 표현된 "한 가지 구체예에서" 또는 "구체예"의 상황은 반드시 본 발명의 동일한 구체예를 나타내지는 않는다. 추가로, 특별한 특징, 형태, 조성, 또는 특성은 하나 이상의 구체예에서 어떠한 적합한 방법으로 조합될 수 있다.Hereinafter, various embodiments described herein are described with reference to the drawings. In the following description, numerous specific details are set forth, such as specific forms, compositions and processes, etc., in order to provide a thorough understanding of the present invention. However, certain embodiments may be practiced without one or more of these specific details, or with other known methods and forms. In other instances, well known processes and manufacturing techniques have not been described in specific detail in order not to unnecessarily obscure the present invention. Reference throughout this specification to “one embodiment” or “an embodiment” means that a particular feature, form, composition or characteristic described in connection with the embodiment is included in one or more embodiments of the invention. Thus, the appearances of "in one embodiment" or "an embodiment" in various places throughout this specification do not necessarily refer to the same embodiment of the invention. Additionally, particular features, forms, compositions, or properties may be combined in one or more embodiments in any suitable way.
명세서에서 특별한 정의가 없으면 본 명세서에 사용된 모든 과학적 및 기술적인 용어는 본 발명이 속하는 기술분야에서 당업자에 의하여 통상적으로 이해되는 것과 동일한 의미를 가진다.Unless otherwise defined in the specification, all scientific and technical terms used herein have the same meaning as commonly understood by a person skilled in the art to which the present invention belongs.
명세서 전체에서, 어떤 부분이 어떤 구성요소를 "포함"한다고 할 때, 이는 특별히 반대되는 기재가 없는 한 다른 구성요소를 제외하는 것이 아니라 다른 구성요소를 더 포함할 수 있는 것을 의미한다.Throughout the specification, when a certain component is said to "include", it means that it may further include other components without excluding other components unless otherwise stated.
본 발명은 고형 오일, 비휘발성 에스테르계 오일, 및 금속산화물을 특정 성분비로 함유하여 지속적인 보습 효과를 가지는 유중 수형 에멀젼 화장료 조성물을 제공한다.The present invention provides a water-in-oil emulsion cosmetic composition containing a solid oil, a non-volatile ester-based oil, and a metal oxide in a specific component ratio and having a continuous moisturizing effect.
상기의 "고형 오일"이란 고형(solid)의 성질을 유지하는 오일 성분인 것이고, 에스테르, 탄화수소, 천연 유래 왁스, 및 실리콘 오일 중 하나 이상에서 선택되는 유상 성분인 것일 수 있으며, 바람직하게는 천연 유래 왁스로서 밀납(bees wax), 카나우바 왁스(carnauba wax), 칸데릴라 왁스(candelilla wax), 셀락 왁스(sellac wax), 쌀겨 왁스(rice bran wax), 카프릴릭 카프릭 미리스틱 스테아릭 트리글리세라이드(caprylic capric myristic stearic triglyceride), 하이드로제네이티드 식물성 오일(hydrogenated vegetable oil), 트리베헤닌(tribehenin), 글리세릴 트리베헤네이트(glyceryl tribehenate), 야자씨드 버터(Astrocaryum Mmurumuru seed butter), 및 호호바 에스테르(jojoba ester)로 이루어진 군에서 선택되는 하나 이상의 유상 성분일 수 있으며, 보다 바람직하게는 하이드로제네이티드 식물성 오일일 수 있다. The above "solid oil" is an oil component that maintains the properties of a solid, and may be an oil component selected from one or more of esters, hydrocarbons, natural waxes, and silicone oils, preferably of natural origin. Waxes include bees wax, carnauba wax, candelilla wax, cellac wax, rice bran wax, caprylic capric myristic stearic triglyceride (caprylic capric myristic stearic triglyceride), hydrogenated vegetable oil, tribehenin, glyceryl tribehenate, palm seed butter (Astrocaryum Mmurumuru seed butter), and jojoba esters ( jojoba ester), and more preferably hydrogenated vegetable oil.
상기의 "비휘발성 에스테르계 오일"이란 휘발 성질이 제한되며 에스터 결합 구조를 가지는 유상 성분인 것으로, 헥실라우레이트(Hexyl laurate), 다이카프릴릴 카보네이트(Dicaprylyl carbonate), 다이아이소스테아릴 말레이트(Diisostearyl malate), 부틸렌 글라이콜다이카프릴레이트/다이카프레이트(Butylene glycol dicaprylate/dicaprate), 세틸 에틸헥사노에이트(Cetyl ethylhexanoate), 트리에틸헥사노인(Triethylhexanoin), 다이세테아릴 다이머 다이리놀리에이트(Dicetearyl dimer dilinoleate), 카프릴릭/카프릭 트라이글리세라이드(Caprylic/Capric Triglyceride), 폴리글리세릴-2 트라이아이소스테아레이트(Polyglyceryl-2 Triisostearate), 옥틸도데실 스테아로일 스테아레이트(Octyldodecyl Stearoyl Stearate) 및 펜타에리스리틸 테트라아이소스테아레이트(Pentaerythrityl Tetraisostearate)로 이루어진 에스테르계 오일 군에서 선택되는 하나 이상일 수 있다.The above "non-volatile ester-based oil" is an oily component having limited volatility and an ester bond structure, and includes hexyl laurate, dicaprylyl carbonate, diisostearyl maleate ( Diisostearyl malate), Butylene glycol dicaprylate/dicaprate, Cetyl ethylhexanoate, Triethylhexanoin, Dicetearyl Dimer Dicetearyl dimer dilinoleate, Caprylic/Capric Triglyceride, Polyglyceryl-2 Triisostearate, Octyldodecyl Stearoyl Stearate Stearoyl Stearate) and pentaerythrityl tetraisostearate (Pentaerythrityl Tetraisostearate) may be at least one selected from the group of ester-based oils.
상기의 "금속산화물"이란 산소와 결합한 금속 화합물의 총칭으로, 파우더 형태의 착색제로서 컨실러 조성물에서 활용도가 높다. 종류에 따라 수분이나 유분을 흡수하는 특징을 가지며, 코팅 처리되어 흡유력 있는 파우더는 그 함량에 따라 컨실러 내용물의 유분감을 조절할 수 있다. 흡유력을 가지는 파우더 성상으로서 티타늄디옥사이드(Titanium Dioxide), 황색산화철(CI 77492), 적색산화철(CI 77491), 흑색산화철(CI 77499), 알루미늄하이드록사이드(Aluminium hydroxide), 다이소듐스테아로일글루타메이트(Disodium Stearoyl Glutamate), 트라이에톡시카프릴릴실레인(Triethoxycaprylylsilane), 아이소프로필티타늄트라이아이소스테아레이트(Isopropyl Titanium Triisostearate) 등 종래 화장료 조성물에 포함되는 금속산화물로 이용이 알려진 것이라면 제한없이 이용할 수 있다.The above "metal oxide" is a general term for metal compounds combined with oxygen, and is highly utilized in concealer compositions as a colorant in a powder form. Depending on the type, it has a characteristic of absorbing moisture or oil, and the oil-absorbent powder coated with oil can adjust the oiliness of the concealer contents according to its content. As a powder with oil absorption, titanium dioxide, yellow iron oxide (CI 77492), red iron oxide (CI 77491), black iron oxide (CI 77499), aluminum hydroxide, disodium stearoyl glutamate (Disodium Stearoyl Glutamate), triethoxycaprylylsilane (Triethoxycaprylylsilane), isopropyl titanium triisostearate (Isopropyl Titanium Triisostearate), etc. As long as it is known to be used as a metal oxide included in conventional cosmetic compositions, it can be used without limitation.
