KR102173818B1 - Manufacturing method of aloeswood water, aloeswood water thereby the same that and aloeswood drink - Google Patents

Manufacturing method of aloeswood water, aloeswood water thereby the same that and aloeswood drink Download PDF

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KR102173818B1
KR102173818B1 KR1020190047289A KR20190047289A KR102173818B1 KR 102173818 B1 KR102173818 B1 KR 102173818B1 KR 1020190047289 A KR1020190047289 A KR 1020190047289A KR 20190047289 A KR20190047289 A KR 20190047289A KR 102173818 B1 KR102173818 B1 KR 102173818B1
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aloes
water
alcohol
added
acupuncture
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KR20200123999A (en
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이성용
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(주)한국국일당
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/60Sweeteners
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/20Removal of unwanted matter, e.g. deodorisation or detoxification
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2250/00Food ingredients
    • A23V2250/18Lipids
    • A23V2250/184Emulsifier
    • A23V2250/1842Lecithin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2250/00Food ingredients
    • A23V2250/70Vitamins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/14Extraction
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/24Heat, thermal treatment
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2300/00Processes
    • A23V2300/31Mechanical treatment

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
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Abstract

본 발명은 건강에 유익하고 음용이 용이한 침향수를 제조할 수 있는 새로운 방식의 침향수 제조방법 및 이에 의해 제조된 침향수, 이를 이용한 침향수 음료제조방법에 관한 것이다.
본 발명에 의하면, (1) 침향나무를 절단하여 침향나무 편을 만드는 과정; (2) 상기 (1)과정에서 만든 침향나무 편에 알코올을 첨가하여 침향의 유효성분을 추출하는 과정; (3)상기 (2)과정에서 침향의 유효성분이 추출된 용액에서 고형분을 제거하여 침향추출액을 수득하는 과정; (4) 상기 (3)과정에서 수득된 침향추출액에 정제수와 레시틴을 첨가하고 교반하는 과정; 및 (5) 상기 (4)과정에서 얻어진 교반액에서 알코올을 제거하는 과정; 포함하는 것을 특징으로 하는 침향수 제조방법 및 이에 의해 제조된 침향수, 이를 이용한 침향수 음료제조방법, 침향수 음료가 제공된다.
The present invention relates to a method for producing aloes water in a new way that can produce aloes water that is beneficial to health and is easy to drink, aloes water prepared thereby, and a method of manufacturing aloes water beverage using the same.
According to the present invention, (1) the process of cutting aloes trees to make aloes wood pieces; (2) extracting the active ingredient of aloes by adding alcohol to the aloes wood piece made in step (1); (3) a process of removing solids from the solution from which the active ingredients of aloes are extracted in the process (2) to obtain an aloes extract; (4) adding and stirring purified water and lecithin to the acupuncture extract obtained in step (3); And (5) removing alcohol from the stirring solution obtained in the step (4). There is provided a method for producing aloes water, and a method for producing aloes water, and a method for producing aloes drink using the same, and aloes water drink.

Description

침향수 제조방법 및 이에 의해 제조된 침향수, 이를 이용한 침향수 음료제조방법{Manufacturing method of aloeswood water, aloeswood water thereby the same that and aloeswood drink}Manufacturing method of aloes wood water, aloeswood water thereby the same that and aloeswood drink

본 발명은 침향수 제조방법 및 이에 의해 제조된 침향수, 이를 이용한 침향수 음료제조방법에 관한 것으로서, 보다 상세하게는 건강에 유익한 침향수를 제조할 수 있는 새로운 방식의 침향수 제조방법 및 이에 의해 제조된 침향수, 이러한 침향수를 이용하여 음용이 용이한 침향수 음료를 제조하는 방법 및 이에 의해 제조된 침향수 음료에 관한 것이다. The present invention relates to a method for producing aloes water and a method for producing aloes water prepared thereby, and a method for producing aloes water beverage using the same, and more particularly, a new method of producing aloes water capable of producing aloes water that is beneficial to health, and thereby It relates to the prepared aloes water, a method of manufacturing an aloes water beverage that is easy to drink by using such aloes water, and to an aloes water beverage prepared thereby.

침향은 팥꽃나무과(Thymelaeaceae)에 속한 상록교목인 침향(Aguilaria agallocha Roxb.)의 수지가 침착된 수간목으로서, 나무에 상처가 나거나 세균, 곰팡이가 침입하였을 때 방어 작용으로 나무 줄기나 뿌리의 내부에 수지가 침착되어 생긴다. Aloes are the bestial tree in which the resin of Aguilaria agallocha Roxb., an evergreen tree belonging to the Thymelaeaceae family, is deposited. It is a protective action when a tree is damaged or when bacteria or fungi invade the inside of a tree trunk or root. It is formed by depositing resin.

