KR102036480B1 - Manufacturing method for composition for eliminating chicken mite and composition for eliminating chicken mite prepared using the same - Google Patents

Abstract

The present invention relates to a method of preparing a composition for eliminating Argas persicus and a composition for eliminating Argas persicus prepared thereby. In one embodiment, the method of preparing a composition for eliminating Argas persicus comprises the steps of: preparing a mixture including fermented Prunus mume fruits, a Scutellaria baicalensis extract, a Lithospermum erythrorhizon Sieb. et Zucc. extract, a Cinnamomum cassia extract, and Phellodendron bark; and aging the mixture. According to the present invention, the composition is harmless to humans and livestock, thereby being environmental friendly.

Description

TECHNICAL MANUFACTURING MANUFACTURING COMPOSITION FOR ELIGIBILITY CHICKET COMPOSITION AND MANUFACTURING COMPOSITION FOR ELIGIBILITY CHICKEN TECHNICAL TECHNICAL FIELD

The present invention relates to a method for preparing chicken mite-treating composition, and a composition for combating chicken mite prepared thereby. More specifically, the present invention relates to a method for preparing chicken mites and a composition for combating chicken mites, which is excellent in killing and controlling environmentally friendly wagumo, which are parasitic in poultry such as chicken, using natural herbal medicines.

Control of chicken mites (chicken scabies or wagumo, Dermanyssus gallinae ) is known as a major problem in farms that raise poultry such as chickens. The chicken tick is a generic term for a group of alternating animals belonging to the spider web mite family, and is distinguished from insects. The body unites the head and abdomen in one body to form an elliptical or ovoid body, and has a mouth ball called a bulge that protrudes in shear. . There is a remarkable difference in size and shape depending on the type, and there is a slight thickness of 0.1 mm or less since the length becomes 1 cm or more. The larva has three generations and the adult has four generations. Mites have many types of blood-sucking and play an important role as pests of humans and livestock and as propagators of various pathogens.

Especially in laying hens, the damage caused by chicken mites is even greater because of the environment in which chickens are raised. These ticks, about 0.5mm in size, are hard to see with the naked eye, hiding in the dark during the day, and at night, they are vampires. In addition, due to the recent domestic climate change, the temperature has risen sharply, and the number of chicken ticks has soared, causing more damage to laying hens.

Chickens have a survival instinct to get rid of pests, such as fleas and ticks, by taking a dirt bath that rubs the soil or spraying sand with their feet. However, in the current environment, chickens can't get rid of ticks on their own, and chickens with better vision than humans can easily find ticks that move in their feathers and around their bodies. Or pecking around the body of the chicken, due to the wound caused by the blood, the chicken is excited to see the blood is more severely damaged the wound, even if the death occurs. For this reason, pesticides are sprayed on chicken farms to control pests.

However, chicken mites become resistant to insecticides, and the spread of insecticides is inevitably increased, and indiscriminate use of insecticides for mass breeding causes residual pesticides to accumulate in the body of poultry such as chickens. There is a possibility of ingesting pesticides, resulting in consumer complaints.

Therefore, while preventing the accumulation of pesticide components in poultry bodies such as chickens, there is an increasing demand for chicken mite control for efficient and healthy poultry breeding.

Meanwhile, plum ( Prunus) mume ) is a natural fire extinguishing agent that stimulates the sour taste organ to make digestive juices and helps the stomach to function properly. Plum is rich in citric acid, which acts to break down and release lactic acid, which can be effective in relieving fatigue. It is good for prevention of food poisoning because it lives. The catechins contained in the plums promote bowel movements, helping to relieve constipation and intestinal health. In addition, the plum is excellent sterilization and detoxification in the body, diarrhea or stomach ache if you drink it helps. Plum tree is a member of the family Rosaceae, also known as plum tree (梅花-). Flowers bloom before leaves in March-April, and fruits ripen round in June-July. Eat fruit called plum. Plum trees are called early blooms for early blooms, cold winters for Dongmae, Hanmae, and snow blooms.

