KR101774000B1

KR101774000B1 - Hair styling wax composition

Info

Publication number: KR101774000B1
Application number: KR1020150135650A
Authority: KR
Inventors: 최화춘; 최수규; 이정래
Original assignee: 주식회사 엘지생활건강
Priority date: 2015-09-24
Filing date: 2015-09-24
Publication date: 2017-09-01
Also published as: KR20170036461A

Abstract

The present invention relates to a hair styling wax composition, wherein the hair styling wax composition according to the present invention has properties that are excellent both in setting power, spreadability (washability) and washability, which have not been achieved in the past.

Description

[0001] Hair styling wax composition [0002]

The present invention relates to hair styling wax compositions and hair styling products containing them.

Hair cosmetics are cosmetics used to keep scalp and hair clean and beautiful. Hair is an important part of a person's appearance, and the condition and shape of the hair have a big impact on the image as well as the face of the person. In normal hair care, shampoo and rinse are used for shaving, and hair cream, hair lotion and hair treatment are used to give a corrective effect and nutrition effect to trim and soften the hair. In order to improve the beauty of the hair, various kinds of hair are used, mainly using perms, dyeing, and dryers. However, since the hair is mostly composed of protein, hair is easily damaged by the use of dyeing, perming and drying, so that many side effects such as loss of gloss and roughness of hair occur. As a result, a hair-finishing product such as a hair styling agent or a hair treatment agent having various functions has been developed and used so that the hair can be polished, the hair can be arranged and the styling shape can be maintained for a long time Has come.

Hair styling products are used to make hair beautiful, add charm, and change appearance. It is used for styling and setting hair. The hair styling agent is applied to the surface of the hair to make it easy to trim the hair into a desired shape or to maintain the hair style for a long time. There are some styling functions in hair conditioner products, but there is a big difference in that there is no setting effect to fix hair style.

Of these, hair styling wax is a cream or solid hair styling agent that gives proper shine to the hair, has natural setting power, and allows you to rebalance hair that has been broken. Such hair styling wax is a form obtained by emulsifying a water-based component and an oil-based component with a surfactant, and an aqueous component such as oil and wax and an aqueous component such as a water-soluble polymer compound is used to impart gloss and styling effect.

In the prior art, hair styling waxes which are available in a container or tube form (Jar or Tube Type) have a high viscosity and use many oily components such as beeswax to have a hair styling function. However, in the case of a hair wax containing a lot of oily components, it is difficult to coat the hair because of high viscosity when it is applied to the hair. It is difficult to uniformly coat the hair. As a result, the hair is bundled and natural, the hair becomes dirty and greasy, There is a disadvantage in that it is not washed well in washing products such as soap and soap, so that it can not give a refreshing feeling. On the other hand, in the case of using excessive amount of wax ingredients to increase the set hold of hair, there is a technical restriction to improve the natural hair fixing ability since the use feeling is more stiff and unfavorable.

On the other hand, there has been a continuous effort by the related industry to develop a product having improved function of hair styling wax product of hair, but as a conventional technology, it has excellent spreadability (spreadability) and setting power when applied to hair, And there is a limit in that development of a product capable of exhibiting an excellent washing-off effect upon washing of hair and hands after use can not be achieved.

Korean Patent Publication No. 2002-0095593

A problem to be solved by the present invention is to provide a hair styling wax composition excellent in setting strength, spreadability (spreadability) and washability.

Accordingly, the present invention provides hair styling wax compositions containing microcrystalline wax and isopentane.

The present invention also provides a hair styling product comprising the composition.

The present invention also provides a method for manufacturing the hair styling wax composition.

In order to solve the above problems, the present invention provides a hair styling wax composition containing microcrystalline wax and isopentane.

Further, the composition according to the present invention may further contain beeswax.

As used herein, the term "beeswax" is also referred to as beeswax, but is not limited to, for example, naturally occurring sugar bees collected from flowers by enzymatic action via biochemical processes It is a yellow substance which is produced in the body and secretes from the secretory gland of the lower abdomen of the worker bees. It may be a substance which constitutes a honeycomb. If it is not a naturally produced natural bean, it may be a substance having the same composition as the natural bean. The wax used in the hair styling wax composition according to the present invention may be processed by removing the impurities after filtering the wax with a filter, if natural wax is used.