이러한 침향은 오래전부터 약재나 향료로 사용되어 왔는데, 본초강목에는 진정, 건위, 통기, 소화불량, 식욕부진, 구토, 기관지천식, 조루, 정력부족 등에 효과가 있는 것으로 기록되어 있다. This acupuncture has long been used as a medicinal or fragrance, but it has been recorded that the herbal medicine is effective in soothing, dry stomach, aeration, indigestion, loss of appetite, vomiting, bronchial asthma, premature ejaculation, and lack of energy.

침향의 약리활성으로는 중추신경계에 대한 억제작용과 사하작용(瀉下作用)이 보고되어 있으며, 이밖에 항균, 항암, 항염증, 항알레르기 효과 등이 보고되고 있다. 뿐만 아니라 침향은 중추신경이완과 머리를 맑게 하는 아가롱스피롤(Agarospirol), 중추신경안정작용을 하는 아가로퓨란(Agarofuran), 항경련 작용을 하는 테르페네올(Terpineol), 중추신경계 안정작용을 하는 디하이드로퓨키논(Dehydrofukinone) 등을 유효성분으로 함유하고 있기 때문에, 중추신경계의 뇌안정작용, 중추신경이완과 뇌를 맑게 하여 기억력 및/또는 인지력 등을 향상시키는 효능을 가진다. As the pharmacological activity of acupuncture, inhibitory and saha effects on the central nervous system have been reported. In addition, antibacterial, anti-cancer, anti-inflammatory, and anti-allergic effects have been reported. In addition, acupuncture is effective in relaxing the central nervous system and clearing the head, agarospirol, agarofuran that stabilizes the central nervous system, terpineol, which acts as an anticonvulsant, and stabilizes the central nervous system. Since it contains dehydrofukinone, etc. as an active ingredient, it has the effect of improving the brain stability of the central nervous system, relaxation of the central nervous system and clearing the brain to improve memory and/or cognition.

따라서 침향은 기억력을 증진시키고, 학습능력을 향상시키므로 영유아 및 청소년의 학습능력 향상과 기억력 증진뿐만 아니라, 초로기 및 노년기의 노화로 인한 기억력 장애 또는 치매의 예방 및 치료제로서도 유용하다. Therefore, since acupuncture improves memory and learning ability, it is useful not only to improve learning ability and memory of infants and young children, but also to prevent and treat memory disorders or dementia caused by aging in early and old age.

한편, 침향나무를 알코올을 용매하여 침향의 유효성분 즉, 수지성분을 추출하는데, 용매, 즉, 알코올을 제거하면 고형의 침향을 얻게 된다. 그런데 침향은 수지성분으로서 유성이기 때문에 침향은 물에 용해되지 않는다. 따라서 침향을 액상으로 만들기 위해서는 알코올에 용해시켜야 하였으므로, 수용액 상태의 침향수를 제조하기가 곤란하였다. On the other hand, the aloes wood is used as a solvent to extract the active ingredient, that is, the resin component of aloes, and when the solvent, that is, alcohol, is removed, solid aloes are obtained. However, since aloes are oily as a resin component, they are not soluble in water. Therefore, in order to make the acupuncture liquid into a liquid state, it has to be dissolved in alcohol, so it was difficult to prepare acupuncture water in an aqueous solution.

대한민국 공개특허 제10-2018-0013245호(2018. 02. 07.)Republic of Korea Patent Publication No. 10-2018-0013245 (2018.02.07.) 대한민국 등록특허 제10-1888587호(2018. 08. 08)Korean Registered Patent No. 10-1888587 (2018. 08. 08) 대한민국 등록특허 제10-1044641호(2011. 06. 21)Korean Patent Registration No. 10-1044641 (2011. 06. 21)

본 발명은 상기와 같은 문제점에 착안하여 제안된 것으로서, 침향의 유효성분들을 물에 분산시킨 침향수를 제조할 수 있는 방법과, 이러한 방법을 이용하여 제조되어 건강에 유익하고 마시기 좋은 침향수 및 침향수 음료를 제공하는 것이다. The present invention has been proposed in view of the above problems, and a method capable of preparing aloes water in which active ingredients of aloes are dispersed in water, and acupuncture water and acupuncture that are beneficial to health and easy to drink are manufactured using this method. It is to provide perfumed drinks.

