KR102482662B1 - Oil-in-water cosmetic composition with improved makeup durability - Google Patents
Oil-in-water cosmetic composition with improved makeup durability Download PDFInfo
- Publication number
- KR102482662B1 KR102482662B1 KR1020220081011A KR20220081011A KR102482662B1 KR 102482662 B1 KR102482662 B1 KR 102482662B1 KR 1020220081011 A KR1020220081011 A KR 1020220081011A KR 20220081011 A KR20220081011 A KR 20220081011A KR 102482662 B1 KR102482662 B1 KR 102482662B1
- Authority
- KR
- South Korea
- Prior art keywords
- cosmetic composition
- powder
- oil
- water
- preparation example
- Prior art date
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- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
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- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
- 229940055577 oleyl alcohol Drugs 0.000 description 1
- 239000004006 olive oil Substances 0.000 description 1
- 235000008390 olive oil Nutrition 0.000 description 1
- 229940101267 panthenol Drugs 0.000 description 1
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- 239000002304 perfume Substances 0.000 description 1
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- 239000002453 shampoo Substances 0.000 description 1
- 239000002884 skin cream Substances 0.000 description 1
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- 239000000126 substance Substances 0.000 description 1
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/062—Oil-in-water emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Cosmetics (AREA)
Abstract
Description
본 발명은 메이크업 지속성이 향상된 수중유형 화장료 조성물에 관한 것이다.The present invention relates to an oil-in-water cosmetic composition with improved makeup durability.
현대에는 산업사회의 발달과 사회활동의 증가로 자기 자신을 적극적으로 표현하고자 하는 자아의식이 높아지면서 화장품의 이용이 매우 활발한 추세이며, 이러한 측면에서 화장품의 이용 편리성이 매우 중요하다. 따라서 외상이 물인 제형으로서 비교적 가볍고 발림성이 좋아 덧바르기도 쉬우며, 다른 제품과 병용하여 사용하기가 용이하고, 대부분이 오일상인 효능 물질을 내부에 효과적으로 담지할 수 있다는 점에서 수중유형 화장료의 이용이 더욱 증가하고 있다. 그러나 수중유형 화장료 조성물의 경우 외상이 물이므로, 외부 스트레스로부터 방어가 약해 내수성이 떨어진다는 단점이 여전히 해결해야 할 과제이다. 또한 내수성/지속성 향상을 위해 파우더를 다량 포함할 경우 파우더의 밀도 차이로 인해 균일성/안정성이 저하되고, 반대로 파우더를 제외할 경우에는 사용감의 다양성에 한계가 있다는 문제점이 있었다. 이러한 문제의 해결을 위해 파우더를 포함하는 수중유형 화장료 조성물에 잔탄검, 젤란검, 폴리비닐알코올, 소듐폴리아크릴레이트 등의 수상 점증제, 또는 피막 형성제를 포함시키는 노력이 있었으나, 이 또한 잔탐검을 사용하는 경우에는 특이 취가 있거나 미생물 오염에 취약하고, 젤란검을 사용하는 경우에는 특유의 끈적하고 미끌거리는 사용감으로 인해 부착성이 떨어지며, 폴리비닐알코올을 사용하는 경우에는 부착성은 개선되나 안정성이 매우 저하되고, 소듐폴리아크릴레이트를 사용하는 경우에는 진득한 질감으로 피부에 무거운 느낌을 주고, 제형 적용의 활용도가 낮은 문제점이 발생하였다.In modern times, with the development of industrial society and the increase in social activities, the use of cosmetics is a very active trend as the self-consciousness to actively express oneself increases, and in this respect, the convenience of use of cosmetics is very important. Therefore, as a formulation in which the external surface is water, it is relatively light and easy to reapply because of good spreadability, it is easy to use in combination with other products, and most of the effective substances in the oil form can be effectively contained inside. is increasing further. However, in the case of the water-in-water cosmetic composition, since the trauma is water, the disadvantage of poor defense from external stress and poor water resistance is still a problem to be solved. In addition, when a large amount of powder is included to improve water resistance / durability, uniformity / stability is lowered due to the difference in density of the powder, and on the contrary, when the powder is excluded, there is a problem that the variety of feeling is limited. In order to solve this problem, efforts have been made to include an aqueous phase thickener such as xanthan gum, gellan gum, polyvinyl alcohol, sodium polyacrylate, or a film forming agent in an oil-in-water cosmetic composition containing powder, but this also When used, it has a specific odor or is vulnerable to microbial contamination. When gellan gum is used, the adhesiveness is poor due to the unique sticky and slippery feeling. When polyvinyl alcohol is used, the adhesiveness is improved but the stability is very low. In the case of using sodium polyacrylate, problems such as giving a heavy feeling to the skin with a thick texture and low utilization of formulation application occurred.
따라서 본 발명은 상기의 문제를 해결하기 위해 안출된 것으로, 파우더를 포함하는 수중유형 제형이면서도 우수한 피지 흡착력 및 지속성을 가지는 신규한 화장료 조성물에 관한 것이다. 파우더를 포함하는 수중유형 제형의 화장료 조성물에 있어서, 종래 문제점을 현저히 개선한 본 발명의 화장료 조성물은 미용 분야에서 크게 이용될 것으로 기대된다.Therefore, the present invention has been made to solve the above problems, and relates to a novel cosmetic composition having excellent sebum adsorption and durability even though it is an oil-in-water formulation containing a powder. In the cosmetic composition of an oil-in-water formulation containing a powder, the cosmetic composition of the present invention, which significantly improves the conventional problems, is expected to be greatly used in the cosmetic field.
본 발명은 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물을 제공하는 것을 목적으로 한다.An object of the present invention is to provide a cosmetic composition comprising a thickening film agent and further comprising a powder.
또한 본 발명은 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물의 제조방법을 제공하는 것을 목적으로 한다.In addition, an object of the present invention is to provide a method for producing a cosmetic composition comprising a thickening film agent and further comprising a powder.
그러나 본 발명이 이루고자 하는 기술적 과제는 이상에서 언급한 과제에 제한되지 않으며, 언급되지 않은 또 다른 과제들은 아래의 기재로부터 당업계에서 통상의 지식을 가진 자에게 명확하게 이해될 수 있을 것이다.However, the technical problem to be achieved by the present invention is not limited to the above-mentioned problems, and other problems not mentioned will be clearly understood by those skilled in the art from the following description.