In the present invention, the wax may contain 40 to 90 wt% of wax ester, 1 to 30 wt% of free fatty acid, 0.1 to 5 wt% of free alcohol, or a mixture of two or more thereof, based on the total weight of the wax, From 62 to 75% by weight, from 5 to 16% by weight of free fatty acids, from 1 to 2% by weight of free alcohol or a mixture of two or more thereof, more preferably all of them. In addition, it may contain 10 to 20 wt% of C ₂₀ to C ₄₀ hydrocarbons or 2 to 5 wt% of glycerides (C ₁₄ , C ₁₆ or C ₁₈ ).

As used herein, the term "microcrystalline wax" refers to a wax having a molecular weight of C ₂₅ to C ₈₀ , preferably C ₃₁ to C _70, of 300 to 1500, preferably of 400 to 1200, To 1000 of isoparaffin as the main component.

In the hair styling wax composition according to the present invention, the components are contained in the composition at a specific content and a specific mass ratio with other compositions, as described in detail below, and are excellent in setting power, spreadability (spreading ability) The washability can be achieved.

As used herein, the term "isopentane" is a substance represented by the following formula (1), the molecular formula is C ₅ H ₁₂ , the name of IUPAC is 2-methylbutane, and the molecular weight is 72.15 . In the present invention, naturally occurring isopentane, artificially synthesized isopentane, and commercially available isopentane can be used as the substance represented by the following formula (1).

[Chemical Formula 1]

Among the hair styling products containing the hair styling wax composition according to the present invention, when the hair styling wax is rolled after a proper amount of the hair styling wax is taken out on the palm of the hand, the isopentane is volatilized simultaneously with the foam due to the physical temperature of the palm, As shown in Fig. As will be described in detail below, the hair styling wax composition according to the present invention is contained at a specific content of isopentane and a specific mass ratio with other compositions, thereby achieving excellent effects. In particular, when it is contained in an amount less than a certain amount, it is impossible to expect an effect of improving the setting power, spreadability (spreading ability) and washability when applied to hair, and when it is contained in an amount exceeding a certain amount, a viscosity as hair styling wax can not be formed, It is not only inconvenient but also may cause a problem in safety when using a general container other than an aerosol container.

The hair styling wax composition according to the present invention is characterized in that it contains both the microcrystalline wax and isopentane, and may further contain additional wax. A single substance that does not contain all of the above materials; Or microcrystalline wax and beeswax; Or a combination of isopentane and beeswax alone, it is impossible to solve the problem of providing a composition which is excellent in all of the setting power, spreadability (spreadability) and washability in the hair styling wax which is a technical subject to be achieved by the present invention.

In the present invention, the composition may contain 1 to 30% by weight of the microcrystalline wax and 0.1 to 15% by weight of isopentane based on the total weight of the composition. Preferably, the microcrystalline wax By weight to 10% by weight and isopentane by 5% by weight to 15% by weight.

The composition according to the present invention may further contain 4.5 to 8% by weight of the microcrystalline wax and 5 to 12% by weight of isopentane based on the total weight of the composition.

Also, when the composition according to the present invention contains beeswax, the composition may contain 1 to 30% by weight of the wax, 1 to 30% by weight of microcrystalline wax and 0.1 to 20% by weight of isopentane And preferably 5 to 15% by weight of the wax, 1 to 10% by weight of microcrystalline wax and 5 to 15% by weight of isopentane based on the total weight of the composition.

The composition according to the present invention may further contain 8.5 to 13% by weight of the wax, 4.5 to 8% by weight of microcrystalline wax and 5 to 12% by weight of isopentane relative to the total weight of the composition.

When the wax and microcrystalline wax are mixed in the hair styling wax composition containing the wax according to the present invention, if the wax and microcrystalline wax are less than 2% by weight based on the total weight of the composition, And the wax and microcrystalline wax are each not more than 30% by weight, the viscosity is too high, hard and does not spread well to the hair, and the spreadability is not good, Which is undesirable.

