KR101664863B1 - Method for Manufacturing Liquid Seasoning for Sailfin Sandfish - Google Patents
Method for Manufacturing Liquid Seasoning for Sailfin Sandfish Download PDFInfo
- Publication number
- KR101664863B1 KR101664863B1 KR1020160049860A KR20160049860A KR101664863B1 KR 101664863 B1 KR101664863 B1 KR 101664863B1 KR 1020160049860 A KR1020160049860 A KR 1020160049860A KR 20160049860 A KR20160049860 A KR 20160049860A KR 101664863 B1 KR101664863 B1 KR 101664863B1
- Authority
- KR
- South Korea
- Prior art keywords
- weight
- parts
- red ginseng
- saponin
- seasoning
- Prior art date
Links
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Classifications
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- A23L17/00—Food-from-the-sea products; Fish products; Fish meal; Fish-egg substitutes; Preparation or treatment thereof
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- A—HUMAN NECESSITIES
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- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/50—Soya sauce
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/20—Natural extracts
- A23V2250/21—Plant extracts
- A23V2250/2124—Ginseng
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/60—Sugars, e.g. mono-, di-, tri-, tetra-saccharides
- A23V2250/64—Sugar alcohols
- A23V2250/642—Sorbitol
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
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Abstract
The present invention relates to a method for preparing a seasoning for Dorimuk cooking which can improve the taste and storage stability of Dorumuk before or during cooking.
The seasoning solution prepared by the method according to the present invention can add a useful ingredient contained in red ginseng to the seasoning solution to produce a high-quality seasoning solution, and the antioxidative and antimicrobial components of red ginseng improve the storage stability of the seasoning solution Also, since the red ginseng ingredient is not destroyed by external factors such as oxygen, sunlight and heat, the effect of addition of red ginseng ingredient can be maintained even after a lapse of time.
Description
The present invention relates to a method for preparing a seasoning for Dorimuk cooking which can improve the taste and storage stability of Dorumuk before or during cooking.
Dorukmu is a fish belonging to the Doruk mushroom, which is mainly in the area where the bottom sand, mud, and mud are mixed at a depth of 150 m. The most suitable spawning season is from November to December. It is mainly scattered around the coast.
It is the most delicious in the spawning season. It is full of eggs, eggs, and oil because it is best for spawn from late autumn to early winter. It is popular for winter delicacies such as salt, steam, and stew. Is cheaper than females, but its utilization rate is relatively low compared to females.
It is rich in protein and minerals. It is especially beneficial for pregnant, lactating and developing children. It has a high content of phosphorus, which is a component of bone and dental tissues. It maintains the balance between acid and alkali. It is also an excellent food that can supplement the amino acid in the diet centered on cereal because it has excellent composition of amino acid constituting protein and contains large amount of lysine and threonine.
Because it does not have scales, it is easy to care for, and because it is small, it is steamed, fried in oil, eaten as bones, and boiled or cooked.
However, since Dulmuk is a common fish and its price is low, selling fish as it is fish is not beneficial to income, so it is necessary to improve the value added by making it processed food.
Korean Patent Registration No. 1549444 discloses a method for manufacturing fish paste containing fish meat, and the invention relates to a method for preparing fish meat by immersing raw fish meat in saline or pretreating the fish meat raw material for heating and cooling And then preparing a fish paste containing at least one gel-strengthening agent selected from Transglutaminase (TG-ase) and Glucono Delta Lactone (GDL).
The Dorumuk Kaomo can replace the conventional fish paste ingredients such as pollack or cod, which can lower the manufacturing cost of fish cake and does not use a synthetic sweetener. Therefore, it is advantageous to be free from the risk of harming the human body. However, It is disadvantageous in that the texture of the original texture is lowered because artificial gel strengthening agent is used for aggregation.
Korean Patent Laid-Open Publication No. 2015-0144163 discloses a method for producing a dumpling eel, which comprises adding Aspergillus kawachii koji to a crushed fish meat and storing the same at 10 to 20 ° C. And then adding the salt thereto and aging at 10 to 20 ° C. It is made by increasing the utilization of the dull mulch, and even if the salting time is shortened and the ripening period is shortened, it has the sensory properties of the eel.
However, aspergillus kawachikochi is grown at an appropriate temperature of 37 ° C. As described above, fish meat is not decomposed or aged at 10 to 20 ° C, and when the temperature is raised to the growth temperature, the fish meat is easily decayed, Is not properly implemented.
Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made to solve the above-mentioned problems, and it is an object of the present invention to provide a method for manufacturing a seasoning liquid for a sake- And the like.
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In order to solve the above-mentioned problems, the present invention provides a method for producing an oil-in-water emulsion, comprising: mixing 100 parts by weight of vegetable oil with 80-120 parts by weight of ethanol and 0.2-10.0 parts by weight of saponin extracted from red ginseng; 10 to 20 parts by weight of sugar, 10 to 20 parts by weight of D-sorbitol, 10 to 20 parts by weight of starch syrup and 0.5 to 10 parts by weight of soy sauce are mixed with 100 parts by weight of purified water to prepare an aqueous phase; Mixing the water phase and the oil phase at a weight ratio of 100: 30 to 70 and homogenizing the mixture at 3000 to 4000 rpm for 3 to 10 minutes; And drying the homogenized mixture. The present invention also provides a method for preparing a seasoning for oral cavity.
The saponin is prepared by mixing 1000 to 1500 parts by weight of alkaline ionized water having a pH of 9 to 11 and 1000 to 1500 parts by weight of 95 to 99% (v / v) ethanol with 100 parts by weight of red ginseng and extracting it at 50 to 70 ° C for 20 to 30 hours Preparing a red ginseng extract; Separating the red ginseng extract into a supernatant and a precipitate by standing at -5 to 5 ° C for 30 to 70 hours; And concentrating the supernatant at 50 to 70 ° C for 1 to 2 hours to obtain a concentrate having a total of Rg1, Rb1 and Rg3 contents of 20 to 60 mg / g, Is more preferable.
It is preferable to add 1 to 5 parts by weight of vinegar or 0.1 to 1.0 part by weight of the cultured lactic acid bacteria to 100 parts by weight of the purified water.
The seasoning solution prepared by the method according to the present invention can add a useful ingredient contained in red ginseng to the seasoning solution to produce a high-quality seasoning solution, and the antioxidative and antimicrobial components of red ginseng improve the storage stability of the seasoning solution .
In addition, by removing the starch or free sugars contained in red ginseng, it is possible to inhibit the spoilage of the ginseng by inhibiting the spoilage of the ginseng, and by inhibiting the loss of the useful ingredient of red ginseng in the process of removing such starch or free sugar, Can be added.
Also, since the red ginseng ingredient is not destroyed by external factors such as oxygen, sunlight, heat, etc., the effect of adding red ginseng component can be maintained even after a lapse of time.
In the present invention, seasonings are prepared by mixing sugar, D-sorbitol, starch syrup and soy sauce into purified water, and then saponin extracted from red ginseng is added thereto to prepare a seasoning for Dorukku.
The saccharide of sugar, D-sorbitol, and starch syrup imparts a sweet taste to the fish meat while preventing the fish from being disturbed, and the soy sauce improves the taste of the fish meat due to its unique flavor and taste, and cancels the fishy fishy fish.
However, when the fish meat and sugar are mixed, the activity of the spoilage bacteria that make the sugar as a nutrient is increased, and the corruption of the fish meat may be promoted. To prevent this, the saponin component extracted from red ginseng is added to the sauce.
Saponins are classified into three groups according to their chemical structure: protopanaxadiol, protopanaxatriol, and oleanolic acid. These saponins have a wide effect on the central nervous system, endocrine system, immune system, metabolism system, It is known that it exerts an excellent effect in normalizing the physiological function.
Especially, red ginseng prepared by boiling ginseng is composed of glycosides of ginseng, panacen, polyacetylenic compounds, nitrogenous components, flavonoids, vitamins (B group), trace elements, enzymes, , Amino acids, etc., as well as various chemical changes such as saponin modification, amino acid change, browning, etc. during the drying of the ginseng, and the ginsenosides ginsenoside) Saponins such as Rg2, Rg3, Rh1, and Rh2 are newly generated. These saponin-specific saponins of red ginseng inhibit cancer-inhibiting action, cancer cell growth inhibitory action, blood pressure lowering action, brain nerve cell protecting action, , Antioxidant activity, antimicrobial activity, etc., and thus it is possible to obtain an excellent pharmacological effect of only red ginseng.
According to the method of extracting red ginseng, there is a difference in the saponin content which is a quality measure of the red ginseng extract. There are physical factors such as extraction solvent and extraction temperature and time, chemical factors include organic acid present in the extract, The saponin content in the extract greatly changes.
