KR102268849B1 - 그래핀 산화물의 합성을 위한 개선된 방법 - Google Patents
그래핀 산화물의 합성을 위한 개선된 방법 Download PDFInfo
- Publication number
- KR102268849B1 KR102268849B1 KR1020197005673A KR20197005673A KR102268849B1 KR 102268849 B1 KR102268849 B1 KR 102268849B1 KR 1020197005673 A KR1020197005673 A KR 1020197005673A KR 20197005673 A KR20197005673 A KR 20197005673A KR 102268849 B1 KR102268849 B1 KR 102268849B1
- Authority
- KR
- South Korea
- Prior art keywords
- graphene oxide
- graphite
- mixture
- kmno
- graphene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/198—Graphene oxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/23—Oxidation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/22—Intercalation
- C01B32/225—Expansion; Exfoliation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Nanotechnology (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US15/221,386 | 2016-07-27 | ||
| US15/221,386 US10336619B2 (en) | 2016-07-27 | 2016-07-27 | Method for the synthesis of graphene oxide |
| PCT/IB2017/054540 WO2018020439A1 (en) | 2016-07-27 | 2017-07-26 | An improved method for the synthesis of graphene oxide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20190038585A KR20190038585A (ko) | 2019-04-08 |
| KR102268849B1 true KR102268849B1 (ko) | 2021-06-28 |
Family
ID=61012180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020197005673A Expired - Fee Related KR102268849B1 (ko) | 2016-07-27 | 2017-07-26 | 그래핀 산화물의 합성을 위한 개선된 방법 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US10336619B2 (enExample) |
| JP (1) | JP6917454B2 (enExample) |
| KR (1) | KR102268849B1 (enExample) |
| AU (1) | AU2017304275B2 (enExample) |
| CA (1) | CA3031731C (enExample) |
| WO (1) | WO2018020439A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108545724B (zh) * | 2018-07-23 | 2020-06-09 | 山东玉皇新能源科技有限公司 | 石墨烯及其生产方法、用途与电池 |
| CN113213464B (zh) * | 2021-05-31 | 2022-04-29 | 杭州高烯科技有限公司 | 一种纺丝级单层氧化石墨烯浆料的制备方法 |
| KR102483223B1 (ko) * | 2021-12-23 | 2023-01-02 | 주식회사 랩엠제로 | 화학적 박리법에 기반한 산화 그래핀 제조 방법 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110262341A1 (en) * | 2010-04-25 | 2011-10-27 | Sri Lanka Institute of Nanotechnology (Pvt) Ltd. | Process for preparation of carbon nanotubes from vein graphite |
| US20130190449A1 (en) * | 2010-10-07 | 2013-07-25 | Ian Kinloch | Method of producing graphene oxide and its uses |
| US20150071844A1 (en) | 2013-09-12 | 2015-03-12 | The Hong Kong University Of Science And Technology | Synthesis of Ultra-Large Graphene Oxide Sheets |
| US20150108400A1 (en) * | 2012-06-28 | 2015-04-23 | Idt International Co., Ltd. | Method and apparatus for manufacturing graphite oxide |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2798878A (en) | 1954-07-19 | 1957-07-09 | Nat Lead Co | Preparation of graphitic acid |
| CA2762430A1 (en) | 2009-05-22 | 2011-02-10 | William Marsh Rice University | Highly oxidized graphene oxide and methods for production thereof |
| KR102514830B1 (ko) * | 2011-09-30 | 2023-03-30 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 양극, 리튬 이차 전지, 전기 자동차, 하이브리드 자동차, 이동체, 시스템, 및 전기 기기 |
| JP2014034480A (ja) * | 2012-08-07 | 2014-02-24 | Toshiba Corp | 微細炭素の製造方法、その製造方法により製造された微細炭素及びその微細炭素を母材に添加した複合材料 |
| KR101472915B1 (ko) * | 2012-10-09 | 2014-12-16 | 주식회사 그래핀올 | 산화그래핀 형성 방법 |
| US9755227B2 (en) * | 2012-11-20 | 2017-09-05 | Nanyang Technological University | Method for forming a reduced graphene oxide/metal sulfide composite and its use as an anode for batteries |
