KR101758327B1 - A cleansing Composition comprising a extract of Acorus calamus L, and the aromatic oil of Schizonepeta tenuifolia var. japonica and Chrysanthemum indicum L. as an active ingredient with moisturizing effect - Google Patents

A cleansing Composition comprising a extract of Acorus calamus L, and the aromatic oil of Schizonepeta tenuifolia var. japonica and Chrysanthemum indicum L. as an active ingredient with moisturizing effect Download PDF

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KR101758327B1
KR101758327B1 KR1020150044836A KR20150044836A KR101758327B1 KR 101758327 B1 KR101758327 B1 KR 101758327B1 KR 1020150044836 A KR1020150044836 A KR 1020150044836A KR 20150044836 A KR20150044836 A KR 20150044836A KR 101758327 B1 KR101758327 B1 KR 101758327B1
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weight
parts
extract
sodium
active ingredient
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KR20160116691A (en
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민유홍
윤호기
이가연
김미래
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대구한의대학교산학협력단
주식회사 홀마
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Abstract

The present invention relates to an animal cleansing composition comprising an iris extract, a mold, and an aroma oil of camphor, as an active ingredient. The animal cleansing composition prepared by the method of the present invention is used for skin moisturization And skin irritation were measured. As a result, it was confirmed that they have excellent moisturizing effect and skin irritation inhibiting effect as compared with the comparison group which does not contain the above-mentioned effective ingredient. Therefore, it is an excellent detergent for animals and can be used safely even when used for a long time.

Description

TECHNICAL FIELD The present invention relates to an animal cleansing composition comprising an iris extract having a moisturizing effect, a mold extract, and an aroma oil of the palm kernel as an active ingredient. The present invention relates to an animal cleansing composition comprising an extract of Acerus calamus L and an aromatic oil of Schizonepeta tenuifolia var. japonica and Chrysanthemum indicum L. as an active ingredient with moisturizing effect}

The present invention relates to an animal cleansing composition comprising an iris extract, a mold, and an aroma oil of camellia as an active ingredient.

[Literature 1] Lee, Hyung-Sup, and others, The Dictionary of Fragrances, Yeonglim Publishing House, pp.278 ~ 281, 1998

[Literature 2] I, Hyung-Sup, and 1 other person, Encyclopedia of Fragrances, Yeonglim, pp.863 ~ 864, 1998

[Literature 3] Ipseup et al. 1, Encyclopedia of Enlightenment, Young Lim, pp.1038 ~ 1039, 1998

[Document 4] Wahlberg JE, Patch Testing. In Textbook of Contact Dermatitis, ed. R. Richard, pp. 241-268, Springer-Verlag, New York, 1995

The present invention relates to an animal cleansing composition comprising an iris extract, a mold, and an aroma oil of greenery as an active ingredient, and a method of using the same.

Humans and animals are always exposed to various pollution environments. Such a contaminated environment has an adverse effect on the body of a human being or an animal particularly, it contaminates the skin and hair which form the outer surface of the body, and basically deteriorates the sensation of refreshing. In addition, If left untreated for a long time, it causes various diseases such as skin and hair.

However, the pollution environment can not be avoided, and thus a detergent has been designed and used for a long period of time to clean skin and hair that have been exposed to polluted environment and contaminated.

These detergents are designed to be optimized for human pollution environment, pollution conditions to humans, and human skin and hair. In recent years, only detergents for human use have been devised and used. In the past, Rather than designing detergents for animals, the detergents used by humans have been applied to animals as such.

An animal cleansing agent distributed in the animal market in the past has been made to have the same composition and viscosity as the shampoo (hair shampoo) used by humans.

However, since the animal is weaker in skin than a person and has different skin properties, conventional detergents are extremely irritating to the skin of animals. For example, in the case of dogs (dogs), the epidermis of the skin is composed of 3 to 5 layers and is weaker than the human skin, and the skin properties are weakly acidic in humans, whereas they are weakly alkaline in dogs, ≪ / RTI > is very irritating to the skin of dogs. That is, a conventional pet cleaning agent contains a large amount (40 to 50% by weight) of a surfactant which is irritating to the skin among constituents of the cleaning agent even if the hygiene state and the glazed state are improved, and the pH is about 4 to 5 And the animals with sensitive skin are irritated to the skin, and thus the skin health of the animal is deteriorated.