본 발명은 고형 오일로 하이드로제네이티드 식물성 오일, 비휘발성 에스테르계 오일로 헥실라우레이트, 및 금속산화물을 특정 성분비로 함유하여 지속적인 보습 효과를 가지는 유중 수형 에멀젼 화장료 조성물을 제공한다.The present invention provides a water-in-oil emulsion cosmetic composition containing hydrogenated vegetable oil as a solid oil, hexylaurate as a non-volatile ester-based oil, and a metal oxide in a specific ratio to have a continuous moisturizing effect.
상기 고형 오일로서의 하이드로제네이티드 식물성 오일은 식물성 오일의 탄화수소 작용기에 수소첨가(Hydrogenation)하여 액정(액체와 고체의 중간 상태에 있는 물질)을 형성하는 물질로 상온에서는 왁스와 같은 고형을 유지하나, 성분 자체가 지질이기에 왁스와 구분되며 높은 보습감을 가진다. 탄화수소 작용기가 많아 오일과 상용성이 우수하며 흐름성이 높은 오일 성분에 고르게 분산되어 피부에 잘 부착되도록 붙잡아주는 기능을 가진다. 본 발명의 화장료 조성물에 있어서 상기 하이드로제네이티드 식물성 오일은 하이드로제네이티드 올리브 오일, 하이드로제네이티드 쌀겨 오일, 하이드로제네이티드 캐스터 오일, 하이드로제네이티드 코코넛 오일, 하이드로제네이티드 알로에 오일 등 식물 성분 유래의 하이드로제네이티드 오일이라면 제한없이 이용할 수 있다. 또한 본 발명의 화장료 조성물에 있어서 상기 하이드로제네이티드 식물성 오일은 전체 화장료 조성물 중 20 중량% 이하로, 10 중량% 이하로, 또는 5 중량% 이하로 포함될 수 있고, 바람직하게는 0.1 중량% 초과 내지 4 중량% 미만으로 포함될 수 있으며, 더욱 바람직하게는 1 내지 4 중량%로 포함될 수 있으며, 가장 바람직하게는 1 내지 3 중량%로 포함될 수 있다. 본 발명의 결과에 따르면 화장료 조성물 내 고형 오일의 함량이 전혀 포함되지 않는 경우에는 오일 흐름성이 높아 파우더 밀착력이 저하되어 커버력이 저하되고, 함량이 4 중량% 이상인 경우에는 흡수가 느리고 발림이 두꺼워 파우더 밀착력이 저하되어 커버력이 저하된다.The hydrogenated vegetable oil as the solid oil is a material that forms a liquid crystal (a material in an intermediate state between a liquid and a solid) by hydrogenating the hydrocarbon functional group of the vegetable oil, and maintains a wax-like solid at room temperature, but the component Because it is a lipid itself, it is distinguished from wax and has a high moisturizing effect. It has excellent compatibility with oil because it has many hydrocarbon functional groups and is evenly dispersed in oil components with high flowability to hold onto the skin so that it adheres well. In the cosmetic composition of the present invention, the hydrogenated "vegetable" oil is derived from plant ingredients such as hydrogenated "olive" oil, hydrogenated "rice bran" oil, hydrogenated "castor" oil, hydrogenated "coconut" oil, and hydrogenated "aloe" oil. Ted oil can be used without restrictions. In addition, in the cosmetic composition of the present invention, the hydrogenated vegetable oil may be included in 20% by weight or less, 10% by weight or less, or 5% by weight or less, preferably more than 0.1% by weight to 4% by weight of the total cosmetic composition. It may be included in less than weight%, more preferably 1 to 4% by weight, and most preferably 1 to 3% by weight. According to the results of the present invention, when the content of the solid oil in the cosmetic composition is not included at all, the oil flowability is high, and the adhesion of the powder is reduced, resulting in a decrease in the coverage. Adhesion is lowered and coverage is lowered.
상기 비휘발성 에스테르계 오일로 헥실라우레이트는 헥실알코올과 라우릭애씨드의 에스터이다. 본 발명의 화장료 조성물에 있어서 상기 헥실라우레이트는 전체 화장료 조성물 중 50 중량% 이하로, 40 중량% 이하로, 30 중량% 이하고, 또는 25 중량% 이하로 포함될 수 있고, 바람직하게는 0.1 중량% 초과 내지 35 중량% 미만으로 포함될 수 있으며, 더욱 바람직하게는 1 내지 30 중량%로 포함될 수 있으며, 가장 바람직하게는 5 내지 10 중량%로 포함될 수 있다. 본 발명의 결과에 따르면 화장료 조성물 내 비휘발성 에스테르계 오일의 함량이 전혀 포함되지 않는 경우에는 화장료 조성물의 보습감이 시간이 경과할수록 현저히 저하되나, 화장료 조성물 내 비휘발성 에스테르계 오일의 함량이 15 중량% 이상 포함되는 경우에 오일 흐름성이 높아 파우더 밀착력이 저하되어 커버력이 저하된다.As the non-volatile ester-based oil, hexyllaurate is an ester of hexyl alcohol and lauric acid. In the cosmetic composition of the present invention, the hexylaurate may be included in 50% by weight or less, 40% by weight or less, 30% by weight or less, or 25% by weight or less, preferably 0.1% by weight of the total cosmetic composition. It may be included in more than 35% by weight, more preferably 1 to 30% by weight, and most preferably 5 to 10% by weight. According to the results of the present invention, when the content of the non-volatile ester-based oil in the cosmetic composition is not included at all, the moisturizing feeling of the cosmetic composition decreases significantly over time, but the content of the non-volatile ester-based oil in the cosmetic composition is 15% by weight If it is included more than that, the oil flowability is high and the powder adhesion is lowered, resulting in a lowered coverage.
상기 금속산화물은 전체 화장료 조성물 중 55 중량% 이하로, 45 중량% 이하로, 또는 35 중량% 이하로 포함될 수 있고, 바람직하게는 0.1 내지 40 중량%로 포함될 수 있으며, 더욱 바람직하게는 0.1 내지 35 중량%로 포함될 수 있으며, 가장 바람직하게는 15 내지 35 중량%로 포함될 수 있다. 본 발명의 결과에 따르면 화장료 조성물 내 금속산화물의 함량이 45 중량% 미만으로 포함되는 경우에 보습감이 안정적으로 유지된다. 커버력의 경우에는 금속산화물의 함량이 5 중량% 초과 내지 45 중량% 미만으로 포함되는 경우에 안정적으로 유지된다.The metal oxide may be included in 55% by weight or less, 45% by weight or less, or 35% by weight or less in the total cosmetic composition, preferably 0.1 to 40% by weight, more preferably 0.1 to 35% by weight. It may be included in weight%, and most preferably may be included in 15 to 35% by weight. According to the results of the present invention, when the content of metal oxide in the cosmetic composition is less than 45% by weight, the moisturizing feeling is stably maintained. In the case of covering power, it is stably maintained when the content of the metal oxide is included in more than 5% by weight and less than 45% by weight.
