KR100840508B1 - A manufacturing method of bodycleaner using red ginseng maltol and a bodycleaner thereof - Google Patents
A manufacturing method of bodycleaner using red ginseng maltol and a bodycleaner thereof Download PDFInfo
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Abstract
Description
도 1은 본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져 제조방법 순서도1 is a flow chart of a body cleanser manufacturing method using the red ginseng maltol extract according to the present invention
본 발명은 홍삼말톨(Maltol)추출액을 원료로 하여 바디클린져를 제조하는 방법에 관한 것으로, 피부노화방지 및 아토피 등의 가려움증에 효과를 나타내는 바디클린져 제조방법 및 그 방법을 이용한 바디클린져에 관한 것이다. The present invention relates to a method of manufacturing a body cleanser using red ginseng maltol extract as a raw material, and a method of manufacturing a body cleanser which has an effect on itching, such as prevention of skin aging and atopy, and a body cleanser using the method.
시중에 판매되고 있는 통상의 바디클린져는 대부분 유지와 알카리금속 및 화학약품을 혼합하여 만들어진 것으로, 피부의 세정에 사용할 경우 수용액이 알카리성을 나타내어 피부의 피지 성분이 과다하게 제거되고 각질층을 연화시켜 피부의 건조 및 거칠어짐을 유발하는 문제가 있었다.Most of the common body cleansers on the market are made by mixing fats and oils with alkali metals and chemicals. When used to clean the skin, aqueous solutions show alkalinity, which removes excessive sebum in the skin and softens the stratum corneum. There was a problem causing drying and roughness.
따라서, 상기 단순한 세척력만을 강조한 제품을 개선하여 기능성을 표방하는 고가의 바디클린져 제품이 출시되고 있으며, 그 중 약초를 이용한 제품도 보이고 있으나, 홍삼의 유효성분중 노화방지에 탁월한 효과가 있는 말톨을 주원료로 하는 바디클린져는 알려진 것이 없다.Therefore, an expensive body cleanser product has been released to improve functionality by emphasizing only the simple washing power, and among them, a product using herbal medicine is shown, but the main ingredient is maltol, which has an excellent effect on preventing aging among the active ingredients of red ginseng. There is no known body cleanser.
홍삼은 의약품으로서는 물론이고, 기호성이 강조된 건강식품 등으로도 다양화되어 많은 분야에 쓰여지고 있고, 그 효능으로 항스트레스, 항당뇨, 항암, 항피로 등의 수많은 약리효능이 보고되고 있으나, 피부노화방지에 관한 연구는 미진한 실정이다.Red ginseng is not only used as a medicine but also diversified as a health food with emphasis on palatability, and has been used in many fields.As a result, numerous pharmacological effects such as anti-stress, anti-diabetic, anti-cancer and anti-fatigue have been reported. The research on is insufficient.
한편, 홍삼의 약리 성분중에 노화방지에 효과가 입증된 황산화 물질 즉 Phenolic acids에 속하는 caffeic acid, ferulic acid, vanillic acid와 말톨(Maltol), salicylic acid 등의 페놀성 황산화 물질은 종래의 홍삼 엑기스추출과정으로는 거의 산화하여 소멸되는 문제점이 있었는데, 이와 관련하여 본 출원인은, 한국 특허출원 제2006-0026719호에서 사포닌 및 노화억제에 효능이 뛰어난 말톨 성분의 증발을 막기 위하여 홍삼농축액의 제조시 물과 에탄올을 사용하는 방법을 개시하였었다.Meanwhile, among the pharmacological components of red ginseng, sulfated substances that have been proven to prevent aging, ie caffeic acid, ferulic acid, vanillic acid belonging to Phenolic acids, and phenolic sulfated substances such as maltol and salicylic acid are conventional red ginseng extracts. In the extraction process, there was a problem of almost oxidizing and disappearing. In this regard, the present applicant, in Korean Patent Application No. 2006-0026719, water in the preparation of red ginseng concentrate in order to prevent evaporation of saponin and maltol component which is effective in inhibiting aging. And a method of using ethanol.
