KR101824380B1 - Process for producing the hydrogen soaps - Google Patents
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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Abstract
Description
본 발명은 수소 비누 및 그 제조 방법에 관한 것으로, 더욱 상세하게는 수소화마그네슘(Mgh2) 또는 수소화칼슘(CaH2) 분말을 천연 지용성 오일로 표면 코팅하여 비누를 구성함으로써, 코팅에 의해 용존 수소가 장기간 보존될 수 있도록 하면서 물과 접촉 시 수소화마그네슘 또는 수소화칼슘이 반응하여 용존 수소가 발생하는 수소 비누 및 그 제조 방법에 관한 것이다.More particularly, the present invention relates to a hydrogen soap and a method of manufacturing the hydrogen soap, and more particularly, to a method of manufacturing a hydrogen soap and a method of manufacturing the hydrogen soap, And hydrogen sulfide is produced by reacting magnesium hydride or calcium hydride upon contact with water, and a production method thereof.
일반적으로 비누는 몸이나 옷 따위에 묻은 때나 얼룩 따위를 씻어 내거나 뺄 때 사용하는 것으로, 보통 고급 지방산의 알칼리 금속염을 주성분으로 만들며, 물에 녹으면 거품이 일어나 미끈미끈한 성질을 가진다.Generally, soap is used when washing or removing stains or stains on body or clothes. It usually makes alkaline metal salts of higher fatty acids as its main ingredient. When it is dissolved in water, it becomes bubbly and has a slippery property.
우리의 몸 피부는 온도, 습도 및 자외선 등과 같은 외부 자극과 인체 유해 미생물 등으로부터 인체를 보호하는 중요한 보호막 역할을 한다. 그러나 나이가 들면서 자연적인 노화와 각종 오염물질, 강한 자외선, 스트레스 및 영양 결핍 등으로 인해 피부는 손상을 입게 되는데, 이로 인해 피부 세포들의 본래 기능이 제대로 이루어지지 않게 되어 주름 생성, 건조, 탄력 손실, 각질화 등 피부노화 현상이 발생하게 된다.Our body skin is an important protective layer for protecting the human body from external stimuli such as temperature, humidity, ultraviolet rays and harmful microorganisms. However, as the age increases, the skin becomes damaged due to natural aging, various pollutants, strong ultraviolet rays, stress and nutritional deficiency. As a result, the skin cells do not function properly, and wrinkles, dryness, Skin aging phenomenon such as keratinization occurs.
한편, 수소는 지구상에 존재하는 가장 가벼운 비금속원소로서, 수소의 항산화력은 비타민C보다 176배, 코엔자임의 863배의 항산화력을 가진다. 이러한 수소는 인체의 유해 활성산소와 결합하여 무해한 물로 만들어 배출시키는 강력한 황산화 물질이다.On the other hand, hydrogen is the lighter nonmetal element that exists on the earth. Antioxidant power of hydrogen is antioxidant power of 176 times of vitamin C and 863 times of coenzyme. This hydrogen is a strong sulfated substance that binds with harmful active oxygen of the human body and is discharged as harmless water.
따라서, 피부 건조 및 거칠어짐을 유발하지 않고, 저자극성이며, 피부 노화를 방지하고 탄력을 부여할 수 있는 수소 비누의 개발이 요구되는 실정이다.Therefore, there is a need to develop a hydrogen soap that is hypoallergenic, does not cause skin dryness and roughness, can prevent skin aging, and can impart elasticity.
본 발명은 종래와 같은 문제점을 해결하기 위해 창안한 것으로, 세안 또는 세척하는 과정에서 물과 반응 시에만 용존 수소가 발생하도록 하여 비누 내의 용존 수소 보존기간을 대폭 연장하고 표면의 갈라짐을 방지하는 수소 비누 및 그 제조 방법을 제공하는데 그 목적이 있다.DISCLOSURE Technical Problem The present invention has been made in order to solve the conventional problems, and it is an object of the present invention to provide a hydrogen soap which can dissolve dissolved hydrogen only in the course of washing or washing, And a manufacturing method thereof.
