KR101059000B1 - Feed for swine containing extract from galic and coriandrum sativum,method for manufacturing the same, swine feeding the same,and pork produced by the swine - Google Patents

Abstract

PURPOSE: A producing method of pig feed containing a garclic extract and a coriandrum sativum extract is provided to transform carbon dioxide into supercritical fluid to extract garlic and coriandrum sativum. CONSTITUTION: A producing method of pig feed comprises the following steps: crushing garlic and coriandrum sativum into the size smaller than 3mm, and inserting the crushed garlic and coriandrum sativum into a supercritical fluid extraction apparatus; transforming carbon dioxide into supercritical fluid at 30~50deg C with the pressure of 150~300atm; generating bubbles inside the supercritical fluid using an ultrasonic wave oscillator; extracting the garlic and coriandrum sativum using the supercritical fluid; separating the garlic and coriandrum sativum extracts by decompressing the carbon dioxide; and collecting the separated carbon dioxide from the extracts.

Description

FEED FOR SWINE CONTAINING EXTRACT FROM GALIC AND CORIANDRUM SATIVUM, METHOD FOR MANUFACTURING THE SAME, SWINE FEEDING THE SAME , AND PORK PRODUCED BY THE SWINE}

The present invention, a supercritical fluid with a carbon dioxide pressure of 150 to 300 atm, temperature of 30 ℃ to 50 ℃ method for producing a feed for pigs comprising extracts extracted garlic and hoyu room, pig feed and thus prepared pigs It relates to pigs and pork which are swine for feed.

In general, the feed for pigs refers to a feed formulated with a balanced mix of nutrients for the purpose of breeding pigs by combining various sweet feeds and feed additives, and it contains nutrients that are well-preserved and easy to use. to be.

When preparing a blended feed, several short feeds are combined, taking into account many factors such as permanent value, color, price, preference, and particle size. This makes it possible to economically make products suitable for the purpose of use.

On the other hand, in recent years, due to foot-and-mouth disease, the supply of pigs has dropped sharply due to the mass killing of pigs, resulting in a shortage of pigs. Therefore, much attention has been focused on the pig swine method which can increase the immunity which can stably raise a pig from foot-and-mouth disease, etc.

As one of such hog methods, conventionally, antibiotics were administered to pig feed to improve disease productivity as well as to prevent disease and promote growth. In regulating its use, the importance of developing alternatives for antibiotics is emphasized. As one of such alternatives, the present invention is characterized by the use of extracts of garlic and hoyusil.

Supercritical solvents are solvents that, unlike liquid solvents in general, seem to behave like gases but are in a different state from the liquid state.

The phase equilibrium of pure components shows the range of temperatures and pressures at which a substance can remain in a single phase (solid, liquid and gas). Such single phase regions are distinguished by line segments that represent regions in which two phases (solid-gas, solid-liquid, liquid-gas respectively sublimate, melt and evaporate equilibrium) can coexist. These three segments intersect at the so-called triple point.

Coexistence curves representing equilibrium between two phases at different internal symmetries (eg, solid-liquid or solid-gas) tend to be infinity, or they can coexist. However, vapor pressure segments representing liquid-gas equilibrium abruptly disappear at the so-called critical point. In this case, the critical point is defined as one point in the phase balance diagram designated by the critical temperature Tc and the critical pressure Pc.

Triple point (TP) refers to the point where the solid, liquid, and gaseous phases coexist in equilibrium. However, liquefaction does not occur even when the pressure is increased (the pressure at this time is the critical pressure Pc). ② The gas is not formed even when the temperature is raised (the critical temperature at this time is the critical temperature Tc). It is called a critical point (CP).

Therefore, a supercritical fluid refers to a fluid in which a gas is heated above a critical temperature and simultaneously compressed above a critical pressure.

The basic operation of supercritical solvent extraction consists of extraction stage and separation.

In the extractor, the raw material and the supercritical solvent come into contact with each other so that the solute as an active ingredient in the extract is dissolved into the supercritical solvent due to the difference in solubility. Supercritical solvents containing solutes are separated from the solutes in the separator by temperature, pressure or other operating parameters. In some cases, the separation step may be multiplexed for complete separation of the supercritical solvent and the solute. The separated supercritical solvent is recycled to the extraction stage after the pressure and temperature are readjusted.