Especially in the past, the use of the cleaner used by humans in the past led to the creation of a new harmful environment in animals, and in the modern age, recognizing that animals are different from humans, it is possible to use animal-specific detergents, especially moisturizing and environmentally friendly animals Development of detergents was required.

On the other hand, the iris is the outpost of Aracea calamus L belonging to the Araceae family, and known components include essential oil components such as eugenol, asarylaldehyde and asarone, tannin, axorin, and palmitic acid, and is known to exhibit sedative, analgesic, astringent, and deep-seated gingham function (Lee, Seong-Sup, et al. 278-281, 1998).

The mold is the outpipe of the lobule (Schizonepeta tenuifolia var japonica Kitagawa) belonging to the labiatae. It is known that essential components such as menthone and limonene are known, and it is known to have a cold and antipyretic analgesic effect (1) (1), and (2).

It is also known as Chrysanthemum indicum L., which belongs to the Compositae family. The known components are acacetin-7-rhamnoglucoside, chrysanthemin thujone, The antihypertensive effect, antiviral and antimicrobial action have been known (1 case, 1 case, pp. 1038 ~ 1039, 1998).

However, none of the above documents mention or disclose a composition for cleaning an animal, which contains an iris extract, a mold, and an aroma oil of green tea as an active ingredient.

The present inventors measured skin moisturizing degree and skin irritation degree on animal skin such as horses by using a composition containing iris extract, mold and aroma oil as an active ingredient, and as a result, The present inventors completed the present invention by confirming that they have excellent moisturizing effect and skin irritation inhibiting effect.

In order to accomplish the above object, the present invention provides an animal cleansing composition comprising an iris extract, a mold, and an aroma oil of camellia as an active ingredient.

The active ingredient as defined herein is preferably present in an amount of from 10 to 1000: 1 to 100: 1, more preferably from 100 to 800: 1 to 50: 1, most preferably from 10: 1000: 1 to 100: By weight is mixed with 300 to 600: 1 to 20: 1 blend parts.

The iris extracts as defined herein may contain one or more solvents selected from the group consisting of water, ethanol, methanol, propanol, butanol, acetone, ethyl acetate, hexane, butylene glycol, propylene glycol, hydrolyzed butylene glycol, , Preferably water, methanol, ethanol or a mixed solvent thereof, more preferably a water extract.

The moldable or native aroma oils defined herein include aroma oil layers obtained by extraction of moldings and native colors by water distillation using a vacuum low temperature concentrator.

The animals defined herein are collectively referred to as mammals except for the human body, including, but not limited to, cats such as cats, dogs and the like, livestock such as horses, cows, pigs and the like.

Hereinafter, the present invention will be described in detail.

For example, water having a volume of about 1 to 300 times, preferably about 1 to 150 times the volume of the irritated dry matter, ethanol, methanol, propanol, butanol, acetone, ethyl acetate, hexane, butylene glycol, propylene Preferably from about 0 to about 150 DEG C, preferably from about 50 to about 150 DEG C, in water, in at least one solvent selected from the group consisting of glycerin, glycerol, hydrolyzed butylene glycol, water-containing propylene glycol and water glycerin, preferably water, methanol, ethanol or a mixed solvent thereof, At a temperature of 120 to 120 ° C for about 10 minutes to 48 hours, preferably for 30 minutes to 12 hours by a conventional extraction method such as a normal temperature extraction method, a heating extraction method, an ultrasonic extraction method and a reflux extraction method, Preferably 2 to 7 times; A second step of filtrating and concentrating the extract obtained in the above step under reduced pressure; And a third step of lyophilizing the concentrated extract at a temperature of about -50 ° C to -30 ° C for about 24 to 72 hours to obtain an iris extract of the present invention.

In addition, the mold-making and aromatherapy oils of the present invention can be produced, for example, by adding water having a volume of about 1 to 3000 times, preferably about 1 to 1500 times, And extracting it by a water distillation method according to the manual of the apparatus; A second step of extracting aroma oil by a distillation method of the first step and separating the water layer and the aroma oil layer using a separating funnel; And a third step of recovering the separated aroma oil layer in the second step, respectively, to obtain the mold-forming and aromatizing aroma oils of the present invention, respectively.