본 발명의 특징에 따르면, (1) 침향나무를 절단하여 침향나무 편을 만드는 과정; (2) 상기 (1)과정에서 만든 침향나무 편에 알코올을 첨가하여 침향의 유효성분을 추출하는 과정; (3)상기 (2)과정에서 침향의 유효성분이 추출된 용액에서 고형분을 제거하여 침향추출액을 수득하는 과정; (4) 상기 (3)과정에서 수득된 침향추출액에 정제수와 레시틴을 첨가하고 교반하는 과정; 및 (5) 상기 (4)과정에서 얻어진 교반액에서 알코올을 제거하는 과정; 포함하는 것을 특징으로 하는 침향수 제조방법 및 이에 의해 제조된 침향수가 제공된다.According to a feature of the present invention, (1) the process of cutting aloes trees to make aloeswood pieces; (2) extracting the active ingredient of aloes by adding alcohol to the aloes wood piece made in step (1); (3) a process of removing solids from the solution from which the active ingredients of aloes are extracted in the process (2) to obtain an aloes extract; (4) adding and stirring purified water and lecithin to the acupuncture extract obtained in step (3); And (5) removing alcohol from the stirring solution obtained in the step (4). There is provided a method for producing aloes water, characterized in that it comprises and aloes water produced thereby.

본 발명의 다른 특징에 따르면, 상기 (5)과정 이후에는 상기 (5)과정에서 알코올이 제거된 용액에 80℃의 정제열수를 첨가하는 과정;이 더 추가된다. According to another feature of the present invention, after the step (5), the step of adding purified hot water of 80° C. to the solution from which the alcohol is removed in the step (5) is further added.

본 발명의 또 다른 특징에 따르면, (1) 침향나무를 절단하여 침향나무 편을 만드는 과정; (2) 상기 (1)과정에서 만든 침향나무 편에 알코올을 첨가하여 침향의 유효성분을 추출하는 과정; (3)상기 (2)과정에서 침향의 유효성분이 추출된 용액에서 고형분을 제거하여 침향추출액을 수득하는 과정; (4) 상기 (3)과정에서 수득된 침향추출액에 정제수와 레시틴을 첨가하여 교반하는 과정; (5) 상기 (4)과정에서 얻어진 교반액에서 알코올을 제거하는 과정; 및 (6) 상기 (5)과정에서 알코올이 제거된 용액에 감미제를 첨가하는 과정;을 포함하는 것을 특징으로 하는 침향수 음료제조방법 및 이에 의해 제조된 침향수 음료가 제공된다. According to another feature of the present invention, (1) the process of making aloes wood by cutting the aloes; (2) extracting the active ingredient of aloes by adding alcohol to the aloes wood piece made in step (1); (3) a process of removing solids from the solution from which the active ingredients of aloes are extracted in the process (2) to obtain an aloes extract; (4) adding purified water and lecithin to the acupuncture extract obtained in step (3) and stirring; (5) removing alcohol from the stirring solution obtained in (4) above; And (6) adding a sweetener to the solution from which the alcohol has been removed in the step (5), and a method for producing an aloes water beverage, and a flavored water beverage prepared thereby.

이상과 같은 구성을 가지는 본 발명은 침향의 유효성분들이 물에 분산된 침향수를 용이하게 제조할 수 있는 새로운 방법이 제안된다. 따라서 이러한 방법에 의해 제조된 침향수를 사용하면 건강에 유익하고 마시기 좋은 음료를 만들 수 있다.The present invention having the configuration as described above proposes a new method for easily preparing aloes water in which the active ingredients of aloes are dispersed in water. Therefore, if you use the acupuncture water prepared by this method, you can make a drink that is beneficial to your health and is easy to drink.

더욱이 본 발명에 위한 침향수는 레시틴이 함유되어 침향의 약리작용과 더불어 레시틴의 효능을 얻을 수 있으므로 건강에 한층 더 유익하다. Moreover, the acupuncture water for the present invention contains lecithin, so that the pharmacological action of acupuncture and the efficacy of lecithin can be obtained, so it is more beneficial to health.

특히, 본 발명은 침향수를 희석하는 과정에서 정제열수를 사용함으로써, 희석과정에서 잔류 알코올의 제거효과도 얻을 수 있으므로 잔류 알코올을 제거하기 위해 침향수를 재차 알코올을 제거하기 위한 처리를 하지 않아도 알코올에 의한 유독성이나 부작용을 가지지 않는 침향수를 제조할 수 있는 장점을 가진다. In particular, since the present invention uses purified hot water in the process of diluting the aloes water, it is possible to obtain an effect of removing residual alcohol during the dilution process. It has the advantage of being able to manufacture acupuncture water that does not have toxicity or side effects caused by.

도 1은 본 발명의 제1실시예에 따른 제조공정도
도 2는 상기 실시예에 의해 제조된 침향수 사진
도 3은 본 발명의 비교예에 의해 제조된 침향수 사진
도 4는 본 발명의 제2실시예에 따른 제조공정도
1 is a manufacturing process diagram according to a first embodiment of the present invention
2 is a photograph of aloes water prepared according to the above example
3 is a photograph of aloes water prepared by a comparative example of the present invention
4 is a manufacturing process diagram according to a second embodiment of the present invention

이하에서, 본 발명을 좀 더 구체적으로 설명한다.In the following, the present invention will be described in more detail.