The conventional method of extracting saponin from red ginseng is generally a method of extracting water at a high temperature of 85 to 90 ° C for 24 to 48 hours. However, when red ginseng is treated in high temperature water for a long time, There is a problem that saponin which is an active ingredient of red ginseng is decomposed by the influence of organic acids contained in red ginseng.
When ethanol is used instead of water as the extraction solvent, the extraction yield of saponin is lower than that of water, and the odor such as soil odor is strong, so that the flavor of red ginseng is weakened.
Accordingly, in the present invention, the red ginseng is extracted with alkaline ionized water and ethanol to increase the extraction yield, thereby preserving the original flavor of red ginseng, and then adding the red ginseng to the seasoning solution for Dorumuk to improve the taste and functionality of the Dorumk.
First, red ginseng is extracted with alkaline ionized water and ethanol as an extraction solvent.
Alkali ionized water is water obtained by applying an electric force to general water such as tap water or ground water. When platinum-plated titanium of an anode and an anode is put in water and electricity of direct current is passed through water, anion Are collected to become acidic ionized water, and cations are gathered on the (-) polar side to generate alkaline ionized water.
Such alkaline ionized water promotes the elution of water-soluble components from red ginseng because the minerals such as calcium, magnesium, and potassium, which are dissolved in water, have more beneficial minerals than water and have higher protein and fat solubility than common solvents. Serves as a catalyst for allowing red ginseng component to be eluted into alkaline ionized water so that red ginseng saponin can be extracted at low temperature without component breakage.
The extract of red ginseng is prepared by mixing 1000 to 1500 parts by weight of alkaline ionized water having a pH of 9 to 11 and 1000 to 1500 parts by weight of 95 to 99% (v / v) ethanol with 100 parts by weight of red ginseng and extracting at 50 to 70 ° C for 20 to 30 hours If the pH of the alkaline ionized water is less than 9, the extraction temperature is less than 50 ° C, or the extraction time is less than 20 hours, the extraction yield decreases. If the pH exceeds 11 or the extraction temperature exceeds 70 ° C or the extraction time If the reaction time exceeds 30 hours, saponin, which is an active ingredient of red ginseng, is decomposed due to the influence of organic acids contained in red ginseng.
In addition, the amount of the extraction solvent is a minimum amount sufficient to extract the saponin component of red ginseng, which can be minimized in the subsequent process of concentrating, and the mixing ratio of alkaline ionized water and ethanol is determined by mixing the water- It is a range optimized for component extraction according to the component ratio of saponin.
However, red ginseng contains saponin as well as non-saponin components, such as starch and free sugar, which deteriorate storage stability. Therefore, it is preferable to remove these components. For this purpose, starch, free sugars and the like It is preferable to add the supernatant to the seasoning solution after removing the precipitate contained therein.
For this purpose, the extract is allowed to settle in a refrigerated condition at -5 to 5 ° C for 30 to 70 hours to precipitate precipitable substances such as starch and free sugar in the extract. When the extract is precipitated in a refrigerated condition as described above, It is possible to increase the removal efficiency of the precipitable substance because the solute dissolved in the solution precipitates and precipitates due to the decrease of the solubility according to the temperature drop.
When the non-saponin component is cooled and precipitated, the supernatant is separated and recovered, and then added to the seasoning to prepare a seasoning liquid for cooking. 10 to 20 parts by weight of sugar, 10 to 20 parts by weight of D-sorbitol 10 to 20 parts by weight of starch syrup, 0.5 to 10 parts by weight of soy sauce, and 0.1 to 5.0 parts by weight of saponin extracted from red ginseng.
As the saponin added to the above seasoning solution, a concentrate obtained by concentrating the supernatant may be used. The supernatant is concentrated at 50 to 70 ° C for 1 to 2 hours so that the sum of Rg1, Rb1 and Rg3 is 20 to 60 mg / g After preparing the concentrate, 0.01 to 0.50 parts by weight of the concentrate may be added based on 100 parts by weight of purified water.
Since the concentration of the solvent is not more than the boiling point of the alkaline ionized water as the solvent of the supernatant liquid and the ethanol, the solvent evaporates only on the surface and does not cause rapid vaporization inside. Therefore, the saponin component dissolved in the supernatant liquid is prevented from being lost together with the water vapor And is concentrated at a low temperature, so that the saponin component can be prevented from being destroyed by heat.
