KR102245041B1 - Method for preparing bathbomb without rest period - Google Patents
Method for preparing bathbomb without rest period Download PDFInfo
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- KR102245041B1 KR102245041B1 KR1020190163916A KR20190163916A KR102245041B1 KR 102245041 B1 KR102245041 B1 KR 102245041B1 KR 1020190163916 A KR1020190163916 A KR 1020190163916A KR 20190163916 A KR20190163916 A KR 20190163916A KR 102245041 B1 KR102245041 B1 KR 102245041B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
Description
본 발명은 휴지기간이 없는 입욕제 제조방법 및 입욕제 조성물에 관한 것이다.The present invention relates to a bath agent manufacturing method and bath agent composition without a rest period.
입욕제는 욕제라고도 불리우며, 입욕제를 넣은 욕탕을 약탕이라고 하며, 수치요법(水治療法)에 포함되는 환자용 외에, 보건용ㅇ미용용으로도 알려져 있다. 즉, 적당한 농도로 염류나 황을 욕탕에 넣으면 피부에 대한 자극이 완화되어 장시간의 입욕에 견딜 수 있게 되므로 온천요법과 비슷한 효과를 기대할 수 있게 된다.Bathing agents are also called baths, and baths containing bathing agents are called medicinal baths, and in addition to those for patients included in hydrotherapy, they are also known for health use and beauty. In other words, if salts or sulfur are added to the bath at an appropriate concentration, irritation to the skin is relieved, allowing you to withstand a long bathing period, so you can expect an effect similar to that of hot spring therapy.
한편, 기존의 입욕제의 제조기술은 휴지기간이 있으며, 이 휴지기간을 거치지 않거나 적정시간 이상이 넘어가게 되면 입욕제의 성형이 제대로 되지 않았다. 이러한 휴지기간을 적절히 맞춘다는 것은 입욕제의 대량생산에 있어 큰 걸림돌이 되었다. On the other hand, the existing bath agent manufacturing technology has a period of rest, and if the period of rest is not passed or exceeds an appropriate period of time, the bath agent has not been properly molded. Proper adjustment of these rest periods has become a major obstacle to mass production of bath products.
이에, 휴지기간을 거치지 않고 천연 입욕제를 대량 생산할 수 있는 기술의 개발이 필요한 실정이다.Accordingly, there is a need to develop a technology capable of mass-producing natural bath products without going through a period of rest.
본 발명의 목적은 대량생산을 위한 휴지기간이 없는 천연 입욕제 제조방법을 제공하는 데에 있다.It is an object of the present invention to provide a method for manufacturing a natural bathing agent that does not have a rest period for mass production.
또한, 본 발명의 다른 목적은 대량생산을 위한 휴지기간이 없는 입욕제 조성물을 제공하는 데에 있다.In addition, another object of the present invention is to provide a bath composition for mass production without a rest period.
상기 목적을 달성하기 위하여, 본 발명은 조성물 총 100g 중에 중탄산나트륨 40-80g, 유기산 40-80g, 수용성 추출물 0.01-2g, 오일 0.01-5g 및 잔량의 정제수를 포함하며, 수분 함량이 1-3 v/v%인 것을 특징으로 하는 입욕제 조성물을 제공한다.In order to achieve the above object, the present invention comprises 40-80 g of sodium bicarbonate, 40-80 g of organic acid, 0.01-2 g of aqueous extract, 0.01-5 g of oil, and the remaining amount of purified water in a total of 100 g of the composition, and the moisture content is 1-3 v It provides a bath composition, characterized in that /v%.
또한, 본 발명은 중탄산나트륨, 유기산, 분말형 계면활성제를 혼합하는 단계(제1단계); 수용성 추출물, 향유 및 오일을 혼합하는 단계(제2단계); 상기 제1단계의 혼합물과 제2단계의 혼합물을 섞어 반죽하는 단계(제3단계); 상기 제3단계의 반죽을 성형틀에 넣어 몰딩하는 단계(제4단계); 및 상기 제4단계의 성형틀에 넣은 반죽을 건조하여 굳도록 만드는 단계(제5단계)를 포함하는 입욕제의 제조방법을 제공한다.In addition, the present invention comprises the steps of mixing sodium bicarbonate, an organic acid, and a powdery surfactant (first step); Mixing the water-soluble extract, the fragrance oil, and the oil (second step); Mixing and kneading the mixture of the first step and the mixture of the second step (third step); Putting the dough of the third step into a mold for molding (step 4); And it provides a method for producing a bath agent comprising the step of drying the dough put in the molding mold of the fourth step to harden (step 5).