이하, 본원에 기재된 다양한 구체예가 도면을 참조로 기재된다. 하기 설명에서, 본 발명의 완전한 이해를 위해서, 다양한 특이적 상세사항, 예컨대, 특이적 형태, 조성물 및 공정 등이 기재되어 있다. 그러나, 특정의 구체예는 이들 특이적 상세 사항 중 하나 이상 없이, 또는 다른 공지된 방법 및 형태와 함께 실행될 수 있다. 다른 예에서, 공지된 공정 및 제조 기술은 본 발명을 불필요하게 모호하게 하지 않게 하기 위해서, 특정의 상세사항으로 기재되지 않는다. "한 가지 구체예" 또는 "구체예"에 대한 본 명세서 전체를 통한 참조는 구체예와 결부되어 기재된 특별한 특징, 형태, 조성 또는 특성이 본 발명의 하나 이상의 구체예에 포함됨을 의미한다. 따라서, 본 명세서 전체에 걸친 다양한 위치에서 표현된 "한 가지 구체예에서" 또는 "구체예"의 상황은 반드시 본 발명의 동일한 구체예를 나타내지는 않는다. 추가로, 특별한 특징, 형태, 조성, 또는 특성은 하나 이상의 구체예에서 어떠한 적합한 방법으로 조합될 수 있다.Hereinafter, various embodiments described herein are described with reference to the drawings. In the following description, numerous specific details are set forth, such as specific forms, compositions and processes, etc., in order to provide a thorough understanding of the present invention. However, certain embodiments may be practiced without one or more of these specific details, or with other known methods and forms. In other instances, well known processes and manufacturing techniques have not been described in specific detail in order not to unnecessarily obscure the present invention. Reference throughout this specification to “one embodiment” or “an embodiment” means that a particular feature, form, composition or characteristic described in connection with the embodiment is included in one or more embodiments of the invention. Thus, the appearances of "in one embodiment" or "an embodiment" in various places throughout this specification do not necessarily refer to the same embodiment of the invention. Additionally, particular features, forms, compositions, or properties may be combined in one or more embodiments in any suitable way.
명세서에서 특별한 정의가 없으면 본 명세서에 사용된 모든 과학적 및 기술적인 용어는 본 발명이 속하는 기술분야에서 당업자에 의하여 통상적으로 이해되는 것과 동일한 의미를 가진다.Unless otherwise defined in the specification, all scientific and technical terms used herein have the same meaning as commonly understood by a person skilled in the art to which the present invention belongs.
명세서 전체에서, 어떤 부분이 어떤 구성요소를 "포함"한다고 할 때, 이는 특별히 반대되는 기재가 없는 한 다른 구성요소를 제외하는 것이 아니라 다른 구성요소를 더 포함할 수 있는 것을 의미한다.Throughout the specification, when a certain component is said to "include", it means that it may further include other components without excluding other components unless otherwise stated.
본 발명의 일 양태에 따르면, 본 발명은 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물을 제공한다.According to one aspect of the present invention, the present invention provides a cosmetic composition comprising a thickening film agent and further comprising a powder.
상기 본 발명의 화장료 조성물이란 미용 목적으로 화장료에 포함되는 조성물이다. 본 발명의 조성물을 포함하는 화장료 조성물은 화장수, 영양로션, 영양에센스, 마사지 크림, 미용 목욕물 첨가제, 바디로션, 바디밀크, 배스 오일, 베이비오일, 베이비파우더, 샤워겔, 샤워크림, 선스크린로션, 선스크린크림, 선탠크림, 스킨로션, 스킨크림, 자외선차단용 화장품, 컨실러, 파운데이션, 크렌징밀크, 탈모제{화장용}, 페이스 및 바디로션, 페이스 및 바디크림, 피부미백크림, 핸드로션, 헤어로션, 화장용크림, 쟈스민오일, 목욕비누, 물비누, 미용비누, 샴푸, 손세정제(핸드클리너), 약용비누{비의료용}, 크림비누, 페이셜워시, 헤어린스, 화장비누, 치아미백용 겔, 치약 등의 형태로 제조될 수 있고, 화장료 조성물의 제조에 통상적으로 사용하는 적절한 담체, 부형제 또는 희석제를 더 포함할 수 있다. 본 발명의 화장료 조성물 내에 더 추가될 수 있는 담체, 부형제 또는 희석제로는 정제수, 오일, 왁스, 지방산, 지방산 알콜, 지방산 에스테르, 계면활성제, 흡습제(humectant), 증점제, 항산화제, 점도 안정화제, 킬레이팅제, 완충제, 저급 알콜 등이 포함되지만, 이에 제한되는 것은 아니다. 또한, 필요에 따라 미백제, 보습제, 비타민, 자외선 차단제, 향수, 염료, 항생제, 항박테리아제, 항진균제를 포함할 수 있다. 상기 오일로서는 수소화 식물성유, 피마자유, 면실유, 올리브유, 야자인유, 호호바유, 아보카도유가 이용될 수 있으며, 왁스로는 밀랍, 경랍, 카르나우바, 칸델릴라, 몬탄, 세레신, 액체 파라핀, 라놀린이 이용될 수 있다. 지방산으로는 스테아르산, 리놀레산, 리놀렌산, 올레산이 이용될 수 있고, 지방산 알콜로는 세틸알콜, 옥틸도데칸올, 올레일알콜, 판텐올, 라놀린알콜, 스테아릴 알콜, 헥사데칸올이 이용될 수 있으며 지방산 에스테르로는 이소프로필미리스테이트, 이소프로필 팔미테이트, 부틸스테아레이트가 이용될 수 있다. 계면활성제로는 당업계에 알려진 양이온 계면활성제, 음이온 계면활성제 및 비이온성 계면활성제가 사용가능하며 가능한 한 천연물 유래의 계면활성제가 바람직하다. 그 외에도 화장품 분야에서 널리 알려진 흡습제, 증점제, 항산화제 등을 포함할 수 있으며, 이들의 종류와 양은 당업계에 공지된 바에 따른다. 본 발명의 화장료조성물 은 섬유에 침적되어 이용되는 것을 특징으로 한다.The cosmetic composition of the present invention is a composition included in cosmetics for cosmetic purposes. Cosmetic compositions containing the composition of the present invention are lotion, nutrient lotion, nutrient essence, massage cream, beauty bath water additive, body lotion, body milk, bath oil, baby oil, baby powder, shower gel, shower cream, sunscreen lotion, Sunscreen cream, suntan cream, skin lotion, skin cream, sunscreen cosmetics, concealer, foundation, cleansing milk, depilatory agent {for cosmetics}, face and body lotion, face and body cream, skin whitening cream, hand lotion, hair lotion , cosmetic cream, jasmine oil, bath soap, water soap, beauty soap, shampoo, hand sanitizer (hand cleaner), medicated soap {non-medical}, cream soap, facial wash, hair rinse, cosmetic soap, tooth whitening gel, toothpaste It may be prepared in the form of, etc., and may further include an appropriate carrier, excipient or diluent commonly used in the manufacture of cosmetic compositions. Carriers, excipients, or diluents that may be further added to the cosmetic composition of the present invention include purified water, oil, wax, fatty acids, fatty alcohols, fatty acid esters, surfactants, humectants, thickeners, antioxidants, viscosity stabilizers, and kills. rating agents, buffering agents, lower alcohols, and the like, but are not limited thereto. In addition, whitening agents, moisturizing agents, vitamins, sunscreens, perfumes, dyes, antibiotics, antibacterial agents, and antifungal agents may be included as necessary. Hydrogenated vegetable oil, castor oil, cottonseed oil, olive oil, coconut oil, jojoba oil, and avocado oil may be used as the oil, and beeswax, spermaceti, carnauba, candelilla, montan, ceresin, liquid paraffin, and lanolin may be used as the wax. can be used As fatty acids, stearic acid, linoleic acid, linolenic acid, and oleic acid may be used, and as fatty alcohols, cetyl alcohol, octyldodecanol, oleyl alcohol, panthenol, lanolin alcohol, stearyl alcohol, and hexadecanol may be used. Isopropyl myristate, isopropyl palmitate, and butyl stearate may be used as fatty acid esters. As the surfactant, cationic surfactants, anionic surfactants, and nonionic surfactants known in the art can be used, and surfactants derived from natural products are preferred as much as possible. In addition, it may include a moisture absorbent, thickener, antioxidant, etc. widely known in the field of cosmetics, and the type and amount thereof are known in the art. The cosmetic composition of the present invention is characterized in that it is used by being deposited on fibers.