도 1은 본 발명의 제1실시예에 따른 침향수의 제조공정도이다. 본 발명의 제1실시예에 따른 제조방법을 살펴보면 다음과 같다.1 is a manufacturing process diagram of acupuncture water according to a first embodiment of the present invention. The manufacturing method according to the first embodiment of the present invention will be described as follows.

1) 침향나무를 절단한다.1) Cut the aloes trees.

침향나무를 적당한 크기로 절단하여 침향나무 편을 만든다. 바람직하게는 건조감량 8% 이하의 침향나무를 준비하여 5×8 크기로 절단한다. Cut aloes trees into suitable size to make aloes trees side. Preferably, aloes trees having a loss on drying of 8% or less are prepared and cut into 5×8 sizes.

2) 침향의 유효성분을 추출한다. 2) Extract the active ingredient of acupuncture.

침향나무 편에 알코올(주정)을 붓고 소정 시간 방치하여 침향의 유효성분을 추출한다. 바람직하게는 추출효율을 고려할 때 침향나무와 알코올 1 : 3∼5 중량비로 혼합하고 30℃에서 72시간 정도 방치하여 침향의 유효성분을 추출한다. 그리고 고형분을 제거하고 침향추출액을 수득한다. Alcohol (alcohol) is poured onto the aloes tree side and left for a predetermined time to extract the active ingredients of aloes. Preferably, when considering the extraction efficiency, the aloes wood and alcohol are mixed in a weight ratio of 1:3 to 5 and left at 30° C. for 72 hours to extract the active ingredient of the aloes. Then, the solid content is removed, and acupuncture extract is obtained.

3) 침향추출액에 정제수와 레시틴을 첨가한다. 3) Add purified water and lecithin to the acupuncture extract.

레시틴(lecithin)은 한 쪽에는 친유성이 강한 지방산기를 가지고 있고, 다른 쪽에는 친수성이 강한 , 콜린 부분을 가지고 있어서 물과 유지의 혼합물을 안정화시켜주는 유화제로서 기능을 한다. 이러한 레시틴이 사용됨에 따라 후술하는 바와 같이, 유성의 침향 유효성분들이 알코올이 제거된 상태에서 물과 안정된 에멀젼(emulsion)용액을 이룬다. Lecithin has a strong lipophilic fatty acid group on one side and a strong hydrophilic, choline portion on the other, so it functions as an emulsifier that stabilizes the mixture of water and oil. As such lecithin is used, as described later, oily acupuncture active ingredients form a stable emulsion solution with water in a state in which alcohol is removed.

다양한 종류의 유화제가 있으나, 레시틴은 알코올에 용해되기 때문에 본 발명에서 사용이 바람직한데, 특히, 레시틴은 생체막을 구성하는 주요성분으로서, 세포막의 활동을 활발하게 함으로써 세포파괴를 늦추고 조직활동을 자극해 뇌활동의 저하를 막아주며, 비타민E를 비롯한 지용성 비타민(A, D, K)의 흡수를 도와 체내효율성을 높여 피부노화를 막고 혈액순환을 원활히 해주고, 또한, 콜레스테롤의 가용화에 관여하며 혈중콜레스테롤 양을 감소시킴으로써 심근경색 등과 같은 심혈관질환의 예방에 효과가 있는 등 건강에 유용한 효능을 가지므로 본 발명에서 사용이 적합하다. There are various types of emulsifiers, but since lecithin is soluble in alcohol, it is preferred to be used in the present invention.In particular, lecithin is a major component constituting a biological membrane, and by activating the activity of the cell membrane, it slows cell destruction and stimulates tissue activity. It prevents the decline of brain activity, helps absorption of fat-soluble vitamins (A, D, K) including vitamin E, improves body efficiency, prevents skin aging and facilitates blood circulation, is also involved in the solubilization of cholesterol, and the amount of cholesterol in the blood It is suitable for use in the present invention because it has useful effects on health, such as being effective in preventing cardiovascular diseases such as myocardial infarction by reducing

바람직하게는 사용되는 침향나무 1kg 당 레시틴 100g을 첨가한다. 그리고 정제수는 전술한 과정에서 사용되는 알코올과 동량을 첨가한다. Preferably, 100 g of lecithin is added per 1 kg of aloes wood used. And purified water is added in the same amount as the alcohol used in the above-described process.