Golden ( Scutellaria baicalensis ) is native to northern China. In Korea, about 10 species grow, including thimble flowers and shading thimble flowers. Breed as seeds. It grows at the foot of mountains all over the country and is also grown as a herb. It is about 60cm tall and several square stems come from the root. Leaves are opposite, 4.5cm long, 8mm butterfly, lanceolate, narrow at both ends, flat at the edges, and smaller at the top. Petiole almost 2mm long. Purple flowers bloom in July-August, forming a gunshot inflorescence at the end of stems and branches. Inflorescences have leaves, with one flower per axillary. The flower is 1.5 ~ 2.5cm long, curled at the bottom, and stands straight. The bottom is tubular, the top is both lips, and the top is divided into two. The calyx is also shaped like a lip and has a prominent appendage at the top. Surgery 4 and 2 long. The pistil is one and the ovary is deeply divided into four. The gold is used for food, industrial, wheat, and ornamental, and it can be used for treatment of symptoms such as blue-heat damp bath, detoxification, anxiety, gastritis, enteritis, antitussive, etc.

Yellow-backed Phellodendron Bark or Phellodendron amurense RUPR ) is also known as the Rhubarb , and lives in deep mountainous areas. It is about 15m high and thick branches spread all around. The bark is light gray, deeply cracked due to the development of cork. Mature branches are yellowish grey, and the endothelium is bright yellow. The leaves of the yellowish white leaves are 20-40 cm in length, have a mesenchymal disease, and are a single right upper lobe composed of 5 to 13 leaflets. Leaflets are narrow ovate or ovate oblong, 5 ~ 10㎝ long, 3 ~ 5㎝ wide, pointed long like tail, rounded at the bottom, dark green on the surface and white on the back.

The yellow and white flowers run on the male and female trees, bloom in June, and hang on the inflorescences. Inflorescences have fine hairs, 5-7cm in diameter. Flowers are short, 6mm long, petals and calyxes are 5 ~ 8 each, calyx is 1mm long, petals are 4mm long, with hairs on the inside of the operating table. The fruits of the yellow and white are black and round, and the branch is 5, each containing one seed and matures in September. Fruits do not fall in winter and remain on the tree. The yellow wall is a name that comes from the yellow inner skin. The oriental medicine is used as a medicinal endothelium of the yellow and white, weakness (고) and high (苦), health, cleansing, suit, humidity (燥濕), detoxification, convergence and sterilization effect is known. The soybean is used for symptoms such as indigestion, gastritis, enteritis, diarrhea, hepatitis, jaundice, cirrhosis, meningitis, target pain, stomatitis and swelling. The endothelium has also been used as a yellow dye. In the main river, it is called wall tree, and it is called yellow white depending on the area.

Cinnamomum cassia is native to Sri Lanka and southern India and is grown today in all tropical regions. Dried bark is curved or half curled, forming irregular pieces. The thickness is usually 3mm and the color of the outer part is blackish brown or black red, and there are spots like grey-white flowers. Inner dark red to black red. The outer layer of the cut surface is grayish brown. The essential oil component of cinnamon is cinnamaldehyde (cinnamaldehyde) is the main component. This ingredient improves blood circulation, anti-cancer, anti-inflammatory effect and is also used as a food additive or flavoring.

The cinnamon put the stem bark 1 ~ 5g in 800mL of water, decoction, can be divided into half and drink in the morning and evening. In Korea, Cinnamomum cassia Blume (肉桂) or bark of bark of the same plant is removed from the bark. China is the same as Korea, and Japan is the broiler with Cinnamomum zeylanicum Blume : 玉桂) is a process herbal medicine.