본 발명에 따른 입욕제 제조방법은 완제품의 표면을 매끄럽게 하며, 찰기를 더욱 빠르게 부여하는 방식으로 구연산 등의 유기산 원료를 분쇄하여 사용할 수 있으며, 이로 인해 유기산 원료의 케이킹(Caking) 현상을 유도할 수 있다. 또한, 본 발명에 따르면, 휴지기간을 거치지 않고 제조할 수 있어 기존의 입욕제 제조방법에서 원료의 특성을 훼손시키지 않으며 영양공급이 되는 원료들을 그대로 사용하면서 대량생산이 가능하며, 피부질환과 각질제거, 입욕의 특성을 유지할 수 있는 장점이 있다.The bath agent manufacturing method according to the present invention can be used by pulverizing organic acid raw materials such as citric acid in a manner that smoothes the surface of the finished product and imparts stickiness more quickly, thereby inducing a caking phenomenon of the organic acid raw material. have. In addition, according to the present invention, since it can be manufactured without going through a period of rest, it does not impair the characteristics of the raw materials in the conventional bathing agent manufacturing method, and mass production is possible while using the raw materials that are supplied with nutrition as they are, and skin diseases and dead skin cells are removed, There is an advantage of maintaining the characteristics of bathing.
이하, 본 발명을 보다 상세하게 설명한다.Hereinafter, the present invention will be described in more detail.
본 발명자는 입욕제 제조에 있어서, 기존 제조방법에서 반드시 포함하는 휴지기간을 거치지 않고 생산을 할 수 있으며, 원료끼리 반응하여 단단하게 경화되는 시간이 짧기에 대량생산에 적합한 천연 입욕제 제조방법을 개발하고자 예의노력한 결과, 본 발명을 완성하게 되었다.The present inventor is polite to develop a natural bath agent manufacturing method suitable for mass production because it can be produced without going through the pause period that is necessarily included in the existing manufacturing method, and the time to harden hard due to reaction between raw materials is short. As a result of efforts, the present invention has been completed.
본 발명에서 "휴지기간이 없다"는 것은 원료상의 반응이 적다는 것이고, 수성성분과 만나서 탄산염(염기)와 유기산이 반응하여 발생하는 이산화탄소의 소실이 적다는 것을 의미하며, 이러한 부분은 완제품의 생산에 있어 제품의 탄산력을 한층 강하게 해 주어 제품의 탄산거품 분사력 면에서 더욱 우수하게 될 수 있다는 것을 의미한다.In the present invention, "there is no rest period" means that the reaction on the raw material is small, and the carbon dioxide (base) and organic acid react with the aqueous component, resulting in less loss of carbon dioxide. It means that the product's carbonation power can be further strengthened, so that the product's carbonic acid foam spraying power can be more excellent.
이에, 본 발명은 조성물 총 100g 중에 중탄산나트륨 40-80g, 유기산 40-80g, 수용성 추출물 0.01-2g, 오일 0.01-5g 및 잔량의 정제수를 포함하며, 수분 함량이 1-3 v/v%인 것을 특징으로 하는 입욕제 조성물을 제공한다.Accordingly, the present invention includes 40-80g of sodium bicarbonate, 40-80g of organic acid, 0.01-2g of aqueous extract, 0.01-5g of oil, and the remaining amount of purified water in a total of 100g of the composition, and the moisture content is 1-3 v/v%. It provides a bath composition characterized in that.
상기 조성물은 소듐라우릴설포아세테이트(SLSA) 또는 소듐코코일이세치오네이트(SCI) 등의 기타 계면활성제와 향유 중 하나 이상을 더 포함할 수 있고, 조성물 100g 당 0.1-2g의 함량으로 포함될 수 있다.The composition may further include one or more of other surfactants and perfume oils such as sodium lauryl sulfoacetate (SLSA) or sodium cocoyl isethionate (SCI), and may be included in an amount of 0.1-2 g per 100 g of the composition. have.
상기 유기산은 구연산, 사과산 및 주석산으로 이루어진 군에서 선택된 하나 이상의 유기산일 수 있지만, 이에 한정되는 것은 아니다.The organic acid may be one or more organic acids selected from the group consisting of citric acid, malic acid, and tartaric acid, but is not limited thereto.