The present invention specifically relates to a composition comprising (a) an active ingredient consisting of iris extract, mold-opening aroma oil and azalea oil; (b) at least one thickening agent selected from coconut diethanolamides, sodium carboxymethyl cellulose, Carbomer, Xanthan gum, and salt; (c) Coco-betaine, Sodium Laureth Sulfate, ES-430 (Sodium Lauryl Sulphate, SLS, Glucopon, Cognis), Coca There may be mentioned Cocamidopropylamine Oxide, Alkyltrimethylammonium chloride, Dialkyl dimethyl ammonium chloride, Benzalkonium chloride, Alkyl dimethylaminoacetic acid betaine And at least one surfactant selected from alkyl amidopropyl aminoacetic acid betaine; (d) benzalkonium chloride, paraben, benzoic acid, sodium benzoate, dichlorobenzyl alcohol, phenoxyethanol, DMDM hydantoin, and One or more sterilizing agents selected from sodium sulfite; (e) one or more fragrances selected from lemon, lavender, musk, and fruit flavors; (f) glycerin, polyethylene glycol, propylene glycol, butylene glycols, sorbitol, hyaluronic acid, panthenol, and the like; One or more humectants selected from tocopherol; (g) at least one herbal extract selected from wormwood, green tea, aloe, chamomile, calendula, lemongrass, rose hip, whitish, side, and mouthwash, and (h) water.

The active ingredient composed of the iris extract (a), the open mouth aroma oil and the azalea oil is 10 to 60 parts by weight, preferably 30 to 50 parts by weight, more preferably 30 to 50 parts by weight, based on 100 parts by weight of the cleansing composition, 35 to 45 parts by weight; (b) 0.055 to 12.0 parts by weight of at least one thickening agent selected from coconut diethanolamides, sodium carboxymethyl cellulose, Carbomer, Xanthan gum, and salt. Preferably 0.1 to 3.5 parts by weight, more preferably 0.2 to 4.0 parts by weight; (c) Coco-betaine, Sodium Laureth Sulfate, ES-430 (Sodium Lauryl Sulphate, SLS, Glucopon, Cognis), Coca There may be mentioned Cocamidopropylamine Oxide, Alkyltrimethylammonium chloride, Dialkyl dimethyl ammonium chloride, Benzalkonium chloride, Alkyl dimethylaminoacetic acid betaine 10 to 69.925 parts by weight, preferably 30 to 60 parts by weight, more preferably 35 to 55 parts by weight, of at least one surfactant selected from alkylamidopropyl dimethylaminoacetic acid betaine; (d) benzalkonium chloride, paraben, benzoic acid, sodium benzoate, dichlorobenzyl alcohol, phenoxyethanol, DMDM hydantoin, and 0.005 to 2.0 parts by weight, preferably 0.05 to 1.0 part by weight, more preferably 0.01 to 0.5 part by weight of at least one sterilizing agent selected from sodium sulfite; (e) 0.005 to 4.0 parts by weight, preferably 0.05 to 2.0 parts by weight, more preferably 0.01 to 1.0 part by weight of at least one fragrance selected from lemon fragrance, lavender fragrance, musk fragrance, and fruit fragrance; (f) glycerin, polyethylene glycol, propylene glycol, butylene glycols, sorbitol, hyaluronic acid, panthenol, and the like; 0.005 to 4.0 parts by weight, preferably 0.05 to 2.0 parts by weight, more preferably 0.01 to 1.0 part by weight of at least one humectant selected from tocopherol; (g) 0.005 to 4.0 parts by weight, preferably 0.05 to 2.0 parts by weight, more preferably 0.01 to 2 parts by weight of at least one herbal extract selected from wormwood, green tea, aloe, chamomile, calendula, lemongrass, rose hip, And (h) 0.05 to 20 parts by weight, preferably 0.5 to 10 parts by weight, more preferably 1 to 5.0 parts by weight of water.