본 발명의 화장료 조성물은 상기 고형 오일로 하이드로제네이티드 식물성 오일, 비휘발성 에스테르계 오일로 헥실라우레이트, 및 금속산화물 이외에 추가로 폴리글리세릴-6폴리리시놀리에이트(Polyglyceryl-6 Polyricinoleate), 폴리글리세릴-6폴리하이드록시스테아레이트(Polyglyceryl-6 Polyhydroxystearate), 솔비탄올리베이트(Sorbitan Olivate), 및 솔비탄세스퀴올리에이트(Sorbitan Sesquioleate)를 유화제 또는 분산제, 제형 안정화 등의 목적으로 포함할 수 있다. 이러한 경우에, 폴리글리세릴-6폴리리시놀리에이트: 폴리글리세릴-6폴리하이드록시스테아레이트: 솔비탄올리베이트: 솔비탄세스퀴올리에이트는 1: 1: 2: 2의 중량% 비율로 포함될 수 있다. 또한, 본 발명의 화장료 조성물은 다이스테아다이모늄헥토라이트(Disteardimonium Hectorite)를 분산력 향상, 제형의 점도 조절 또는 안정화 등의 목적으로서 0 내지 2 중량%의 양으로 포함할 수 있고, 보론나이트라이드(Boron Nitride)을 불투명화제 또는 미끄럼개선제 등의 목적으로서 0 내지 5 중량%의 양으로 포함할 수 있으며, 폴리글리세릴-2아이소스테아레이트/다이머다이리놀리에이트코폴리머(Polyglyceryl-2 Isostearate/Dimer Dilinoleate Copolymer)를 점증제, 수분차단제 또는 밀착력 향상 등의 목적으로서 0 내지 2 중량%의 양으로 포함할 수 있으며, 소듐클로라이드(Sodium Chloride)를 수용성 전해질로서 제형 안정화 목적으로서 0.5 내지 1.5 중량%의 양으로 포함할 수 있으며, 글리세린(Glycerin)을 보습제, 피부 컨디셔닝제 또는 점도 감소제 등의 목적으로서 0 내지 2 중량%의 양으로 포함할 수 있으며, 방부 목적으로 1,2-헥산디올(1,2-Hexanediol), 및/또는 펜틸렌글라이콜(Pentylene Glycol)을 0.2 내지 1 중량%의 양으로 포함할 수 있으며, 또는 잔부 용매로 물, 정제수, 또는 알코올을 포함할 수 있으나, 이에 제한되는 것은 아니다.The cosmetic composition of the present invention further contains polyglyceryl-6 polyricinoleate, polyglyceryl-6 polyricinoleate in addition to hydrogenated vegetable oil as the solid oil, hexylaurate as the non-volatile ester oil, and metal oxide. Polyglyceryl-6 Polyhydroxystearate, Sorbitan Olivate, and Sorbitan Sesquioleate may be included for the purpose of emulsifier or dispersant, formulation stabilization, and the like. In this case, polyglyceryl-6 polyricinoleate: polyglyceryl-6 polyhydroxystearate: sorbitan olivate: sorbitan sesquioleate may be included in a weight percent ratio of 1: 1: 2: 2. there is. In addition, the cosmetic composition of the present invention may include disteardimonium hectorite in an amount of 0 to 2% by weight for the purpose of improving dispersion, adjusting or stabilizing the viscosity of the formulation, and boron nitride ( Boron Nitride) may be included in an amount of 0 to 5% by weight for the purpose of an opacifier or slip improver, and polyglyceryl-2 isostearate / dimer dilinoleate copolymer (Polyglyceryl-2 Isostearate / Dimer Dilinoleate Copolymer) in an amount of 0 to 2% by weight for the purpose of thickening agent, moisture barrier or improving adhesion, and sodium chloride as a water-soluble electrolyte in an amount of 0.5 to 1.5% by weight for the purpose of stabilizing the formulation. It may contain glycerin in an amount of 0 to 2% by weight for purposes such as a moisturizer, skin conditioning agent or viscosity reducing agent, and 1,2-hexanediol (1,2- Hexanediol), and/or pentylene glycol (Pentylene Glycol) in an amount of 0.2 to 1% by weight, or may include water, purified water, or alcohol as the remaining solvent, but is not limited thereto.
본 발명의 화장료 조성물은 유중수형(W/O)인 것이며, 이는 연속상이 오일, 분산상이 수상인 것이 바람직하다. The cosmetic composition of the present invention is a water-in-oil (W/O) type, and it is preferable that the continuous phase is an oil and the dispersed phase is an aqueous phase.
또한 본 발명에 있어서, 상기 화장료 조성물은 화장수, 영양 로션, 영양 에센스, 마사지 크림, 미용목욕물 첨가제, 바디 로션, 바디 밀크, 배스 오일, 베이비 오일, 베이비파우더, 샤워겔, 샤워크림, 선스크린 로션, 선스크린 크림, 선탠 크림, 스킨 로션, 스킨 크림, 자외선차단용 화장품, 컨실러, 클렌징밀크, 탈모제화장용, 페이스 및 바디로션, 페이스 및 바디크림, 피부미백크림, 핸드로션, 헤어로션, 화장용크림, 쟈스민 오일, 목욕비누, 물비누, 미용비누, 샴푸, 손세정제(핸드클리너), 약용비누비의료용, 크림비누, 페이셜워시, 전신 세정제, 두피 세정제, 헤어린스, 화장비누, 치아미백용 겔, 치약 등의 형태로 제조될 수 있고, 바람직하게는 컨실러 형태로 제조될 수 있다. 이를 위해 본 발명의 조성물은 화장료 조성물의 제조에 통상적으로 사용하는 용매나, 적절한 담체, 부형제 또는 희석제를 더 포함할 수 있다.In addition, in the present invention, the cosmetic composition is lotion, nutrient lotion, nutrient essence, massage cream, beauty bath water additive, body lotion, body milk, bath oil, baby oil, baby powder, shower gel, shower cream, sunscreen lotion, Sunscreen cream, suntan cream, skin lotion, skin cream, sunscreen cosmetics, concealer, cleansing milk, depilatory makeup, face and body lotion, face and body cream, skin whitening cream, hand lotion, hair lotion, cosmetic cream , Jasmine oil, bath soap, water soap, beauty soap, shampoo, hand sanitizer (hand cleaner), medicated soap, medical soap, cream soap, facial wash, body cleanser, scalp cleanser, hair rinse, cosmetic soap, tooth whitening gel, toothpaste It may be prepared in the form of a back, preferably in the form of a concealer. To this end, the composition of the present invention may further include a solvent or an appropriate carrier, excipient or diluent commonly used in the preparation of cosmetic compositions.
본 발명에 있어서 상기 화장료 조성물 내에 더 추가될 수 있는 용매의 종류는 특별히 한정하지 않으나, 예를 들어, 물, 식염수, DMSO 또는 이들의 조합을 사용할 수 있다. 또한, 담체, 부형제 또는 희석제로는 정제수, 오일, 왁스, 지방산, 지방산 알콜, 지방산 에스테르, 계면활성제, 흡습제(humectant), 증점제, 항산화제, 점도 안정화제, 킬레이팅제, 완충제, 저급 알콜 등이 포함되지만, 이에 제한되는 것은 아니다. 또한, 필요에 따라 미백제, 보습제, 비타민, 자외선차단제, 향수, 염료, 항생제, 항박테리아제, 항진균제를 포함할 수 있다.In the present invention, the type of solvent that can be further added to the cosmetic composition is not particularly limited, but, for example, water, saline, DMSO, or a combination thereof may be used. In addition, carriers, excipients or diluents include purified water, oil, wax, fatty acids, fatty alcohols, fatty acid esters, surfactants, humectants, thickeners, antioxidants, viscosity stabilizers, chelating agents, buffers, lower alcohols, and the like. Includes, but is not limited to. In addition, whitening agents, moisturizing agents, vitamins, sunscreens, perfumes, dyes, antibiotics, antibacterial agents, and antifungal agents may be included as necessary.
본 발명의 화장료 조성물에서 상기 오일로서는 탄화수소계 오일, 실리콘계 오일, 수소화 식물성유, 피마자유, 면실유, 올리브유, 야자인유, 호호바유, 아보카도유가 이용될 수 있으며, 왁스로는 밀랍, 경랍, 카르나우바, 칸델릴라, 몬탄, 세레신, 액체 파라핀, 라놀린이 추가로 이용될 수 있다.In the cosmetic composition of the present invention, hydrocarbon-based oil, silicone-based oil, hydrogenated vegetable oil, castor oil, cottonseed oil, olive oil, coconut oil, jojoba oil, and avocado oil may be used as the oil, and beeswax, spermaceti, and carnauba may be used as the wax. , candelilla, montan, ceresin, liquid paraffin, lanolin may additionally be used.