Lithospermum erythrorhizon Sieb et Zucc . ) Is the Chinese character of vinegar, vinegar, and root. The size is 50-100cm and bristles are densely located in the whole. Stems stand straight and upper branches split into two or three branches. The flower of the white 5th edition has 5 scales in the flower bed. The size of the flower is 5-8 mm. The leaves are alternate, thick, and sharp at both ends, and there are no crabs. The root is divided into ginseng shape. It is thick and thick purple color is formed around the outer skin, which is strong purple. Therefore, the earthy color around which we grow grows purple. Growth conditions are suitable for the condition that only the stems are sunshine in the weeds of the mountain meadows and there is no direct sunlight on the roots. In our country, it is wild throughout the country except North Hamgyong, Gyeongsangnam-do, and Jeju. The cultivation of the soybean is not moist, but is sown in March in white soft soil or blue limbs of high fields. It is easy to cultivate for a year, but it is difficult to cultivate it for perennial plants because it blooms and seeds for a year.

Licorice root is used as a dye or medicine. It is known that the dye was already used during Qi, according to Han Bisa. By the time of the war, the purple symbolizes authority and is used for round trips and clothes worn by high-ranking people. In our country, Goguryeo, Baekje, and Silla all have institutionalized grace with color, and purple was the highest color.

The prior art related to the present invention is Republic of Korea Patent Publication No. 10-1537197 (2015.07.15 Announcement, the name of the invention: produced by the method of spraying for killing the weevils of poultry and the method of killing weaving of poultry and the method of killing the poultry wagumo Poultry and eggs).

One object of the present invention relates to a method for preparing a composition for combating chicken mites, which has excellent pest control, pest avoidance and killing effects such as chicken mite in chicken kennels, and has excellent sustainability of the control effect.

Another object of the present invention is harmless to humans and livestock and is excellent in environmental friendliness, and relates to a method for preparing a composition for combating chicken mites that can be directly sprayed in cages.

Still another object of the present invention is to provide a method for preparing a composition for combating chicken mites, which has excellent storage stability and excellent odor reduction effect in cages.

Another object of the present invention relates to a method for producing a composition for combating chicken mites excellent in economics and productivity.

Another object of the present invention relates to a method for producing a composition for combating chicken mites with less animal avoidance and excellent feed palatability when spraying in a kennel.

Another object of the present invention relates to a composition for combating chicken mites prepared by the method for producing a composition for combating chicken mites.

One aspect of the invention relates to a method for preparing a composition for combating chicken mites. In one embodiment the method for the composition for combating chicken mite is plum ( Prunus mume ) Fermented, Scutellaria baicalensis Extract, Lithospermum erythrorhizon Sieb et Zucc . ) Preparing a mixture comprising the extract, Cinnamomum cassia extract and Phellodendron Bark ; And aging the mixture.

In one embodiment, the fermented plum is fermented to a mixed composition comprising 100 parts by weight of plum and 50 to 150 parts by weight of sugar at 35 ~ 45 ℃ 20 days or more, wherein the golden extract is golden 45 It is prepared, including; extracting the solvent at ~ 65 ℃, the porcelain extract can be obtained by solvent extraction at 80 ~ 100 ℃.

In one embodiment, the mixture may include 100 parts by weight of plum fermentation, 30 to 80 parts by weight of golden extract, 30 to 80 parts by weight of licorice extract, 20 to 50 parts by weight of cinnamon extract and 1 to 10 parts by weight of sulfur white.

In one embodiment the mixture is a Zanthoxylum piperitum ) extract and horseradish ( Eutrema japonicum ) extract may further include one or more.

Another aspect of the present invention relates to a composition for combating chicken mites prepared by the method for preparing a composition for combating chicken mites. In one embodiment the composition for combating chicken mite is plum ( Prunus mume ) Fermented, Scutellaria baicalensis Extract, Lithospermum erythrorhizon Sieb et Zucc . ) Extract, Cinnamomum cassia extract and Phellodendron Bark .

When applying the composition for combating chicken mites prepared by the composition for combating chicken mites of the present invention, the insect pests such as chicken mites in chicken kennels, pest control and killing effect is excellent, the durability of the control effect is excellent, the human body and Harmless to livestock, Eco-friendly, excellent storage stability of composition, excellent odor reduction effect in cages, low production cost, excellent economic efficiency and productivity, and less avoidance of livestock when spraying on kennels .