In the hair styling wax composition according to the present invention, if the isopentane is less than 0.1% by weight based on the total weight of the composition, spreadability (putting ability), fixing force (setting power) and washability in hair may not be improved If the content is more than 20% by weight, a high viscosity is not formed and flow phenomenon occurs, which is inconvenient to use. In addition, when a general container other than an aerosol container is used, it is difficult to secure hermeticity at high temperatures in summer, Which is undesirable.

On the other hand, in a hair styling product containing a hair styling wax composition, if any of the setting force (fixation force), spreadability (spreadability) and washability is not excellent, it may be inconvenient to use.

More specifically, the setting force (fixing force) uses a hair styling wax for the desired hair styling as a main purpose of using the hair styling wax for both men and women. Despite applying a certain amount of hair styling wax to hair, if the hair is not fixed at a desired position and easily changed by external factors (for example, wind, light contact, etc.), it can not be used as hair styling wax have.

In addition, when spreading the hair-styling wax composition using the product, spreading it on the palm of the hand as in the usual method of using the hair-styling wax, rolling the hair, applying the hair to the hair, It can mean whether or not it is uniformly and well applied. At this time, hair styling wax may not be worth as hair styling wax if the hair wax product is so stiff that the hair does not clump or can not be applied to the hair as much as desired. Hair styling products must have a viscosity above a certain level in order to have a high level of setting power, but in this case, spreadability (spreadability) may not be good due to too high viscosity. Therefore, it is very difficult to produce a hair styling wax composition having high setting power and exhibiting excellent spreadability (spreadability). The hair styling wax composition according to the present invention shows excellent effects as shown in the following experimental examples, And has an excellent effect as a wax composition.

In addition, the cleansing property of hair styling products can be said to be an important characteristic when the hair is applied, but it can not be said that the hair styling wax composition is excellent when the wax product applied on the hair does not wash off. A product with a high level of setting power and spreadability can have a good effect of keeping the hair set for a long time but if the wax composition remains on the hair after washing due to insufficient washability, Which is an important factor in evaluating hair styling wax. The hair styling wax containing the hair styling wax composition according to the present invention has remarkable effect as a hair styling wax composition because it has excellent setting power and spreadability (wettability) and excellent washability as proved by the following experimental examples.

The hair styling wax composition according to the present invention can exhibit the excellent effects not only in the contents of the wax, microcrystalline wax and isopentane but also in a specific weight ratio.

More specifically, the composition may contain microcrystalline wax and isopentane in a weight ratio of 1: 0.5 - 4, and preferably the composition comprises microcrystalline wax and isopentane in a weight ratio of 1: 1.5-3 More preferably, the composition may contain microcrystalline wax and isopentane in a weight ratio of 1: 1.5 to 2.5.

In addition, when the composition according to the present invention comprises beeswax, the composition may contain beeswax, microcrystalline wax and isopentane in a weight ratio of 1: 4: 1: 0.5 - 4, Microcrystalline wax and isopentane in a weight ratio of 1.5 - 3: 1: 1.5 - 3, and more preferably the composition comprises beeswax, microcrystalline wax and isopentane in a ratio of 1.5 - 2.5: 1: 1.5 to 2.5 by weight.

If the weight ratio is exceeded, the level of the setting force, spreadability (wettability) or washability as a hair styling wax may be significantly lowered. More specifically, when isopentane is contained in an amount exceeding the above weight ratio, a double layer in which a part of isopentane exists in the upper layer may be formed, which may result in poor stability and may not have uniform quality. In addition, when isopentane is contained in a small amount beyond the above-mentioned weight ratio, isopentane may not exhibit an effective effect, so that the level of setting force, spreadability (spreadability) or washability may be significantly lowered.

The hair styling wax composition according to the present invention may contain polyvinylpyrrolidone (PVP) or polyvinylpyrrolidone / vinyl acetate copolymer (PVP / VA copolymer).

The polyvinylpyrrolidone (PVP) or polyvinylpyrrolidone / vinyl acetate copolymer (PVP / VA copolymer) may be contained in an amount of 0.1 to 5 wt%, preferably 0.5 to 4 wt% By weight, and more preferably 1 to 2.5% by weight.

The hair styling wax composition according to the present invention may further contain at least one additive component selected from the group consisting of copper, vegetable oils, emulsifiers, neutralizing agents, thickeners and preservatives.