본 발명의 화장료 조성물에서 상기 지방산으로는 스테아르산, 리놀레산, 리놀렌산, 올레산이 이용될 수 있고, 지방산 알콜로는 세틸 알콜, 옥틸 도데칸올, 올레일 알콜, 판텐올, 라놀린 알콜, 스테아릴 알콜, 헥사데칸올이 이용될 수 있으며 지방산 에스테르로는 이소프로필 미리스테이트, 이소프로필 팔미테이트, 부틸 스테아레이트가 이용될 수 있다. 계면 활성제로는 당업계에 알려진 양이온 계면활성제, 음이온 계면활성제 및 비이온성 계면활성제가 사용 가능하며 가능한 한 천연물 유래의 계면활성제가 바람직하다. In the cosmetic composition of the present invention, stearic acid, linoleic acid, linolenic acid, and oleic acid may be used as the fatty acid, and cetyl alcohol, octyl dodecanol, oleyl alcohol, panthenol, lanolin alcohol, stearyl alcohol, and hexadecyl alcohol may be used as the fatty acid. Decanol may be used, and isopropyl myristate, isopropyl palmitate, and butyl stearate may be used as the fatty acid ester. As the surfactant, cationic surfactants, anionic surfactants, and nonionic surfactants known in the art can be used, and surfactants derived from natural products are preferred as much as possible.
본 발명의 화장료 조성물에서 그 외에도 화장품 분야에서 널리 알려진 흡습제, 증점제, 항산화제 등을 포함할 수 있으며, 이들의 종류와 양은 당업계에 공지된 바에 따른다.In addition, the cosmetic composition of the present invention may include a moisture absorbent, a thickener, an antioxidant, and the like, which are widely known in the field of cosmetics, and the types and amounts thereof are known in the art.
또한 본 발명에 있어서 상기 화장료 조성물은 색조를 포함할 수 있다.In addition, in the present invention, the cosmetic composition may include a color tone.
또한 본 발명에 있어서 상기 화장료 조성물은 에멀젼의 형태로서 파우더 내에 포함될 수 있고, 상기 파우더는 탤크, 카올린, 마이카, 세리사이트, 실리카, 실리카디메칠실릴레이트, 나일론-12, 메틸메타크릴레이트크로스폴리머, 폴리메틸메타크릴레이트, 보론나이트라이드, 알루미나, 티타늄디옥사이드, 징크옥사이드, 산화철, 실리카, 펄, 유기 염료, 레이크, 및 유기 안료로 이루어진 군으로부터 선택된 어느 하나 이상의 혼합물일 수 있으며, 당업계에서 통상적으로 사용되는 파우더류에 해당한다면 이에 제한되는 것은 아니다. In addition, in the present invention, the cosmetic composition may be included in a powder in the form of an emulsion, and the powder may include talc, kaolin, mica, sericite, silica, silica dimethyl silylate, nylon-12, methyl methacrylate crosspolymer, It may be any one or more mixtures selected from the group consisting of polymethyl methacrylate, boron nitride, alumina, titanium dioxide, zinc oxide, iron oxide, silica, pearl, organic dyes, lakes, and organic pigments, and is commonly used in the art. If it corresponds to the type of powder used, it is not limited thereto.
또한 본 발명의 화장료 조성물은 피부 항산화, 미백, 항염, 및 주름 억제 기능성 화장료 조성물로서 이용될 수 있다. 이러한 경우에, 상기 피부 항산화는 피부의 산화를 억제한다는 것으로, 세포의 노화를 억제하는 개념이다. 개체의 호흡을 통해 체내로 들어온 산소는 인체에 필요한 에너지를 만드는 것과 동시에 유해한 여분의 산소인 활성산소(Free Radical)를 생성한다. 활성산소는 체내의 정상 세포를 공격하여 노화나 각종 질병의 원인으로 작용하므로, 활성산소를 제거하는 것이 세포의 산화(노화)를 막는 방법이며, 이러한 세포의 산화를 억제하는 것이 항산화이다. 대표적인 항산화 물질로는 비타민C(키위, 양배추 등에 다량 함유), 비타민E(아몬드, 해바라기씨 등에 다량 함유), 베타카로틴(당근, 토마토 등에 다량 함유), 셀레늄(각종 해산물에 다량 함유됨) 등이 있다. 상기 미백은 피부가 자외선에 지속적으로 노출되어 멜라닌 세포가 증가하고 그로 인해 피부에 멜라닌 색소가 과도하게 침착되는 것을 방지하거나, 기존에 침착된 멜라닌 색소를 엷게 하는 기능을 일컫는다. 이에 따라, 과도한 멜라닌 색소의 침착으로 생기는 기미, 주근깨, 검버섯, 및 흑색종의 생성을 억제할 수 있다. 상기 항염은 염증을 가라앉히고 저항하는 효능을 의미한다. 화장료에 있어서 항염 기능은 피부를 보호하고 안정시키며, 소독과 살균작용을 하는 것으로 볼 수 있다. 상기 주름은 햇빛을 포함하여 여러 가지 요인에 의해서 진피 속의 콜라겐섬유, 탄력섬유 등에 변성이 일어나고, 피부 수분이 감소하여 피부의 탄력이 떨어져 피부가 접히게 되는 현상이다. 피하 지방의 흡수도 주름을 더욱 악화시킨다. 노화된 피부에서는 Extracellular Matrix의 대부분을 차지하는 콜라겐 섬유의 저하와 히알루론산, 세라마이드 등 피부 성분의 변화로 주름이 생성되고 피부 보습력이 떨어져 건조하고 탄력을 잃는다. 노화된 피부에서는 진피와 표피 세포의 수가 감소하고, 세포의 기능이 저하되어 주름 형성, 색소 침착, 건성, 두터운 피부, 탄성 감소가 나타난다. 자외선에 노출되면 피부에서 MMP(Matrix Metalloproteinase) 생성을 유도하는데, 이 MMP는 콜라겐, 엘라스틴, 프로테오글리칸과 같은 Extracellular MatrixECM 단백질의 저하를 일으킨다. 이 중, MMP-1은 콜라겐 분해효소로서 피부의 주요 형태인 제1형 콜라겐(COL1A1)과 3형 콜라겐(COL3A1)을 분해한다. 자연적으로 노화된 피부와 광노화된 피부에서 콜라겐 합성이 감소하는 것으로 보고되었다. 따라서 항주름 또는 주름 억제란 주름의 생성을 지연시키거나, 억제하거나, 개선하는 것을 의미한다. In addition, the cosmetic composition of the present invention can be used as a skin antioxidant, whitening, anti-inflammatory, and anti-wrinkle functional cosmetic composition. In this case, the skin antioxidant inhibits oxidation of the skin, which is a concept of inhibiting cell aging. Oxygen that enters the body through the breathing of the object creates energy necessary for the human body and at the same time creates free radicals, which are harmful extra oxygen. Since active oxygen attacks normal cells in the body and acts as a cause of aging or various diseases, removing active oxygen is a way to prevent oxidation (aging) of cells, and suppressing such oxidation of cells is antioxidant. Representative antioxidants include vitamin C (contained in large amounts in kiwi, cabbage, etc.), vitamin E (contained in large amounts in almonds, sunflower seeds, etc.), beta-carotene (contained in large amounts in carrots, tomatoes, etc.), and selenium (contained in large amounts in various seafood). there is. The whitening refers to a function of preventing melanin pigment from being excessively deposited on the skin or thinning the previously deposited melanin pigment because the skin is continuously exposed to ultraviolet rays to increase melanocytes. Accordingly, it is possible to suppress the formation of melasma, freckles, age spots, and melanoma caused by the deposition of excessive melanin pigment. The anti-inflammatory means the efficacy of relieving and resisting inflammation. In cosmetics, the anti-inflammatory function can be seen as protecting and stabilizing the skin, and disinfecting and sterilizing. The wrinkles are a phenomenon in which degeneration occurs in collagen fibers, elastic fibers, etc. in the dermis due to various factors including sunlight, and skin moisture decreases and the elasticity of the skin decreases and the skin folds. Absorption of subcutaneous fat also exacerbates wrinkles. In aging skin, wrinkles are formed due to the degradation of collagen fibers, which make up most of the extracellular matrix, and changes in skin components such as hyaluronic acid and ceramide, and the skin's moisturizing ability decreases, resulting in dryness and loss of elasticity. In aged skin, the number of dermal and epidermal cells decreases, and cell function deteriorates, resulting in wrinkle formation, pigmentation, dryness, thick skin, and loss of elasticity. Exposure to UV rays induces the production of MMP (Matrix Metalloproteinase) in the skin, which causes the degradation of Extracellular MatrixECM proteins such as collagen, elastin, and proteoglycan. Among them, MMP-1 is a collagen degrading enzyme that degrades type 1 collagen (COL1A1) and type 3 collagen (COL3A1), which are the main types of skin. Decreased collagen synthesis has been reported in both naturally aged and photoaged skin. Accordingly, anti-wrinkle or anti-wrinkle means to retard, inhibit or ameliorate the formation of wrinkles.