상기 목적을 달성하기 위한 본 발명에 따른 수소 비누 및 그 제조 방법은,According to an aspect of the present invention, there is provided a hydrogen-
천연 식물성 파우더를 제조하는 제1단계;A first step of producing a natural vegetable powder;
수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재를 코팅하는 제2단계;A second step of coating one or two kinds of materials selected from magnesium hydride and calcium hydride;
천연 오일을 비누화하는 제3단계;A third step of saponifying the natural oil;
상기 천연 식물성 파우더와, 코팅된 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재와, 비누화된 페이스트를 혼합하여 교반하는 제4단계; 및A fourth step of mixing and stirring the natural vegetable powder, one or two kinds of materials selected from coated magnesium hydride and calcium hydride, and a saponified paste; And
제4단계에 의해 혼합된 재료를 비누 틀에 부어 모양을 형상화하는 제5단계; 를 포함함을 특징으로 한다.A fifth step of pouring the mixed material into the soap mold by the fourth step to shape the shape; .
또한, 상기 제1단계는, 식물성 잎을 100℃에서 수증기로 30~40초 쪄서 즉시 건조하되, 수분함량이 1~2중량%가 될 때까지 건조한 후 1~20㎛ 크기로 분쇄함을 특징으로 한다.In the first step, the vegetable leaves are steamed at 100 ° C with steam for 30 to 40 seconds, immediately dried, and dried until the moisture content reaches 1 to 2% by weight, and then pulverized to a size of 1 to 20 μm do.
또한, 상기 제2단계는, 40~70㎛의 입도 크기를 가지는 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재 70~80중량%와, 에센셜 오일 또는 식물성 오일 20~30중량%를 혼합한 후 온도 40~50℃에서 5~10RPM 속도로 4~6분 교반하며 코팅함을 특징으로 한다.In the second step, 70 to 80% by weight of one or two kinds of materials selected from magnesium hydride and calcium hydride having a particle size of 40 to 70 μm and 20 to 30% by weight of essential oil or vegetable oil Followed by coating with stirring at a temperature of 40 to 50 ° C at a rate of 5 to 10 RPM for 4 to 6 minutes.
또한, 상기 제3단계는, 올리브 오일 200g, 코코넛 오일 270g, 팜 오일 300g 으로 정제수 300g에 가성소다 110g을 녹인 후 오일과 혼합하여 상온 20~60℃에서 서서히 교반하여 트레이스가 되도록 함을 특징으로 한다.In the third step, 110 g of caustic soda is dissolved in 300 g of purified water, 200 g of olive oil, 270 g of coconut oil and 300 g of palm oil, mixed with oil, and slowly stirred at a temperature of 20 to 60 ° C to be traced .
또한, 상기 제4단계는, 천연 식물성 파우더 0.5~1중량%와, 코팅된 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재는 0.2~0.5중량%와, 비누화된 페이스트는 98.5~99.3중량%를 혼합함을 특징으로 한다.In the fourth step, 0.2 to 0.5% by weight of a natural vegetable powder, 0.5 to 1% by weight of a natural vegetable powder, 1 to 2% of a coated magnesium hydride and calcium hydride, 98.5 to 99.3% by weight of a saponified paste, Is mixed.
상기와 같은 방법에 의해 제조된 수소 비누는 비누 제조 시 첨가되는 수소화마그네슘 또는 수소화칼슘에 지용성 오일이 코팅됨으로써 미사용 시에는 수소가 발생하지 않고 물과 접촉하여 마찰이 이루어질 때에만 수소가 발생하도록 하여 비누 내의 용존 수소를 장기간 보존할 수 있는 효과가 있다.The hydrogenated soap produced by the above-mentioned method is produced by coating hydrogenated magnesium or hydrogenated calcium added during the production of soap with oil-soluble oil so that hydrogen is not generated at the time of non-use, hydrogen is generated only when friction is brought into contact with water, There is an effect that the dissolved hydrogen in the hydrogen gas can be stored for a long period of time.
또한, 식물성 파우더를 첨가하여 비누의 갈라지는 현상을 방지하고, 인체 및 환경에 해롭지 않은 식물 계열에 천연 제품을 제조할 수 있는 효과가 있다.In addition, the addition of vegetable powder prevents the soap from cracking, and it is possible to produce a natural product in plant series which is harmless to the human body and the environment.
그리고 비누 사용 시 발생하는 수소에 의해 피부 속 진피까지 침투하여 황산화 작용을 하고, 콜라겐 합성을 1.8~2배 증가시켜 피부탄력 저하를 예방 및 복원시키며, 세포막을 통과하여 활성산소에 상처를 입은 세포를 원상태로 돌려준다.And it can penetrate the dermis in the skin by the hydrogen generated in the use of soap, and it acts as a sulfating agent. It increases the collagen synthesis by 1.8 to 2 times to prevent and restore skin elasticity. As a result.
