KR101873931B1 - Manufacturing method for functional mineral water of ionized calcium using natural material - Google Patents

Abstract

The present invention relates to a method for producing functional mineral aqueous solution of ionic calcium using natural materials, which comprises a first calcination step, a superfine particle crushing step, a second calcination step, a stirring step, a chelating step, an ionization step, a high frequency scanning step, ≪ / RTI >

Description

TECHNICAL FIELD [0001] The present invention relates to a method for producing functional mineral aqueous solution of ionic calcium using natural materials,

The present invention relates to a method for producing an aqueous solution of ionic calcium functional mineral using a natural material.

In general, functional water refers to an active water which has been subjected to a special treatment with water to make the water have a specific function, in other words, water activated by electrolysis, magnetic treatment, ultrasonic treatment, or the like.

Accordingly, there are various kinds of functional water such as electrolytic water, magnetically treated water, electronic water, ultrasonic wave treated water, resonator water, stoneware or mineral functional water. In addition to these, various kinds of ozonated water, deaerated water, The number of branches is known.

Among them, mineral functional water is water which has various kinds of minerals added to daily life water such as mineral water and natural mineral water, and recently, as a result of addition of research results on natural mineral water, It is possible to add more functionalities.

In addition, in the human body, the mineral is 4% of the body weight, but the role of the minerals in the life phenomenon has been found to be indefinitely large. These minerals can be divided into massive elements and trace elements, and the major elements are calcium, phosphorus, potassium, sulfur, sodium, chlorine, magnesium, etc. These elements are about 3.5% Copper, iodine, zinc, molybdenum, fluorine, chromium, and arsenic account for 0.5%.

Carbohydrates, fats, and proteins, the three major nutrients in the body, do not physically work well even if water or vitamins coexist. This is because of the chemical nature of organic matter, and minerals such as minerals are required to participate in metabolism such as decomposition and synthesis.

Calcium intake is very important, and it can be a component of bone, teeth, and blood. It is essential to stimulate or inhibit metabolism with vitamins. to be.

Since all of the functional calcium present in the body is made of calcium-peptide type calmodulin, only the molecular structure can be transported, stored and used in the body. Therefore, the absorption of calcium is necessary for the absorption of calcium It must be water-soluble ionization. Calcium ion is absorbed through the small intestine membrane before it is chelated by binding to the peptide, which is a degradation product of protein in the body.

Therefore, there is a need for a technique of enhancing the functionality by increasing the absorption rate by ionizing calcium and applying the magnetizing power.

Korean Registered Patent No. 0922719 (registered on October 14, 2009, entitled "Mineral Functional Water Production Method, Mineral Functional Water Produced Therefrom"

The present invention provides a method for producing functional mineral aqueous solution of ionic calcium using natural materials extracted from calcium and minerals contained in natural materials and formed into functional water.

The present invention also provides a method for producing functional mineral aqueous solution of ionic calcium using natural materials reinforcing functionalities by ionizing calcium to increase absorption rate and applying magnetizing power.

The technical objects to be achieved by the present invention are not limited to the above-mentioned technical problems.

In order to accomplish the above object, the present invention provides a method for producing functional mineral aqueous solution of ionic calcium using natural materials, comprising the steps of: washing a natural material and firing it in a furnace at a temperature of 1000 to 1500 ° C. for 3 to 4 hours; ; In this process, the first fired natural material can be simultaneously crushed and crushed at a temperature of 20 ° C to 30 ° C. The continuous grinding process is performed using an extruder, a roll mill, a rod mill, or the like Followed by grinding; A second firing step of firing the natural powder at a temperature of 1000 to 1500 DEG C for 1 to 2 hours; An agitation step of adding an organic acid to the secondary fired natural powder and stirring to form a mixture; A chelating step of chelating the natural powder of said mixture; An ionization process in which the chelated composition is ionized by a distillation method to form ionized water; A high frequency scanning step of amplifying the wave power at the wave resonance frequency of the ionized water; And a filtration step of filtering the resultant amplified wave power to extract functional water.

Specifically, the method further includes a sterilizing step of sterilizing the functional water with ultraviolet rays.

The natural material may be at least one of marine pearl, oyster, shellfish, coral, crustacean, and fish bone.