본 발명은 종래의 바디클린져를 개선하고자 안출된 것으로, 홍삼을 잘게 부수어 분말로 만든 후, 물에 대한 에탄올의 비율이 55%~70%인 에탄올수용액과 홍삼분말을 가열탱크에 넣고, 75℃~85℃온도로 1시간이상 가열하며 홍삼말톨을 추출탱크로 추출 및 냉각시킨 추출액에, 라우린산(Lauric acid), 알란토인(Allantoin), 미리스틱산(Myristic acid), 동백유, 알로에(Aloe), 해초추출물(Marine Ext), 참깨오일(Sasame Oil) 등을 혼합하는 바디클린져 제조방법을 제공함으로써, 그에 함유된 말톨(Maltol)성분에 의한 피부노화방지는 물론 아토피증상의 완화 및 보습효과에 탁월한 효과가 있는 바디클린져를 제공하는 것을 목적으로 한다.The present invention was devised to improve the conventional body cleanser, crushed red ginseng into fine powder, put the ethanol aqueous solution and red ginseng powder with 55% to 70% of ethanol to water in a heating tank, 75 ℃ ~ Extracted and cooled red ginseng maltol into an extraction tank by heating at 85 ° C for at least 1 hour, lauric acid, allantoin, myristic acid, camellia oil, aloe, By providing a method of manufacturing a body cleanser that contains seaweed extract (Marine Ext), sesame oil (Sasame Oil), etc., it is excellent in preventing skin aging by the maltol component contained therein, as well as relieving and moisturizing effect of atopic symptoms. An object of the present invention is to provide a body cleanser.
본 발명은 홍삼말톨추출액을 원료로 하여 바디클린져를 제조하는 방법에 관한 것으로, 피부노화방지 및 아토피 등의 가려움증에 효과를 나타내는 바디클린져 제조방법 및 그 방법을 이용한 바디클린져에 관한 것이다. The present invention relates to a method of manufacturing a body cleanser using red ginseng maltol extract as a raw material, and a method of manufacturing a body cleanser which has an effect on the itch, such as prevention of skin aging and atopic dermatitis, and a body cleanser using the method.
본 발명은 홍삼을 잘게 부수어 분말로 만든 후, 물에 대한 에탄올의 비율이 55%~70%인 에탄올수용액과 홍삼분말을 가열탱크에 넣고, 75℃~85℃온도로 1시간이상 가열하며 홍삼말톨을 추출탱크로 추출 및 냉각시킨 추출액에, 보습과 각질 연화작용에 효과가 있는 라우린산(Lauric acid)과, 피부진정 및 가려움 완화효과가 있는 알란토인(Allantoin), 미리스틱산(Myristic acid), 아토피치료에 효과가 있는 동백유, 피부 수분공급 및 아토피치료 보조효과가 있는 알로에(Aloe)와, 피부 영양 공급 및 피부 재생의 효과가 있는 해초추출물(Marine Ext)과, 보습효과가 탁월한 참깨오일(Sasame Oil) 등을 혼합하여 만드는 바디클린져 제조방법 및 그 방법을 이용한 바디클린져에 관한 것이다.In the present invention, finely crushed red ginseng into a powder, and put the ethanol solution and red ginseng powder of 55% to 70% of ethanol to water in a heating tank, heated at 75 ℃ to 85 ℃ for more than 1 hour and red ginseng maltol The extract was extracted and cooled in the extraction tank, lauric acid, which is effective for moisturizing and softening of keratin, allantoin, myristic acid, and atopy, which have skin soothing and itching effects. Camellia oil for treatment, Aloe for supplementing skin hydration and atopy treatment, Marine Ext for nourishing and regenerating skin, and Sesame oil for excellent moisturizing effect It relates to a body cleanser manufacturing method made by mixing) and the body cleanser using the method.
본 발명에 의하면, 홍삼말톨추출액에 라우린산(Lauric acid), 알란토 인(Allantoin), 미리스틱산(Myristic acid), 동백유, 알로에(Aloe), 해초추출물(Marine Ext), 참깨오일(Sasame Oil) 등을 혼합함으로써, 그에 함유되는 말톨(Maltol)성분에 의한 피부노화방지는 물론 아토피증상의 완화 및 보습효과에 탁월한 효과가 있는 바디클린져 제조방법 및 그 방법을 이용한 바디클린져를 제공한다.According to the present invention, red ginseng maltol extract lauric acid (Lauric acid), allantoin (Allantoin), myristic acid (Myristic acid), camellia oil, Aloe (Aloe), seaweed extract (Marine Ext), sesame oil (Sasame) By mixing oil), the present invention provides a body cleanser manufacturing method and a body cleanser using the method, which have an excellent effect on the prevention of skin aging by the maltol component contained therein, as well as the relief and moisturizing effect of atopic symptoms.
