KR101727475B1 - Method of producing a hair loss prevention and hair growth promoting composition of shampoo type - Google Patents

Abstract

The present invention relates to a method for producing a hair loss preventing and hair growth promoting agent of a shampoo type by combining extracts of roots of Acorus asiaticus and Glycyrrhizae Radix, mineral water containing natural mineral components and shampoo components. According to the present invention, a hair loss preventing and hair growth promoting agent manufactured by the method contains soap having natural components, thereby preventing damage of hairs during washing after using a hair growth promoting agent, and combines medicinal herb components and mineral of natural mineral water, thereby being safe to scalp and having excellent affinity and absorption abilities. Accordingly, the composition is effective in preventing hair loss and promoting hair growth.

Description

TECHNICAL FIELD The present invention relates to a hair growth promoting agent and a hair growth promoting agent,

The present invention relates to a shampoo type hair loss prevention and hair growth promoting agent, and more particularly, to a shampoo type hair loss prevention and hair growth promoting agent in which a natural plant ingredient and a natural mineral ingredient are harmonized with a shampoo.

In general, hair loss is caused by changes or damage of the scalp due to various factors. Hair loss is caused by genetic factors caused by hormone effect, air pollution, ultraviolet rays, dry wind, detergent (shampoo) , External factors such as perms and the like, and internal factors such as physical disease, progress of aging, mental stress, and the like. In order to prevent hair loss, to alleviate or cure hair loss, or to stimulate hair growth, Many types of hair loss treatment agents have been developed by drug therapy using agents such as a blood circulation promoter and the like. Natural remedies using a hair growth agent made of natural herbal medicine extracts, far infrared ray irradiation or physical stimulation to the scalp to prevent hair loss, Research and development are under way, but most of them As fit a case indicating the improvement of the scalp and hair condition as a whole has a slightly insufficient problems.

Recently, attention has been paid to a hair removing agent made of a natural extract which is not harmful to human body, a skin external preparation and a natural detergent (shampoo) for preventing or alleviating hair loss by washing waste products of the scalp and supplying artificial nutrients. Korean Patent Registration No. 10-1242736 discloses a composition containing a lotus root, a lotus leaf, a red ginseng, a vitamin tree leaf and a stem, a persimmon leaf, a cabbage, a ginger, a rosemary, a black bean, a black sesame, an aloe, a mulberry leaf, The herbal medicines containing mint, blueberry, blueberry, garlic and garlic are put into an aging machine and kept at 65 ~ 95 ℃ for 3 ~ 21 days depending on the materials. Discloses a natural shampoo having a hair growth promoting function, and Korean Patent Laid-Open Publication No. 10-2008-2224 discloses a method of producing a golden and grape seed extract System; Drying and pulverizing the gold and grapefruit seed extract; Mixing the dry powders of the golden and grapefruit seed extracts in a ratio of 1: 2: 1 (w: w); Adding the dried powder mixture of the golden and grapefruit seed extracts to the shampoo composition in an amount of 0.5 to 20.0% based on the total weight of the shampoo composition, and mixing the same uniformly. Also disclosed is a method for producing an antibacterial shampoo No. 10-1229762 discloses a skin external preparation for the formulation of liquid form, cream form, paste form, or solid form for improving hair growth and prevention of hair loss, which comprises a combination extract of Hanshik Cho, Pae Yabyeop, Chojyo, .

The present invention confirms that the natural plant ingredient containing the active ingredient for prevention of hair loss and hair growth promoting action is harmonized with the natural mineral ingredient to accelerate transdermal absorption of the active ingredient required for hair growth and to improve hair loss prevention and hair growth promoting effect, .

The present invention aims to provide a method for producing a shampoo type hair loss prevention and hair growth promoting agent in which a natural plant ingredient containing an active ingredient for prevention of hair loss and hair growth promotion is harmonized with a natural mineral ingredient and specifically, And a method for producing a hair shampoo-type hair loss-inhibiting and hair growth promoting agent by harmonizing an extract of licorice and mineral water containing a natural mineral component and a shampoo ingredient.