아울러 수소화마그네슘은 모공에 남은 미세한 오염을 배출시키고, 피부에서 수분이 날아가는 것을 방지하는 세라마이드의 합성을 높여주며, 깨끗하고 윤기 있는 피부를 만드는 데 도움을 준다.Magnesium hydride also helps to create fine, shiny skin by enhancing the synthesis of ceramides, which helps to eliminate the minute pollution that remains in the pores and prevents moisture from flying out of the skin.
그뿐만 아니라 항바이러스 작용으로 피부 면역력을 회복시켜 아토피를 진정시키는 데 도움을 주며, 과도하게 배출된 피지를 깨끗이 제거하고, 항염 작용으로 여드름 등의 염증을 예방하는 효과가 있다.In addition, it has an effect of restoring skin immunity by antiviral action, helping to calm atopic dermatitis, removing excess sebum cleanly, and preventing inflammation such as acne by anti-inflammatory action.
도 1은 본 발명에 따른 수소 비누의 제조 공정을 도시한 순서도.BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a flow chart showing a process for producing hydrogen soap according to the present invention; FIG.
이하, 본 발명에 따른 수소 비누 및 그 제조 방법의 바람직한 실시 예를 첨부된 도면을 참조하여 상세히 설명한다.Hereinafter, preferred embodiments of the hydrogen soap and the manufacturing method thereof according to the present invention will be described in detail with reference to the accompanying drawings.
도 1은 본 발명에 따른 수소 비누의 제조 공정을 도시한 순서도로서, 도면에 도시된 바와 같이 천연 식물성 파우더를 제조하는 제1단계; 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재를 코팅하는 제2단계; 천연 오일을 비누화하는 제3단계; 상기 천연 식물성 파우더와, 코팅된 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재와, 비누화된 페이스트를 혼합하여 교반하는 제4단계; 및 제4단계에 의해 혼합된 재료를 비누 틀에 부어 모양을 형상화하는 제5단계; 를 포함한다.FIG. 1 is a flow chart illustrating a process for producing hydrogen soap according to the present invention. As shown in FIG. 1, a first step of producing a natural vegetable powder; A second step of coating one or two kinds of materials selected from magnesium hydride and calcium hydride; A third step of saponifying the natural oil; A fourth step of mixing and stirring the natural vegetable powder, one or two kinds of materials selected from coated magnesium hydride and calcium hydride, and a saponified paste; And a fifth step of pouring the mixed material into the soap mold by the fourth step to shape the shape thereof; .
상기 제1단계는 천연 식물성 파우더를 제조하는 단계로서, 녹차 잎, 허브 잎, 해초류 등 식물성 위주의 잎을 준비하고, 준비된 식물성 잎을 100℃에서 수증기로 30~40초 쪄서 즉시 건조하되, 수분함량이 1~2중량%가 될 때까지 건조한 후 1~20㎛ 크기로 분쇄한다. The first step is a step of preparing a natural vegetable powder, which is prepared by preparing plant-based leaves such as green tea leaves, herb leaves and seaweed, immediately drying the prepared plant leaves by steam for 30 to 40 seconds at 100 ° C, Is dried to 1 to 2% by weight, and then pulverized to a size of 1 to 20 탆.
식물성 잎을 쪄서 건조하는 이유는 산화효소활동을 중지시켜 비누화가 된 후 첨가 시 산패 및 부패하는 것을 방지하기 위함이다. The reason why steamed vegetable leaves are dried is to prevent oxidative enzymes from stopping their activity and sapping and decaying after addition of saponification.
이때, 1000g 기준으로 40초 이상 찌게 되면 변색 및 영양성분이 파괴될 수 있고, 수분함량이 1중량% 이하이면 분쇄 시 열에 의해 탄화될 수 있으며, 20㎛ 이상의 크기를 사용하면 제품의 표면이 거칠어 질 수 있다.If the moisture content is less than 1% by weight, it may be carbonized by heat at the time of milling. If the size is more than 20 μm, the surface of the product may be rough .