상기 본 발명의 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물에 있어서, 상기 점증피막제는 셀룰로오스 혼합물, 잔탄검(Xanthan Gum), 젤란검(Gellan Gum), 폴리비닐알코올(Polyvinyl Alcohol), 및 소듐폴리아크릴레이트(Sodium Polyacrylate)로 구성된 그룹으로부터 선택되는 어느 하나 이상일 수 있다. 상기의 셀룰로오스 혼합물은 셀룰로오스 검(Cellulose Gum)과 마이크로크리스탈린 셀룰로오스(Microcrystalline Cellulose)가 혼합된 것을 의미하고, '셀룰로오스 검 : 마이크로크리스탈린 셀룰로오스'의 혼합 비율은 5 : 95 내지 10 : 90인 것이 바람직하고, 5 : 95 내지 8 : 92 인 것이 더욱 바람직하며, 5: 95 내지 6 : 94 인 것이 가장 바람직하나, 이에 제한되는 것은 아니다.In the cosmetic composition comprising the thickening film agent of the present invention and further comprising a powder, the thickening film agent is a cellulose mixture, xanthan gum, gellan gum, polyvinyl alcohol, And it may be any one or more selected from the group consisting of sodium polyacrylate. The above cellulose mixture means a mixture of cellulose gum and microcrystalline cellulose, and the mixing ratio of 'cellulose gum: microcrystalline cellulose' is preferably 5: 95 to 10: 90 And, it is more preferably 5: 95 to 8: 92, and most preferably 5: 95 to 6: 94, but is not limited thereto.
상기 점증피막제는 전체 화장료 조성물에 0.01 내지 2.5 중량%로 포함되는 것이 바람직하고, 0.05 내지 1.5 중량%로 포함되는 것이 더욱 바람직하며, 0.1 내지 1 중량%로 포함되는 것이 더욱 바람직하며, 0.2 내지 0.7 중량%로 포함되는 것이 더욱 바람직하며, 0.2 내지 0.5 중량%로 포함되는 것이 가장 바람직하나, 이에 제한되는 것은 아니다.The thickening agent is preferably included in an amount of 0.01 to 2.5% by weight, more preferably in an amount of 0.05 to 1.5% by weight, more preferably in an amount of 0.1 to 1% by weight, and more preferably in an amount of 0.2 to 0.7% by weight in the total cosmetic composition. It is more preferably included in %, and most preferably included in 0.2 to 0.5% by weight, but is not limited thereto.
상기 본 발명의 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물에 있어서, 상기의 파우더는 폴리메틸메타크릴레이트(Polymethyl Methacrylate), 실리카(Silica), 나일론12(Nylon-12), 비닐다이메티콘/메티콘실세스퀴옥세인크로스폴리머(Vinyl Dimethicone/Methicone Silsesquioxane Crosspolymer), 마이카(Mica), 보론나이트라이트(Boron Nitride), 바륨설페이트(Barium Sulfate), 및 카올린(Kaolin)으로 구성된 그룹으로부터 선택되는 어느 하나 이상일 수 있다. In the cosmetic composition comprising the thickening film agent of the present invention and further comprising a powder, the powder is polymethyl methacrylate, silica, nylon 12, vinyl die Selected from the group consisting of Methicone/Methicone Silsesquioxane Crosspolymer, Mica, Boron Nitride, Barium Sulfate, and Kaolin can be one or more of the
또는 상기 파우더는 구상 파우더일 수 있다. Alternatively, the powder may be a spherical powder.
또는 상기 파우더의 평균 입경은 2~40㎛ 일 수 있다.Alternatively, the average particle diameter of the powder may be 2 to 40 μm.
상기 파우더는 전체 화장료 조성물에 2 내지 15 중량%로 포함되는 것이 바람직하고, 4 내지 11 중량%로 포함되는 것이 더욱 바람직하며, 5 내지 10 중량%로 포함되는 것이 더욱 바람직하며, 6 내지 9 중량%로 포함되는 것이 더욱 바람직하며, 7 내지 8 중량%로 포함되는 것이 가장 바람직하나, 이에 제한되는 것은 아니다.The powder is preferably included in an amount of 2 to 15% by weight, more preferably in an amount of 4 to 11% by weight, more preferably in an amount of 5 to 10% by weight, and more preferably in an amount of 6 to 9% by weight in the total cosmetic composition. It is more preferably included as, and most preferably, it is included in 7 to 8% by weight, but is not limited thereto.
상기 본 발명의 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물은 공지된점증제를 추가로 포함할 수 있다. 여기서의 점증제는 물을 흡수하고 유지, 점증시키는 능력이 뛰어난 수상점증제인 것이 바람직하고, 카보머, 암모늄아크릴로일다이메틸타우레이트/브이피코폴리머, 아크릴레이트/C10-30알킬아크릴레이트크로스폴리머 등인 것이 더욱 바람직하나, 이에 제한되는 것은 아니며, 필요에 따라 중화 과정을 통해 점증시키는 것도 가능한다. 본 발명에 상기 점증제가 추가되는 경우에, 전체 전체 화장료 조성물에 0.01 내지 1 중량%로 포함되는 것이 바람직하고, 0.05 내지 0.5 중량%로 포함되는 것이 더욱 바람직하며, 0.05 내지 0.2로 포함되는 것이 더욱 바람직하나, 이에 제한되는 것은 아니다.The cosmetic composition including the thickening film agent of the present invention and further comprising powder may further include a known thickening agent. The thickener here is preferably an aqueous phase thickener having excellent ability to absorb, retain, and increase water, and carbomer, ammonium acryloyldimethyltaurate/Vpicopolymer, acrylate/C10-30 alkyl acrylate crosspolymer And the like is more preferable, but is not limited thereto, and it is also possible to gradually increase through a neutralization process if necessary. When the thickener is added to the present invention, it is preferably included in 0.01 to 1% by weight, more preferably included in 0.05 to 0.5% by weight, and more preferably included in 0.05 to 0.2% by weight in the total cosmetic composition. However, it is not limited thereto.