In the present invention, the copper or vegetable oil may include paraffin wax, candelilla wax, carnauba wax, squalane, or mineral oil.

In the present invention, the emulsifier may be an emulsifier commonly used in hair styling wax compositions, preferably glyceryl stearic acid or PEG stearic acid.

In the present invention, the neutralizing agent may be a neutralizing agent commonly used in a hair styling wax composition, and preferably triethanolamine may be used.

In the present invention, the thickening agent may be an increasing agent commonly used in a hair styling wax composition, preferably an alkyl / acrylate crosslinked polymer having 10 to 30 carbon atoms.

In the present invention, the preservative may be a preservative commonly used in hair styling wax compositions, preferably, paraoxybenzoic acid ester.

The hair styling product may be a hair styling wax. If the product comprises the composition, the hair styling product may be manufactured by a method generally used in the art.

The hair styling wax may be manufactured in various formulations such as, but not limited to, a mat type, a cream type, or an emulsion type.

The present invention also provides a method of making a hair styling wax composition comprising the steps of:

S1) dissolving the aqueous phase component in purified water;

S2) adding an oil phase component comprising wax, microcrystalline wax or a mixture thereof to the water phase prepared in step S1) and emulsifying; And

S3) adding isopentane.

In the present invention, wax, microcrystalline wax and isopentane added to the above production method can be added in the content and weight ratio of the hair styling wax composition.

In the present invention, the step S1) is a step of preparing an aqueous phase.

The water phase is preferably prepared by dissolving the water phase component in purified water, preferably by adding glycerin and an emulsifier.

In step S1), the water component may be dissolved in the purified water, followed by heating, and the heating may preferably be performed at a temperature of 65 to 95 ° C.

In the present invention, the step S2) is a step of producing an oil phase.

The oil phase component may contain beeswax and / or microcrystalline wax, and an oil component such as squalene, carnauba wax and the like may be further added.

Also, in step S2), after the emulsification, it may be subjected to a heating step, and the heating may be preferably performed at a temperature of 65 to 95 ° C.

Further, in the present invention, cooling may be performed after step S2).

The cooling can be preferably carried out at a temperature of from 45 to 65 占 폚.

In the present invention, the step S3) is a step of adding isopentane.

The isopentane may be added after the step S2), preferably after cooling to room temperature.

The hair styling wax composition according to the present invention has properties that are excellent both in setting power, spreadability (washability) and washability which have not been achieved in the past.

Hereinafter, embodiments of the present invention will be described in detail to facilitate understanding of the present invention. However, the embodiments according to the present invention can be modified into various other forms, and the scope of the present invention should not be construed as being limited to the following embodiments. Embodiments of the invention are provided to more fully describe the present invention to those skilled in the art.

Example And Comparative Example Produce

Hair styling waxes of the emulsified form having the same composition and contents as in the following Table 1 (Group of Examples) and Table 2 (Comparative Example Group) were prepared by the following method.

Example 1 to 8

First, each component having a content as shown in Table 1 below was prepared, and glycerin (Category 2) and emulsifier (Category 3) were added and dissolved in purified water (Category 1) to make a water phase and heated to 85 ° C. Thereafter, the oily ingredient (squalene) (Category 4), carnauba wax (Category 5) and beeswax (Category 6) microcrystalline wax (Category 7) The emulsion was added to the water phase prepared by warming and emulsified, followed by cooling to 55 캜. Finally, the neutralizing agent (Category 9), the setting agent (Category 10), the thickening agent (Category 11) and the preservative (Category 12) were cooled to 55 ° C and added to the prepared oil phase sequentially and uniformly mixed. Next, isopentane (Segment 8) was placed in a sealed container and uniformly mixed to prepare a sample according to each example.