In the extraction step, it is possible to selectively extract specific components in the extract by changing the dissolving power of the supercritical solvent by adjusting the operating conditions of temperature and pressure. Likewise, in the separation step, it is possible to separate the components of the extract by changing the operating conditions.

The present invention provides a method of preparing a feed for pigs including garlic and a lake oil extract extracted using garlic and a horse oil chamber using carbon dioxide as a supercritical fluid, and to provide a feed for pigs, such as pigs and pork meat.

Pig feed manufacturing method according to the present invention, the step of grinding the size of the garlic and arc oil chamber particles less than 3mm; Injecting the crushed garlic and arc oil particles into a supercritical fluid extraction device;

Converting carbon dioxide into a supercritical fluid at a pressure of 150 to 300 atm and a temperature of 30 to 50 ° C. in the supercritical fluid extraction device; Liquid-bubbling the supercritical fluid carbon dioxide with an ultrasonic oscillator; Extracting the extracts of garlic and lake oil crushed with the liquid bubbled carbon dioxide; Separating the extract through decompression of the carbon dioxide; Recovering and circulating the carbon dioxide separated from the garlic and lake oil extract; The garlic and horse oil extract 3-5 parts by weight, corn 20-40 parts by weight, soybean 10 parts by weight, wheat 12-17 parts by weight, chaff 3 parts by weight, gluten wheat 3.5-5.5 parts by weight, starch 2 parts by weight, resin It includes 5-8 parts by weight, calcium phosphate 0.2 parts by weight, 13-15 parts by weight of one or more selected nutrients consisting of calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, vitamins as nutrients It relates to a pig feed manufacturing method characterized by.

In the step of separating and recovering carbon dioxide from the garlic and lake oil extract,

It relates to a pig feed method comprising a garlic and horse oil extract, characterized in that it further comprises means for adjusting the pressure and temperature.

The supercritical fluid carbon dioxide is a pig feed production method comprising garlic and hoyusil extract, characterized in that the 150 to 170atm and the temperature is 30 ℃ to 35 ℃.

Another object of the present invention, garlic and arc oil chamber extract of the garlic and arc oil chamber with a particle size of 3mm or less, the pressure is 150 to 300atm, temperature is extracted by supercritical fluidization of carbon dioxide at 30 ℃ to 50 ℃ 20 parts by weight of corn, 10 parts by weight of soybeans, 12-17 parts by weight of wheat, 3 parts by weight of chaff, 3.5-5.5 parts by weight of gluten wheat, 2 parts by weight of starch, 5-8 parts by weight of resin, 0.2 weight of calcium phosphate Part, nutrients 13-15 parts by weight of at least one selected from the group consisting of calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, vitamins; relates to a pig feed comprising a.

Another object of the present invention, garlic and arc oil chamber extract of the garlic and arc oil chamber with a particle size of 3mm or less, the pressure is 150 to 300atm, temperature is extracted by supercritical fluidization of carbon dioxide at 30 ℃ to 50 ℃ 20 parts by weight of corn, 10 parts by weight of soybeans, 12-17 parts by weight of wheat, 3 parts by weight of chaff, 3.5-5.5 parts by weight of gluten wheat, 2 parts by weight of starch, 5-8 parts by weight of resin, 0.2 weight of calcium phosphate To the pigs and pigs swine with pig feed comprising: 13-15 parts by weight of one or more selected nutrients consisting of calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, vitamins as a nutrient. It is about.

The present invention is an antibiotic replacement material conventionally used in pig feed, the production of pig feed comprising garlic and horse oil extract extracted by supercritical fluidization of carbon dioxide at a pressure of 150 to 300 atm, temperature of 30 ℃ to 50 ℃ Methods and feeds, pigs and pigs sown. Pork and pork swine made from extracts of garlic and hossil by supercritical fluidization of carbon dioxide were found not only to have low cholesterol levels, but also to increase immunity and to be extremely high in water retention.

1 is a diagram illustrating a manufacturing process of a pig feed comprising garlic and horse oil extract according to an embodiment of the present invention.
FIG. 2 shows a specific immunity against bacteria after 6 months in comparison with a feed group consisting of pigs raised with a pig feed containing garlic and a horse oil extract, and a non-pay group fed with a general feed according to an embodiment of the present invention. graph.
Figure 3 is a graph comparing the immunity against the virus after six months, compared to the non-paying group of the feed group and pigs raised in a pig feed containing pigs containing garlic and horse oil extract in accordance with an embodiment of the present invention.