상기 제2단계는 수소화마그네슘 또는 수소화칼슘을 코팅하는 단계로서, 더욱 상세하게는 수소화마그네슘 또는 수소화칼슘 중 택 1 또는 2종의 소재 70~80중량%에 에센셜 오일 또는 식물성 오일 20~30중량%를 혼합한 후 온도 40~50℃에서 5~10RPM 속도로 교반하여 4~6분 코팅하며 모두 1000g을 기준으로 한다.The second step is a step of coating magnesium hydride or calcium hydride. More specifically, 70 to 80% by weight of one or two kinds of materials selected from magnesium hydride or calcium hydride, 20 to 30% by weight of essential oil or vegetable oil, After mixing, the mixture is stirred at a temperature of 40 to 50 ° C at a rate of 5 to 10 RPM for 4 to 6 minutes.
본 발명은 수소화마그네슘 1종을 선택하여 실시한 것으로, 수소화마그네슘은 입도 크기는 40~70㎛ 크기를 사용한다. 이때, 크기 40㎛ 이하가 되면 수소화마그네슘 파우더가 물과의 반응에서 파우더 표면부터 반응이 시작되어 수소가 발생하므로 세안 및 세척이 끝나기 전에 수소가 증발되는 현상으로 인해 효과가 미미할 수 있고, 70㎛ 크기 이상이면 비누 표면과 세안시 거친 특성을 나타낼 수 있다.The present invention is carried out by selecting one type of magnesium hydride. Magnesium hydride has a particle size of 40 to 70 mu m. At this time, when the size is less than 40 탆, the hydrogenation magnesium powder starts to react from the powder surface due to reaction with water and hydrogen is generated. Therefore, the effect may be insignificant due to evaporation of hydrogen before washing and washing, , It is possible to exhibit roughness characteristics on the soap surface and cleansing.
그리고 에센셜 오일 또는 식물성 오일의 함량이 30중량% 이상이 되면 수소화마그네슘과 물의 반응을 느리게 하고, 20중량% 이하가 되면 세안 시 물과 반응하는 과정에서 수소 발생이 너무 빠르게 진행되거나 보관 시 흡습된 수분과의 접촉 경계면이 약하여 용존 수소의 보관 기간이 짧다.When the content of the essential oil or the vegetable oil is 30 wt% or more, the reaction of magnesium hydride and water is slowed. When the content of the essential oil or the vegetable oil is 20 wt% or less, And the storage period of dissolved hydrogen is short.
수소화마그네슘은 물과 반응하여 Mg(OH)2 와 H2가 발생 되며 마그네슘 중량대비 6~7.6 중량%에 수소 저장이 가능하다.Magnesium hydride reacts with water to generate Mg (OH) 2 and H2, and hydrogen can be stored at 6 ~ 7.6 wt% of magnesium.
상기 제3단계는 천연 오일을 비누화하는 단계로서, 저온 숙성법에 의해 제조한다. 천연 비누 제조 방법은 기존에 이미 많이 알려졌으며 본 발명은 다양한 오일을 사용하여 제조할 수 있으나 선택적으로 비누화 값을 계산하여 다음과 같이 제조한다.The third step is a step of saponifying a natural oil, which is produced by a low-temperature aging method. The method of manufacturing natural soap has been already known and the present invention can be produced by using various oils, but the saponification value is selectively calculated and prepared as follows.
올리브 오일 200g, 코코넛 오일 270g, 팜 오일 300g으로 정제수 300g에 가성소다 110g을 녹인 후 오일과 혼합하여 상온 20~60℃에서 서서히 교반하여 트레이스가 되게 한다.200g of olive oil, 270g of coconut oil, 300g of palm oil, dissolved in 110g of caustic soda in 300g of purified water, mixed with oil and stirred slowly at room temperature 20 ~ 60 ℃.
물론, 상기 지방산 유지 외에 피마자 오일, 포도씨 오일, 녹차 오일, 아마 오일 등 다양한 천연 지방산 오일의 비누화 값을 계산하여 제조할 수 있음을 밝혀둔다.Of course, in addition to the above-mentioned fatty acid oils, it is possible to prepare saponified oils of various natural fatty acid oils such as castor oil, grape seed oil, green tea oil and flax oil.
상기 제1단계 내지 제3단계는 그 순서를 변경 또는 동시에 진행하여도 무관함을 밝혀둔다.It is to be noted that the first to third steps may be changed or proceeded at the same time.