1 shows a method for preparing a composition for combating chicken mite according to one embodiment of the present invention.
Figure 2 (a) shows a control of the present invention, Figure 2 (b) is a photograph showing the effect of killing chicken mites during the application of Example 1 of the present invention.
Figure 3 is a photograph showing a composition for combating chicken mite of Example 1 of the present invention.

In the following description of the present invention, when it is determined that detailed descriptions of related well-known technologies or configurations may unnecessarily obscure the subject matter of the present invention, the detailed description will be omitted.

The terms to be described below are terms defined in consideration of functions in the present invention, and may be changed according to intentions or customs of users or operators, and the definitions should be made based on the contents throughout the present specification for describing the present invention.

Chicken tick  Manufacturing method for combating

One aspect of the invention relates to a method for preparing a composition for combating chicken mites. 1 shows a method for preparing a composition for combating chicken mite according to one embodiment of the present invention. Referring to FIG. 1, the method for preparing the composition for combating chicken mites includes (S10) a mixture manufacturing step; And (S20) aging step. More specifically, the chicken mite eradication composition manufacturing method (S10) plum ( Prunus mume ) Ferment, Scutellaria baicalensis Extract, Lithospermum erythrorhizon Sieb et Zucc . ) Preparing a mixture comprising the extract, Cinnamomum cassia extract and Phellodendron Bark ; And (S20) aging the mixture.

Hereinafter, the method for preparing the composition for combating chicken mite of the present invention will be described in detail step by step.

(S10) Mixture Preparation Step

In one embodiment, the mixture may include 100 parts by weight of plum fermentation, 30 to 80 parts by weight of golden extract, 30 to 80 parts by weight of licorice extract, 20 to 50 parts by weight of cinnamon extract and 1 to 10 parts by weight of sulfur white.

In the preparation of the mixture, the extract of the plum fermentation and the extract of golden, nachos, cinnamon may proceed in a range that does not destroy the components useful in the preparation.

In one embodiment, the golden, nachos, and cinnamon may be pulverized and powdered after natural drying in the shade after washing with water. It can be powdered to the extent that useful components can be extracted sufficiently during the extraction process. The said drying and grinding | pulverization process can be reversed or performed repeatedly in order as needed. The grinding may be a size of 0.01 ~ 5mm, but is not limited thereto.

In addition, in the present invention, the solvent used in the preparation of the golden, nachos and cinnamon extract may include one or more of alcohol having 1 to 5 carbon atoms, hexane, chloroform, spirits and water.

The plum fermentation may use the seed part of the plum. When the plum is applied, it is excellent in insect repelling and killing effect such as chicken mite, and due to the unique fermentation fragrance, the avoidance of livestock during the spraying of the kennel may be excellent, palatability.

In one embodiment, the fermented plums may be prepared by fermenting a mixed composition including 100 parts by weight of plum and 50 to 150 parts by weight of sugar at 35 to 45 ° C. for 20 days or more. In addition, the fermentation may be carried out under dark conditions without sunlight. When fermenting the mixed composition containing plum and sugar in the above content range, the fermentation efficiency of the useful components contained in the plum is excellent, excellent killing effect and persistence of chicken mite of the present invention, excellent storage stability of the composition, When sprayed in cages, livestock may be less repelled and may have better palatability. When the fermentation is not applied under the above conditions, the killing and repelling effect of chicken mite and the effect persistence may all be reduced. For example, the mixed composition may be obtained by fermentation for at least 30 days, followed by filtration.

The golden extract can be extracted using a portion such as roots, flowers and stems of gold. For example, a golden root can be used. When applying the golden extract, chicken mite repellent and killing effect may be excellent.

In one embodiment, the golden extract may be prepared by solvent extraction of the gold at 45 ~ 65 ℃. When the solvent is extracted under the above temperature conditions, useful components contained in gold may be extracted without being denatured or destroyed.

For example, the golden extract may be prepared by adding 0.5 to 10 parts by weight of gold to 100 parts by weight of a solvent, and heating at 45 to 65 ° C. for 1 to 10 hours. When extracted under the above conditions, the extraction effect of the useful components contained in the gold may be excellent.