As used herein, the term "surfactant" includes nonionic surfactants, anionic surfactants, cationic surfactants, amphoteric surfactants, nonionic surfactants or combinations thereof, preferably Sodium Cocoyl Apple Amino Acids, Cocamidopropyl Betaine, Sodium Peg-7 Olive Oil Catecholate, Cocamide DEA (CDA, CDE), Disodium Laureth Sulfosuccinate (LES, CORUM 3510, CORUM 9807), Decyl Polyglucose (APG) , A sugar surfactant (DLS), and the like are preferably used.

Anionic surfactants, as defined herein, can be anionic surfactants such as sodium alkyl sulfates, triethanol amine alkyl sulfates, ammonium alkyl sulfates, ammonium alkyl ether sulfates containing ethoxy groups, and derivatives such as sodium alkyl ether sulfates.

As used herein, the term " nonionic surfactant " refers to derivatives such as alkanolamide and alkyl oxide amines, preferably lauric acid diethanolamide, lauryldiethylamine oxide, palm oil alkyldimethylamine oxide, palm oil fatty acid diethanolamide, And coconut oil fatty acid monoethanolamide, or a mixture of two or more thereof. More preferably a non-ionic surfactant such as Cocoamide DEA which is inexpensive.

Other nonionic surfactants, anionic surfactants, cationic surfactants, and amphoteric surfactants, which can be used in the present invention, include the following nonionic surfactants.

Examples of the nonionic surfactant include self emulsifying monostearate glycerin, propylene glycol fatty acid ester, glycerin fatty acid ester, polyglycerin fatty acid ester, sorbitan fatty acid ester, POE (polyoxyethylene) sorbitan fatty acid ester, POE sorbit fatty acid ester, POE (Polyoxyethylene / polyoxypropylene) copolymer, POE.POP alkyl ether, polyether-modified silicone, polyether-modified silicone, polyoxyethylene-polyoxypropylene (POE) Alkanolamides, alkylamine oxides, hydrogenated soybean phospholipids, and the like.

Examples of the anionic surfactant include fatty acid soap, alpha-acylsulfonate, alkylsulfonate, alkylarylsulfonate, alkylnaphthalenesulfonate, alkylsulfate, POE alkyl ether sulfate, alkylamide sulfate, alkyl phosphate, POE alkyl ginseng salt, Alkylsulfosuccinic acid salts, acylated hydrolyzed collagen peptide salts, and perfluoroalkyl phosphoric acid esters, and the like can be mentioned. have.

Examples of the cationic surfactant include alkyl trimethyl ammonium chloride, stearyl trimethyl ammonium chloride, stearyl trimethyl ammonium bromide, cetostearyl trimethyl ammonium chloride, distearyl dimethyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride, behenyl trimethyl ammonium chloride, Benzalkonium, diethylaminoethylamide stearate, dimethylaminopropylamide stearate, quaternary ammonium salts of lanolin derivatives, and the like.

Examples of the amphoteric surfactant include carboxybetaine type, amide betaine type, sulfobetaine type, hydroxysulfobetaine type, amidosulfobetaine type, phosphobetaine type, aminocarboxylate type, imidazoline derivative type and amide amine type Amphoteric surfactants and the like.

When the surfactant is used in an amount of less than 30 parts by weight, the detergency against skin and hair is insufficient. When the surfactant is used in an amount exceeding 50 parts by weight, excess foaming occurs, and more water and time are required than in rinsing.

The cleaning composition may contain an additional component such as a bactericide, pigment, flavor, preservative, and the like.

As the bactericide, sulfur, tricoic acid, and conazole derivatives can be used. As the coloring matter, a water-soluble coloring matter or the like can be used, and natural flavoring agents (apple, herb flavor, etc.) can be used as the flavoring agent. In this case, the natural flavor (apple flavor, herb flavor) can be dissolved in the composition of the present invention by using a trace amount of ethanol and a solubilizing agent. Natural fruit extracts are added as vitamins and substitutes for flavors, for example, apple extracts can be used.

The moisturizing agent may be glycerin, propylene glycol or oils.

As an example of the "herbal extract" as defined herein, chamomile, calendula, lemongrass, rosehip, whitish, horsetail, wormwood, and herb extract can be preferably used, but other herb materials are also possible.