상기 제4단계는 코팅된 소재와 비누화된 페이스트를 혼합하는 단계로서, 비누화가 된 천연비누 페이스트 98.5~99.3중량%와, 상기와 같은 방법으로 분쇄된 식물성 가루 파우더 0.5~1중량%와, 코팅된 수산화마그네슘, 수산화칼슘 중 택 1 또는 2종의 소재 0.2~0.5중량%를 혼합한다.The fourth step is a step of mixing the coated material with the saponified paste, which comprises 98.5 to 99.3% by weight of the saponified natural soap paste, 0.5 to 1% by weight of the pulverized vegetable powder, 0.2 to 0.5% by weight of one or two kinds of materials selected from magnesium hydroxide and calcium hydroxide are mixed.
식물성 가루 파우더는 비누화가 된 분자구조에 가교 역할을 하여 비누 표면이 갈라지는 것을 방지한다. 식물성 가루 파우더는 0.5중량% 이하가 되면 제품이 완성된 후 숙성하는 과정에서 갈라짐 현상이 발생할 수 있다.The vegetable powder powder bridges the saponified molecular structure and prevents the surface of the soap from cracking. If the vegetable powder powder is less than 0.5% by weight, cracking may occur during the aging process after the product is completed.
물론, 화학합성계인 글리세롤을 첨가하여 개선할 수도 있지만 천연 식물계 비누에는 적합하지 않으며, 1중량% 이상이 되면 화장실이나 세면장 등의 습도가 높은 실내 경우 수분을 흡수하고, 사용 전에 수소화마그네슘과 반응하여 사용 시 수소 발생량을 매우 떨어뜨리며, 용존 수소량을 급감시킬 수 있다.Of course, it can be improved by adding glycerol, which is a chemical synthetic system, but it is not suitable for natural botanical soap. If it is more than 1% by weight, it absorbs moisture in a room with a high humidity such as a toilet or a washroom and reacts with magnesium hydride The amount of hydrogen generated is greatly reduced, and the amount of dissolved hydrogen can be reduced rapidly.
트레이스 정도는 중간단계가 될 때 혼합하는 것이 적당하며 트레이스가 너무 많이 진행된 상태는 첨가물 분산에 문제될 수 있다.It is advisable to mix the traces at the intermediate stage and the traces may be too much dispersed.
식물성 가루 파우더의 소재 즉, 녹차 가루가 이용되면 녹차 수소 비누가 되며, 허브 가루가 이용되면 허브 수소 비누가 되고, 해초 가루가 이용되면 해초 수소 비누가 된다.When the green powdered powder is used, the green powdered hydrogen soap is used. When the herbal powder is used, the herbal hydrogen soap is used. When the seaweed powder is used, the hydrogenated soap becomes the seaweed hydrogenated soap.
상기 제5단계는 제4단계에 의해 혼합된 재료를 비누 틀에 부어 모양을 형상화하는 단계로서, 7일 숙성시켜 상품화함으로써 수소 비누의 제조를 완료한다.In the fifth step, the mixed material is poured into a soap mold to form a shape, and the hydrogen soap is completed by commercializing the material by aging for 7 days.
이와 같은 방법에 의해 제조된 수소 비누는 세안 및 세척 시 마찰에 의해서 수소화마그네슘 또는 수소화칼슘 소재가 물과 반응하여 수소가 발생하므로 미사용 시에는 비누 내의 용존 수소 보존기간을 장기간 유지할 수 있다.Hydrogen soap produced by such a method reacts with water or hydrogenated magnesium or hydrogenated calcium material due to friction during washing and washing, and hydrogen is generated, so that the dissolved hydrogen storage period in the soap can be maintained for a long time when not used.
(실험 예 1)(Experimental Example 1)
천연 식물성 파우더 첨가 없이 수소화마그네슘만 첨가하여 제조된 비누를 관능 테스트하였다.The soap prepared by adding only hydrogenated magnesium without addition of natural vegetable powder was subjected to a sensory test.
(실험 예 2)(Experimental Example 2)
천연 식물성(녹차) 파우더 1중량% 를 첨가한 후 수소화마그네슘을 첨가하여 제조된 비누를 관능 테스트 하였다.The soap prepared by adding 1 wt% of natural vegetable (green tea) powder and adding magnesium hydride was subjected to a sensory test.
(실험 예 3)(Experimental Example 3)
천연 식물성(녹차) 파우더 1중량%를 사용하고, 수소화마그네슘에 오일을 30중량% 표면 코팅하여 코팅된 수소화마그네슘 첨가량에 따라 비누의 수소 발생량 측정을 하였다.1% by weight of natural vegetable (green tea) powder was used, 30% by weight of oil was surface-coated on magnesium hydride, and the amount of generated hydrogen in the soap was measured according to the amount of coated magnesium hydride.