The numerical values for the respective components shown in Tables 1 to 12 in the following Table 1 indicate the content, and the unit thereof is% by weight.

division Ingredients Example (Unit: wt%) One 2 3 4 5 6 7 8 One Purified water Balance Balance Balance Balance Balance Balance Balance Balance 2 glycerin 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 3 Emulsifier 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 4 Squalene 4.0 4.0 4.0 4.0 4.0 4.0 4.0 3.0 5 Carnauba wax 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 6 Wax 10.0 10.0 10.0 10.0 10.0 8.0 8.0 8.0 7 Microcrystalline wax 5.0 5.0 5.0 5.0 5.0 3.0 3.0 3.0 8 Isopentane 2.0 4.0 6.0 8.0 10.0 2.0 4.0 6.0 9 corrector 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 10 Setting agent 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 11 Incrementer 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 12 antiseptic 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2

In Table 1 above, the emulsifier (Category 3) is partially dissolved in boiling alcohol, glyceryl stearate (Glyceryl Stearate) and PEG-100 Stearate, Carnauba wax (Category 5) ) And ether, but it does not dissolve in water, and has a specific gravity of about 0.997 and a melting point of 80 to 86 ° C. Beeswax (Category 6) contains about 62-75% wax ester, about 5-16% free fatty acid, and about 1-2% free alcohol. Microcrystaline wax (Category 7) is a mixture of solid hydrocarbons obtained from petroleum and is mainly composed of isoparaffin. Isopentane ₍ Category 8) is a solvent having a boiling point (bp) of 30 to 30.2 ° C and a density (d, 20 ° C) of 0.62. Neutralizer (Category 9) neutralizes the thickener (Category 11) while containing 99.0 to 105.0% of triethanolamine (C ₆ H ₁₅ NO ₃ : 149.19) as triethanolamine (TEA). The setting agent (Category 10) is a polyvinylpyrrolidone (PVP) polymer, the thickener (Category 11) is an alkyl / acrylate crosspolymer having 10 to 30 carbon atoms (NOVEON, USA) 12), p-hydroxybenzoic acid ester was used.

Comparative Example 1 to 8

First, each component having a content as shown in Table 2 below was prepared, and glycerin (Category 2) and emulsifier (Category 3) were added and dissolved in purified water (Category 1) to make a water phase and heated to 85 ° C. Thereafter, squalene (Category 4), carnauba wax (Category 5) and wax (Category 6) microcrystalline waxes (Category 7), which are oil components, were heated to 85 ° C and added to the water phase prepared and emulsified and then cooled to 55 ° C. Finally, the neutralizing agent (Category 9), the setting agent (Category 10), the thickening agent (Category 11) and the preservative (Category 12) were cooled to 55 ° C and added to the prepared oil phase sequentially and uniformly mixed. Next, isopentane (Category 8) was placed in a closed container and uniformly mixed to prepare a sample according to each comparative example.

The numerical values for the respective components shown in Tables 1 to 12 in the following Table 2 indicate the content, and the unit thereof is% by weight.

division Ingredients Comparative Example (unit: wt%) One 2 3 4 5 6 7 8 One Purified water Balance Balance Balance Balance Balance Balance Balance Balance 2 glycerin 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 3 Emulsifier 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 4 Squalene 4.0 4.0 4.0 4.0 4.0 4.0 4.0 3.0 5 Carnauba wax 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 6 Wax 12.0 10.0 10.0 - 12.0 10.0 8.0 8.0 7 Microcrystalline wax - - 5.0 15.0 - - 4.0 4.0 8 Isopentane - - - - 4.0 4.0 6.0 4.0 9 corrector 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 10 Setting agent 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 11 Incrementer 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 12 antiseptic 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2

On the other hand, most of the component materials used in Table 2 above were used in the same manner as the component materials shown in Table 1, though they were used in different amounts.

Each of the samples prepared according to Examples (1 to 8) and Comparative Examples (1 to 8) was subjected to sensory evaluation for setting performance, washing ability and hair clustering (spreadability) .

One. In Set Hold Equipment evaluation

Each of the hair styling waxes prepared according to the above Examples (1 to 8) and Comparative Examples (1 to 8) was uniformly wound on a spiral and dried. Curl Retention (CR (%)] as shown in Equation (1) is measured in a curl state in a constant temperature and humidity chamber having a temperature of 25 ° C and a relative humidity of 60% Respectively.

[Equation 1]

In Equation (1), L ₀ denotes a hair tress length, L _t denotes a length of a hair tress after a lapse of t, L _s denotes a curl initial hair tension Tress) length (t = 0). (Albert L. Mikchelli, BA, and F.Theodore Koehler, BS Polymer Properties Influencing Curl Retention at High Humidity, J.Soc. Cosmetic Chemists. 19, 863-880 (Dec 9, 1968) to be.