상기 화장료 조성물은 수중유형(Oil-in-water) 제형일 수 있다. 본 발명의 수중유형 제형의 화장료 조성물은 상기 성분 외에 본 발명의 효과를 방해하지 않는 범위에서 일반적인 화장료에 함유되는 임의 성분, 즉 저급 알코올, 또한 상기 기재된 성분 이외의 수성 성분, 상기 기재된 성분 이외의 유성 성분, 분체, 수용성 고분자, 피막 형성제, 계면활성제, 지용성 겔화제, 유기 변성 점토 광물, 수지, 착색제, 자외선 흡수제, 방부제, 항균제, 향료, 산화 방지제, pH조정제, 킬레이트제, 미용 성분 등을 함유할 수 있다. 또한 본 발명의 수중유형 제형의 화장료 조성물은 다른 성분과의 병용에 의해 다양한 형태로 응용될 수 있다. 구체적으로는 액상형, 겔형, 페이스트형, 크림형, 고형상 등, 다양한 형태로 제조될 수 있다. 예를 들면, 화장수, 유액, 크림, 미용액, 마사지료, 팩료, 핸드 크림, 바디 로션, 바디 크림, 자외선 차단제 등의 스킨 케어 화장료, 파운데이션, 아이섀도우, 아이라이너, 마스카라, 아이브로우 다, 컨실러, 립스틱, 립 크림 등의 마무리용 화장료, 헤어 미스트, 트리트먼트, 헤어 크림, 등의 두발용 화장료 등을 예시할 수 있다. 그 사용 방법은 손이나 손가락, 코튼으로 사용하는 방법, 부직포 등에 함침시켜 사용하는 방법 등을 들 수 있다.The cosmetic composition may be an oil-in-water formulation. In addition to the above components, the cosmetic composition of the oil-in-water formulation of the present invention is an optional component contained in general cosmetics, that is, a lower alcohol, an aqueous component other than the components described above, and an oil component other than the components described above, other than the above components. Ingredients, powders, water-soluble polymers, film formers, surfactants, oil-soluble gelling agents, organic modified clay minerals, resins, colorants, ultraviolet absorbers, preservatives, antibacterial agents, fragrances, antioxidants, pH adjusters, chelating agents, cosmetic ingredients, etc. can do. In addition, the oil-in-water cosmetic composition of the present invention can be applied in various forms by combination with other ingredients. Specifically, it may be prepared in various forms such as liquid, gel, paste, cream, and solid forms. For example, lotion, lotion, cream, beauty essence, massage fee, pack fee, hand cream, body lotion, body cream, skin care cosmetics such as sunscreen, foundation, eye shadow, eyeliner, mascara, eyebrow, concealer, Cosmetics for finishing, such as lipstick and lip balm, cosmetics for hair, such as hair mist, treatment, and hair cream, etc. can be illustrated. The method of use includes a method of using with hands, fingers, cotton, a method of impregnating nonwoven fabric, etc., and the like.
또한 상기 화장료 조성물은 피부결 정돈, 피부의 밀착감, 유분기 제어 정도, 메이크업 고정력(부스터), 및/또는 지속력을 포함한 사용감이 개선되는 것을 특징으로 한다.In addition, the cosmetic composition is characterized in that the feeling of use including skin texture adjustment, skin adhesion, oil control degree, makeup fixing power (booster), and / or durability is improved.
본 발명의 다른 양태에 따르면, 본 발명은 (a) 점증피막제를 용해하는 단계; 및, (b) 파우더를 첨가하는 단계;를 포함하는 화장료 조성물의 제조방법을 제공한다. 상기 화장료 조성물의 제조 방법은 수중유형 제형의 조성물을 제조하기 위한 방법으로서 공지된 유화 방법이면 특별히 한정되지 않고 이용 가능하다. 구체적으로는 분산 유화법, 전상 유화법, 전상온도 유화법 등을 들 수 있다. 이에 제한되는 것은 아니나, 유화 안정성이 우수한 수중유형 화장료 조성물을 제조한다는 점에서 보다 구체적으로 기술하면, 본 발명의 화장료 조성물은 하기 1 내지 6단계의 과정 중 어느 하나 이상의 단계를 포함하여 제조될 수 있다.According to another aspect of the present invention, the present invention comprises (a) dissolving the thickening coating agent; And, (b) adding a powder; provides a method for producing a cosmetic composition comprising a. The method for preparing the cosmetic composition may be used without particular limitation as long as it is an emulsification method known as a method for preparing an oil-in-water formulation composition. Specifically, a dispersion emulsification method, an inversion emulsification method, an inversion temperature emulsification method, and the like are exemplified. Although not limited thereto, in more detail in terms of preparing an oil-in-water cosmetic composition having excellent emulsion stability, the cosmetic composition of the present invention may be prepared by including any one or more of the steps 1 to 6 below. .
1 단계: 정제수에 점증피막제를 첨가한 후 80℃로 가온하며 용해시킨다.Step 1: After adding a thickening agent to purified water, dissolve it by heating to 80℃.
2 단계: 별도의 유상성분을 70℃로 가온하며 용해시킨다.Step 2: Dissolve the separate oily ingredients by heating them to 70℃.
3 단계: 상기 1 단계의 결과물과 2 단계의 결과물이 모두 용해되면, 이를 혼합 후 60℃에서 10분간 4000rpm으로 빠르게 교반하며 유화시킨다.Step 3: When both the result of step 1 and the result of step 2 are dissolved, they are mixed and emulsified while rapidly stirring at 4000 rpm for 10 minutes at 60 ° C.
4 단계: 날림에 주의하며 파우더를 첨가한 후, 5분간 4000rpm으로 빠르게 교반하며 분산 및 유화시킨다.Step 4: After adding the powder, being careful not to blow it, disperse and emulsify it by rapidly stirring at 4000 rpm for 5 minutes.
5 단계: 30℃까지 서서히 냉각시킨다.Step 5: Slowly cool down to 30°C.
6 단계: 진공 압을 가하여 탈포시킨다.Step 6: Degas by applying vacuum pressure.
상기 1 단계에서의 정제수는 수중유형 제형의 조성물을 제조하기 위해 함유되는 것으로, 화장료에 일반적으로 이용되는 베이스로서 수형 조성물이라면 특별히 제한되지 않는다. 정제수 이외에도 물, 온천수, 심층수, 혹은 식물의 수증기 증류수일 수 있고, 필요에 따라 1종 또는 2종 이상을 적절히 혼합하여 이용할 수 있다. 또한 함유량은 특별히 제한되지 않으며 적절히, 다른 성분량을 제외한 잔량으로 함유될 수 있고, 10 내지 90 중량%가 바람직하다.Purified water in the first step is contained to prepare the composition of the oil-in-water formulation, and is not particularly limited as long as it is a water-type composition as a base commonly used in cosmetics. In addition to purified water, it may be water, hot spring water, deep sea water, or plant steam distilled water, and one or two or more kinds may be appropriately mixed and used as necessary. In addition, the content is not particularly limited and may be appropriately contained in a residual amount excluding the amount of other components, and 10 to 90% by weight is preferable.