상기 실험은 제조된 비누 표면에 물 10g을 떨어뜨리고 5분 후 수소측정기를 통해 물이 떨어진 곳을 측정하여 5회 측정된 평균 수치임.The above experiment is an average value measured 5 times after 10 g of water is dropped on the surface of the manufactured soap and water is separated from the water by a hydrogen analyzer after 5 minutes.
(실험 예 4)(Experimental Example 4)
실험 예 3을 기준으로 오일이 코팅된 수소화마그네슘과 오일이 코팅되지 않은 수소화마그네슘을 첨가 했을때 수소 발생량을 비교하였다.The amount of hydrogen generated when oil-coated magnesium hydride and oil-unhydrogenated magnesium hydride were added based on Experimental Example 3 was compared.
상기 실험은 비누 표면에 물 10g을 떨어뜨리고 5분 후 수소측정기로 물이 떨어진 곳을 측정하여 5회 측정된 평균 수치임.The above experiment is an average value measured five times by dropping water on a soap surface with a hydrogen meter after dropping 10 g of water.
Claims (7)
40~70㎛의 입도 크기를 가지는 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재 70~80중량%와, 에센셜 오일 또는 식물성 오일 20~30중량%를 혼합한 후 온도 40~50℃에서 5~10RPM 속도로 4~6분 교반하며 코팅하는 제2단계;
천연 오일을 비누화하는 제3단계;
상기 천연 식물성 파우더와, 코팅된 수소화마그네슘, 수소화칼슘 중 택 1 또는 2종의 소재와, 비누화된 페이스트를 혼합하여 교반하는 제4단계; 및
제4단계에 의해 혼합된 재료를 비누 틀에 부어 모양을 형상화하는 제5단계; 를 포함함을 특징으로 하는 수소 비누 제조 방법.
A first step of producing a natural vegetable powder;
70 to 80% by weight of one or two kinds of materials selected from magnesium hydride and calcium hydride having a particle size of 40 to 70 μm and 20 to 30% by weight of essential oil or vegetable oil are mixed, A second step of coating with stirring at a speed of ~ 10 RPM for 4 to 6 minutes;
A third step of saponifying the natural oil;
A fourth step of mixing and stirring the natural vegetable powder, one or two kinds of materials selected from coated magnesium hydride and calcium hydride, and a saponified paste; And
A fifth step of pouring the mixed material into the soap mold by the fourth step to shape the shape; ≪ / RTI >
[3] The method according to claim 1, wherein the first step comprises drying the vegetable leaves at 100 [deg.] C with steam for 30 to 40 seconds and immediately drying until the moisture content reaches 1 to 2% by weight, Wherein the hydrogen-containing gas is hydrogen.
[Claim 3] The method according to claim 2, wherein the vegetable leaf is any one of green tea leaves, herb leaves, and seaweed.
4. The method according to any one of claims 1 to 3, wherein the third step comprises dissolving 110 g of caustic soda in 300 g of purified water, 200 g of olive oil, 270 g of coconut oil and 300 g of palm oil, mixing with oil, Wherein the water is stirred to gradually form a trace.
4. The method according to any one of claims 1 to 3, wherein in the fourth step, 0.5 to 1% by weight of a natural vegetable powder and one or two kinds of coated magnesium hydride and calcium hydride are contained in an amount of 0.2 to 0.5 wt% %, And 98.5 to 99.3% by weight of a saponified paste.
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| KR20230081489A (en) * | 2021-11-30 | 2023-06-07 | 이경순 | Natural hydrogen soap compositon and method for manufacturing natural hydrogen soap using the same |
| KR20240079902A (en) | 2022-11-29 | 2024-06-05 | 최고은 | Manufacturing method of hydrogen soap containing alcohol-treated h2-occluded calcium material |
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| KR101972160B1 (en) | 2017-10-11 | 2019-08-23 | 농업회사법인 주식회사 하이그린팜 | Manufacturing method for hydrogen powder soap |
| KR20230081489A (en) * | 2021-11-30 | 2023-06-07 | 이경순 | Natural hydrogen soap compositon and method for manufacturing natural hydrogen soap using the same |
| KR102668189B1 (en) * | 2021-11-30 | 2024-05-21 | 이경순 | Natural hydrogen soap compositon and method for manufacturing natural hydrogen soap using the same |
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