As a solution for achieving the object of the present invention, a method for producing shampoo type hair loss prevention and hair growth promoting agent comprises the steps of: a) preparing a solid natural soap from palmstearic acid, palmystolic acid and fumaric acid; b) . 8 to 10 parts by weight of glucose, 8 to 10 parts by weight of white sugar, 0.01 to 0.02 parts by weight of dietary fiber, 25 to 30 parts by weight of potato starch, 5 to 10 parts by weight of sugar alcohol, and 10 to 30 parts by weight of boric acid 30 To 35 parts by weight, mixing the mixture uniformly while injecting carbonic acid gas, and then drying and pulverizing to prepare an active ingredient powder, and c). A third step of mixing 8 to 15 parts by weight of the powder of the active ingredient of the second step and 80 to 100 parts by weight of the primer mineral water with 100 parts by weight of the solid natural detergent component of the first step to prepare a liquid combination by wet pulverization .

Palm stearic acid, palmystolic acid, palmallow acid, which is selected in the first step of producing the solid natural soap according to the present invention is a vegetable fatty acid obtained from (Palm Fatty Acid), and palm oil is palm oil, (Oil Palm) Vegetable oil extracted from the pulp of wood. It is the most used cooking oil in the world together with soybean oil. Palm oil contains almost one to one unsaturated fatty acid and saturated fatty acid. Linoleic acid, which is an essential fatty acid, 10%. The content of saturated fatty acid is similar to that of animal fat, but it contains tocopherol which is characteristic of vegetable oil and it is distinct from animal fat without cholesterol.

The natural soap according to the present invention is prepared by a conventional method of producing soap using a palm fatty acid, which is a natural vegetable oil obtained from palm oil, as a raw material, and an auxiliary component such as a moisturizer and a perfume is added as needed. In order to prevent deterioration and ease of handling during the process, it is frozen and solidified.

The root of the iris formed in the second step of preparing the active ingredient powder according to the present invention is the root of iris (Acdrus asiaticus), which is a perennial herb of iris, and when the head is wrapped around iris roots and leaves in May, In the present invention, the extract of hot water extracted with hot water is used as an active ingredient. The liquorice is also a herb medicine widely known in the art. In the present invention, 100 parts by weight of iris root To 20 to 30 parts by weight of licorice, and the mixture is subjected to hot water extraction.

In addition, the glucose and white sugar produced in the second step acts as a nutrient for hair growth. Dietary fiber and potato starch are swollen or gelated to form a thin coating layer on the scalp or hair surface by viscosity, And during the application to the hair, the active ingredient is absorbed into the scalp while exhibiting a favorable action, while being adsorbed on the surface of hair and so on, the hair is kept thick and strong, and the dietary fiber is a mixture of water-soluble and water-insoluble dietary fibers Of dietary fiber can be used, but it is preferable that water-soluble dietary fiber is formed.

The sugar alcohol is referred to as a polyhydric alcohol, a polyol, etc., and imparts a moisturizing and refreshing sensation to the sugar alcohol. The sugar alcohol exhibits an action of preventing the aging of the starch by hygroscopicity. In the present invention, glycerol, sorbitol, And the like.

In addition, the boric acid formed in the second step functions as a disinfectant and an antiseptic agent as well as a function of reducing the luxurious action of the starch to prevent deterioration of the hair growth agent according to the present invention, and the boric acid is toxic, In the present invention, the above-mentioned licorice extract is used in combination to reduce or neutralize the toxicity of boric acid.

In the second step of mixing the carbonic acid gas in the second step according to the present invention, uniform mixing and harmful volatile components are volatilized together with the carbonic acid gas while preventing agglomeration of the starch and liquid components in the mixing of the active ingredients Which is then mixed and then dried at 25 to 35 ° C.

In the third stage of manufacturing the liquid combination according to the present invention, the primary mineral water to be selected is the world's largest mineral water (FDA approved) with a history of more than 600 years as the world's third mineral spring with the Shasta mineral spring in the United States and the Napaurin mineral spring in England. It is known that minerals are rich in minerals beneficial to human body along with Ca, Si, Mg, K, and Na, and are effective for hypertension, diabetes, gastrointestinal diseases, skin diseases and eye diseases.