또한 본 발명은 고형 오일로 하이드로제네이티드 식물성 오일, 비휘발성 에스테르계 오일로 헥실라우레이트, 및 금속산화물을 특정 성분비로 함유하여 지속적인 보습 효과를 가지는 유중 수형 에멀젼 화장료 조성물의 제조방법을 제공한다.In addition, the present invention provides a method for preparing a water-in-oil emulsion cosmetic composition having a continuous moisturizing effect by containing hydrogenated vegetable oil as a solid oil, hexylaurate as a non-volatile ester oil, and a metal oxide in a specific ratio.
상기 제조방법은 고형 오일, 비휘발성 에스테르계 오일, 및 금속산화물을 혼합하는 단계;를 포함한다. 이러한 경우에, 상기 제조방법은 밀납(bees wax), 카나우바 왁스(carnauba wax), 칸데릴라 왁스(candelilla wax), 셀락 왁스(sellac wax), 쌀겨 왁스(rice bran wax), 카프릴릭 카프릭 미리스틱 스테아릭 트리글리세라이드(caprylic capric myristic stearic triglyceride), 하이드로제네이티드 식물성 오일(hydrogenated vegetable oil), 트리베헤닌(tribehenin), 글리세릴 트리베헤네이트(glyceryl tribehenate), 야자씨드 버터(Astrocaryum Mmurumuru seed butter), 및 호호바 에스테르(jojoba ester)로 이루어진 군에서 선택되는 어느 하나 이상의 고형 오일을 전체 화장료 조성물 중 5 중량% 이하로 혼합하는 단계를 포함하는 것일 수 있다. 헥실라우레이트(Hexyl laurate), 다이카프릴릴 카보네이트(Dicaprylyl carbonate), 다이아이소스테아릴 말레이트(Diisostearyl malate), 부틸렌 글라이콜다이카프릴레이트/다이카프레이트(Butylene glycol dicaprylate/dicaprate), 세틸 에틸헥사노에이트(Cetyl ethylhexanoate), 트리에틸헥사노인(Triethylhexanoin), 다이세테아릴 다이머 다이리놀리에이트(Dicetearyl dimer dilinoleate), 카프릴릭/카프릭 트라이글리세라이드(Caprylic/Capric Triglyceride), 폴리글리세릴-2 트라이아이소스테아레이트(Polyglyceryl-2 Triisostearate), 옥틸도데실 스테아로일 스테아레이트(Octyldodecyl Stearoyl Stearate) 및 펜타에리스리틸 테트라아이소스테아레이트(Pentaerythrityl Tetraisostearate)로 이루어진 군에서 선택되는 에스테르계 오일에서 선택되는 어느 하나 이상의 비휘발성 에스테르계 오일을 전체 화장료 조성물 중 35 중량% 이하로 혼합하는 단계를 포함하는 것일 수 있다. 또는 상기 제조방법은 티타늄디옥사이드(Titanium Dioxide), 황색산화철(CI 77492), 적색산화철(CI 77491), 흑색산화철(CI 77499), 알루미늄하이드록사이드(Aluminium hydroxide), 다이소듐스테아로일글루타메이트(Disodium Stearoyl Glutamate), 트라이에톡시카프릴릴실레인(Triethoxycaprylylsilane), 및 아이소프로필티타늄트라이아이소스테아레이트(Isopropyl Titanium Triisostearate)로 이루어진 군에서 선택되는 어느 하나 이상의 금속산화물을 전체 화장료 조성물 중 35 중량% 이하로 혼합하는 단계를 포함하는 것일 수 있다.The manufacturing method includes mixing a solid oil, a non-volatile ester-based oil, and a metal oxide. In this case, the manufacturing method is beeswax, carnauba wax, candelilla wax, shellac wax, rice bran wax, caprylic capric Myristic stearic triglyceride, hydrogenated vegetable oil, tribehenin, glyceryl tribehenate, Astrocaryum Mmurumuru seed butter ), and jojoba ester (jojoba ester), and mixing any one or more solid oils selected from the group consisting of 5% by weight or less of the total cosmetic composition. Hexyl laurate, Dicaprylyl carbonate, Diisostearyl malate, Butylene glycol dicaprylate/dicaprate, Cetyl ethylhexanoate, Triethylhexanoin, Dicetearyl dimer dilinoleate, Caprylic/Capric Triglyceride, Poly In ester-based oils selected from the group consisting of Polyglyceryl-2 Triisostearate, Octyldodecyl Stearoyl Stearate and Pentaerythrityl Tetraisostearate It may include mixing one or more selected non-volatile ester-based oils in an amount of 35% by weight or less of the total cosmetic composition. Alternatively, the manufacturing method is titanium dioxide, yellow iron oxide (CI 77492), red iron oxide (CI 77491), black iron oxide (CI 77499), aluminum hydroxide, disodium stearoyl glutamate (Disodium Stearoyl Glutamate), triethoxycaprylylsilane (Triethoxycaprylylsilane), and isopropyl titanium triisostearate (Isopropyl Titanium Triisostearate) at least one metal oxide selected from the total cosmetic composition 35% by weight or less It may include mixing.
상기 제조방법은 상기 화장료 조성물을 유중수형(W/O) 제형으로 제조하는 단계를 포함하는 것일 수 있다.The manufacturing method may include preparing the cosmetic composition as a water-in-oil (W/O) formulation.
또한 상기 제조방법은 상기 화장료 조성물을 화장수, 영양 로션, 영양 에센스, 마사지 크림, 미용목욕물 첨가제, 바디 로션, 바디 밀크, 배스 오일, 베이비 오일, 베이비파우더, 샤워겔, 샤워크림, 선스크린 로션, 선스크린 크림, 선탠 크림, 스킨 로션, 스킨 크림, 자외선차단용 화장품, 컨실러, 클렌징밀크, 탈모제화장용, 페이스 및 바디로션, 페이스 및 바디크림, 피부미백크림, 핸드로션, 헤어로션, 화장용크림, 쟈스민 오일, 목욕비누, 물비누, 미용비누, 샴푸, 손세정제(핸드클리너), 약용비누비의료용, 크림비누, 페이셜워시, 전신 세정제, 두피 세정제, 헤어린스, 화장비누, 치아미백용 겔, 또는 치약의 형태로 제조하는 단계를 포함하는 것일 수 있다. In addition, the manufacturing method is to use the cosmetic composition as lotion, nutrient lotion, nutrient essence, massage cream, beauty bath water additive, body lotion, body milk, bath oil, baby oil, baby powder, shower gel, shower cream, sunscreen lotion, sunscreen Screen cream, suntan cream, skin lotion, skin cream, sunscreen cosmetics, concealer, cleansing milk, depilatory makeup, face and body lotion, face and body cream, skin whitening cream, hand lotion, hair lotion, cosmetic cream, Jasmine oil, bath soap, water soap, beauty soap, shampoo, hand sanitizer (hand cleaner), medicated soap, medical soap, cream soap, facial wash, body cleanser, scalp cleanser, hair rinse, cosmetic soap, tooth whitening gel, or toothpaste It may be to include the step of preparing in the form of.