The present invention relates to a method of producing a pig feed, feed, pigs and pork meat pigs in such a feed, in particular, to increase the immunity of pigs by participating in the feed extract extracted garlic and hoyusil through a supercritical fluid extraction process, The present invention relates to a method of preparing a pig feed comprising an extract of garlic and hossil having lowering cholesterol levels and improving water retention capacity, and to a pig feed and pigs and pork that are fed with such feed.

Supercritical fluid extraction is a technology that takes advantage of the advantages of supercritical fluids and has a number of unique advantages because it is a complex technology in which the principles of distillation and extraction are applied together. Supercritical fluids can be set to any condition from high density to low density by manipulation of pressure or temperature, so they have excellent selectivity for fractionation, separation, etc., resulting in high purity products and almost complete recovery without loss of extraction solvent. It is possible to obtain a purified product with no residual solvent.

In addition, the viscosity of the supercritical fluid is small, so the penetration into the sample is good, the extraction efficiency is high, and the diffusion coefficient is large, so the extraction speed is fast, and the damage by heat can be avoided by extracting at a relatively low temperature. Since the density difference with the fluid is large and the viscosity of the supercritical fluid is low, it has many advantages, such as an easy separation of the extraction residue and the solvent. However, since the use of a high pressure device has a disadvantage of high facility cost and maintenance cost, extraction using a supercritical fluid is known to be economical only when it is made with high efficiency.

On the other hand, garlic is known as a beneficial food for health maintenance because it contains a useful ingredient that regulates biological functions as well as a spice. The functionality of garlic is allicin (diallylthiosulfinate), methyl aryl (methy allyl), 1-propenyl allyl, aryl 1-propenyl, 1-propenyl methyl (1- Thiosulfinate compounds such as propenyl methyl) and dimethyl thiosulfinate play the greatest role and have antithrombotic action, anticancer action, lowering blood pressure, lowering cholesterol and preventing aging. Allicin ([C3H5-S (O) -C3H5]), a major component of the thiosulfinate compound, has many biochemical activities such as antibacterial action and inhibition of cell metabolism of garlic. Therefore, many efforts have been made to exploit the functionality of this garlic.

One embodiment of the present invention comprises the steps of injecting the garlic and arc oil particles pulverized to less than 3mm in the extraction reactor of the supercritical fluid extraction device to the supercritical fluid extraction device; Converting carbon dioxide into a supercritical fluid at a pressure of 150 to 300 atm and a temperature of 30 to 50 ° C. in the supercritical fluid extraction device; Liquid-bubbling the supercritical fluid carbon dioxide with an ultrasonic oscillator; Extracting the extracts of garlic and lake oil crushed with the liquid bubbled carbon dioxide; Separating the extract through decompression of the carbon dioxide; Recovering and circulating the carbon dioxide separated from the garlic and lake oil extract; The garlic and horse oil extract 3-5 parts by weight, corn 20-40 parts by weight, soybean 10 parts by weight, wheat 12-17 parts by weight, chaff 3 parts by weight, gluten wheat 3.5-5.5 parts by weight, starch 2 parts by weight, resin Pigs comprising 5-8 parts by weight, calcium phosphate 0.2 parts by weight, nutrients calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, 13-15 parts by weight of one or more selected nutrients consisting of vitamins; It is to provide a method for preparing a feed for.

Maintaining the pressure inside the extraction reactor of the supercritical extraction device at 150 to 170 atm and temperature at 30 to 35 ° C. for 60 minutes is most preferred for extraction of garlic and arc oil chambers, and the carbon dioxide is separated into liquid by using an ultrasonic oscillator. By bubbling, carbon dioxide can be maximized by increasing the contact area between garlic and the effective chamber.

In the step of recovering and circulating the carbon dioxide from the garlic and lake oil extract, the means may further comprise a means for adjusting the pressure and temperature. By adjusting the pressure and temperature, carbon dioxide can be supplied into the extraction reactor at a constant temperature and pressure.