상기 수용성 추출물은 프로폴리스 추출물일 수 있지만, 이에 한정되는 것은 아니다.The water-soluble extract may be a propolis extract, but is not limited thereto.
상기 오일은 올리브오일, 녹차씨오일, 달맞이꽃오일, 아보카도오일, 아르간커넬오일 및 메도우폼씨드오일로 이루어진 군에서 선택된 하나 이상의 식물성 오일일 수 있지만, 이에 한정되는 것은 아니다.The oil may be one or more vegetable oils selected from the group consisting of olive oil, green tea seed oil, evening primrose oil, avocado oil, argan kernel oil, and meadow foam seed oil, but is not limited thereto.
또한, 본 발명에서는 휴지기간이 없는 천연 입욕제의 대량생산방법을 제공한다.In addition, the present invention provides a mass production method of a natural bathing agent without a rest period.
보다 상세하게는, 본 발명은 중탄산나트륨, 유기산, 분말형 계면활성제를 혼합하는 단계(제1단계); 수용성 추출물, 향유 및 오일을 혼합하는 단계(제2단계); 상기 제1단계의 혼합물과 제2단계의 혼합물을 섞어 반죽하는 단계(제3단계); 상기 제3단계의 반죽을 성형틀에 넣어 몰딩하는 단계(제4단계); 및 상기 제4단계의 성형틀에 넣은 반죽을 건조하여 굳도록 만드는 단계(제5단계)를 포함하는 입욕제의 제조방법을 제공한다.More specifically, the present invention comprises the steps of mixing sodium bicarbonate, an organic acid, and a powdered surfactant (first step); Mixing the water-soluble extract, the fragrance oil, and the oil (second step); Mixing and kneading the mixture of the first step and the mixture of the second step (third step); Molding the dough of the third step into a mold (step 4); And it provides a method for producing a bath agent comprising the step of drying the dough put in the molding mold of the fourth step to harden (step 5).
상기 제조방법은 22-28℃의 온도에서 20-50%의 습도 조건 하에서 수행되는 것이 바람직하다. The manufacturing method is preferably carried out under a humidity condition of 20-50% at a temperature of 22-28 ℃.
보다 상세하게는, 상기 제조방법에 있어서 온도와 습도는 매우 중요한 부분을 차지한다. 온도는 28℃ 이하가 적절하며, 28℃에서 22℃까지의 온도 차이는 반죽의 수분기를 유지시간에서 차이를 만들게 된다. 온도가 28℃에서 27℃로 내려가면 수분 유지시간은 1~2분 정도 향상되고, 22℃까지 1℃씩 내려감에 따라 반죽의 수분 유지시간이 일정하게 늘어나게 된다. 22℃ 미만에서 유지시간은 거의 비슷하다. 이 때, 습도는 50% 이하로 유지되어야 하고, 20% 미만의 반죽 상태는 거의 비슷하다. 수분 유지시간은 반죽을 손으로 뭉쳤을 때 그 모습이 부서지지 않고 유지되는 것으로 확인할 수 있다.More specifically, temperature and humidity occupy a very important part in the manufacturing method. The temperature should be less than 28℃, and the difference in temperature from 28℃ to 22℃ makes a difference in the retention time of the moisture content of the dough. When the temperature decreases from 28℃ to 27℃, the moisture retention time improves by 1 to 2 minutes, and as the temperature decreases by 1℃ to 22℃, the moisture retention time of the dough increases. The holding time is almost the same below 22℃. At this time, the humidity should be kept below 50%, and the state of the dough below 20% is almost the same. Moisture retention time can be confirmed that the shape of the dough remains unbroken when it is lumped together by hand.
상기 제2단계는 향유 및 오일을 먼저 투입하고 수용성 추출물을 나중에 투입하여 유중수형(water-in-oil (w/o))의 형태로 혼합하는 것이 바람직하다. 이는 수용성 성분이 반죽에 직접적으로 닿는 것을 어느 정도 방지해 주며, 반죽의 반응을 지연시켜 오랫동안 반죽의 찰기가 유지되도록 해 준다.In the second step, it is preferable that the perfume oil and oil are first added, followed by the aqueous extract, and mixed in a water-in-oil (w/o) form. This prevents the water-soluble ingredients from directly contacting the dough to some extent, and delays the reaction of the dough to keep the dough sticky for a long time.