However, since saponin is an amphipathic molecule having both a hydrophilic group and an oil and a close hydrophobic group which are close to water, it is possible to form a foam like a soap by giving a seasoning liquid to a syrup, or an emulsifying action while cooking a syrup with a seasoning liquid, Bubbles are generated on the surface, which causes a deterioration in visual aesthetics.
In order to overcome such disadvantages, it is preferable to mix the saponin with the seasonings by microencapsulation, and the encapsulation process can also prevent oxidation and decomposition mechanisms of the saponin active ingredient.
The microencapsulation of the saponin is carried out by dissolving vegetable oil in ethanol, adding saponin to prepare an oil phase, dissolving sugar, D-sorbitol, starch syrup and soy sauce in purified water to prepare a water phase, mixing the oil phase into water phase and homogenizing Followed by drying the emulsion.
Saponins extracted from red ginseng provide a very useful effect on the human body, but the saponin has a low human absorption rate, so that the human body has a sufficient effect of the saponin The vegetable oil improves the absorption efficiency of saponin of the present invention and improves the efficacy of the present invention.
In addition, Dulmuk is a typical low-calorie fish, which is effective in preventing cardiovascular diseases and adult diseases by abundantly containing unsaturated fatty acids such as docosahexaenoic acid (DHA) and eicosapentaenoic acid (EPA), which lower the blood cholesterol level and reduce triglycerides Among the vegetable oils, especially the perilla oil, alpha-linolenic acid which is metabolized to DHA and EPA in the body is very abundant, so that nutrition of the fish is further improved and the effect of the fish is canceled.
For example, 80 to 120 parts by weight of ethanol and 0.2 to 10.0 parts by weight of saponin extracted from red ginseng are mixed with 100 parts by weight of vegetable oil to prepare an oil phase. 10 to 20 parts by weight of sugar is added to 100 parts by weight of purified water 10 to 20 parts by weight of D-sorbitol, 10 to 20 parts by weight of starch syrup and 0.5 to 10 parts by weight of soy sauce are mixed to prepare an aqueous phase. The aqueous phase and the aqueous phase are mixed at a weight ratio of 100: 30 to 70, Followed by homogenization and drying for 3 to 10 minutes.
When the vegetable oil dissolved in ethanol as described above is emulsified in the form of o / w in the form of water in the form of o / w, the oily ethanol and purified water of the aqueous phase are removed and saponin is coated on the surface of the vegetable oil particles, And the vegetable oil and saponin components are protected from oxygen, sunlight, heat and the like by the coating film of saccharides, so that oxidation and decomposition mechanisms can be blocked.
The microcapsules can be used as the seasoning liquid for oral use of the present invention while being converted into an o / w type emulsion which is easy to handle because of its powdery state and is excellent in dispersibility when mixed with purified water, and can be used in the production of microcapsules such as sugar, D-sorbitol, When the content of the soy sauce is insufficient, it is possible to add a component insufficient to purified water for mixing the microcapsules to control the mixing ratio of the components.
In order to prevent this, it is preferable to add vinegar to the seasoning solution or 1 to 5 parts by weight of vinegar based on 100 parts by weight of purified water. It reduces the breakage of fish meat during cooking and reduces the fishy smell and also prevents the reaction between the protein of fish meat and the metal component of cooker to prevent the fish from being caught on the cooking device Can be obtained.
However, the protein is not easily digested by carbohydrate or fat, and the digestion and absorption rate of the elderly person is low.
Accordingly, the seasoning liquid may further contain a culture medium for lactic acid bacteria that helps digest protein, and 0.1 to 1.0 part by weight of the culture medium of lactic acid bacteria based on 100 parts by weight of purified water is preferably added.
The lactic acid bacteria culture solution can be prepared by fermenting saccharides with lactic acid bacteria and culturing the lactic acid bacteria for more than 60 days using saccharides such as sugar as a nutrient source. The metabolites produced by the cultivation of lactic acid bacteria exert a beneficial effect on the human body, It serves as a seasoning to improve the taste of Dorumuk and to prevent the food poisoning by sterilizing harmful bacteria.
In addition, most lactic acid bacteria contain proteolytic enzymes that degrade proteins into oligopeptides and then decompose into smaller peptides that cooperate to form di- or tri-peptides, or amino acids .