상기 본 발명의 화장료 조성물의 제조방법에 있어서, 화장료 조성물, 점증피막제, 또는 파우더에 대한 제한사항은 상기 점증피막제를 포함하고, 파우더를 추가로 포함하는 화장료 조성물에서 기재한 바와 중복되어, 이하 본 명세서의 과도한 복잡성을 피하기 위하여 생략한다.In the manufacturing method of the cosmetic composition of the present invention, the cosmetic composition, the thickening coating agent, or the restrictions on the powder overlap with those described in the cosmetic composition including the thickening coating agent and further comprising a powder, and the following specification are omitted to avoid excessive complexity.
이하 본 발명을 실시예에 입각하여 구체적으로 설명한다.Hereinafter, the present invention will be described in detail based on examples.
수중유형 화장료는 이용이 편리한 장점이 있으나, 수중유형 화장료의 내수성/지속성 향상을 위해 파우더를 다량 포함할 경우 파우더의 밀도 차이로 인해 균일성/안정성이 저하되고, 반대로 파우더를 제외할 경우에는 사용감의 다양성에 한계가 있다는 문제점이 있었다.Water-in-water cosmetics have the advantage of being convenient to use, but if a large amount of powder is included to improve the water resistance/continuity of water-in-water cosmetics, uniformity/stability is lowered due to the difference in powder density, and conversely, when powder is excluded, the feeling of use is reduced. The problem was that the diversity was limited.
본 발명은 파우더를 포함하는 수중유형 제형이면서도 우수한 피지 흡착력 및 지속성을 가지는 신규한 화장료 조성물에 관한 것이다. 파우더를 포함하는 수중유형 제형의 화장료 조성물에 있어서, 종래 문제점을 현저히 개선한 본 발명의 화장료 조성물은 미용 분야에서 크게 이용될 것으로 기대된다.The present invention relates to a novel cosmetic composition having excellent sebum adsorption and durability even though it is an oil-in-water formulation containing a powder. In the cosmetic composition of an oil-in-water formulation containing a powder, the cosmetic composition of the present invention, which significantly improves the conventional problems, is expected to be greatly used in the cosmetic field.
도 1은 본 발명의 일 실시예에 따른, 점증피막제, 및 파우더가 포함되거나, 또는 포함되지 않은 유중수형 화장료 조성물 도포 후 모공 면적비율(%)에 따른 지속성 평가 결과를 나타낸 것이다.
도 2는 본 발명의 일 실시예에 따른, 점증피막제, 및 파우더가 포함되거나, 또는 포함되지 않은 유중수형 화장료 조성물 도포 후 피지 개수에 따른 지속성 평가 결과를 나타낸 것이다.1 shows the results of evaluation of durability according to the pore area ratio (%) after application of a water-in-oil cosmetic composition with or without a thickening film agent and powder according to an embodiment of the present invention.
Figure 2 shows the results of evaluation of durability according to the number of sebum after application of a water-in-oil cosmetic composition with or without a thickening film agent and powder according to an embodiment of the present invention.
이하, 실시예를 통하여 본 발명을 더욱 상세히 설명하고자 한다. 이들 실시예는 오로지 본 발명을 보다 구체적으로 설명하기 위한 것으로, 본 발명의 요지에 따라 본 발명의 범위가 이들 실시예에 의해 제한되지 않는다는 것은 당업계에서 통상의 지식을 가진 자에 있어서 자명할 것이다.Hereinafter, the present invention will be described in more detail through examples. These examples are only for explaining the present invention in more detail, and it will be apparent to those skilled in the art that the scope of the present invention is not limited by these examples according to the gist of the present invention. .
실시예 1: 우수한 메이크업 지속성을 갖는 수중유형 화장료 조성물의 제조Example 1: Preparation of an oil-in-water cosmetic composition having excellent makeup durability
파우더를 포함하는 수중유형 화장료 조성물의 지속성 개선을 확인하기 위해 하기 표 1과 같은 베이스의 화장료 조성물을 제조하여 시험하였다.In order to confirm the improvement in the durability of the oil-in-water cosmetic composition containing the powder, the cosmetic composition of the base as shown in Table 1 below was prepared and tested.
상기 화장료 조성물의 구체적인 제조 단계를 하기에 기술하였다.The specific manufacturing steps of the cosmetic composition are described below.
1 단계: 정제수에 점증피막제를 첨가한 후 80℃로 가온하며 용해시킨다.Step 1: After adding a thickening agent to purified water, dissolve it by heating to 80℃.
2 단계: 별도의 유상성분을 70℃로 가온하며 용해시킨다.Step 2: Dissolve the separate oily ingredients by heating them to 70℃.
3 단계: 상기 1 단계의 결과물과 2 단계의 결과물이 모두 용해되면, 이를 혼합 후 60℃에서 10분간 4000rpm으로 빠르게 교반하며 유화시킨다.Step 3: When both the result of step 1 and the result of step 2 are dissolved, they are mixed and emulsified while rapidly stirring at 4000 rpm for 10 minutes at 60 ° C.
4 단계: 날림에 주의하며 파우더를 첨가한 후, 5분간 4000rpm으로 빠르게 교반하며 분산 및 유화시킨다.Step 4: After adding the powder, being careful not to blow it, disperse and emulsify it by rapidly stirring at 4000 rpm for 5 minutes.
5 단계: 30℃까지 서서히 냉각시킨다.Step 5: Slowly cool down to 30°C.
6 단계: 진공 압을 가하여 탈포시킨다.Step 6: Degas by applying vacuum pressure.
실시예 2: 최적의 수상 점증제 및 피막제 종류 탐색 시험Example 2: Optimal aqueous phase thickener and coating agent type search test
실시예 1의 화장료 조성물을 베이스로 하되, 파우더를 포함하는 수중유형 화장료 조성물에 포함되는 최적의 수상 점증제 및 피막제 종류를 선택하기 위한 시험을 수행하였다.The cosmetic composition of Example 1 was used as a base, but a test was performed to select the optimal water-phase thickening agent and coating agent type included in the water-in-water cosmetic composition containing powder.
화장료 조성물 중 수상 점증제 및 피막제(0.2 중량%), 정제수(to 100 중량%), 수상점증제(0.1 중량%), 폴리올(5 중량%), 오일(15 중량%), 보조유화제(1 중량%), 및 파우더(7 중량%)의 조성은 동일하게 적용하되, 수상 점증제 및 피막제 종류는 하기 표 2와 같이 셀룰로오스 검(Cellulose Gum)과 마이크로크리스탈린 셀룰로오스(Microcrystalline Cellulose)가 혼합된 셀룰로오스 혼합물, 잔탄검, 젤란검, 폴리비닐알코올, 또는 소듐폴리아크릴레이트를 시험하였다. 상기 셀룰로오스 혼합물은 셀룰로오스 검(Cellulose Gum)과 마이크로크리스탈린 셀룰로오스(Microcrystalline Cellulose)의 혼합물을 이용하였다.Among the cosmetic compositions, aqueous phase thickener and coating agent (0.2% by weight), purified water (to 100% by weight), aqueous phase thickener (0.1% by weight), polyol (5% by weight), oil (15% by weight), auxiliary emulsifier (1% by weight) %), and the composition of the powder (7% by weight) are applied in the same way, but the type of aqueous phase thickener and coating agent are as shown in Table 2 below. A cellulose mixture in which cellulose gum and microcrystalline cellulose are mixed , xanthan gum, gellan gum, polyvinyl alcohol, or sodium polyacrylate were tested. As the cellulose mixture, a mixture of cellulose gum and microcrystalline cellulose was used.