In one embodiment, the golden extract may be included 30 to 80 parts by weight based on 100 parts by weight of the plum fermentation. When included in the content range, the composition is excellent in the mixing and dispersibility, the killing effect and persistence of chicken mites, may be excellent in the storage stability of the composition. For example, 45 to 70 parts by weight may be included.

The porcelain extract may be used as a part of the root, stem, flowers and leaves of the grass.

In one embodiment, the licorice extract may be prepared by extracting the solvent from the solvent at 80 to 100 ° C. When the solvent is extracted under the above temperature conditions, useful components contained in the porcelain can be extracted without being denatured or destroyed.

For example, the licorice extract may be prepared by adding 1-20 parts by weight of licorice to 100 parts by weight of a solvent, and heating at 80-100 ° C. for 1 minute to 60 minutes. When extracted under the above conditions, the extraction effect of useful components contained in the porcelain may be excellent.

In one embodiment the licorice extract may be included 30 to 80 parts by weight based on 100 parts by weight of the plum fermentation. When included in the content range, the composition is excellent in the mixing and dispersibility, the killing effect and persistence of chicken mites, may be excellent in the storage stability of the composition. For example, 45 to 70 parts by weight may be included.

The cinnamon extract may use the bark portion of the cinnamon tree ( Cinnamomum cassia ) corresponding to camphor. When the cinnamon extract is included, it is excellent in insect repelling and killing effects such as chicken mite, and due to the peculiar fermentation fragrance, the avoidance of livestock during the spraying of the kennel may be excellent, palatability.

The cinnamon extract, 0.5 to 10 parts by weight of cinnamon with respect to 100 parts by weight of the solvent may be prepared, including the step of extracting at room temperature for 15 to 30 hours. When extracted under the above conditions, the useful components of cinnamon can be easily extracted without being damaged.

In one embodiment the cinnamon extract may be included 20 to 50 parts by weight based on 100 parts by weight of the plum fermentation. When included in the above weight range, while excellent dispersibility and mixing properties of the composition, the killing and repelling effect of chicken mite, and the effect persistence may all be excellent.

The yellow and white can use the parts such as leaves, stems, fruits, flowers and bark of the yellow wall. In one embodiment, the sulfur white may be used in the form of powdered sulfur white to a size of 0.1 ~ 5mm.

In one embodiment, the sulfur white may include 1 to 10 parts by weight based on 100 parts by weight of the plum fermentation. When included in the above range, the composition is excellent in the mixing and dispersibility, it can be excellent chicken kill killing effect.

In one embodiment, the cinnamon extract, the licorice extract, the golden extract and plum fermentation in the mixture may be included in a weight ratio of 1: 1 to 2: 1 to 2: 2 to 5. When included in the weight ratio, the unexpected synergistic effect of the constituents is excellent, the dispersibility and mixing properties of the composition is excellent, the storage stability is excellent, the odor removal effect of the kennel and the killing effect of chicken mite Can be. For example, it may be included in a weight ratio of 1: 1.5-2: 1.5-2: 2-4.

In one embodiment, the content of plum fermentation in the mixture may be higher than the content of golden extract, licorice extract, cinnamon extract or sulfur white. The content of the golden extract in the mixture may be more than the content of the porcelain extract. The content of the golden extract in the mixture may be higher than the content of cinnamon extract or sulfur white.

The content of the licorice extract in the mixture may be higher than the content of the cinnamon extract or sulfur white. In addition, the content of the cinnamon extract in the mixture may be greater than the content of the sulfur white.

In one embodiment the mixture is a Zanthoxylum piperitum ) extract and horseradish ( Eutrema japonicum ) extract may further include one or more.

Zephyr is also called chopi, and is a plant belonging to the family Unhyang. It is about 3-5m high. The thorns with the chin leaves changed in a pair under the petiole, and the thorns bend slightly below. Leaves are alternate, odd one-time quills. Small leaves are egg-shaped, long, with 4-7 dull sawtooth, occupied below the sawtooth, with yellowish green pattern in the center and strong scent.