Therefore, the protein contained in the mushroom is easily decomposed into peptides or amino acids easily absorbed into the human body by the culture solution of the lactic acid bacteria contained in the mushroom while being digested in the body. Therefore, in the case of using the seasoning liquid of the present invention, There is an effect to be improved.
Hereinafter, the present invention will be described in more detail with reference to the following examples, comparative examples and test examples.
It is to be understood, however, that the invention is not to be construed as being limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete, and will fully convey the scope of the invention to those skilled in the art. Will be apparent to those skilled in the art to which the present invention pertains.
≪ Example 1 >
Alkaline ionized water having a pH of 10 was prepared by using an alkaline ionizer (Alkaline Water Ionizer LYdia 8080, MAGICCOS Co., Ltd., Korea), 12 liters of the alkaline ionized water, 12 liters of 97% (v / v) ethanol and 1 kg of 6- Were mixed and extracted at 60 ℃ for 25 hours to prepare red ginseng extract.
The red ginseng extract was stored in a refrigerator operated at -1 ° C for 2 days, and the sediment deposited on the floor was removed to obtain red ginseng supernatant.
1.5 kg of sugar, 1.5 kg of D-sorbitol, 1.5 kg of starch syrup, and 100 g of soy sauce were mixed with 10 kg of purified water, and 200 g of the red ginseng supernatant was added thereto.
≪ Example 2 >
The red ginseng supernatant obtained in Example 1 was concentrated at 60 ° C for 90 minutes using a concentrator (10 L Rotary Evaporator, R1010, Zhengzhou Great Wall Scientific Industrial and Trade Co., Ltd., China), and the sum of Rg1, Rb1 and Rg3 30 mg / g of red ginseng concentrate was obtained.
1 kg of sugar, 1 kg of D-sorbitol, 1 kg of starch syrup, and 100 g of soy sauce were mixed with 10 kg of purified water, and 20 g of the above red ginseng concentrate was added thereto to prepare a seasoning for Dorukku.
≪ Example 3 >
In Example 2, red ginseng supernatant was concentrated with a concentrator at 60 DEG C for 120 minutes to obtain a red ginseng concentrate having a total of Rg1, Rb1 and Rg3 contents of 40 mg / g.
To 10 ㎏ of purified water, 2 ㎏ of sugar, 2 ㎏ of D-sorbitol, 2 ㎏ of starch syrup and 100 g of soy sauce were mixed and 20 g of the red ginseng concentrate (40 mg / g) was added thereto.
<Example 4>
In Example 2, red ginseng supernatant was concentrated with a concentrator at 60 DEG C for 150 minutes to obtain a red ginseng concentrate having a total of Rg1, Rb1 and Rg3 contents of 50 mg / g.
3 kg of sugar, 3 kg of D-sorbitol, 3 kg of starch syrup and 100 g of soy sauce were mixed with 10 kg of purified water, and 20 g of the above red ginseng concentrate (50 mg / g) was added thereto to prepare a seasoning for Dorukku.
≪ Example 5 >
Four kilograms of perilla oil was mixed with 4 liters of 97% (v / v) ethanol and 200 g of the red ginseng supernatant obtained in Example 1 to prepare an oil phase. To 10 kg of purified water was added 1.5 kg of sugar, 1.5 kg of D-sorbitol, And 100 g of soy sauce were mixed to prepare an aqueous phase.
The oil phase was slowly added to the aqueous phase and emulsified at 3500 rpm for 7 minutes using a homogenizer (TK Homomixer Mark II Medel 2.5, PRIMIX, Japan) to prepare an o / w emulsion. The emulsion was again homogenized at 1000 bar with a high-pressure homogenizer (M-110F, Microfluidics, USA).
The homogenized emulsion was cooled to -25 ° C using a freeze drier (Freeze Dryer-FD8508, Ilshin BioBase Co., Ltd., Korea) and lyophilized for 24 hours to obtain microcapsules in which saponin components of red ginseng and saccharides were sequentially coated on the surface of perilla To prepare a seasoning powder.
≪ Example 6 >
In the same manner as in Example 1 except that 300 g of vinegar was further added to the purified water in Example 1, a seasoning solution for sake brewing was prepared.
≪ Example 7 >
80% by weight of the ground apple and 20% by weight of sugar were mixed, lactic acid bacteria were inoculated thereto, and then cultured at room temperature for 100 days to obtain a culture solution of lactic acid bacteria.