In the present invention, carbon dioxide (CO2) is used as the supercritical fluid as the extraction solvent. It is a solvent mainly used in supercritical fluid extraction. It is vaporized under atmospheric pressure after extraction and released into the atmosphere. Therefore, it is non-toxic and non-hazardous because there is no remaining solvent, so it can be used to make the product without contamination in the food and pharmaceutical manufacturing industries. Liquid extraction leaves residual toxic organic solvents after distillation or vacuum separation steps. Compared with the density and solvent capacity of the supercritical fluid, the density and solvent capacity of the supercritical fluid have higher transfer efficiency such as lower viscosity and higher diffusion force. Therefore, even though the various components as oligomers have a similar volatility, the extract has various advantages that can be separated into each component. In the present invention, a supercritical fluid extraction apparatus using carbon dioxide as an extraction solvent is used.

On the other hand, garlic has a large amount of aryl sulfides and derivatives thereof, which has effects on its own taste, smell, and preservation, and contains various ingredients such as sugars and essential amino acids. As effective ingredients have been proved in various ways, they are widely applied as special ingredients such as industrial products, cosmetics, and medicines.

In the active ingredient of garlic, allin (S-allyl L-cysteine Sulfoxide), a type of sulfur-containing amino acid, is decomposed into allicin and pyruvic acid by its own enzyme allinase, and allicin is decomposed into diallyl sulfide to obtain lower sulfide.

In addition, the lower sulfide, an active ingredient of garlic, plays a role in delaying or suppressing rancidity of fats and oils by sulphating the fats and oils in foods. It has the effect of sterilization and the like and its value is increasing today.

In addition, Hoyu-sil is also called coriander, which is used as a medicine called 'Ho-yu-sil' in Chinese medicine, which makes the stomach strong, digestive, stops coughing, eliminates bad breath, and heals wounds. In addition, it cures anemia, benefits the large and small intestine, allows the stomach to pass through the stomach, eliminates the heat of the extremities, and treats headaches. In addition, Hoyusil's seeds are effective in worm poisoning, hemorrhoids, meat poisoning, hemorrhage, bleeding, boiling juice, squeezing oil, and applying them to children's soles. In addition, it is recorded that the effect of diarrhea, diarrhea and headache, toothache, pain, digestion, bile secretion, antifungal action, indigestion, anorexia treatment.

Accordingly, the present invention minimizes the deformation or destruction of the active ingredient by using a supercritical fluid extraction device, garlic and lake oil having a component having many effects as described above to efficiently extract and mix the raw material of pig feed This is a result of research to provide a pig feed, a method of preparing the pig and pigs fed with the extract of garlic and hoyusil.

The following describes the high-efficiency extraction method of garlic and lake oil chamber using the supercritical fluid extraction technology according to the present invention in order. In the present invention, a supercritical fluid extraction device used ISFX SFX3560. First, the garlic and arc oil chamber crushed to 3mm or less in the extraction reactor of the supercritical fluid extraction device are introduced, and the carbon dioxide (CO2) pressurized to the nozzle (valve) is supplied from the lower layer through a pump through a heat exchanger. The pressure in the reactor is controlled by a back pressure regulator to maintain a constant temperature through the heater surrounding the reactor.

And, the extraction solvent CO2 is extracted in the up-flow (up-flow) method in contact with the garlic and the arc oil chamber from the lower layer, wherein the temperature and pressure inside the extraction reactor is a pressure range of 150 to 300 atm, which is a critical range condition of CO2, The temperature is extracted for 60 minutes at 30 ℃ to 50 ℃. At this time, the pressure is 150 to 170 atm, the temperature is 30 ℃ to 35 ℃ can extract the most extract. In order to increase the extraction efficiency, if the supercritical fluid carbon dioxide is bubbled with liquid using an ultrasonic oscillator, the extraction efficiency can be further increased.

The extracted extract is depressurized while passing through the valve valve through the upper valve to separate the CO2 and the extract in the separator. The separated carbon dioxide is recovered and circulated.

Garlic and horse oil extract extracted from the above 3-5 parts by weight, corn 20-40 parts, soybeans 10 parts by weight, wheat 12-17 parts by weight, chaff 3 parts by weight, gluten wheat 3.5-5.5 parts by weight, starch 2 weight 5-15 parts by weight of resin, 0.2 parts by weight of calcium phosphate, 13-15 parts by weight of one or more selected nutrients consisting of calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, vitamins as a nutrient component; To prepare a feed containing pigs.

The pig feed prepared by the above method was configured as shown in Table 1 below so that the pigs were ingested for 6 months.