Animal skin and hair have a disadvantage of being very dry compared to humans, while the pH of the skin and hair is in the neutral range, so they have favorable conditions for simultaneous cleaning and nutrition. In view of the above, in the present invention, an oil content of up to 10% is added to the detergent composition. As a result, the degree of irritation of the cleaning component can be lowered and a sufficient amount of oil can be supplied, thereby providing a composition optimized for animal cleaning.

The addition and mixing of the individual components are carried out at room temperature, and the mixture is agitated for sufficient mixing, thereby completing the animal detergent composition.

In addition, the animal cleaning composition prepared by the production method of the present invention showed skin moisturization degree and skin irritation degree on animal skin such as horses and showed superior moisturizing effect It is confirmed that it has a skin irritation inhibiting effect, and therefore, it can be used safely even when it is used for a long time as an excellent animal cleansing agent.

Accordingly, the present invention provides an animal cleaning composition with the above-described manufacturing method and the above-described manufacturing method.

The detergent composition according to the present invention can control the components of the detergent composition according to the skin and hair condition of an animal and the kinds of animals and can be used as an additive component such as organic and inorganic pigments, organic powders, preservatives, pH adjusters, May be further added. Hereinafter, equivalent components of the components described later may be further present, and it is possible to substitute the components described below for their equivalent components, so that the present invention should not be construed as being limited to the components described below .

Examples of the organic and inorganic pigments include inorganic pigments such as silicic acid, silicic anhydride, magnesium silicate, talc, sericite, mica, kaolin, Bengala, clay, bentonite, titanium mica, titanium oxide, bismuth chloride, zirconium oxide, magnesium oxide, Inorganic pigments such as calcium sulfate, barium sulfate, magnesium sulfate, calcium carbonate, magnesium carbonate, iron oxide, chromium oxide, chromium oxide, chromium hydroxide, But are not limited to, polyamide, polyester, polypropylene, polystyrene, polyurethane, vinyl resin, urea resin, phenol resin, fluororesin, silicon resin, acrylic resin, melamine resin, epoxy resin, polycarbonate resin, Silk powder, cellulose, CI Pigment Yellow, CI Pigment Orange, and composite pigments of inorganic pigments and organic pigments thereof.

As the organic powder, metallic soap such as calcium stearate; Metal salts of alkyl phosphates such as sodium zinc cetylate, zinc laurylate and calcium lauryl laurate; Acylamino acid polyvalent metal salts such as N-lauroyl-beta-alanine calcium, N-lauroyl-beta-alanine zinc and N-lauroylglycine calcium; Amidosulfonic acid multivalent metal salts such as N-lauroyl-taurine calcium and N-palmitoyl-taurine calcium; Such as N-epsilon-lauroyl-L-lysine, N-epsilon-palmitoylidene, N-alpha-paratyylnitine, N-alpha-lauroyl arginine, Acyl basic amino acids; N-acylpolypeptides such as N-lauroylglycylglycine; Alpha-amino fatty acids such as alpha-aminocaprylic acid, alpha-aminoaurauric acid, and the like; Polyethylene, polypropylene, nylon, polymethylmethacrylate, polystyrene, divinylbenzene-styrene copolymer, ethylene tetrafluoride, and the like.

Examples of the disinfectant include hinokitiol, trichloroacid, trichlorohydroxydiphenyl ether, crohexidine gluconate, phenoxyethanol, resorcin, isopropylmethylphenol, azulene, salicylic acid, zinc filitione, benzalkonium chloride, No. 301, mononitro and eicol sodium, and undecylenic acid.

Examples of the pH adjuster include citric acid, sodium citrate, malic acid, sodium malate, fumaric acid, sodium fumarate, succinic acid, sodium succinate, sodium hydroxide, sodium monohydrogenphosphate and the like.

Examples of the alcohol include higher alcohols such as cetyl alcohol.

In addition, any of the above components may be blended within the range not to impair the objects and effects of the present invention, but it is preferably 0.01 to 5% by weight based on the total weight, Preferably 0.01 to 3% by weight.