이하 본 발명을 실시예에 입각하여 구체적으로 설명한다.Hereinafter, the present invention will be described in detail based on examples.
종래의 컨실러 조성물은 다량의 휘발성 오일을 포함하는 것이 일반적인데, 이는 휘발되는 성질에 의하여 시간이 경과되면 피부에 건조함을 야기하고 금속산화물을 포함하는 화장료 조성물이 갈라지는 문제점이 있었다.Conventional concealer compositions generally contain a large amount of volatile oil, which causes dryness to the skin over time due to its volatilization property and causes a cosmetic composition containing a metal oxide to crack.
본 발명의 고형 오일, 비휘발성 에스테르계 오일, 및 금속 산화물을 포함하는 화장료 조성물은 비휘발성 오일의 흐름성을 제어하면서, 동시에 우수한 보습력을 가지므로, 미용 분야에서 크게 이용될 것으로 기대된다.The cosmetic composition comprising the solid oil, the non-volatile ester-based oil, and the metal oxide of the present invention is expected to be widely used in the cosmetic field because it controls the flowability of the non-volatile oil and at the same time has excellent moisturizing power.
이하, 실시예를 통하여 본 발명을 더욱 상세히 설명하고자 한다. 이들 실시예는 오로지 본 발명을 보다 구체적으로 설명하기 위한 것으로, 본 발명의 요지에 따라 본 발명의 범위가 이들 실시예에 의해 제한되지 않는다는 것은 당업계에서 통상의 지식을 가진 자에 있어서 자명할 것이다.Hereinafter, the present invention will be described in more detail through examples. These examples are only for explaining the present invention in more detail, and it will be apparent to those skilled in the art that the scope of the present invention is not limited by these examples according to the gist of the present invention. .
실시예 1: 화장료 내 적정 고형 오일 함량의 확인Example 1: Confirmation of appropriate solid oil content in cosmetics
고형 오일을 함유하는 유중수형 화장료 조성물의 보습력 및 파우더 부착력 효과 차이를 확인하기 위해, 하기 표 1과 같이 화장료 제형을 제조하여 보습감 및 커버력 평가 실험을 실시하였다. In order to confirm the difference in moisturizing power and powder adhesion effect of the water-in-oil cosmetic composition containing solid oil, a cosmetic formulation was prepared as shown in Table 1 below and an experiment was conducted to evaluate moisturizing feeling and covering power.
구체적으로, 고형 오일로는 하이드로제네이티드 식물성 오일을 이용하였고, 표 1의 유상 성분을 70℃까지 가열하여 용해시킨 뒤, 티타늄디옥사이드를 포함한 금속산화물(착색제) 성분을 투입하여 분산시켰다. 이후, 수상 성분을 70℃까지 가열하여 천천히 투입하고 호모믹서를 이용하여 유화하였다. 이어서 탈포 후 냉각하였다.Specifically, hydrogenated vegetable oil was used as the solid oil, and after dissolving the oily components of Table 1 by heating to 70 ° C., a metal oxide (colorant) component including titanium dioxide was added and dispersed. Thereafter, the aqueous phase component was slowly added by heating to 70 °C and emulsified using a homomixer. It was then cooled after defoaming.
상기 표 1의 비교예 1, 및 제조예 1 내지 5의 조성물에 대하여 보습력과 파우더 부착력을 평가하기 위하여 보습감 및 커버력 평가 시험을 실시하였다. 구체적으로는, 25 내지 45세의 여성 30명을 대상으로 각 화장료 조성물을 적용하여 도포 직후와 8시간 후의 보습감 및 커버력을 평가하도록 하였다. 평가 기준은 아주 양호한 경우 5점, 양호한 경우 4점, 보통인 경우 3점, 약간 불만족인 경우 2점, 매우 불만족인 경우 1점으로 하였고, 1주일 단위로 3회 반복 사용하게 한 후 그 평균 값을 계산하여 하기 표 2에 나타내었다.In order to evaluate the moisturizing power and powder adhesion to the compositions of Comparative Example 1 and Preparation Examples 1 to 5 in Table 1, a moisturizing feeling and coverage evaluation test was conducted. Specifically, each cosmetic composition was applied to 30 women between the ages of 25 and 45, and the moisturizing feeling and covering power immediately after application and 8 hours later were evaluated. The evaluation criteria were 5 points for very good, 4 points for good, 3 points for normal, 2 points for slightly dissatisfied, and 1 point for very unsatisfactory. Calculated and shown in Table 2 below.
평가 결과, 화장료 조성물 내 고형 오일의 함량이 전혀 포함되지 않는 경우에는 오일 흐름성이 높아 파우더 밀착력이 저하되어 커버력이 저하되는 것을 확인할 수 있었고, 함량이 4 중량% 이상인 경우에는 흡수가 느리고 발림이 두꺼워 파우더 밀착력이 저하되어 커버력이 저하되는 것을 확인할 수 있었다. 그러나 고형 오일이 화장료 조성물 내에 1 중량% 이상 내지 3 중량% 이하의 양으로 포함되는 경우에는 보습감과 커버력이 모두 높게 유지되는 것을 확인할 수 있었다.As a result of the evaluation, when the content of solid oil in the cosmetic composition was not included at all, it was confirmed that the oil flowability was high and the powder adhesion was reduced, resulting in a decrease in the coverage. It was confirmed that the powder adhesion was lowered and the covering power was lowered. However, when the solid oil is included in an amount of 1% by weight or more to 3% by weight or less in the cosmetic composition, it was confirmed that both the moisturizing feeling and the covering power are maintained high.
실시예 2: 화장료 내 적정 비휘발성 에스테르계 오일 함량의 확인Example 2: Confirmation of appropriate non-volatile ester-based oil content in cosmetics
고형 오일과 함께 비휘발성 에스테르계 오일을 추가로 함유하는 유중수형 화장료 조성물의 보습력 및 파우더 부착력 효과 차이를 확인하기 위해, 하기 표 3과 같이 화장료 제형을 제조하여 보습감 및 커버력 평가 실험을 실시하였다. In order to confirm the difference in moisturizing power and powder adhesion effect of the water-in-oil cosmetic composition additionally containing a non-volatile ester-based oil along with the solid oil, a cosmetic formulation was prepared as shown in Table 3 below, and an experiment was conducted to evaluate moisturizing feeling and covering power.
구체적으로, 고형 오일로는 하이드로제네이티드 식물성 오일을 이용하였고, 비휘발성 에스테르계 오일로는 헥실라우레이트를 이용하였으며, 표 3의 유상 성분을 70℃까지 가열하여 용해시킨 뒤, 티타늄디옥사이드를 포함한 금속산화물(착색제) 성분을 투입하여 분산시켰다. 이후, 수상 성분을 70℃까지 가열하여 천천히 투입하고 호모믹서를 이용하여 유화하였다. 이어서 탈포 후 냉각하였다.Specifically, hydrogenated vegetable oil was used as the solid oil, hexylaurate was used as the non-volatile ester oil, and the oily components of Table 3 were dissolved by heating to 70 ° C. An oxide (colorant) component was added and dispersed. Thereafter, the aqueous phase component was slowly added by heating to 70 ° C. and emulsified using a homomixer. It was then cooled after defoaming.