이와 같이 침향추출액에 정제수와 레시틴을 첨가하고 충분히 교반시켜 교반액을 만든다. In this way, purified water and lecithin are added to the acupuncture extract and sufficiently stirred to prepare a stirring solution.

4) 알코올을 제거한다.4) Remove alcohol.

상기 과정에서 만든 교반액에서 알코올을 제거한다. 감압증발, 증류 등의 공지된 방법으로 알코올을을 제거한다. Alcohol is removed from the stirring solution made in the above process. Alcohol is removed by known methods such as vacuum evaporation and distillation.

본 과정에서 알코올이 제거되더라도 침향의 유효성분들은 물과 분리되지 않고 레시틴에 의해 물에 안정적으로 분산되며, 이에 따라 알코올이 제거된 용액은 정제수에 침향의 유효성분이 레시틴에 의해 분산된 용액(이하, '침향수'라 칭함)이다. Even if alcohol is removed in this process, the active ingredients of acupuncture are not separated from water and are stably dispersed in water by lecithin. Accordingly, the solution from which alcohol is removed is a solution in which the active ingredient of acupuncture is dispersed by lecithin in purified water (hereinafter, It is called'chim hyangsoo').

최종적으로 0.45㎛ 크기의 필터를 사용하여 침향수를 한번 더 필터링하여 침향수를 완성한다. Finally, the aloes water is filtered once more using a 0.45㎛ size filter to complete the aloes.

실험예 1Experimental Example 1

침향나무를 5×8 크기로 절단하여 침향나무 편을 만들고, 침향나무 편 1kg에 주정 5L를 넣고 30℃에서 72시간 교반하여 침향나무의 유효성분을 추출하였다. 이어서 고형분을 제거하고 정제수 5L와 레시틴 100g을 넣고 충분히 교반시킨 후에 감압증발장치를 이용하여 주정을 제거하여 침향수를 제조하였다. The aloes trees were cut into 5×8 size to make aloeswood slices, and 5L of alcohol was added to 1kg of aloeswood slices and stirred at 30℃ for 72 hours to extract the active ingredients of the aloes trees. Subsequently, the solids were removed, 5 L of purified water and 100 g of lecithin were added, stirred sufficiently, and the alcohol was removed using a vacuum evaporator to prepare acupuncture water.

도 2는 이와 같이 제조된 침향수의 사진이다. 제조된 침향수의 침향 유효성분의 함량을 측정한 결과 침향 유효성분 함량이 10000ppm이였다. 2 is a photograph of acupuncture water prepared in this way. As a result of measuring the content of the aloes active ingredient in the prepared aloes water, the content of the aloes active ingredient was 10000ppm.

이와 같이 제조된 침향수는 도 2를 통해 확인할 수 있는 바와 같이, 침향 유효성분이 균일하게 분산된 용액으로서, 시간이 경과하더라도 침전물이 생성되지 않았다. As can be seen from FIG. 2, the aloes water prepared as described above is a solution in which the active aloes ingredients are uniformly dispersed, and no precipitate was formed even after time.

한편, 표 1은 실험예1에 의해 제조된 침향수의 항균성을 테스트한 결과이다. On the other hand, Table 1 shows the results of testing the antibacterial properties of the acupuncture water prepared according to Experimental Example 1.

시험항목Test Items 단위 unit 시험방법Test Methods 시험결과 Test result 일반세균Common bacteria Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 효모 및 곰팡이 Yeast and mold Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 대장균, 대장균군Coli, coliform Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected

비교예 1Comparative Example 1

침향나무를 5×8 크기로 절단하여 침향나무 편을 만들고, 침향나무 편 1kg에 주정 5L를 넣고 30℃에서 72시간 교반하여 침향의 유효성분을 추출하였다. 이어서 고형분을 제거하고, 정제수 5L를 넣고 충분히 교반시킨 다음, 감압증발장치를 이용하여 주정을 제거하였다. The aloes tree was cut into 5×8 size to make aloeswood slices, and 5L of alcohol was added to 1kg of aloeswood slices and stirred at 30℃ for 72 hours to extract the active ingredients of aloes. Subsequently, the solid content was removed, 5 L of purified water was added, stirred sufficiently, and the alcohol was removed using a vacuum evaporator.

도 3은 이와 같이 하여 제조된 용액의 사진으로서, 이와 같이 제조된 용액은 도 3을 통해 확인할 수 있는 바와 같이, 침향의 유효성분이 분산되지 못하고 침전되었다. 3 is a photograph of the solution prepared in this way. As can be seen through FIG. 3, the prepared solution was precipitated without dispersing the active ingredient of acupuncture.