In Example 1, a seaweed seasoning solution was prepared in the same manner as in Example 1, except that 50 g of the culture liquid of lactic acid bacteria was further mixed with purified water.
≪ Comparative Example 1 &
In Example 1, 1.5 kg of sugar, 1.5 kg of D-sorbitol, 1.5 kg of starch syrup, and 100 g of soy sauce were mixed with 10 kg of purified water without adding the red ginseng supernatant to prepare a seasoning for syrup.
≪ Comparative Example 2 &
In Example 1, a seaweed seasoning solution was prepared in the same manner as in Example 1, except that red ginseng extract without a precipitate was used instead of red ginseng supernatant.
≪ Comparative Example 3 &
In Example 1, a corn steep liquor was prepared in the same manner as in Example 1, except that red ginseng powder obtained by pulverizing red ginseng instead of red ginseng supernatant was used.
≪ Test Example 1 >
The seasoning solutions of Examples 1 to 7 and Comparative Examples 1 to 3 were kept in contact with air at room temperature, and the change with time of occurrence of discoloration and removal was visually observed, and the results are shown in Table 1 below.
Table 1 shows that the storage stability was the best when the seasoning solution was dried and the microcapsule-form powder of Example 5 was stored for 12 weeks without any changes in properties. Comparative Example 1 in which the red ginseng ingredient was not added was stored After 1 week, discoloration and swelling occurred and storage stability was the worst.
In other words, the moisture of the seasoning liquid is removed and the other ingredients are coated by using the saccharides in the ingredient, so that the coating layer of the saccharide protects the seasoning liquid from external factors such as oxygen, sunlight and heat to improve storage stability, The antimicrobial effect increases the storage stability of the seasoning solution.
Compared with Comparative Example 3 using red ginseng powder, it was found that the red ginseng was extracted with alkaline ionized water and ethanol, rather than using all of red ginseng, In Example 1 using the supernatant of the red ginseng extract, discoloration and removal occurred at a similar time as compared with Comparative Example 2. From the result that the discoloration and dehydration slowly proceeded, the starch and free sugars contained in the precipitate in the extract of red ginseng It can be seen that the perishable material lowers the storage stability of the corn steep liquor.
In addition, it was found that the discoloration and swelling of Examples 2 to 4, in which the red ginseng supernatant was concentrated compared to Example 1, occurred late, and that the use of the red ginseng supernatant by concentrating the red ginseng supernatant was advantageous for improving the shelf life. / g was more favorable to the storage stability as the degree of coloration and detachment was increased later than that of Example 2 and Example 3 which were concentrated at 30 mg / g and 40 mg / g.
Therefore, it is more advantageous to improve the storage stability of the seasoning liquid by adding red ginseng components to the seasoning ingredients when preparing the seasoning liquid for the syrup, and to use the red ginseng extract with alkaline ionized water and ethanol rather than using the whole ingredients of the red ginseng It is more advantageous to use a supernatant obtained by removing the precipitate from the extracted red ginseng extract. It is more preferable to concentrate the supernatant, and it is more preferable to use the supernatant liquid in the form of microcapsule powder coated with saccharide It is judged to be most preferable.
Test Example 2 Measurement of volatile basic nitrogen (VBN) change
The freshness maintenance effect of seasoning liquid was investigated by measuring the content of volatile basic nitrogen as an index of quality of fresh fish. The measurement was carried out by the microdiffusion method using conway unit.
The seasoning liquids of the examples and comparative examples were mixed in a fresh mortar (freshly prepared mortar was dispersed in 10 kg of purified water in the case of Example 5, and used as a liquid phase), and stored at room temperature for 3 days 10 ml of distilled water and 20 ml of 10% trichloroacetic acid were added to 10 g of the collected samples, and a small amount of seawater was added thereto, followed by washing with water. Then, 5 ml of trichloroacetic acid was added thereto, To prepare a sample solution.
1 ml of the sample solution is placed in the outer chamber of the Conway unit, 1 ml of boric acid (H 3 BO 3 ) is added to the inner chamber, 1 ml of saturated potassium carbonate (K 2 CO 3 ) is rapidly injected into the outer chamber, The mixture was stirred at 37 ° C for 1 hour and titrated with 0.02 N sulfuric acid (H 2 SO 4 ) solution to measure volatile basic nitrogen.