Kinds 1 month 3 months 6 months Compounding ratio (part by weight) Compounding ratio (part by weight) Compounding ratio (part by weight) Garlic and Horseshoe Extract 3-5 3-5 3-5 corn 20 30 40 bean 10 10 10 Wheat 12 15 17 chaff 3 3 3 Gluten wheat 5.5 4.5 3.5 Starch 2 2 2 Suzy 8 5 6 Calcium phosphate 0.2 0.2 0.2 Sodium chloride 8 7 6 Lysine 5 8 8

By comparing the two groups divided into a salary group intake of pig feed according to the present invention and a non-salary group (control) not ingested (control group) was able to confirm the effect of improving immunity, lowering cholesterol and improving water retention. Non-paid groups (control) used commercially available feed.

In order to confirm the effect of improving immunity, blood was separated from pigs of the feed group and the non-pay group (control group), and serum was separated. The immunological activity was measured by immunofluorescent antibody staining using lymphocytes (a type of lymphocyte in the white blood cells). 2 and 3 are shown as control graphs.

FIG. 2 shows a comparison between the pay group and the non-pay group after 6 months. As a result, the pay group is significantly improved in the specific immunity against bacteria (see FIG. 2), and FIG. As a result of comparing after 6 months, it can be seen that the pay group also improved immunity against the virus against the non-pay group (see Fig. 3).

The test method for analyzing cholesterol is shown in Table 2 by the international chemical analysis standard AAOAC) Official Method 994.10.

1 month 3 months 6 months Cholesterol (Payment Group) 173 147 137 Cholesterol (non-wage group) 173 175 183 Reduction rate 16% 25%

In addition, payoff and non-payment (control) were applied to Grau and Hamm's filter paper press method, filter paper (Whatman No. 2) was placed in the center of plexiglass plate, 300 mg of sample was placed on it, and then 1 plexiglass plate was placed. After superimposed on it and squeezed at a constant pressure for 2 minutes, the filter paper was taken out, and the area of the meat-eaten portions and the total area of the water-wet portions were measured using a planimeter (Type KP-21, Japan), and the results are shown in Table 2. .

Water retention rate (%) = [area (M) where meat tissue is buried / total area with less moisture (T)] X 100

1 month 3 months 6 months Conservative Force (Payment Group) 45% 48% 53% Non-payroll (control) 40% 40 41 Increase 11% 17% 23%

As shown in Table 2, it can be seen that the salary increases by about 23% after 6 months in the salary group according to the present invention.

As such, the present invention is not limited to the described embodiments, and it is apparent to those skilled in the art that various modifications and variations can be made without departing from the spirit and scope of the present invention. Therefore, such modifications or variations will have to be belong to the claims of the present invention.

Claims (6)

In the pig feed manufacturing method,
Pulverizing the size of the garlic and arc oil particles to 3 mm or less;
Injecting the crushed garlic and arc oil particles into a supercritical fluid extraction device;
Converting carbon dioxide into a supercritical fluid at a pressure of 150 to 300 atm and a temperature of 30 to 50 ° C. in the supercritical fluid extraction device;
Liquid-bubbling the supercritical fluid carbon dioxide with an ultrasonic oscillator;
Extracting the extracts of garlic and lake oil crushed with the liquid bubbled carbon dioxide;
Separating the extract through decompression of the carbon dioxide;
Recovering and circulating the carbon dioxide separated from the garlic and lake oil extract;
The garlic and horse oil extract 3-5 parts by weight, corn 20-40 parts by weight, soybean 10 parts by weight, wheat 12-17 parts by weight, chaff 3 parts by weight, gluten wheat 3.5-5.5 parts by weight, starch 2 parts by weight, resin 5-8 parts by weight, calcium phosphate 0.2 parts by weight, 13-15 parts by weight of one or more selected nutrients consisting of calcium carbonate, sodium chloride, salt, lysine, methionine, choline chloride, vitamins as nutrients; Feed manufacturing method. The method of claim 1,
Separating and recovering and circulating supply of carbon dioxide from the garlic and lake oil extract, Pig feed production method comprising a pig and garlic extract, characterized in that it further comprises means for adjusting the pressure and temperature. The method of claim 1,
Carbon dioxide which is a supercritical fluid is a pig-to-pig feed comprising a garlic and horse oil extract, characterized in that the temperature is 150 to 170atm and the temperature is 30 ℃ to 35 ℃. delete delete delete

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