이와 같은 방법으로 제조되는 침향수는 침향의 유효성분이 안정적으로 분산된 용액으로서, 다양한 용도로 사용이 가능하나, 음료용 원료로 사용이 적합하다. 본 발명에 의한 침향수로 음료를 제조하는 경우에는 침향수에 다른 영양성분을 추가하거나 음료에 사용되는 통상적인 감미제 등을 추가하면 거부감 없이 마시기에 좋은 음료를 만들 수 있다. Aloes water prepared in this way is a solution in which the active ingredients of aloes are stably dispersed, and can be used for various purposes, but is suitable for use as a raw material for beverages. In the case of manufacturing a beverage with aloes water according to the present invention, if other nutrients are added to the aloes water or a conventional sweetener used in beverages is added, a beverage that is good for drinking can be made without a feeling of rejection.

이때 추가되는 영양성분의 종류가 특별히 한정되지는 않으나, 전술한 바와 같이, 레시틴이 지용성 비타민의 흡수를 도와주기 때문에 비타민 E를 비롯한 지용성 비타민을 추가하는 것이 바람직하다. At this time, the type of nutrient added is not particularly limited, but as described above, since lecithin helps absorption of fat-soluble vitamins, it is preferable to add fat-soluble vitamins including vitamin E.

이하에서는 본 발명의 다른 실시예를 설명하되, 전술한 실시예와 동일한 구성 및 효과에 대해서는 설명을 생략한다.Hereinafter, other embodiments of the present invention will be described, but descriptions of the same configuration and effects as those of the above-described embodiments will be omitted.

도 4는 본 발명의 제2실시예에 따른 제조공정도이다, 본 실시예에서는 전술한 바와 같이, 교반액에서 알코올을 제거한 다음에, 80℃로 가열된 정제열수를 첨가하여 침향수를 희석하는 과정이 더 추가된다.4 is a manufacturing process diagram according to the second embodiment of the present invention. In this embodiment, after removing alcohol from the stirring liquid, as described above, the process of diluting aloes water by adding purified hot water heated to 80°C. More is added.

본 과정에서 침향수를 희석하기 위해 정제열수를 사용하는 것은 침향수에 잔류할 수 있는 알코올을 추가로 제거하여 알코올이 잔류되지 않도록 하기 위한 것이다. 즉, 희석수로 정제열수를 첨가함에 따라 정제열수의 열기에 의해 알코올이 휘발되어 추가로 제거됨으로써 알코올이 잔류할 우려가 없다. 물론, 알코올이 잔류되지 않도록 하기 위해 감압증발, 증류 등의 방법을 추가로 행할 수도 있으나, 이 경우에는 시간이 많이 소요되어 생산성이 떨어질 우려가 있는 반면에 정제열수를 사용하면 침향수를 희석하면서 아울러 잔류되는 알코올을 추가로 제거할 수 있으므로 공정이 간단하고 생산성도 향상된다. The use of purified hot water to dilute the aloes water in this process is to prevent alcohol remaining by additionally removing alcohol that may remain in the aloes water. That is, as purified hot water is added to the diluted water, alcohol is volatilized by the heat of the purified hot water and further removed, so that there is no fear that alcohol remains. Of course, in order to prevent alcohol from remaining, additional methods such as vacuum evaporation and distillation may be additionally performed.However, in this case, it takes a lot of time to reduce productivity. Since residual alcohol can be further removed, the process is simple and productivity is improved.

한편, 본 과정에서 사용되는 알코올의 끓는점(78.3℃) 보다 높은 온도의 정제열수를 사용하는데, 정제열수의 온도가 높을수록 알코올의 제거효과는 향상될 것이나, 정제열수의 온도가 높을수록 알코올이 제거되는 과정에서 침향의 향도 함께 휘발되어 침향의 향이 감소될 우려가 커지므로 이러한 점을 고려하여 정제열수의 온도를 적절히 조절할 필요가 있다. 실험에 의하면 온도가 80℃인 정제열수를 사용하는 경우에 침향의 향이 상대적으로 덜 감소되면서도 잔류되는 알코올을 효과적으로 제거할 수 있다. On the other hand, purified hot water with a temperature higher than the boiling point (78.3℃) of the alcohol used in this process is used. The higher the temperature of the purified hot water, the better the alcohol removal effect, but the higher the temperature of the purified hot water, the more alcohol is removed. In the process of becoming, the scent of acupuncture is also volatilized, and there is a greater concern that the scent of acupuncture decreases. Therefore, it is necessary to properly adjust the temperature of purified hot water in consideration of this point. According to an experiment, when purified hot water having a temperature of 80°C is used, the aroma of acupuncture is relatively reduced, and residual alcohol can be effectively removed.