상기 제3단계의 반죽은 수분이 1-3 v/v%이며, 5-10분 동안 수행하는 것이 바람직하다. 이때, 반죽시간이 10분을 초과하여 길어지면 공기 중에 수분이 더 많이 날라가게 되어 반죽의 수분 유지시간이 줄어들게 된다. 또한 손으로 반죽 시 손의 열기가 반죽에 닿게 되어 마찬가지로 반죽의 수분 유지시간이 줄어들게 된다.The dough in the third step has a moisture content of 1-3 v/v%, and is preferably performed for 5-10 minutes. At this time, if the kneading time is longer than 10 minutes, more moisture is carried out into the air, so that the moisture retention time of the dough is reduced. In addition, when kneading by hand, the heat of the hand touches the dough, thus reducing the moisture retention time of the dough.
상기 제4단계에서 반죽을 성형틀에 넣어 몰딩하는 것은 반죽의 양을 조절하여 총 시간이 30분을 초과하지 않도록 하는 것이 바람직하다.In the fourth step, it is preferable that the total time does not exceed 30 minutes by adjusting the amount of dough to mold the dough into a mold.
상기 제5단계는 몰드를 빼지 않고 그대로 6시간-12시간 동안 건조하여 덜 굳었을 때 모양이 망가지는 것을 방지한다.In the fifth step, the mold is dried for 6 to 12 hours without removing the mold to prevent the shape from being damaged when it is less hardened.
본 발명에 따른 제조방법에서 중탄산나트륨과 같은 탄산염과 구연산과 같은 유기산을 제외한 분말타입 원료의 총 합이 11%가 넘지 않도록 한다. 11%가 넘어가게 되면 탄산염과 유기산이 반응하며 고체화되는 과정을 방해하여 제품의 경도가 떨어지게 될 수 있다. 이러한 방해 원료에는 옥수수전분, 계면활성제, 소금 등도 포함이 된다.In the manufacturing method according to the present invention, the total amount of the powder type raw materials excluding carbonates such as sodium bicarbonate and organic acids such as citric acid is not to exceed 11%. If the content exceeds 11%, the carbonic acid salt and the organic acid react, and the solidification process may be hindered, resulting in a decrease in the hardness of the product. These interfering ingredients include corn starch, surfactants, salt, and the like.
본 발명에 따른 입욕제의 성능을 확인하기 위하여, 목욕을 하는 사람들 100명을 대상으로 본 발명에 따른 입욕제를 일주일에 3회씩 한달간 사용하게 한 후, 혈액순환 개선 효과, 노폐물 배출 효과, 피로 회복 효과, 혈압 강하 효과, 피부질환 개선 효과 및 냄새 제거 효과를 분석하였다. In order to confirm the performance of the bath agent according to the present invention, after making the bath agent according to the present invention use the bath agent according to the present invention three times a week for a month for 100 people taking a bath, the effect of improving blood circulation, the effect of discharging wastes, the effect of recovering from fatigue, Blood pressure lowering effect, skin disease improvement effect, and odor removal effect were analyzed.
이때, 물을 목욕하기에 적당한 온도인 섭씨 40 내지 42℃로 맞추고, 물의 양은 몸의 2/3이 잠길 정도의 양을 용기에 담아 놓은 후, 본 발명의 입욕제 100mg을 넣고 15분 정도로 목욕을 수행하였다.At this time, the water is set to a temperature of 40 to 42°C, which is an appropriate temperature for bathing, and the amount of water is about 2/3 of the body soaked in a container, and then 100 mg of the bath agent of the present invention is added and the bath is performed for about 15 minutes. I did.
그 결과, 하기 표 1을 참조하여 보면, 본 발명의 입욕제가 혈액순환 개선, 노폐물 배출, 피로 회복, 혈압 강하, 피부질환 효과 및 냄새 제거에 있어서 우수한 효과를 나타내는 것을 확인할 수 있었다. As a result, referring to Table 1 below, it was confirmed that the bath agent of the present invention exhibited excellent effects in improving blood circulation, discharging waste products, recovering from fatigue, lowering blood pressure, skin disease effects, and odor removal.