| KR101500692B1 (ko) * | 2013-04-11 | 2015-03-09 | 주식회사 아이디티인터내셔널 | 산화흑연의 제조방법 및 제조장치 |
| EP2983808A1 (en) | 2013-04-12 | 2016-02-17 | General Electric Company | Membranes comprising graphene |
| WO2014188454A1 (en) * | 2013-05-24 | 2014-11-27 | Council Of Scientific And Industrial Research | Process for preparation of nanoporous graphene and graphene quantum dots |
| US9761894B2 (en) * | 2013-07-05 | 2017-09-12 | Daimler Ag | Porous inserts for improved coolant distribution in bipolar plate assemblies for fuel cells |
| CN105540869B (zh) | 2015-12-17 | 2018-04-03 | 苏州大学 | 一种负载脱氮副球菌的改性氧化石墨烯复合材料及其制备方法和用途 |
-
2016
- 2016-07-27 US US15/221,386 patent/US10336619B2/en active Active - Reinstated
-
2017
- 2017-07-26 AU AU2017304275A patent/AU2017304275B2/en not_active Ceased
- 2017-07-26 CA CA3031731A patent/CA3031731C/en not_active Expired - Fee Related
- 2017-07-26 KR KR1020197005673A patent/KR102268849B1/ko not_active Expired - Fee Related
- 2017-07-26 WO PCT/IB2017/054540 patent/WO2018020439A1/en not_active Ceased
- 2017-07-26 JP JP2019526384A patent/JP6917454B2/ja not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110262341A1 (en) * | 2010-04-25 | 2011-10-27 | Sri Lanka Institute of Nanotechnology (Pvt) Ltd. | Process for preparation of carbon nanotubes from vein graphite |
| US20130190449A1 (en) * | 2010-10-07 | 2013-07-25 | Ian Kinloch | Method of producing graphene oxide and its uses |
| US20150108400A1 (en) * | 2012-06-28 | 2015-04-23 | Idt International Co., Ltd. | Method and apparatus for manufacturing graphite oxide |
| US20150071844A1 (en) | 2013-09-12 | 2015-03-12 | The Hong Kong University Of Science And Technology | Synthesis of Ultra-Large Graphene Oxide Sheets |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2017304275B2 (en) | 2019-11-14 |
| CA3031731C (en) | 2021-06-08 |
| US10336619B2 (en) | 2019-07-02 |
| AU2017304275A1 (en) | 2019-03-14 |
| US20180029887A1 (en) | 2018-02-01 |
| JP2019523210A (ja) | 2019-08-22 |
| KR20190038585A (ko) | 2019-04-08 |
| CA3031731A1 (en) | 2018-02-01 |
| JP6917454B2 (ja) | 2021-08-11 |
| WO2018020439A1 (en) | 2018-02-01 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Sharma et al. | Investigation of bandgap alteration in graphene oxide with different reduction routes | |
| Lavin-Lopez et al. | Influence of the reduction strategy in the synthesis of reduced graphene oxide | |
| Yang et al. | Influence of pH on the fluorescence properties of graphene quantum dots using ozonation pre-oxide hydrothermal synthesis | |
| Santamaría-Juárez et al. | Safer modified Hummers’ method for the synthesis of graphene oxide with high quality and high yield | |
| Sengupta et al. | Characterization of structural transformation of graphene oxide to reduced graphene oxide during thermal annealing | |
| Romero et al. | Comparative study of different scalable routes to synthesize graphene oxide and reduced graphene oxide | |
| Yang et al. | A facile green strategy for rapid reduction of graphene oxide by metallic zinc | |
| Mhamane et al. | From graphite oxide to highly water dispersible functionalized graphene by single step plant extract-induced deoxygenation | |
| Hassan et al. | Microwave synthesis of graphene sheets supporting metal nanocrystals in aqueous and organic media | |