In the third step of the present invention, the hair growth effect according to the present invention can be achieved by replacing water with primary mineral water as a mixed solvent of natural soap and active ingredient powder to combine beneficial mineral components contained in primary mineral water with active ingredients In the present invention, when the primer mineral water is not added, the primer mineral water is an essential component for the hair growth promoter of the present invention since it does not affect the hair growth promoting effect. The active ingredient powder is added to 100 parts by weight of the solid natural detergent component, 15 parts by weight of water and 80-100 parts by weight of primed mineral water are wet pulverized by a known wet pulverizer such as a millstone mill to achieve the hair growth promoting effect according to the present invention.

The shampoo type hair loss prevention and hair growth promoter, which is a liquid combination prepared by the first to third steps according to the present invention, may further include supplementary ingredients generally used in scalp and hair preparations such as a coloring agent and a flavoring agent Can be used.

The method of using the hair shampoo type hair loss preventing agent according to the present invention is a method of using the hair growth promoting agent of the present invention as a whole on the basis of the hair loss severely, Gently massage the scalp with your fingertips, then wash your hair after 7 to 10 minutes.

Since the hair growth promoting agent of the present invention has a shampoo ingredient, it is not necessary to use a separate detergent when washing the hair after 7 to 10 minutes have elapsed after application of the hair growth promoter, and the use frequency of the hair growth promoter of the present invention is 1 ~ 2 times, preferably once in the morning or twice in the morning and evening

The shampoo type hair loss prevention and hair growth promoting agent produced by the manufacturing method of the present invention has the effect of preventing the damage of the hair during washing after using the hair removing agent by containing the soap of the natural ingredient and also the combination of the herbal medicine ingredient and the mineral mineral of natural mineral water It is safe for the scalp, and has excellent affinity and absorption ability, so that it exhibits an excellent effect for prevention of hair loss and promotion of hair growth. At the same time, the hair is thick and strong because of action of dietary fiber and starch.

FIG. 1 is a photograph showing the growth of mouse hair in the control group and the test group (application group) for 5 weeks with the hair growth stimulant according to the present invention
2 is a graph showing the hair growth inducing effect of the hair growth stimulant according to the present invention

Hereinafter, the present invention will be described in detail with reference to examples and test examples, but the present invention is not limited by the examples described below.

<Examples>

a). Production of solid natural soap (first step)

50 parts by weight of palmistillic acid, 75 parts by weight of fumaric acid, and 10 parts by weight of an anionic surfactant were added to 100 parts by weight of palm stearic acid in a prepared vessel, and 300 parts by weight of an aqueous sodium hydroxide solution (about 9 wt%) was slowly added The mixture is heated to about 75 캜 while being poured, then slowly cooled to separate the soap component, and the container is frozen to prepare a solid soap.

b). Preparation of active ingredient powder according to the present invention (second step)

100 parts by weight of dried iris roots and 25 parts by weight of licorice were added to the prepared heating vessel and heated at 100 DEG C for 4 hours with water. After cooling to room temperature, the solid content was removed by filtration to obtain a hot water extract of iris root and licorice root .

10 parts by weight of glucose, 8 parts by weight of white sugar, 5 parts by weight of glycerin, 3 parts by weight of sorbitol, 3 parts by weight of propylene glycol, 0,01 parts by weight of dietary fiber, 30 parts by weight of boric acid and 35 parts by weight of boric acid were charged and mixed for about 30 minutes while carbon dioxide was being injected under stirring. The mixture was dried at about 30 DEG C and the resulting dried material was pulverized by a pulverizer to prepare an active ingredient powder.

c). Preparation of liquid combination (hair growth promoter) according to the present invention (third step)

10 parts by weight of the powdery active ingredient was added to 100 parts by weight of the above-prepared solid natural soap in a pulverizer, and 100 parts by weight of the granular mineral water was added thereto to wet-mill the mixture first. The obtained primary pulverized material was used as an auxiliary ingredient Rosemary) and a coloring agent, and finely pulverized and mixed with a mill grinder to prepare a liquid combination (hair growth promoter) according to the present invention.