The present invention relates to an animal cleansing composition comprising an iris extract, a mold, and an aroma oil of camphor, as an active ingredient. The animal cleansing composition prepared by the method of the present invention is used for skin moisturization And skin irritation were measured. As a result, it was confirmed that they have excellent moisturizing effect and skin irritation inhibiting effect as compared with the comparison group which does not contain the above-mentioned effective ingredient. Therefore, it is an excellent detergent for animals and can be used safely even when used for a long time.

Below, The present invention will be described in detail by the following examples and experimental examples.

However, the following examples and experimental examples are illustrative of the present invention, and the content of the present invention is not limited by the following examples and experimental examples.

Example  1. Preparation of Extracts and Oils

1-1. Mold  Manufacture of aroma oils

21 kg of dried mold (Schizonepeta tenuifolia var. Japonica) purchased from the wholesale market of Daegu Jung-ku Chinese herbal medicine and 100 L of water were placed in a high-speed vacuum low-temperature concentrator (COSMOS660, Kyunghee E & P) and extracted with water distillation method The water layer and the aroma oil layer were separated using a funnel (10-437G, Fisher). A separate aroma oil layer was used in the following composition.

1-2. Country  Manufacture of aroma oils

21 kg of dried yam (Chrysanthemum indicum L.) purchased from the wholesale market of Jung-gu, Jung-gu, Daegu and 100 L of water were placed in a high-speed vacuum low-temperature concentrator (COSMOS660, KyungSha E & P) and extracted with the water distillation method according to the manufacturer's manual to extract the aroma oil. (10-437G, Fisher) was used to separate the water layer and the aroma oil layer. A separate aroma oil layer was used in the following composition.

1-3. calamus Water extract  Produce

2.5 kg of dried iris (Acorus calamus L), purchased from the wholesale market of Jung-gu, Jung-gu, Daegu, and 100 L of water were added to a large capacity hot water pot (KS-220, 100 L of iris extract was used for the composition to be obtained.

Example  2. The cleaning composition  Produce

The animal cleansing compositions as described in the following Table 1 were prepared using the iris extracts, molds and myrtle aroma oil prepared in the above Examples as active ingredients, and a comparative group in which the active ingredient was replaced with water was also prepared, Respectively.

(active ingredient, 0.010% by weight), camellia aroma oil (active ingredient, 0.001% by weight),

(b) Gradual component

Coconut diethanolamine (CDE, COCONUT DIETHANOLAMIDE, thickener, 0.500 wt%)

(c) a surfactant component

- Cationic surfactant: Coco-betaine (cationic surfactant, 20.000 wt%),

- Anionic Surfactant: Sodium Laureth Sulfate (SLES anionic surfactant, 10.000 wt.%), ES-430 (sodium lauryl sulfate, SLS, sodium lauryl sulfate, surfactant, 10.000 wt.%), Glucopone Glucopon, Germany Cognis, surfactant, 10.000 wt.%),

- Nonionic surfactant: Cocamidopropylamine oxide (nonionic surfactant, 6.000 wt%),

(d)

Benzalkonium chloride (ST-A50, Southeast synthesis, bactericide, 0.100% by weight)

(e) friable (pentadecanoic acid , thickener, 1.500% by weight),

(f)

      (Fragrance, 0.250% by weight), lavender (fragrance, fragrance, 0.250% by weight)

(g) Herbal ingredients

(Mugwort extract, 0.100% by weight of herbal extract) Green tea extract (0.100% by weight of soap parchment, herbal extract)

(h) Moisturizing agent component

Glycerin (humectant, triethylalcohol, 0.500 wt%),

ingredient function ratio (%) Example Comparative Example Iris extract Active ingredient 40.689 0.000 Aromatherapy oil Active ingredient 0.010 0.000 Aromatic Oils Oil Active ingredient 0.001 0.000 water moisture 0.000 40.700 CDE Coconut diethanolamine
(COCONUT DIETHANOLAMIDE)
Incrementer 0.500 0.500
Coco-betaine Cationic surfactant 20,000 20,000 SLES Anionic surfactant 10,000 10,000 ES-430 (SLS) Surfactants 10,000 10,000 Glucopon Surfactants 10,000 10,000 Amine oxide Nonionic surfactant 6.000 6.000 Benzalkonium chloride disinfectant 0.100 0.100 Salt Incrementer 1.500 1.500 Lemon incense Spices 0.250 0.250 Lavender incense Spices 0.250 0.250 Mugwort extract Herbal extract 0.100 0.100 Green tea extract Herbal extract 0.100 0.100 glycerin Moisturizer 0.500 0.500 Sum 100,000 100,000

Example 3 Preparation of Shampoo Composition for Cleaning

Using the cleaning composition prepared in Example 2, the following shampoo was prepared and used in the following experimental examples.