실험예 2Experimental Example 2

침향나무를 5×8 크기로 절단하여 침향나무 편을 만들고, 침향나무 편 1kg에 주정 5L를 넣고 30℃에서 72시간 교반하여 침향나무의 유효성분을 추출하였다. 이어서 고형분을 제거하고 정제수 5L와 레시틴 100g을 넣고 충분히 교반시킨 후에 감압증발장치를 이용하여 주정을 제거하여 침향 유효성분 함량이 10000ppm인 침향수를 제조하였다. 제조된 침향수 100ml에 80℃인 정제열수 1L를 추가하고 고르게 교반시켜서 침향수를 희석하여, 10ppm의 희석 침향수를 만들었다. The aloes trees were cut into 5×8 size to make aloeswood slices, and 5L of alcohol was added to 1kg of aloeswood slices and stirred at 30℃ for 72 hours to extract the active ingredients of the aloes trees. Subsequently, the solids were removed, 5 L of purified water and 100 g of lecithin were added, stirred sufficiently, and the alcohol was removed using a vacuum evaporator to prepare aloes water having a content of 10000 ppm of active aloes. 1L of purified hot water at 80°C was added to 100 ml of the prepared aloes water and stirred evenly to dilute the aloes to prepare 10 ppm of diluted aloes.

이와 같이 제조된 희석 침향수의 잔류 알코올 양을 측정한 결과 표 2와 같은 결과를 얻었다. 시험방법은 KP일반시험법 중 잔류용매시험법을 사용하였다.As a result of measuring the amount of residual alcohol in the diluted aloes water prepared as described above, the results shown in Table 2 were obtained. The test method used the residual solvent test method among KP general test methods.

그리고 희석 침향수의 항균성을 테스트한 결과는 표 3과 같다.And the results of testing the antimicrobial properties of the diluted aloes are shown in Table 3.

비교예 2Comparative Example 2

정제열수 대신 상온의 정제수를 사용하는 것을 제외하고, 실험예 2와 동일한 방법으로 희석 침향수를 만들었다. 제조된 희석 침향수의 잔류 알코올 양을 측정한 결과 표 2와 같은 결과를 얻었다. 그리고 희석 침향수의 항균성을 테스트한 결과는 표 3과 같다. Diluted aloes water was prepared in the same manner as in Experimental Example 2, except that purified water at room temperature was used instead of purified hot water. As a result of measuring the amount of residual alcohol in the prepared diluted aloes water, the results shown in Table 2 were obtained. And the results of testing the antimicrobial properties of the diluted aloes are shown in Table 3.

시험항목 Test Items 단위 unit 시험결과 Test result 실험예 2Experimental Example 2 잔류용매 중 EtOHEtOH in residual solvent ppmppm 불검출Not detected 비교예 2 Comparative Example 2 잔류용매 중 EtOHEtOH in residual solvent ppmppm 0.180.18

표 2를 통해 확인할 수 있는 바와 같이, 침향수를 정제열수로 희석한 결과, 잔류알코올이 검출되지 않았다. 이를 통해 정제열수로 희석하는 과정에서 잔류하는 알코올이 추가로 제거된 것을 확인할 수 있다. As can be seen from Table 2, as a result of diluting the acupuncture water with purified hot water, residual alcohol was not detected. Through this, it can be confirmed that residual alcohol was additionally removed during the dilution with purified hot water.

시험항목Test Items 단위 unit 시험방법Test Methods 시험결과 Test result 실험예 2Experimental Example 2 일반세균Common bacteria Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 효모 및 곰팡이 Yeast and mold Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 대장균, 대장균군Coli, coliform Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 비교예 2Comparative Example 2 일반세균Common bacteria Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 효모 및 곰팡이 Yeast and mold Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected 대장균, 대장균군Coli, coliform Cfu/g(ml)Cfu/g(ml) 식품공전Food Code 불검출Not detected

표 3에서 확인할 수 있는 바와 같이, 실험예 2와 비교예 2에 의한 희석 침향수는 모두 우수한 항균성을 보였다. As can be seen in Table 3, both diluted acupuncture water according to Experimental Example 2 and Comparative Example 2 showed excellent antibacterial properties.

Claims (7)