The skin extract may be prepared using an area such as flowers, seeds, stems, and roots of the skin of the skin (pipi).

The epidermis extract may be prepared by adding 1 to 10 parts by weight of the epidermis, and extracting at 50 to 100 ° C. for 1 to 30 hours, based on 100 parts by weight of the solvent. When extracted under the above conditions, the useful components of cinnamon can be easily extracted without being damaged. For example, it may be prepared by the step of extracting at 60 ℃ for 12 hours.

In one embodiment, the skin extract may be included 5 to 10 parts by weight based on 100 parts by weight of the plum fermentation. When included in the above range, the composition is excellent in the mixing and dispersibility, it can be excellent chicken kill killing effect.

Wasabi ( Eutrema) japonicum ) is a perennial herbaceous genus Papaver cruciferous, and the variety that grows in Japan is often called wasabi. The horseradish extract, it is possible to prepare an extract using the site, such as flowers, seeds, stems and roots of the wasabi.

The wasabi extract may be prepared by adding 0.1-30 parts by weight of wasabi to 100 parts by weight of a solvent, and extracting at 40-100 ° C. for 1-30 hours. When extracted under the above conditions, the useful components of cinnamon can be easily extracted without being damaged. For example, it may be prepared by including the extraction for 24 hours at 40 ℃.

In one embodiment the horseradish extract may be included 5 to 15 parts by weight based on 100 parts by weight of the plum fermentation. When included in the above range, it is excellent in the mixing and dispersibility of the composition, it may be excellent in removing odor and killing chicken mite when spraying kennels. For example, 5 to 10 parts by weight may be included.

In one embodiment, the epidermal extract and horseradish extract may be included in a 1: 0.5 to 1: 3 weight ratio. When included in the above weight range, while excellent in storage stability, mixing and dispersibility of the composition, it can be excellent in removing odors and killing chicken ticks in the kennel spraying.

(S20) ripening step

The step is the step of ripening the mixture. For example, the aging may be aged for 5 days or more at 25 ~ 30 ℃ the mixture. When aged under the above conditions, an unpredictable synergistic effect occurs between the components of the mixture, killing and repelling chicken ticks, and the effect persistence is further improved, the avoidance of livestock during breeding spraying can be excellent, palatability have. For example, it can be aged for 10 days or more.

Chicken tick  Prepared by a composition for combating Chicken tick  Fighting composition

Another aspect of the present invention relates to a composition for combating chicken mites prepared by the composition for combating chicken mites. In one embodiment the composition for combating chicken mite is plum ( Prunus mume ) ferment, golden ( Scutellaria baicalensis Extract, Lithospermum erythrorhizon Sieb et Zucc . ) Extract, Cinnamomum cassia extract and Phellodendron Bark .

Constituents and contents of the chicken mite fighting composition can be the same as described above.

In one embodiment, the composition for combating chicken mite may include 100 parts by weight of plum fermented product, 30 to 80 parts by weight of golden extract, 30 to 80 parts by weight of licorice extract, 20 to 50 parts by weight of cinnamon extract, and 1 to 10 parts by weight of sulfuric acid. Can be.

In one embodiment the composition for combating chicken mite, cinnamon extract, licorice extract, golden extract and plum fermentation may include 1: 1 to 2: 1 to 2: 2: 5 by weight. When included in the weight ratio, excellent dispersibility and mixing properties of the composition, excellent storage stability, can be excellent in removing odor of the kennel, killing effect of chicken mite. For example, it may be included in a weight ratio of 1: 1.5-2: 1.5-2: 2-4.

In one embodiment the composition for combating chicken ticks ( Zanthoxylum) piperitum ) Extract and Wasabi ( Eutrema) japonicum ) may further include one or more of the extract.

In one embodiment, the composition for combating chicken mites and water may be mixed in a weight ratio of 1: 1 to 1:20 and sprayed to a kennel.