상기 제조예 1 내지 5에 대하여 25-45세의 여성 30명을 대상으로 피부결 정돈, 피부의 밀착감, 메이크업 고정력(부스터), 및 지속력을 포함한 사용감에 대해 관능평가를 실시하였다. 평가 기준은 아주 양호한 경우 5점, 양호한 경우 4점, 보통인 경우 3점, 약간 불만족인 경우 2점, 매우 불만족인 경우 1점으로 하였고, 30개의 데이터를 평균 처리하여, 그 결과를 하기 표 3에 나타내었다.With respect to Preparation Examples 1 to 5, 30 women aged 25 to 45 were subjected to sensory evaluation on skin texture, skin adhesion, makeup fixing power (booster), and feeling of use including lasting power. The evaluation criteria were 5 points for very good, 4 points for good, 3 points for normal, 2 points for slightly unsatisfied, and 1 point for very unsatisfactory. 30 data were averaged and the results are shown in Table 3 below. shown in
시험 결과, 점증피막제로 잔탄검을 이용한 경우에는 파우더가 수중유형 내에 고르게 부유되지 못하고 가라앉는 현상으로 인해 관능 평가가 불가하였다(제조예 2). 소듐폴리아크릴레이트를 이용한 경우에는 파우더 엉김 현상으로 수중유형 내에 고르게 분산되지 못하여 관능 평가가 불가하였다(제조예 5). 시험된 모든 항목에서 점증피막제로 셀룰로오스 혼합물을 이용한 경우가 가장 우수한 관능 결과를 나타내었다(제조예 1). 제조예 1의 경우 조성물이 피부 위 얇게 도포가 가능하고, 이로 인해 피부결 정돈과 밀착감에 효과가 있으며, 지속력이 우수한 것을 확인하였다. 젤란검(제조예 4), 또는 폴리비닐알코올(제조예 5)가 이용된 경우에는 상대적으로 밀착감이 저하됨으로 인해 메이크업 고정력(부스터) 및 지속성에 한계가 있음을 알 수 있었다.As a result of the test, when xanthan gum was used as a thickening agent, sensory evaluation was not possible due to a phenomenon in which the powder did not float evenly in the water type and sank (Preparation Example 2). When sodium polyacrylate was used, sensory evaluation was not possible because it was not evenly dispersed in the water type due to powder agglomeration (Preparation Example 5). In all tested items, the case of using a cellulose mixture as a thickening agent showed the best sensory results (Preparation Example 1). In the case of Preparation Example 1, it was confirmed that the composition can be applied thinly on the skin, and thus has an effect on skin texture and adhesion, and excellent durability. When gellan gum (Preparation Example 4) or polyvinyl alcohol (Preparation Example 5) was used, it was found that there was a limit to makeup fixing power (booster) and durability due to a relatively lowered feeling of adhesion.
셀룰로오스 혼합물 내 셀룰로오스 검과 마이크로크리스탈린 셀룰로오스의 최적의 혼합 비율에 대한 추가 실험 결과, '셀룰로오스 검 : 마이크로크리스탈린 셀룰로오스'의 혼합 비율은 5 : 95 내지 10 : 90인 것이 바람직하고, 5 : 95 내지 8 : 92 인 것이 더욱 바람직하며, 5: 95 내지 6 : 94 인 것이 가장 바람직한 것을 알 수 있었다.As a result of further experiments on the optimal mixing ratio of cellulose gum and microcrystalline cellulose in the cellulose mixture, the mixing ratio of 'cellulose gum: microcrystalline cellulose' is preferably 5:95 to 10:90, and 5:95 to It was found that the ratio of 8:92 is more preferable, and the ratio of 5:95 to 6:94 is most preferable.
실시예 3: 최적의 수상 점증제 및 피막제 혼합비 탐색 시험Example 3: Optimal aqueous phase thickener and coating agent mixing ratio search test
실시예 2에서 도출된 결과에 따라 점증피막제를 셀룰로오스 혼합물로 고정하되, 최적의 수상 점증제 및 피막제 혼합비를 선택하기 위한 시험을 수행하였다.According to the results obtained in Example 2, the thickener was fixed as a cellulose mixture, but a test was conducted to select the optimal water phase thickener and coating agent mixing ratio.
이를 위해 하기 표 4와 같이 점증피막제를 0.01 내지 3의 비율로 혼합한 화장료 조성물을 제조하였다. 기타 화장료 조성물 중 정제수(to 100 중량%), 수상점증제(0.1 중량%), 폴리올(5 중량%), 오일(15 중량%), 보조유화제(1 중량%), 및 파우더(7 중량%)의 조성은 동일하게 적용하였다.To this end, as shown in Table 4 below, a cosmetic composition was prepared by mixing the thickening film agent at a ratio of 0.01 to 3. Among other cosmetic compositions, purified water (to 100% by weight), aqueous phase thickener (0.1% by weight), polyol (5% by weight), oil (15% by weight), auxiliary emulsifier (1% by weight), and powder (7% by weight) The composition of was applied the same.
상기 제조예 6 내지 10에 대하여 실시예 2에서와 동일한 방법으로 피부결 정돈, 피부의 밀착감, 유분기 제어 정도, 메이크업 고정력(부스터), 및 지속력을 포함한 사용감에 대해 관능평가를 실시하여, 그 결과를 하기 표 5에 나타내었다.For Preparation Examples 6 to 10, sensory evaluation was performed on the feeling of use including skin texture, skin adhesion, oil control, makeup fixing power (booster), and lasting power in the same manner as in Example 2, and the results were It is shown in Table 5 below.
시험 결과, 점증피막제 혼합 비율에 있어서 임계적 비율이 있는 것을 알 수 있었다. 파우더를 포함하는 수중유형 화장료 조성물에 점증피막제가 0.2 중량% 포함되는 경우가 피부 밀착감과 유분기 제거에서 가장 우수한 결과를 보이며, 메이크업 고정력(부스터)이 우수한 것으로 나타났다(제조예 7). 점증피막제가 과하게 포함되는 경우(제조예 10), 오히려 피부결 정돈을 방해해 밀착감을 저하시키고, 이로 인해 밀림이 발생하며, 지속력도 저하되는 것으로 나타났다. 따라서 상기 결과로부터 파우더를 포함하는 수중유형 화장료 조성물에 포함되는 점증피막제의 최적 혼합비는 0.01 내지 2.5인 것이 바람직하고, 0.05 내지 1.5인 것이 더욱 바람직하며, 0.1 내지 1인 것이 더욱 바람직하며, 0.2 내지 0.7인 것이 더욱 바람직하며, 0.2 내지 0.5인 것이 가장 바람직한 것을 알 수 있었다.As a result of the test, it was found that there is a critical ratio in the mixing ratio of the thickening agent. The case in which 0.2% by weight of a thickening agent was included in the water-in-water cosmetic composition containing powder showed the best results in skin adhesion and oil removal, and showed excellent makeup fixing power (booster) (Preparation Example 7). When the thickening film agent is excessively included (Preparation Example 10), it was found that it rather interferes with the skin texture and reduces the sense of adhesion, resulting in slipping and deterioration in durability. Therefore, from the above results, the optimal mixing ratio of the thickening agent included in the water-in-water cosmetic composition containing the powder is preferably 0.01 to 2.5, more preferably 0.05 to 1.5, more preferably 0.1 to 1, and 0.2 to 0.7 It was found that it is more preferable, and that 0.2 to 0.5 is most preferable.