Volatile basic nitrogen (mg%) = 0.28 x (V1-V2) x F x D x 100 / S
V1: Proper consumption (ml) of 0.02 N sulfuric acid solution in blank test
V2: Proper consumption (ml) of 0.02 N sulfuric acid solution of this test,
F: Potency of 0.02 N sulfuric acid solution
D: Dilution factor (50 ml)
S: Weight of sample (g)
0.28: Volatile basic nitrogen (mg) reacted with 1 ml of 0.02 N sulfuric acid solution
In general, the content of volatile basic nitrogen in fresh fish is 5 ~ 10 ㎎%, 15 ~ 25 ㎎% in fresh fish, 30 ~ 40 ㎎% in early coral fish and 50 ㎎% have.
As shown in the above Table 2, the volatile basic nitrogen content tended to increase as the storage period was increased, and the red ginseng of the Example containing the red ginseng supernatant component except for Example 7 contained no red ginseng component or red ginseng The volatile basic nitrogen content was measured as the amount of volatile basic nitrogen decreased with the passage of time as compared with the comparative example including the perishable material.
In the case of Example 5, the content of volatile basic nitrogen was measured to be higher than that of the other examples until the third day, but it was gradually measured from the 9th day. This is because, in the early stage of storage of the seasoned saururus, the red ginseng saponin component and the perilla oil component It is believed that this effect is due to the fact that the coating film is completely dissolved in the purified water after the coating of the saccharide does not fully exhibit its efficacy.
In the case of Example 7, it is presumed that the content of volatile basic nitrogen increased slightly as the culture solution of the lactic acid bacteria contained in the seasoning solution promoted proteolysis of the fish meat.
From the above results, it was found that the seasoning solution prepared by the method of the present invention had the effect of improving the storage stability of saururus when extracting red ginseng with alkaline ionized water and ethanol and using only the supernatant by removing the precipitate containing the perishable material It can be seen that it is better.
≪ Test Example 3 >
In the above Test Example 2, the dumplings prepared with the seasoning solution were kept in the refrigerator for 3 days and then baked and prepared for grilling. The dumplings were prepared for 70 persons, And the overall preference degree were measured by the 5-point scale method, and the average values thereof are shown in Table 3 below.
As shown in Table 3, the color did not show a significant difference in each group, but the taste and flavor of the Example were better than the Comparative Example.
Particularly, Examples 5 and 6 were highly evaluated. In Example 5, perilla oil and other seasoning ingredients stored in capsules were protected by the coating film and were not lost during storage and cooking, so that the taste and flavor could be felt during eating. In the case of Example 6, it was pointed out that the vinegar made the fish flesh solid and the fish flesh reduced.
In the overall preference, the examples were evaluated to be better than the comparative examples, and the commerciality of the seasoning liquid prepared by the method of the present invention was confirmed.
Claims (6)
10 to 20 parts by weight of sugar, 10 to 20 parts by weight of D-sorbitol, 10 to 20 parts by weight of starch syrup and 0.5 to 10 parts by weight of soy sauce are mixed with 100 parts by weight of purified water to prepare an aqueous phase;
Mixing the water phase and the oil phase at a weight ratio of 100: 30 to 70 and homogenizing the mixture at 3000 to 4000 rpm for 3 to 10 minutes; And
And drying the homogenized mixture.
The saponin,
1000 to 1500 parts by weight of alkaline ionized water having a pH of 9 to 11 and 1000 to 1500 parts by weight of 95 to 99% (v / v) ethanol are added to 100 parts by weight of red ginseng and extracted at 50 to 70 ° C for 20 to 30 hours to prepare a red ginseng extract ;
Separating the red ginseng extract into a supernatant and a precipitate by standing at -5 to 5 ° C for 30 to 70 hours; And
And removing the separated supernatant liquid.
Wherein the saponin is a concentrate obtained by concentrating the supernatant at 50 to 70 DEG C for 1 to 2 hours so that the sum of the Rg1, Rb1 and Rg3 contents is 20 to 60 mg / g.
Wherein 1 to 5 parts by weight of vinegar is added to 100 parts by weight of the purified water.
Wherein 0.1 to 1.0 part by weight of a culture medium of lactic acid bacteria is added to 100 parts by weight of the purified water.
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KR101505881B1 (en) * | 2014-11-25 | 2015-03-25 | 김선석 | Saponin Extract from Red Ginseng, and Method for Manufacturing the Same |
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