When applying the composition for combating chicken mites prepared by the composition for combating chicken mites of the present invention, the insect pests such as chicken mites in chicken kennels, pest control and killing effect is excellent, the durability of the control effect is excellent, the human body and It is harmless to livestock and can solve problems related to pesticides remaining in the body of chicken. It is excellent in eco-friendliness, excellent in storage stability of composition, excellent in reducing odor in cages, and low in production cost. And it can be excellent in productivity, less evacuation of livestock and palatability when spraying the kennel.

Hereinafter, the configuration and operation of the present invention through the preferred embodiment of the present invention will be described in more detail. However, this is presented as a preferred example of the present invention and in no sense can be construed as limiting the present invention.

Example  And Comparative example

The components used in the following Examples and Comparative Examples are as follows.

(A) Plum Fermentation: Plum ( Prunus) mume ) After fermentation for more than 1 month (30 days) while mixing the mixture composition of sugar and 1: 0.8 weight ratio, stir sugar to mix well with fermented product under the dark condition of 35 ~ 45 ℃ without sunlight. Filtration produced liquid plum fermentation.

(B) Golden Extract: Golden ( Scutellaria The stems, roots, and leaves of the baicalensis ) were ground to prepare a ground product. 1 to 5 parts by weight of the gold powder was added to 100 parts by weight of water, heated at 50 ° C. for 3 hours, and then filtered to prepare a golden extract.

(C) Licorice extract: Lithospermum erythrorhizon Sieb et Zucc . The root portion of) was ground to prepare a ground product. 0.1 to 10 parts by weight of the pulverized licorice was added to 100 parts by weight of water, followed by filtration at 100 ° C. for 20 to 30 minutes to prepare a licorice extract.

(D) Cinnamon extract: Cinnamon (cinnamon, bark of Cinnamomum cassia ) was ground to prepare a 5 cm size (maximum length) ground product. 1 to 5 parts by weight of ground cinnamon was added to 100 parts by weight of water, extracted at room temperature for 24 hours, and then filtered to prepare a cinnamon extract.

(E) Yellowish white: Root, stem, and flower parts of yellowish white ( Phellodendron Bark ) were ground to prepare a pulverized form.

(F) Epidermal Extract: The root, stem, leaves and flower parts of Zanthoxylum piperitum were ground to prepare a ground product. Then, 5 to 10 parts by weight of the film was added to 100 parts by weight of water, followed by filtration at 60 ° C. for 12 hours to prepare a film extract.

(G) Wasabi extract: Wasabi ( Eutrema The roots, stems, leaves and flower parts of japonicum ) were ground to prepare a pulverized product. Then, 5 to 10 parts by weight of wasabi was added to 100 parts by weight of water, extracted at 40 ° C. for 25 hours, and then filtered to prepare wasabi.

Example  1-3 and Comparative example  1 ~ 4

To prepare a mixture comprising the components and contents according to Table A, and then aged the mixture for 10 days at 25 ~ 30 ℃ to prepare a chicken tick eradication composition as shown in FIG.

Example  2-3 and Comparative example  1 ~ 4

To prepare a mixture containing the components and contents according to Table A, and then aged the mixture for 10 days at 25 ~ 30 ℃ to prepare a chicken tick eradication composition.

Comparative example  5

To prepare a mixture comprising a component and the content according to Table A below, but was not matured to prepare a composition for combating chicken mites in the same manner as in Example 1.

Test Example

(1) Chicken mite removal effect test: Chicken mite ( Dermanyssus gallinae ) was collected, and the chicken mite was prepared with eight transparent plastic containers, and a sufficient number of individuals visible to the naked eye were spun. The compositions of Examples 1 to 3 and Comparative Examples 1 to 5 were mixed with water at a weight ratio of 1:10, and each of the containers was sufficiently wetted, and then the killing rate of chicken mites was examined for 1 hour at intervals of 10 minutes. The results are shown in Table 2 below.