Also, the natural powder has a size ranging from 0.1 mu m to 1.0 mu m.

The organic acid may be selected from the group consisting of citric acid (C ₆ H ₈ O ₇ ), acetic acid (CH ₃ COOH), formic acid (HCOOH), sodium citrate (C ₆ H ₁₅ Na ₃ O ₇ ), malic acid (C ₄ H ₆ O ₅ ) And succinic acid (C ₄ H ₆ O ₄ ) are mixed with each other.

The chelation is characterized in that edible hydrogen peroxide (H ₂ O ₂ ) and ozone (O ³ ) are simultaneously added to the mixture to induce the chelate of the natural powder of the mixture.

The distillation method is characterized in that the chelated composition is subjected to heat at a temperature of 100 ° C or more to collect distilled water vapor to be water-soluble.

The wave resonance frequency is in the range of 1.2 to 1.5 KHz.

Another aspect of the present invention is to provide an ionic calcium mineral functional water using a natural material according to the present invention, which is prepared by a method for producing functional mineral aqueous solution of ionic calcium using the natural material.

As described above, by forming a functional mineral aqueous solution of ionic calcium using natural materials, nutrients such as minerals and calcium necessary for the recipient are supplemented.

In addition, the present invention has the effect of facilitating bone and tooth health by facilitating ingestion of calcium extracted from natural materials.

The present invention is applicable to health, beauty, food addition, medicinal use, agricultural products, livestock products, aquatic products, and wastewater.

In particular, when feeding the livestock with drinking water, the digestibility of the livestock can be improved by increasing the digestibility of the livestock by the minerals, thereby shortening the breeding period (date of shipment), as well as emitting strong anions and far- And anti-virus to increase the resistance to diseases. The rich dissolved oxygen activates the water molecule to detoxify and absorb various heavy metals, and to maintain the balance of intestinal microorganisms, thereby strengthening the immunity of domestic animals, It has the effect of increasing the resistance to diseases and promoting the growth, thereby significantly reducing the mortality rate.

FIG. 1 is a flowchart illustrating a method for producing functional mineral aqueous solution of ionic calcium using a natural material according to an embodiment of the present invention.
2 is a test result report according to the first embodiment of the present invention.
3 is a test result report according to Comparative Example 1. Fig.
4 is a graph showing the absorption rate of calcium per se.
FIG. 5 is a graph showing the progression of tibial fibrosis in osteoporotic rats according to administered water.
6 is a graph showing the bone mineral density of osteoporotic rats.

Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. In the drawings, the same components are denoted by the same reference symbols whenever possible. In the following description, well-known functions or constructions are not described in detail since they would obscure the invention in unnecessary detail.

FIG. 1 is a flowchart illustrating a method for producing a calcium ion mineral functional water using a natural material according to an embodiment of the present invention. In order to prepare a calcium ion mineral functional water using a natural material, Lt; RTI ID = 0.0 > (S110). ≪ / RTI > At this time, the primary firing leaves only inorganic materials in the gravel material and removes organic matter.

Here, it is preferable to use at least one of natural materials such as marine pearl, oysters, shellfish, coral, crustaceans, and fish bones.

Next, the first calcined natural material is pulverized to form a natural powder (S120). At this time, the equipment capable of simultaneously performing compression and milling at a temperature of 20 ° C to 30 ° C is used as a natural powder, and a continuous milling process is performed using an extruder, a roll mill, a rod mill, Lt; RTI ID = 0.0 > 1.0 < / RTI >

Here, by pulverizing the natural material into a finely divided powder form, dissolution can be easily performed thereafter.

 Next, the natural powder is sintered at 1000 to 1500 ° C. for 1 to 2 hours (S 130). The reason for the secondary firing after the crushing of the natural material is that the organic matter that has not been removed even by the first firing is completely removed and the firing is further facilitated and the secondary firing proceeds to increase the concentration of the extract.

Subsequently, the organic acid is added to the secondary fired natural powder, and then stirred to form a mixture (S140).

The organic acid may be selected from the group consisting of citric acid (C ₆ H ₈ O ₇ ), acetic acid (CH ₃ COOH), formic acid (HCOOH), sodium citrate, malic acid (C ₄ H ₆ O ₅ ), and succinic acid (C ₄ H ₆ O ₄ ) Or a mixture of two or more selected from the above.