상기 표 3의 비교예 2, 및 제조예 6 내지 10의 조성물에 대하여 보습력과 파우더 부착력을 평가하기 위하여 보습감 및 커버력 평가 시험을 실시하였다. 구체적으로는, 25 내지 45세의 여성 30명을 대상으로 각 화장료 조성물을 적용하여 도포 직후와 8시간 후의 보습감 및 커버력을 평가하도록 하였다. 평가 기준은 아주 양호한 경우 5점, 양호한 경우 4점, 보통인 경우 3점, 약간 불만족인 경우 2점, 매우 불만족인 경우 1점으로 하였고, 1주일 단위로 3회 반복 사용하게 한 후 그 평균 값을 계산하여 하기 표 4에 나타내었다.In order to evaluate the moisturizing power and powder adhesion to the compositions of Comparative Example 2 and Preparation Examples 6 to 10 in Table 3, a moisturizing feeling and coverage evaluation test was conducted. Specifically, each cosmetic composition was applied to 30 women between the ages of 25 and 45, and the moisturizing feeling and covering power immediately after application and 8 hours later were evaluated. The evaluation criteria were 5 points for very good, 4 points for good, 3 points for normal, 2 points for slightly dissatisfied, and 1 point for very unsatisfactory. was calculated and shown in Table 4 below.
평가 결과, 화장료 조성물 내 비휘발성 에스테르계 오일의 함량이 전혀 포함되지 않는 경우에는 보습감이 시간이 경과할수록 현저히 저하되는 것을 확인할 수 있었고, 함량이 15 중량% 이상인 경우에는 오일 흐름성이 높아 파우더 밀착력이 저하되어 커버력이 저하되는 것을 확인할 수 있었다. 그러나 비휘발성 에스테르계 오일이 화장료 조성물 내에 5 중량% 이상 내지 10 중량% 이하의 양으로 포함되는 경우에는 보습감과 커버력이 모두 높게 유지되는 것을 확인할 수 있었다.As a result of the evaluation, when the content of non-volatile ester-based oil in the cosmetic composition was not included at all, it was confirmed that the moisturizing feeling significantly decreased over time, and when the content was 15% by weight or more, the oil flowability was high, and the powder adhesion was It was confirmed that the covering power was lowered. However, when the non-volatile ester-based oil was included in an amount of 5% by weight or more to 10% by weight or less in the cosmetic composition, it was confirmed that both the moisturizing feeling and the covering power were maintained high.
실시예 3: 화장료 내 적정 금속산화물 함량의 확인Example 3: Confirmation of proper metal oxide content in cosmetics
고형 오일, 비휘발성 에스테르계 오일과 함께 금속산화물을 추가로 함유하는 유중수형 화장료 조성물의 보습력 및 파우더 부착력 효과 차이를 확인하기 위해, 하기 표 5와 같이 화장료 제형을 제조하여 보습감 및 커버력 평가 실험을 실시하였다. In order to confirm the difference in moisturizing power and powder adhesion effect of a water-in-oil cosmetic composition additionally containing a metal oxide along with solid oil and non-volatile ester-based oil, a cosmetic formulation was prepared as shown in Table 5 below, and an experiment was conducted to evaluate moisturizing feeling and covering power. did
구체적으로, 고형 오일로는 하이드로제네이티드 식물성 오일을 이용하였고, 비휘발성 에스테르계 오일로는 헥실라우레이트를 이용하였으며, 표 3의 유상 성분을 70℃까지 가열하여 용해시킨 뒤, 티타늄디옥사이드를 포함한 금속산화물(착색제) 성분을 투입하여 분산시켰다. 이후, 수상 성분을 70℃까지 가열하여 천천히 투입하고 호모믹서를 이용하여 유화하였다. 이어서 탈포 후 냉각하였다.Specifically, hydrogenated vegetable oil was used as the solid oil, hexylaurate was used as the non-volatile ester oil, and the oily components of Table 3 were dissolved by heating to 70 ° C. An oxide (colorant) component was added and dispersed. Thereafter, the aqueous phase component was slowly added by heating to 70 °C and emulsified using a homomixer. It was then cooled after defoaming.
상기 표 5의 제조예 11 내지 16의 조성물에 대하여 보습력과 파우더 부착력을 평가하기 위하여 보습감 및 커버력 평가 시험을 실시하였다. 구체적으로는, 25 내지 45세의 여성 30명을 대상으로 각 화장료 조성물을 적용하여 도포 직후와 8시간 후의 보습감 및 커버력을 평가하도록 하였다. 평가 기준은 아주 양호한 경우 5점, 양호한 경우 4점, 보통인 경우 3점, 약간 불만족인 경우 2점, 매우 불만족인 경우 1점으로 하였고, 1주일 단위로 3회 반복 사용하게 한 후 그 평균 값을 계산하여 하기 표 6에 나타내었다.In order to evaluate the moisturizing power and powder adhesion to the compositions of Preparation Examples 11 to 16 in Table 5, a moisturizing feeling and covering power evaluation test was performed. Specifically, each cosmetic composition was applied to 30 women between the ages of 25 and 45, and the moisturizing feeling and covering power immediately after application and 8 hours later were evaluated. The evaluation criteria were 5 points for very good, 4 points for good, 3 points for normal, 2 points for slightly dissatisfied, and 1 point for very unsatisfactory. was calculated and shown in Table 6 below.
평가 결과, 화장료 조성물 내 금속산화물의 함량이 5 중량% 이하로 포함되는 경우에 커버력이 저하되는 것을 확인할 수 있었고, 함량이 45 중량% 이상인 경우에는 보습감이 시간이 경과할수록 현저히 저하되는 것을 확인할 수 있었다. 그러나 금속산화물이 화장료 조성물내에 15 중량% 이상 내지 35 중량% 이하의 경우에는 보습감과 커버력이 안정적으로 유지되는 것을 확인할 수 있었다.As a result of the evaluation, it was confirmed that the coverage decreased when the content of the metal oxide in the cosmetic composition was 5% by weight or less, and when the content was 45% by weight or more, the moisturizing feeling significantly decreased over time. . However, it was confirmed that the moisturizing feeling and covering power were stably maintained when the amount of the metal oxide was 15% by weight or more and 35% by weight or less in the cosmetic composition.
이상으로 본 발명의 특정한 부분을 상세히 기술하였는 바, 당업계의 통상의 지식을 가진 자에게 있어서 이러한 구체적인 기술은 단지 바람직한 구현예일 뿐이며, 이에 본 발명의 범위가 제한되는 것이 아닌 점은 명백하다. 따라서 본 발명의 실질적인 범위는 첨부된 청구항과 그의 등가물에 의하여 정의된다고 할 것이다.Having described specific parts of the present invention in detail above, it is clear that these specific techniques are only preferred embodiments for those skilled in the art, and the scope of the present invention is not limited thereto. Accordingly, the substantial scope of the present invention will be defined by the appended claims and equivalents thereof.
Claims (15)
상기 고형 오일은 전체 화장료 조성물 중 1 내지 3중량%로 포함되는 것이고,
상기 비휘발성 에스테르계 오일은 전체 화장료 조성물 중 5 내지 10 중량%로 포함되는 것이며,
상기 금속산화물은 전체 화장료 조성물 중 15 내지 35 중량%로 포함되는 것이며,
상기 고형 오일은 하이드로제네이티드 식물성 오일(hydrogenated vegetable oil)인 것이고,
상기 비휘발성 에스테르계 오일은 헥실라우레이트(Hexyl laurate)인 것인, 화장료 조성물.