<Test Example>

The growth-inducing effect of the liquid combination (hair growth promoter) prepared in the above <Examples> was evaluated during the evaluation of the effect of the wool by the animal test method as described below and is shown in FIG. 1 and FIG.

a). Test Methods

(One). Hair growth induction experiment in C57BL / 6 mouse

Six-week-old female C57BL / 6 mice were purchased from Orient Bio (Seongnam, Gyeonggi, Korea) and adjusted for adaptation and hair cycle in an animal breeding environment for 1 week. The animals were kept in the cages for quarantine, and the experimental diets were fed free. The mouse and the like were epilated with a clipper for small animals before the start of the experiment.

Eight mice were used in the experimental group as the control group (control group) and the liquid combination (hair growth promoting agent) according to the present invention as the application group. In the case of the application group, 1 g of the liquid combination (hair growth promoting agent) according to the present invention was applied to the epilation area every day from day 1 to day 7 (day 7) and wiped with distilled water 10 minutes later. 100 μl of a 10% dilution of the liquid combination (hair growth promoting agent) according to the present invention (prepared by adding sterilized third distilled water to the stock solution to prepare a 10% diluent) was dispensed to the epilating site for 8 days (day 8) After 10 minutes, it was wiped with distilled water. The changes of the dorsal skin of the mice were observed with the naked eye every day, and photographs were taken after anesthesia to compare the growth induction effect on 0, 7, 14, 21, 28, and 35 days after epilation.

The induction of the hair into the growth phase is carried out using a dot matrix planimetry The average of black skin / total skin (total area of black hair area / hair removal area) (%) on 21st day after epilation was measured and the induction to growth period was compared with the average of control group.

(2). Statistical processing

The experimental results are expressed as mean ± standard error (SE). Statistical significance was assessed using Student's t- test to determine the difference between [control group] and [application group], and it was statistically significant at p <0.05.

(3). Results and discussion

C57BL / 6 mice have melanocytes in the skin only in the hair follicles. When the hair cycle progresses from the telogen to the anagen, the skin color changes from pink to black.

As shown in Fig. 1, skin color change was observed from day 14 after epilating in [the application group], and significant hair growth was observed in [application group] compared to [control group] on day 21 after epilating there was.

The growth induction efficacy of the hair of [the application group] was quantitatively analyzed by dot matrix area measurement method. On day 21, the growth induction effect of hair was 99 ± 0.2% ( p <0.01) compared with the control (day21: 0 ± 0.3%) compared to the total area of hair removal area , Indicating a higher hair growth-inducing effect than the control group. The results are shown in Fig.

Claims (6)

a). A first step of producing a solid natural soap from palm fatty acid (Palm Fatty Acid)
b). 8 to 10 parts by weight of glucose, 8 to 10 parts by weight of white sugar, 0.01 to 0.02 parts by weight of dietary fiber, 100 parts by weight of dietary fiber, 100 parts by weight of iris root extract and licorice root extract, , 25-30 parts by weight of potato starch, 5-10 parts by weight of sugar alcohol and 30-35 parts by weight of boric acid, mixing the ingredients uniformly while injecting carbonic acid gas, drying and crushing the mixture to prepare an active ingredient, and
c). A third step of mixing 8 to 15 parts by weight of the active ingredient of the second step and 80 to 100 parts by weight of primer mineral water with 100 parts by weight of the solid natural detergent component of the first step to prepare a liquid combination by wet pulverization Wherein the shampoo-type hair loss preventing and hair growth promoting agent is produced by a method comprising the steps of: The method according to claim 1, wherein the palm fatty acid (Palm Fatty Acid) is at least one selected from palm stearic acid, palmystolic acid, and palmaric acid. delete The method according to claim 1, wherein the sugar alcohols are selected from glycerol, sorbitol, and propylene glycol. The method of claim 4, wherein the dietary fiber is a water-soluble dietary fiber. delete

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