Here, the organic acid is used to convert the calcium powder into a weakly alkaline pH of about 8.5 to about pH 9.5, because it helps to hydrate the calcium powder, and when the calcium powder is dissolved, it becomes strongly alkaline having a pH of not less than 12.5.

The natural powder of the mixture is then chelated (S150). At this time, the chelating is performed by adding edible hydrogen peroxide (H ₂ O _{2 ,} 35%) and ozone (O ₃ ) produced by edible hydrogen peroxide to a mixture of organic acid and natural powder, The water-soluble calcium and the organic acid are mixed and stirred in an equilibrium state in which ozone (O ₃ ) is generated in the edible hydrogen peroxide (H ₂ O ₂ ) and the formation and collapse of the mixed material (H ₂ O _n ) .

Here, the amount of edible hydrogen peroxide is preferably 1 to 3 parts by weight based on the weight of the natural powder. At this time, when the amount of edible hydrogen peroxide is less than 1 part by weight, ozone (O ₃ ) is produced in edible hydrogen peroxide (H ₂ O ₂ ), and the formation and collapse of the mixed substance (H ₂ O _n ) If it is more than 1 part by weight, the effect is similar to that between 1 and 3 parts by weight, and addition of more than 3 parts by weight is unnecessary.

Next, the chelated composition is ionized by a distillation method to form calcium water (S160). At this time, in the distillation-type method, the chelated composition is subjected to heat at 100 ° C or more to collect distilled water vapor to be water-soluble.

Subsequently, a high-frequency wave is scanned so as to amplify the wave power at the wave resonance frequency of calcium water (S170). At this time, the wave resonance frequency is preferably in the range of 1.2 to 1.5 KHz / sec.

Here, when the magnetic resonance frequency is injected into the calcium water, the atomic nucleus of the calcium absorbs a high energy and is transformed into a high energy functional calcium water as an energy wave.

Finally, the resultant amplified wave power is filtered to extract functional water and sterilized (S180).

At this time, the functional water is filtered through a hollow fiber membrane method, a carbon filter, and activated carbon. Here, the sterilization is preferably performed using ultraviolet rays. Here, the hollow fiber membrane method is a filtration method in which bacteria and other impurities are removed and a weakly alkaline water is passed through while containing minerals as it is. The carbon filter removes various odors, and the activated carbon has a strong adsorption property, This carbonaceous material absorbs gas and moisture.

The functional mineral aqueous solution of ionic calcium using the natural material produced by the above-described method can be produced. The functional mineral aqueous solution of ionic calcium using the natural material according to the present invention is a calcium Is preferably ionized to increase the absorption rate and to enhance the functionality by injecting a magnetic force.

≪ Example 1 >

2 g of the pearl powder and 50 g of organic acid were added to 3 g of the pearl powder and 1 g of the pearl powder which had undergone the washing and primary firing step (S110), the ultrafine particle grinding step (S120), and the second firing step (S130) Lt; / RTI >

Thereafter, the mixture was aged for 24 hours through a chelating step, ionized, and injected at a high frequency of 1.2 to 1.5 KHz / sec to prepare a functional mineral aqueous solution of ionic calcium using the natural material according to the present invention.

The test results of the functional mineral aqueous solution of ion calcium prepared by the method are shown in FIG. 2 and Table 1.

≪ Comparative Example 1 &

2 g of the pearl powder and 50 g of organic acid were added to 3 g of the pearl powder and 1 g of the pearl powder which had undergone the washing and primary firing step (S110), the ultrafine particle grinding step (S120), and the second firing step (S130) Lt; / RTI >

Thereafter, after the aging for 24 hours, the chelating step was omitted, ionization was performed, and ionic calcium functional water was prepared by injecting at a high frequency of 1.2 to 1.5 KHz / sec.

The test results of the ion calcium functional water thus prepared are shown in FIG. 3 and Table 1.

division Example 1 Comparative Example 1 Ionic calcium (Ca ⁺⁺ ) concentration 3121.77 ppm 760.54 ppm

Table 1 summarizes the ionic calcium concentrations shown in Figs. 2 and 3, wherein the ionic calcium concentration of the functional mineral aqueous solution of the ionic calcium using the natural material prepared in the example according to the present invention is 3121.77 ppm, Which is about four times higher than that of the concentration.