| Feng et al. | A green reduction of graphene oxide via starch-based materials | |
| Bystrzejewski et al. | Continuous synthesis of carbon-encapsulated magnetic nanoparticles with a minimum production of amorphous carbon | |
| EP2905257A1 (en) | Method of production of graphite oxide and uses thereof | |
| Lu et al. | Preparation of MoO 3 QDs through combining intercalation and thermal exfoliation | |
| US9926202B2 (en) | Graphene quantum dots, their composites and preparation of the same | |
| Samoilov et al. | Formation of graphene aqueous suspensions using fluorinated surfactant-assisted ultrasonication of pristine graphite | |
| Allaedini et al. | Optical investigation of reduced graphene oxide and reduced graphene oxide/CNTs grown via simple CVD method | |
| KR102268849B1 (ko) | 그래핀 산화물의 합성을 위한 개선된 방법 | |
| KR101640988B1 (ko) | 그래핀-산화티타늄 나노복합체 제조방법 | |
| Gupta et al. | Emerging photoluminescence in azo-pyridine intercalated graphene oxide layers | |
| Barman et al. | Hexamethylenetetramine mediated simultaneous nitrogen doping and reduction of graphene oxide for a metal-free SERS substrate | |
| Wang et al. | Thiourea dioxide as a green reductant for the mass production of solution-based graphene | |
| Chen et al. | Synthesis of zirconium carbide (ZrC) nanoparticles covered with graphitic “windows” by pulsed plasma in liquid | |
| KR101970502B1 (ko) | 그래핀 및 이의 제조방법 | |
| Venkanna et al. | Synthesis and characterizations of graphene oxide and reduced graphene oxide nanosheets | |
| Eksik | Large-scale production of few-layer reduced graphene oxide by the rapid thermal reduction of graphene oxide and its structural characterization |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| PA0105 | International application |
St.27 status event code: A-0-1-A10-A15-nap-PA0105 |
|
| PA0201 | Request for examination |
St.27 status event code: A-1-2-D10-D11-exm-PA0201 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
|
| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
|
| PG1501 | Laying open of application |
St.27 status event code: A-1-1-Q10-Q12-nap-PG1501 |
|
| E902 | Notification of reason for refusal | ||
| PE0902 | Notice of grounds for rejection |
St.27 status event code: A-1-2-D10-D21-exm-PE0902 |
|
| T11-X000 | Administrative time limit extension requested |
St.27 status event code: U-3-3-T10-T11-oth-X000 |
|
| E13-X000 | Pre-grant limitation requested |
St.27 status event code: A-2-3-E10-E13-lim-X000 |
|
| P11-X000 | Amendment of application requested |
St.27 status event code: A-2-2-P10-P11-nap-X000 |
|
| P13-X000 | Application amended |
St.27 status event code: A-2-2-P10-P13-nap-X000 |
|
| PE0701 | Decision of registration |
St.27 status event code: A-1-2-D10-D22-exm-PE0701 |
|
| PR0701 | Registration of establishment |
St.27 status event code: A-2-4-F10-F11-exm-PR0701 |
|
| PR1002 | Payment of registration fee |
St.27 status event code: A-2-2-U10-U12-oth-PR1002 Fee payment year number: 1 |
|
| PG1601 | Publication of registration |
St.27 status event code: A-4-4-Q10-Q13-nap-PG1601 |
|
| PC1903 | Unpaid annual fee |
St.27 status event code: A-4-4-U10-U13-oth-PC1903 Not in force date: 20240619 Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE |
|
| PC1903 | Unpaid annual fee |
St.27 status event code: N-4-6-H10-H13-oth-PC1903 Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE Not in force date: 20240619 |