20345 g of iris extract obtained in accordance with the method for producing an extract of the above Example, 5 g of mold open aroma oil, and 0.5 g of yam rice aroma oil were put into a stirrer. Then, 500 g of CDE, 10000 g of Coco Betaine, 5000 g of SLES, 5000 g of glucose, 5000 g of glucose, 3000 g of amine oxide, 50 g of benzalkonium chloride, 750 g of salt, 125 g of lemon fragrance, 125 g of lavender fragrance, 50 g of mugwort extract, And 250 g of glycerin were placed in a stirrer (MSP, Jayotec) and stirred at 25 rpm to prepare 50 kg of the shampoo composition of the Example.

Comparative Example 1. Preparation of Comparative Shampoo Composition for Cleaning

For comparison with the shampoo compositions of the Example, shampoo compositions for comparison were prepared as described below and used in the following Experimental Examples.

500g of salicylic acid, 125g of lemon fragrance, 125g of lemon flavor, 50g of mugwort extract, 50g of green tea extract, 750g of water, 20350g of water, 250g of CDE, 10000g of coco betaine, 5000g of SLES, 5000g of ES-430, 5000g of glucose, 3000g of amine oxide, And 250 g of glycerin were placed in a stirrer (MSP, Jayotec) and stirred at 25 rpm to prepare 50 kg of a comparative shampoo composition.

Experimental Example 1. Measurement of skin moisturizing degree

Using the composition prepared in the above example, the skin moisturizing degree was measured as follows according to the manual of Corneometer, a moisture measurement device of CK elctronic, Germany.

When the temperature 18 ~ 22 ℃, humidity 40% to 60% of the day, say in the examples and comparative examples sufficient (5 to 20 years of age, 10 male and female 10, thoroughbreds, the height 140 ~ 170cm, beacon horse riding) After washing 2 hours later, it was measured according to the manual of the product using Corneometer (MPA5) manufactured by CK elctronic, Germany.

As a result of measuring 10 horses each, it was confirmed that the sample had a moisture retention value of 51.2 AU, which is much better than 35.9 AU of the comparative example (see Table 2).

product Water content (arbitrary unit, mean ± standard deviation) Example 51.2 ± 5.2 Comparative Example 35.9 ± 4.8 n = 10

Experimental Example 2 Measurement of skin irritation degree

Using the composition prepared in the above examples, skin irritation was measured using the method described in literature (Wahlberg JE, Patch Testing. In Textbook of Contact Dermatitis, ed. R. Richard, pp 241-268, Springer-Verlag, New York, 1995).

A patch test was used to evaluate skin irritation. For patch attachment end was epilation as (5 to 20 years of age, 10 male and female 10, thoroughbreds, the height 140 ~ 170cm, beacon horse riding) part a clipper (CL-8300KN, Hitachi) skin (10 X 15 cm , Abdominal region). In the case of Examples and Comparative Examples, it was diluted to 1% in water and diluted to 1% in jojoba oil (tablets, bubble bank) in case of aroma oil.

The diluted solution was absorbed by dropping 20 mu l (one drop) into a Hayes Test Chamber (Hayes Service BV). The adhesive lid around the chamber was removed and a chamber was attached to the back skin. After 48 hours, the chamber strips were removed from the skin and the skin condition was visually confirmed and the results were analyzed according to the International Contact Dermatitis Research Group (ICDRG) criteria (Wahlberg JE, Patch Testing. Textbook of Contact Dermatitis, ed. Richard, pp. 241-268, Springer-Verlag, New York, 1995).

score Symptom - No reaction ± Incomplete erythema + Erythema, infiltration, weak pus ++ Erythema, infiltration, pus, vesicles +++ Severe erythema, infiltration, merged vesicles