2 (a) is the result of a control group in which water is applied to the container, and FIG. 2 (b) is a photograph showing the result after 10 minutes have passed after applying Example 1 of the present invention. Referring to the results of Table 2 and Figure 2, when applying the composition for combating chicken mites according to Examples 1 and 2 of the present invention, after 10 minutes, the movement of more than 50% of the chicken tick disappeared, and after 20 minutes More than 90% of chicken mites were killed, and after 30 minutes, all chicken mites were killed.

On the other hand, in the control group coated with water, 5% of the chicken mites died after 10 minutes, 10% of the chicken mites died after 20 minutes, there was no change, the composition for combating chicken mites of the present invention In the case of Comparative Examples 1 to 4, which do not contain some of the components, and Comparative Example 5, which does not apply the mixture aging, it was found that the killing effect of chicken mite is reduced compared to Examples 1 to 3.

(2) Evaluation of composition storage stability: For the compositions of Examples 1 to 3 and Comparative Examples 1 to 5, storage of the composition for 1 week at 50 ° C, 40 ° C, and 25 ° C, such as agglomeration, separation, odor generation, and discoloration, etc. Comparative results were measured and the results are shown in Table 3 below. At this time, the degree of separation and discoloration of the product was evaluated by classifying into the following six grades.

* Separation and discoloration evaluation criteria

(0: no change, 1: partial agglomeration or separation occurs, 2: agglomeration, separation or discoloration of the composition occurs slightly severe, 3: severe separation or discoloration of the composition, severe odor).

Referring to the results of Table 3, in Examples 1 to 3 of the present invention, it was found that the storage stability of the composition is excellent.

(3) Evaluation of composition blendability and dispersibility: In the preparation of the mixture of Examples 1 to 3 and Comparative Examples 1 to 5, the blendability and dispersibility of the components were evaluated according to the following four criteria and the results are shown in the following table. 4 is shown (◎: very good, ○: good, Δ: poor, X: very poor).

(4) Evaluation of odor removal efficacy: After spraying the above Examples 1 to 3 and Comparative Examples 1 to 5 respectively in poultry farms in Cheonbuk poultry complex, and evaluated the odor improvement in poultry farms according to the following four criteria Is shown in Table 4 (?: Very good,?: Good,?: Poor, X: very poor).

Referring to the results of Table 4, in Examples 1 to 3 of the present invention, the composition was excellent in the mixing and dispersibility, it was found that the odor removal effect is excellent. On the other hand, in Comparative Examples 1 to 5, it was found that the odor removing effect is lower than in Examples 1 to 3.

Simple modifications or changes of the present invention can be easily carried out by those skilled in the art, and all such modifications or changes can be seen to be included in the scope of the present invention.

Claims (5)

100 parts by weight of Prunus mume ferment, 30-80 parts by weight of Golden ( Scutellaria baicalensis ) extract, 30-80 parts by weight of Lithospermum erythrorhizon Sieb et Zucc. , 20-50 parts by weight of Cinnamomum cassia extract And preparing a mixture including 1-10 parts by weight of Phellodendron Bark ; And
Comprising the step of aging the mixture; Chicken mite eradication composition manufacturing method comprising a.
The method of claim 1, wherein the plum fermented product is prepared, comprising: fermenting a mixed composition comprising 100 parts by weight of plum and 50 to 150 parts by weight of sugar at 35 to 45 ℃ for at least 20 days;
The golden extract is prepared, including; extracting the gold at 45 ~ 65 ℃ solvent;
The porcelain extract is a solvent extracting method at 80 ~ 100 ° C to the porcelain; chicken mite eradication composition manufacturing method comprising a.
delete The method of claim 1, wherein the mixture is Zanthoxylum piperitum ) extract and horseradish ( Eutrema japonicum ) extract manufacturing method for chicken mite eradication further comprising at least one.
100 parts by weight of Prunus mume ferment, 30-80 parts by weight of Golden ( Scutellaria baicalensis ) extract, 30-80 parts by weight of Lithospermum erythrorhizon Sieb et Zucc. , 20-50 parts by weight of Cinnamomum cassia extract And hwangbaek ( Phellodendron Bark ) Chicken mite eradication composition comprising 1 to 10 parts by weight.

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