이상으로 본 발명의 특정한 부분을 상세히 기술한 바, 당업계의 통상의 지식을 가진 자에게 있어서 이러한 구체적인 기술은 단지 바람직한 구현 예일 뿐이며, 이에 본 발명의 범위가 제한되는 것이 아닌 점은 명백하다. 따라서, 본 발명의 실질적인 범위는 첨부된 청구항과 그의 등가물에 의하여 정의된다고 할 것이다.As the specific parts of the present invention have been described in detail above, it is obvious that these specific techniques are only preferred embodiments, and the scope of the present invention is not limited thereto for those of ordinary skill in the art. Accordingly, it will be said that the substantial scope of the present invention is defined by the appended claims and their equivalents.
본 발명의 범위는 후술하는 특허청구범위에 의하여 나타내어지며, 특허청구범위의 의미 및 범위 그리고 그 균등 개념으로부터 도출되는 모든 변경 또는 변형된 형태가 본 발명의 범위에 포함되는 것으로 해석되어야 한다.The scope of the present invention is indicated by the claims to be described later, and all changes or modified forms derived from the meaning and scope of the claims and their equivalent concepts should be construed as being included in the scope of the present invention.
Claims (9)
향유 및 오일을 먼저 투입하고 프로폴리스 추출물을 나중에 투입하여 유중수형(water-in-oil (w/o))의 형태로 혼합하는 단계(제2단계);
상기 제1단계의 혼합물과 제2단계의 혼합물을 섞어 반죽하는 단계(제3단계);
상기 제3단계의 반죽을 성형틀에 넣어 몰딩하는 단계(제4단계); 및
상기 제4단계의 성형틀에 넣은 반죽을 건조하여 굳도록 만드는 단계(제5단계)를 포함하는 입욕제의 제조방법으로서,
상기 유기산은 구연산, 사과산 및 주석산으로 이루어진 군에서 선택된 하나 이상의 유기산이고, 상기 분말형 계면활성제는 소듐라우릴설포아세테이트(SLSA) 또는 소듐코코일이세치오네이트(SCI)이고, 상기 오일은 올리브오일, 녹차씨오일, 달맞이꽃오일, 아보카도오일, 아르간커넬오일 및 메도우폼씨드오일로 이루어진 군에서 선택된 하나 이상의 식물성 오일이며, 상기 제조방법은 22-28℃의 온도에서 20-50%의 습도 조건 하에서 수행되며, 상기 제3단계의 반죽은 수분이 1-3 v/v%인 것을 특징으로 하는 입욕제의 제조방법.
Mixing sodium bicarbonate, an organic acid, and a powdered surfactant (first step);
Mixing in the form of a water-in-oil (w/o) by first adding the perfume oil and the oil and then adding the propolis extract later (the second step);
Mixing and kneading the mixture of the first step and the mixture of the second step (third step);
Molding the dough of the third step into a mold (step 4); And
As a method for producing a bath agent comprising the step of drying and hardening the dough put in the molding mold of the fourth step (step 5),
The organic acid is at least one organic acid selected from the group consisting of citric acid, malic acid, and tartaric acid, and the powdered surfactant is sodium lauryl sulfoacetate (SLSA) or sodium cocoyl isethionate (SCI), and the oil is olive oil , Green tea seed oil, evening primrose oil, avocado oil, argan kernel oil and meadowfoam seed oil. And, the method of manufacturing a bath agent, characterized in that the dough in the third step has a moisture content of 1-3 v/v%.
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KR101270917B1 (en) | 2010-04-20 | 2013-06-05 | 재단법인 제주테크노파크 | Functional bath cleanser composition |
KR101447427B1 (en) * | 2013-04-10 | 2014-10-08 | 주식회사 경방 | Carbonated bath preparation composite |
KR101498564B1 (en) * | 2013-04-11 | 2015-03-11 | 양명진 | Manufacturing method of solid bath |
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KR20170009411A (en) * | 2015-07-17 | 2017-01-25 | 신혜경 | Method for manufacturing natural bath preparation |
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KR101270917B1 (en) | 2010-04-20 | 2013-06-05 | 재단법인 제주테크노파크 | Functional bath cleanser composition |
KR101447427B1 (en) * | 2013-04-10 | 2014-10-08 | 주식회사 경방 | Carbonated bath preparation composite |
KR101498564B1 (en) * | 2013-04-11 | 2015-03-11 | 양명진 | Manufacturing method of solid bath |
KR20170009411A (en) * | 2015-07-17 | 2017-01-25 | 신혜경 | Method for manufacturing natural bath preparation |
KR101585635B1 (en) * | 2015-09-02 | 2016-01-14 | 신혜경 | Natural bath preparation and method for manufacturing natural bath preparation |
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