Claims (7)

(a) an active ingredient consisting of iris extract, open-mouth aroma oil and azalea oil; (b) at least one thickening agent selected from coconut diethanolamides, sodium carboxymethyl cellulose, Carbomer, Xanthan gum, and salt; (c) Coco-betaine, Sodium Laureth Sulfate, ES-430 (Sodium Lauryl Sulphate, SLS, Glucopon, Cognis), Coca There may be mentioned Cocamidopropylamine Oxide, Alkyltrimethylammonium chloride, Dialkyl dimethyl ammonium chloride, Benzalkonium chloride, Alkyl dimethylaminoacetic acid betaine And at least one surfactant selected from alkyl amidopropyl aminoacetic acid betaine; (d) benzalkonium chloride, paraben, benzoic acid, sodium benzoate, dichlorobenzyl alcohol, phenoxyethanol, DMDM hydantoin, and One or more sterilizing agents selected from sodium sulfite; (e) one or more fragrances selected from lemon, lavender, musk, and fruit flavors; (f) glycerin, polyethylene glycol, propylene glycol, butylene glycols, sorbitol, hyaluronic acid, panthenol, and the like; One or more humectants selected from tocopherol; (g) one or more herbal extracts selected from wormwood, green tea, aloe, chamomile, calendula, lemongrass, rose hips, whitish, dandelion, and rhizome and (h) water as an active ingredient. delete The method according to claim 1, wherein the iris extract is selected from the group consisting of water, ethanol, methanol, propanol, butanol, acetone, ethyl acetate, hexane, butylene glycol, propylene glycol, hydrolyzed butylene glycol, Wherein the composition is at least one solvent extract. [Claim 2] The composition for animal care according to claim 1, wherein the mold or indigo aroma oil is an aroma oil layer obtained by extracting mold and native flower by water distillation method using a vacuum low-temperature concentrator. 2. The animal cleansing composition according to claim 1, wherein the animal is a cat, a dog, a horse, a cow, or a pig. delete The method according to claim 1,
(A) 10 to 60 parts by weight of an active ingredient consisting of an iris extract, a crimson aroma oil and a camellia aroma oil, based on 100 parts by weight of the cleansing composition; (b) 0.055 to 12.0 parts by weight of at least one thickening agent selected from coconut diethanolamides, sodium carboxymethyl cellulose, Carbomer, Xanthan gum, and salt. ; (c) Coco-betaine, Sodium Laureth Sulfate, ES-430 (Sodium Lauryl Sulphate, SLS, Glucopon, Cognis), Coca There may be mentioned Cocamidopropylamine Oxide, Alkyltrimethylammonium chloride, Dialkyl dimethyl ammonium chloride, Benzalkonium chloride, Alkyl dimethylaminoacetic acid betaine And 10 to 69.925 parts by weight of at least one surfactant selected from alkyl amidopropyl dimethylaminoacetic acid betaine; (d) benzalkonium chloride, paraben, benzoic acid, sodium benzoate, dichlorobenzyl alcohol, phenoxyethanol, DMDM hydantoin, and 0.005 to 2.0 parts by weight of at least one bactericide selected from sodium sulfite; (e) 0.005 to 4.0 parts by weight of at least one fragrance selected from lemon fragrance, lavender fragrance, musk fragrance, and fruit fragrance; (f) glycerin, polyethylene glycol, propylene glycol, butylene glycols, sorbitol, hyaluronic acid, panthenol, and the like; 0.005 to 4.0 parts by weight of at least one moisturizer selected from tocopherol; (g) 0.005 to 4.0 parts by weight of at least one herbal extract selected from wormwood, green tea, aloe, chamomile, calendula, lemongrass, rose hip, A composition for cleaning animals.
KR1020150044836A 2015-03-31 2015-03-31 A cleansing Composition comprising a extract of Acorus calamus L, and the aromatic oil of Schizonepeta tenuifolia var. japonica and Chrysanthemum indicum L. as an active ingredient with moisturizing effect KR101758327B1 (en)

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KR20210140923A (en) 2020-05-14 2021-11-23 이경영 Aromatic composition for relieving itch of companion animal

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