실시예 4: 최적의 파우더 종류 탐색 시험Example 4: Optimal powder type search test
실시예 3에서 도출된 결과에 따라 파우더를 포함하는 수중유형 화장료 조성물에 포함되는 점증피막제를 셀룰로오스 혼합물로 고정하되, 최적의 파우더 종류를 선택하기 위한 시험을 수행하였다.According to the results obtained in Example 3, the thickening agent included in the water-in-water cosmetic composition containing the powder was fixed with a cellulose mixture, but a test was performed to select the optimum type of powder.
화장료 조성물 중 수상 점증제 및 피막제(0.2 중량%), 정제수(to 100 중량%), 수상점증제(0.1 중량%), 폴리올(5 중량%), 오일(15 중량%), 보조유화제(1 중량%), 및 파우더(7 중량%)의 조성은 동일하게 적용하되, 파우더 종류는 하기 표 6과 같이 구상파우더 4종(폴리메틸메타크릴레이트, 실리카, 나일론12, 또는 비닐다이메티콘/메티콘실세스퀴옥세인크로스폴리머)과 판상파우더 4종(마이카, 보론나이트라이트, 바륨설페이트, 또는 카올린)을 비교하였다. 상기 파우더들의 평균 입경은 2~40㎛로 조절하여 사용하였다.Among the cosmetic compositions, aqueous phase thickener and coating agent (0.2% by weight), purified water (to 100% by weight), aqueous phase thickener (0.1% by weight), polyol (5% by weight), oil (15% by weight), auxiliary emulsifier (1% by weight) %), and the composition of the powder (7% by weight) is applied in the same way, but the type of powder is 4 types of spherical powder (polymethyl methacrylate, silica, nylon 12, or vinyl dimethicone / methicone) as shown in Table 6 below. Silsesquioxane Crosspolymer) and four types of plate-shaped powder (mica, boron nitrite, barium sulfate, or kaolin) were compared. The average particle diameter of the powders was adjusted to 2 to 40 μm.
상기 제조예 11 내지 18에 대하여 실시예 2에서와 동일한 방법으로 피부결 정돈, 피부의 밀착감, 유분기 제어 정도, 메이크업 고정력(부스터), 및 지속력을 포함한 사용감에 대해 관능평가를 실시하여, 그 결과를 하기 표 7에 나타내었다.For Preparation Examples 11 to 18, sensory evaluation was performed on the feeling of use including skin texture, skin adhesion, oil control, makeup fixing power (booster), and lasting power in the same manner as in Example 2, and the results were It is shown in Table 7 below.
시험 결과, 구상파우더를 이용한 경우에는 그 종류에 관계없이 모두 우수한 결과를 나타내었다(제조예 11 내지 14). 그러나 판상파우더를 이용한 경우에는 모두 파우더가 수중유형 내에 고르게 부유되지 못하고 가라앉는 현상으로 인해 관능 평가가 불가하였다(제조예 15 내지 18). 상기의 결과로부터, 수중유형 제형 내에 점증피막제로 셀룰로오스 혼합물을 이용하는 경우 혼합되는 파우더는 구상파우더가 적합함을 알 수 있었다.As a result of the test, when spherical powder was used, all showed excellent results regardless of the type (Preparation Examples 11 to 14). However, in the case of using plate-shaped powder, sensory evaluation was not possible due to a phenomenon in which the powder did not float evenly in the water type and sank (Preparation Examples 15 to 18). From the above results, it was found that the spherical powder is suitable for the powder to be mixed when the cellulose mixture is used as a thickening agent in the oil-in-water formulation.
실시예 5: 최적의 파우더 혼합비 탐색 시험Example 5: Optimal Powder Mixing Ratio Exploration Test
실시예 4에서 도출된 결과에 따라 파우더를 포함하는 수중유형 화장료 조성물에 포함되는 점증피막제를 셀룰로오스 혼합물로 고정하고, 파우더는 구상파우더로 고정하되, 최적의 파우더 혼합비를 선택하기 위한 시험을 수행하였다.According to the results obtained in Example 4, the thickening agent included in the water-in-water cosmetic composition containing powder was fixed with a cellulose mixture, and the powder was fixed with a spherical powder, but a test was performed to select the optimal powder mixing ratio.
이를 위해 하기 표 8과 같이 파우더를 2 내지 15의 비율로 혼합한 화장료 조성물을 제조하였다. 기타 화장료 조성물 중 점증피막제(0.2 중량%), 정제수(to 100 중량%), 수상점증제(0.1 중량%), 폴리올(5 중량%), 오일(15 중량%), 및 보조유화제(1 중량%)의 조성은 동일하게 적용하였다.To this end, a cosmetic composition was prepared by mixing the powder in a ratio of 2 to 15 as shown in Table 8 below. Among other cosmetic compositions, thickener (0.2% by weight), purified water (to 100% by weight), aqueous phase thickener (0.1% by weight), polyol (5% by weight), oil (15% by weight), and auxiliary emulsifier (1% by weight) ) The composition of the same was applied.
상기 제조예 19 내지 23에 대하여 실시예 2에서와 동일한 방법으로 피부결 정돈, 피부의 밀착감, 유분기 제어 정도, 메이크업 고정력(부스터), 및 지속력을 포함한 사용감에 대해 관능평가를 실시하여, 그 결과를 하기 표 9에 나타내었다.For Preparation Examples 19 to 23, sensory evaluation was performed on the feeling of use including skin texture, skin adhesion, oil control, makeup fixing power (booster), and lasting power in the same manner as in Example 2, and the results were It is shown in Table 9 below.
시험 결과, 파우더 혼합 비율에 있어서 임계적 비율이 있는 것을 알 수 있었다. 점증피막제를 포함하는 수중유형 화장료 조성물에 파우더가 7 중량% 포함되는 경우가 피부 밀착감과 유분기 제거에서 가장 우수한 결과를 보이며, 메이크업 고정력(부스터)이 우수한 것으로 나타났다(제조예 21). 그보다 파우더가 적거나 또는 많이 포함되는 경우에는 관능 결과가 저하되는 것으로 나타났다. 따라서 상기 결과로부터 점증피막제를 포함하는 수중유형 화장료 조성물에 포함되는 파우더의 최적 혼합비는 2 내지 15인 것이 바람직하고, 4 내지 11인 것이 더욱 바람직하며, 5 내지 10인 것이 더욱 바람직하며, 7 내지 8인 것이 가장 바람직한 것을 알 수 있었다.As a result of the test, it was found that there is a critical ratio in the powder mixing ratio. The case where 7% by weight of powder was included in the water-in-water cosmetic composition containing a thickening film agent showed the best results in skin adhesion and oil removal, and showed excellent makeup fixing power (booster) (Preparation Example 21). It was found that sensory results were lowered when less or more powder was included. Therefore, from the above results, the optimal mixing ratio of the powder included in the oil-in-water cosmetic composition containing the thickening film agent is preferably 2 to 15, more preferably 4 to 11, more preferably 5 to 10, and 7 to 8 was found to be the most desirable.