A cosmetic composition comprising a solid oil, a non-volatile ester-based oil, and a metal oxide,
The solid oil is contained in 1 to 3% by weight of the total cosmetic composition,
The non-volatile ester-based oil is included in 5 to 10% by weight of the total cosmetic composition,
The metal oxide is included in 15 to 35% by weight of the total cosmetic composition,
The solid oil is a hydrogenated vegetable oil,
The non-volatile ester-based oil is hexyl laurate (Hexyl laurate), the cosmetic composition.
상기 금속산화물은 티타늄디옥사이드(Titanium Dioxide), 황색산화철(CI 77492), 적색산화철(CI 77491), 흑색산화철(CI 77499), 알루미늄하이드록사이드(Aluminium hydroxide), 다이소듐스테아로일글루타메이트(Disodium Stearoyl Glutamate), 트라이에톡시카프릴릴실레인(Triethoxycaprylylsilane), 및 아이소프로필티타늄트라이아이소스테아레이트(Isopropyl Titanium Triisostearate)로 이루어진 군에서 선택되는 어느 하나 이상인 것인, 화장료 조성물.
According to claim 1,
The metal oxides are titanium dioxide, yellow iron oxide (CI 77492), red iron oxide (CI 77491), black iron oxide (CI 77499), aluminum hydroxide, disodium stearoyl glutamate Glutamate), triethoxycaprylyl silane (Triethoxycaprylylsilane), and isopropyl titanium triisostearate (Isopropyl Titanium Triisostearate) will at least one selected from the group consisting of, a cosmetic composition.
상기 화장료 조성물은 유중수형(W/O) 제형인 것인, 화장료 조성물.
According to claim 1,
The cosmetic composition is a water-in-oil (W / O) formulation, the cosmetic composition.
상기 화장료 조성물은 화장수, 영양 로션, 영양 에센스, 마사지 크림, 미용목욕물 첨가제, 바디 로션, 바디 밀크, 배스 오일, 베이비 오일, 베이비파우더, 샤워겔, 샤워크림, 선스크린 로션, 선스크린 크림, 선탠 크림, 스킨 로션, 스킨 크림, 자외선차단용 화장품, 컨실러, 클렌징밀크, 탈모제화장용, 페이스 및 바디로션, 페이스 및 바디크림, 피부미백크림, 핸드로션, 헤어로션, 화장용크림, 쟈스민 오일, 목욕비누, 물비누, 미용비누, 샴푸, 손세정제(핸드클리너), 약용비누비의료용, 크림비누, 페이셜워시, 전신 세정제, 두피 세정제, 헤어린스, 화장비누, 치아미백용 겔, 또는 치약의 형태로 제조되는 것인, 화장료 조성물.
According to claim 1,
The cosmetic composition is cosmetic water, nutrient lotion, nutrient essence, massage cream, beauty bath water additive, body lotion, body milk, bath oil, baby oil, baby powder, shower gel, shower cream, sunscreen lotion, sunscreen cream, suntan cream , skin lotion, skin cream, sun protection cosmetics, concealer, cleansing milk, depilatory cosmetic, face and body lotion, face and body cream, skin whitening cream, hand lotion, hair lotion, cosmetic cream, jasmine oil, bath soap , water soap, beauty soap, shampoo, hand sanitizer (hand cleaner), medicated soap, medical soap, cream soap, facial wash, body cleanser, scalp cleanser, hair rinse, cosmetic soap, tooth whitening gel, or toothpaste That is, a cosmetic composition.
상기 고형 오일은 전체 화장료 조성물 중 1 내지 3중량%로 혼합하는 것이고,
상기 비휘발성 에스테르계 오일은 전체 화장료 조성물 중 5 내지 10 중량%로 혼합하는 것이며,
상기 금속산화물은 전체 화장료 조성물 중 15 내지 35 중량%로 혼합하는 것이며,
상기 고형 오일은 하이드로제네이티드 식물성 오일(hydrogenated vegetable oil)인 것이고,
상기 비휘발성 에스테르계 오일은 헥실라우레이트(Hexyl laurate)인 것인, 화장료 조성물의 제조방법.
A method for producing a cosmetic composition comprising mixing a solid oil, a non-volatile ester-based oil, and a metal oxide,
The solid oil is to be mixed in 1 to 3% by weight of the total cosmetic composition,
The non-volatile ester-based oil is mixed in 5 to 10% by weight of the total cosmetic composition,
The metal oxide is mixed in 15 to 35% by weight of the total cosmetic composition,
The solid oil is a hydrogenated vegetable oil,
The non-volatile ester-based oil is a method for producing a cosmetic composition that is hexyl laurate.
상기 화장료 조성물은 유중수형(W/O) 제형으로 제조하는 것인, 화장료 조성물의 제조방법.
According to claim 10,
The method for producing a cosmetic composition, wherein the cosmetic composition is prepared in a water-in-oil (W / O) formulation.
상기 화장료 조성물은 화장수, 영양 로션, 영양 에센스, 마사지 크림, 미용목욕물 첨가제, 바디 로션, 바디 밀크, 배스 오일, 베이비 오일, 베이비파우더, 샤워겔, 샤워크림, 선스크린 로션, 선스크린 크림, 선탠 크림, 스킨 로션, 스킨 크림, 자외선차단용 화장품, 컨실러, 클렌징밀크, 탈모제화장용, 페이스 및 바디로션, 페이스 및 바디크림, 피부미백크림, 핸드로션, 헤어로션, 화장용크림, 쟈스민 오일, 목욕비누, 물비누, 미용비누, 샴푸, 손세정제(핸드클리너), 약용비누비의료용, 크림비누, 페이셜워시, 전신 세정제, 두피 세정제, 헤어린스, 화장비누, 치아미백용 겔, 또는 치약의 형태로 제조하는 것인, 화장료 조성물의 제조방법.According to claim 10,
The cosmetic composition is cosmetic water, nutrient lotion, nutrient essence, massage cream, beauty bath water additive, body lotion, body milk, bath oil, baby oil, baby powder, shower gel, shower cream, sunscreen lotion, sunscreen cream, suntan cream , skin lotion, skin cream, sun protection cosmetics, concealer, cleansing milk, depilatory cosmetic, face and body lotion, face and body cream, skin whitening cream, hand lotion, hair lotion, cosmetic cream, jasmine oil, bath soap , water soap, beauty soap, shampoo, hand sanitizer (hand cleaner), medicated soap, medical soap, cream soap, facial wash, body cleanser, scalp cleanser, hair rinse, cosmetic soap, tooth whitening gel, or toothpaste That is, a method for producing a cosmetic composition.
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JP2006028180A (en) * | 2004-07-16 | 2006-02-02 | L'oreal Sa | Cosmetic composition with improved staying power |
KR20090121848A (en) * | 2008-05-23 | 2009-11-26 | 주식회사 엘지생활건강 | Water-in-oil emulsion-type cosmetic composition for blocking ultraviolet ray |
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KR20200030849A (en) * | 2018-09-13 | 2020-03-23 | (주)아모레퍼시픽 | Stick-type make-up composition with excellent coverage and application |
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JP2006028180A (en) * | 2004-07-16 | 2006-02-02 | L'oreal Sa | Cosmetic composition with improved staying power |
KR20090121848A (en) * | 2008-05-23 | 2009-11-26 | 주식회사 엘지생활건강 | Water-in-oil emulsion-type cosmetic composition for blocking ultraviolet ray |
KR101566826B1 (en) * | 2012-04-30 | 2015-11-06 | (주)아모레퍼시픽 | Powder composition with good coverage and moisturizing effects |
KR20200030849A (en) * | 2018-09-13 | 2020-03-23 | (주)아모레퍼시픽 | Stick-type make-up composition with excellent coverage and application |
KR101979217B1 (en) * | 2018-10-08 | 2019-05-17 | 주식회사 한국화장품제조 | Water in Oil Solid UV-Sunscreen Cosmetic Composition |
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