2. In washability Sensory evaluation

3 g of each of the hair styling waxes prepared according to Examples (1 to 8) and Comparative Examples (1 to 8) was applied to the hair of each evaluator, and after 12 hours, The scale was recorded on a scale of 5 out of 10 according to the same criteria. Each evaluator's score was added and then divided by the number of evaluators (n = 100) to obtain an average value.

division Wash-off state Exam conditions 1 point Very bad
- Cleaning agent (SLES 10% solution): 5 g
- hair styling wax application amount: 3g 2 points Poor 3 points usually 4 points Slightly better 5 points Very good

3. Sensory evaluation of spreadability

3 g of the hair styling wax prepared according to the examples (1 to 8) and the comparative examples (1 to 8) were applied to the hair of each evaluator and then styled by fingers. Then, Were recorded on a 5-point scale on the basis of Table 4 below. Each evaluator's score was added and then divided by the number of evaluators (n = 100) to obtain an average value.

division State of hair clumping Spreadability Exam conditions 1 point Very severe Very bad
- Temperature of constant temperature and humidity room: 25 ℃
- Relative humidity of constant temperature and humidity room: 40%
- hair styling wax application amount: 3g 2 points Severe Poor 3 points Has a little usually 4 points none good 5 points Not very Very good

4. Results

For each of Examples (1 to 8) and Comparative Examples (1 to 8), device evaluation of the setting force and sensory evaluation of stickiness, washability and hair bunching (spreadability) were conducted as follows, Are shown in Table 5 below.

division Evaluation items One 2 3 4 5 6 7 8 Example Setting power (%) 71 74 75 75 75 66 68 69 Washability 3.5 3.9 4.0 4.2 4.4 4.1 4.2 4.3 Spreadability 3.8 4.1 4.2 4.5 4.7 4.3 4.5 4.8 Comparative Example Setting power (%) 63 55 72 75 65 57 70 67 Washability 3.3 3.5 2.8 2.5 3.5 4.1 4.0 3.4 Spreadability 3.5 4.0 3.0 2.7 3.7 4.2 4.1 3.6

As shown in Table 5, Examples (1 to 8) were found to have superior washability and spreadability as a whole in comparison with Comparative Examples (1 to 8). In particular, in the case of Examples 3 to 5 containing 10% by weight of beeswax, 5% by weight of microcrystalline wax and 6 to 10% by weight of isopentane, the fixing power, the washability, And the spreadability was the best.

A preferable effect standard value required in the present invention is a setting force of 74% or more, a washability of 3.9 or more, and a spreadability of 4.0 or more.

Claims

Containing microcrystalline wax, isopentane, and beeswax,
Characterized in that it contains 4.5 to 8 wt% of microcrystalline wax, 5 to 12 wt% of isopentane and 8.5 to 13 wt% of beeswax based on the total weight of the composition.

delete

The method according to claim 1,
Wherein the wax contains from 40 to 90% by weight of wax ester, from 1 to 30% by weight of free fatty acid, from 0.1 to 5% by weight of free alcohol or a mixture of two or more thereof, based on the total weight of the wax.

delete

The method according to claim 1,
Characterized in that the composition further comprises polyvinylpyrrolidone (PVP) or polyvinylpyrrolidone / vinyl acetate copolymer (PVP / VA copolymer).

9. The method of claim 8,
Characterized in that said polyvinylpyrrolidone (PVP) or polyvinylpyrrolidone / vinyl acetate copolymer (PVP / VA copolymer) is present in an amount of 0.1 to 5% by weight based on the total weight of the composition.

The method according to claim 1,
Wherein the composition further comprises at least one additive selected from the group consisting of copper, vegetable oils, emulsifiers, neutralizers, thickeners, and preservatives.

A hair styling product comprising the composition according to claim 1.

A method of making a hair styling wax composition comprising the steps of:
S1) dissolving the aqueous phase component in purified water;
S2) emulsifying an oil component comprising 8.5 to 13% by weight of wax relative to the total weight of the composition, 4.5 to 8% by weight of microcrystalline wax, or a mixture thereof to the aqueous phase prepared in step S1); And
S3) adding 5 to 12 wt% of isopentane to the total weight of the composition.