실시예 6: 본 발명의 수중유형 화장료 조성물의 효과 평가Example 6: Evaluation of the effect of the water-in-water cosmetic composition of the present invention
실시예 1 내지 5에 따라 도출된 최적의 유중수형 화장료 조성물에 대하여 유분기 제어 정도, 메이크업 고정력(부스터), 및 지속성을 평가하기 위해 점증피막제, 및 파우더를 포함하지 않는 제형과 비교하였다. 구체적인 조성을 하기 표 10에 나타내었다.The optimal water-in-oil cosmetic compositions derived according to Examples 1 to 5 were compared with formulations without a thickening agent and powder to evaluate the degree of oil control, makeup fixing power (booster), and durability. The specific composition is shown in Table 10 below.
상기 제조예 24와 25의 안면 피부에 도포하고, 4시간 후 모공 면적비율(%)과 피지의 개수를 분석하였다. 시험은 동일 개체에서, 안면의 오른쪽에 제조예 24를, 안면의 왼쪽에 제조예 25를 도포하는 방법으로 수행하였다. 그 결과를 도 1과 도 2에 나타내었다.Preparation Examples 24 and 25 were applied to the facial skin, and 4 hours later, the pore area ratio (%) and the number of sebum were analyzed. The test was performed by applying Preparation Example 24 to the right side of the face and Preparation Example 25 to the left side of the face in the same subject. The results are shown in Figures 1 and 2.
시험 결과, 점증피막제, 및 파우더가 포함되지 않은 제조예 25에 비하여 점증피막제, 및 파우더가 포함된 제조예 24가 피지 흡착에 의한 메이크업 지속성이 우수한 것을 알 수 있었다.As a result of the test, it was found that the makeup consistency of Preparation Example 24 containing the thickening film agent and the powder was superior to that of Preparation Example 25 without the thickening film agent and powder.
이상으로 본 발명의 특정한 부분을 상세히 기술하였는바, 당업계의 통상의 지식을 가진 자에게 있어서 이러한 구체적인 기술은 단지 바람직한 구현예일 뿐이며, 이에 본 발명의 범위가 제한되는 것이 아닌 점은 명백하다. 따라서 본 발명의 실질적인 범위는 첨부된 청구항과 그의 등가물에 의하여 정의된다고 할 것이다.Having described specific parts of the present invention in detail above, it is clear that these specific techniques are only preferred embodiments for those skilled in the art, and the scope of the present invention is not limited thereto. Accordingly, the substantial scope of the present invention will be defined by the appended claims and equivalents thereof.
Claims (14)
상기 점증피막제는 셀룰로오스 검(Cellulose Gum)과 마이크로크리스탈린 셀룰로오스(Microcrystalline Cellulose)가 혼합된 것이고,
상기 파우더는 구상 파우더인 것인, 화장료 조성물.
A cosmetic composition comprising a thickening film agent and powder,
The thickening agent is a mixture of cellulose gum and microcrystalline cellulose,
The powder is a cosmetic composition that is a spherical powder.
상기 구상 파우더는 폴리메틸메타크릴레이트(Polymethyl Methacrylate), 실리카(Silica), 나일론12(Nylon-12), 및 비닐다이메티콘/메티콘실세스퀴옥세인크로스폴리머(Vinyl Dimethicone/Methicone Silsesquioxane Crosspolymer)로 구성된 그룹으로부터 선택되는 어느 하나 이상인 것인, 화장료 조성물.
According to claim 1,
The spherical powder is composed of Polymethyl Methacrylate, Silica, Nylon-12, and Vinyl Dimethicone/Methicone Silsesquioxane Crosspolymer. Any one or more selected from the group consisting of, a cosmetic composition.
상기 화장료 조성물은 수중유형(Oil-in-water) 제형인 것인, 화장료 조성물.
According to claim 1,
The cosmetic composition is an oil-in-water formulation, a cosmetic composition.
상기 화장료 조성물은 폴리올, 오일, 또는 유화제를 추가로 포함하는 것인, 화장료 조성물.
According to claim 1,
The cosmetic composition further comprises a polyol, an oil, or an emulsifier, the cosmetic composition.
(b) 파우더를 첨가하는 단계;를 포함하는 화장료 조성물의 제조방법으로서,
상기 점증피막제는 셀룰로오스 검(Cellulose Gum)과 마이크로크리스탈린 셀룰로오스(Microcrystalline Cellulose)가 혼합된 것이고,
상기 파우더는 구상 파우더인 것인, 화장료 조성물의 제조방법.
(a) dissolving the thickening agent; and,
As a method for producing a cosmetic composition comprising the; (b) adding powder,
The thickening agent is a mixture of cellulose gum and microcrystalline cellulose,
The powder is a method for producing a cosmetic composition that is a spherical powder.
상기 구상 파우더는 폴리메틸메타크릴레이트(Polymethyl Methacrylate), 실리카(Silica), 나일론12(Nylon-12), 및 비닐다이메티콘/메티콘실세스퀴옥세인크로스폴리머(Vinyl Dimethicone/Methicone Silsesquioxane Crosspolymer)로 구성된 그룹으로부터 선택되는 어느 하나 이상인 것인, 화장료 조성물의 제조방법.
According to claim 8,
The spherical powder is composed of Polymethyl Methacrylate, Silica, Nylon-12, and Vinyl Dimethicone/Methicone Silsesquioxane Crosspolymer. Any one or more selected from the group consisting of, a method for producing a cosmetic composition.
상기 화장료 조성물은 수중유형(Oil-in-water) 제형으로 제조되는 것인, 화장료 조성물의 제조방법.
According to claim 8,
The method for producing a cosmetic composition, wherein the cosmetic composition is prepared in an oil-in-water formulation.
상기 제조방법은,
(c) 폴리올, 오일, 또는 유화제를 혼합하는 단계;를 추가로 포함하는 것인, 화장료 조성물의 제조방법.According to claim 8,
The manufacturing method,
(c) mixing a polyol, oil, or emulsifier; further comprising a method for producing a cosmetic composition.
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JP2021130625A (en) * | 2020-02-19 | 2021-09-09 | 株式会社トキワ | Oil-in-water type solid cosmetic and cosmetic |
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JP2021130625A (en) * | 2020-02-19 | 2021-09-09 | 株式会社トキワ | Oil-in-water type solid cosmetic and cosmetic |
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