Since the difference between Example 1 and Comparative Example 1 is the chelate process after aging, the effect of the chelating process can be seen in the present invention. The present invention can confirm that the concentration of ion calcium is high through Example 1 through Comparative Example 1 .

As shown in FIG. 4, it can be confirmed that the absorption rate of ion calcium contained in the functional mineral aqueous solution of the present invention among the calcium carbonate, calcium phosphate, calcium lactate, calcium citrate, seaweed calcium and ion calcium is remarkably high have.

5 (a) is a tibial trabecula of rats to which ordinary water was administered, (b) is a tibial trabecular meshwork of a rat administered with calcium carbonate water, and (c) ) Shows that tibial trabeculae of rats treated with ion calcium water showed a high density of tibial fibrosis in the week of administration of the ion calcium water of (c).

FIG. 6 is a graph showing the bone mineral density of osteoporosis rats. When bone mineral density is examined, it can be seen that the minerals of the rats administered with the ion calcium water are higher than those of the rats given normal water and calcium carbonate. The maximum energy is shown in Table 2.

rat
(Group) Stiffness
(Stiffness: N / mm) Maximum energy
(Maximum Energy: N) General water supply 110.0 + - 7.08 80.5 ± 5.5 Calcium carbonate administration 120.0 + - 7.02 88.3 ± 7.4 Ionic calcium water administration 145.7 ± 12.4 104.5 ± 5.8

As shown in Table 2, it can be seen that bone strength and maximum energy of rats administered with ordinary water and calcium carbonate are significantly higher than those of mice administered with ion calcium water.

Accordingly, the present invention has an effect of supplementing nutrients such as minerals and calcium necessary for an ingestor by forming a functional mineral aqueous solution of ionic calcium using natural materials.

In addition, the present invention has the effect of facilitating bone and tooth health by facilitating ingestion of calcium extracted from natural materials.

The present invention is applicable to health, beauty, food addition, medicinal use, agricultural products, livestock products, aquatic products, and wastewater.

In particular, when feeding the livestock with drinking water, the digestibility of the livestock can be improved by increasing the digestibility of the livestock by the minerals, thereby shortening the breeding period (date of shipment), as well as emitting strong anions and far- And anti-virus to increase the resistance to diseases. The rich dissolved oxygen activates the water molecule to detoxify and absorb various heavy metals, and to maintain the balance of intestinal microorganisms, thereby strengthening the immunity of domestic animals, It has the effect of increasing the resistance to diseases and promoting the growth, thereby significantly reducing the mortality rate.

  The method for producing an aqueous solution of functional mineral of ionic calcium using natural materials and the aqueous solution of functional mineral of ionic calcium prepared by the method of the present invention are not limited to the construction and operation of the embodiments described above. The embodiments may be configured so that all or some of the embodiments may be selectively combined so that various modifications may be made.

Claims (5)

A first firing step of washing natural materials and firing at a temperature of 1000 to 1500 ° C for 3 to 4 hours;
A pulverizing step of pulverizing the primary fired natural material to a size ranging from 0.1 mu m to 1.0 mu m to form a natural powder;
A second firing step of firing the natural powder at a temperature of 1000 to 1500 DEG C for 1 to 2 hours;
An agitation step of adding an organic acid to the secondary fired natural powder at a weight ratio of 100: 1 and then stirring at 3,000 rpm to form a mixture;
A chelating step of chelating the mixture by adding edible hydrogen peroxide (H ₂ O ₂ );
An ionization step of ionizing the chelated mixture by a distillation method to form calcium water;
A high frequency scanning step of amplifying the breaking power of the calcium water at a wave resonance frequency in the range of 1.2 to 1.5 KHz; And
And a filtering step of filtering the resultant amplified wave power to extract functional water,
The natural material is at least one of marine pearl, oyster, shellfish, coral, crustacean, and fish bone,
The organic acid is a mixture of one or more selected from among citric acid, acetic acid, formic acid, sodium citrate, malic acid and succinic acid,
In the distillation method, the chelated composition is subjected to heat at 100 DEG C or more to collect distilled water vapor to be water-soluble,
Wherein the concentration of the ion calcium contained in the functional water after the filtration process is 3121.77 ppm. delete delete delete delete

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