(1) 건조감량 8% 이하의 침향나무를 절단하여 침향나무 편을 만드는 과정;
(2) 상기 (1)과정에서 만든 침향나무 편에 알코올을 1 : 3∼5 중량비로 혼합하고 30℃에서 72시간 방치하여 침향의 유효성분을 추출하는 과정;
(3) 상기 (2)과정에서 침향의 유효성분이 추출된 용액에서 고형분을 제거하여 침향추출액을 수득하는 과정;
(4) 상기 (3)과정에서 수득된 침향추출액에 정제수와 레시틴을 첨가하고 교반하는 과정; 및
(5) 상기 (4)과정에서 얻어진 교반액에서 알코올을 제거하는 과정;
(6) 상기 (5)과정에서 알코올이 제거된 용액에 80℃의 정제열수를 첨가하는 과정;을 포함하며,
상기 (4) 과정에서, 침향나무 1kg 당 레시틴 100g을 첨가하고, 정제수는 (2) 과정에서 첨가되는 알코올과 동량을 첨가하는 것을 특징으로 하는 침향수 제조방법.
(1) The process of cutting aloes trees with less than 8% loss on drying to make aloes wood slices;
(2) a process of extracting the active ingredient of aloes by mixing alcohol in a 1: 3 to 5 weight ratio to the aloes wood piece made in step (1) and leaving it at 30° C. for 72 hours;
(3) removing solids from the solution from which the active ingredients of aloes are extracted in the process (2) to obtain aloes extract;
(4) adding and stirring purified water and lecithin to the acupuncture extract obtained in step (3); And
(5) removing alcohol from the stirring solution obtained in (4) above;
(6) the process of adding purified hot water of 80°C to the solution from which the alcohol was removed in the step (5); including,
In the step (4), 100 g of lecithin per 1 kg of aloes wood is added, and the purified water is added in the same amount as the alcohol added in step (2).
삭제delete 제1항에 기재된 방법으로 제조된 것을 특징으로 하는 침향수.
Aloes water produced by the method according to claim 1.
(1) 건조감량 8% 이하의 침향나무를 절단하여 침향나무 편을 만드는 과정;
(2) 상기 (1)과정에서 만든 침향나무 편에 알코올을 1 : 3∼5 중량비로 혼합하고 30℃에서 72시간 방치하여 침향의 유효성분을 추출하는 과정;
(3) 상기 (2)과정에서 침향의 유효성분이 추출된 용액에서 고형분을 제거하여 침향추출액을 수득하는 과정;
(4) 상기 (3)과정에서 수득된 침향추출액에 정제수와 레시틴을 첨가하여 교반하는 과정;
(5) 상기 (4)과정에서 얻어진 교반액에서 알코올을 제거하는 과정; 및
(6) 상기 (5)과정에서 알코올이 제거된 용액에 감미제 및 지용성 비타민을 첨가하는 과정;을 포함하며,
상기 (4) 과정에서, 침향나무 1kg 당 레시틴 100g을 첨가하고, 정제수는 (2) 과정에서 첨가되는 알코올과 동량을 첨가하고,
상기 (5)과정과 (6)과정 사이에는 80℃로 가열된 정제열수를 첨가하여 교반시키는 과정;이 더 추가되는 것을 특징으로 하는 침향수 음료제조방법.
(1) The process of cutting aloes trees with less than 8% loss on drying to make aloes wood slices;
(2) a process of extracting the active ingredient of aloes by mixing alcohol in a 1: 3 to 5 weight ratio to the aloes wood piece made in step (1) and leaving it at 30° C. for 72 hours;
(3) removing solids from the solution from which the active ingredients of aloes are extracted in the process (2) to obtain aloes extract;
(4) adding purified water and lecithin to the acupuncture extract obtained in step (3) and stirring;
(5) removing alcohol from the stirring solution obtained in (4) above; And
(6) a process of adding a sweetener and a fat-soluble vitamin to the solution from which the alcohol has been removed in the step (5); and,
In the step (4), 100 g of lecithin per 1 kg of aloes wood is added, and purified water is added in the same amount as the alcohol added in step (2),
A process of stirring by adding purified hot water heated to 80° C. between the (5) and (6) processes; a method for producing aromatized water beverage, characterized in that further added.
삭제delete 삭제delete 제4항에 기재된 방법으로 제조된 것을 특징으로 하는 침향수 음료.Aromatized beverage beverage produced by the method according to claim 4.
KR1020190047289A 2019-04-23 2019-04-23 Manufacturing method of aloeswood water, aloeswood water thereby the same that and aloeswood drink KR102173818B1 (en)

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KR100931880B1 (en) * 2009-08-28 2009-12-15 지영학 An oriental drink containing an aloeswood, a sasa borealis, an polygala tenuifolia and a zizyphus jujuba and manufacturing method thereof

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KR101044641B1 (en) 2008-10-08 2011-06-29 정항교 method for manufacturing an agilawood
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KR20160134375A (en) * 2015-05-15 2016-11-23 주식회사 네이처텍 Water soluble composition comprising ginseng seed oil
KR20180013245A (en) 2016-07-29 2018-02-07 안진희 Method for manufacturing agarwood extract
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KR100931880B1 (en) * 2009-08-28 2009-12-15 지영학 An oriental drink containing an aloeswood, a sasa borealis, an polygala tenuifolia and a zizyphus jujuba and manufacturing method thereof

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