이하, 첨부된 도면을 참조하여 본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져 제조방법 및 그 방법을 이용한 바디클린져의 바람직한 실시예를 상세하게 설명한다.Hereinafter, with reference to the accompanying drawings will be described in detail a preferred embodiment of the body cleanser manufacturing method and the body cleanser using the red ginseng maltol extract according to the present invention.
도 1은 본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져 제조방법 순서도이다. 도 1에 도시한 바와같이, 본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져 제조방법은, 용해탱크에서 증류수에 EDTA-2Na, 부틸히드록시톨루엔(B.H.T), 디소디움 코코암포디아세테이트(Disodium Cocoamphodiacetate), 코카미도프로필 베타인(Cocamidopropyl Betaine), KOH, 디메틸폴리실록산 혼합물(Dimethylpolysiloxane Mixture), 에틸렌글리콜 모노스테아레이트(Ethylene Glycol Monostearate), 라우라마이드 디메틸아인(Lauramide DEA)를 희석하는 단계(S100); 상기 희석액에 70℃~80℃온도에서 라우린산(Lauric acid)과, 알란토인(Allantoin), 미리스틱산(Myristic acid), 동백유, 알로에(Aloe)와, 해초추출물(Marine Ext)과, 참깨오일(Sasame Oil)을 혼합 믹싱하는 단계(S200); 상기 믹싱된 물질을 숙성후 홍삼말톨추출액(Maltol Ext)과 진공상태에서 50℃~60℃온도로 가열하며 배합하는 단계(S300); 상기 배합물에 향수(Perfume), 허브에센스오일(Herb Essential Oil)을 혼합하며 자연 냉각하는 단계(S400)를 포함하여 이루어지는 것을 특징으로 한다. 1 is a flow chart of a body cleanser manufacturing method using the red ginseng maltol extract according to the present invention. As shown in Figure 1, the body cleanser manufacturing method using the red ginseng maltol extract according to the present invention, EDTA-2Na, butylhydroxytoluene (BHT), disodium cocoamphodiacetate (Disodium Cocoamphodiacetate) in distilled water in a dissolution tank Diluting Cocamidopropyl Betaine, KOH, dimethylpolysiloxane mixture, dimethyl glycol monostearate, ethylene glycol monostearate, laramide dimethyl ain (Sur); Lauric acid, Allantoin, Myristic acid, Camellia oil, Aloe, Seaweed extract and Marine sesame oil at 70 ° C. to 80 ° C. (S200) mixing and mixing (Sasame Oil); Aging the mixed material and heating and mixing the red ginseng maltol extract (Maltol Ext) at 50 ° C. to 60 ° C. in a vacuum state (S300); Perfume, the herbal essence oil (Herb Essential Oil) is mixed with the blend, characterized in that it comprises a step of natural cooling (S400).
상기 참깨오일은 탱크에 참깨오일 원액을 물과 3:7의 비율로 투입하고 100℃온도까지 가열하면서 희석시킨 후 식히고 나서, 다시 가열한 후 식히는 과정을 반복함으로써 참깨오일에 포함된 향을 제거한 후 사용하는 것이 바람직하다.The sesame oil is added to the tank sesame oil in a ratio of 3: 7 to water and diluted with heating to 100 ℃ temperature, and then cooled, and then heated again to remove the flavor contained in sesame oil It is preferable to use.
한편, 상기 홍삼말톨추출액은, 홍삼을 잘게 부수어 분말로 만드는 단계(S100'); 상기 분말화된 홍삼과 물에 대한 에탄올의 비율이 55%~70%인 에탄올수용액을 가열탱크에 투입하는 단계(S200'); 상기 가열탱크를 75℃~85℃온도로 1시간 내지 2시간 가열하며 홍삼말톨을 추출탱크로 추출 및 냉각시키는 단계(S300'); 상기 홍삼말톨을 추출 및 냉각시키는 단계를 반복하는 단계(S400'); 상기 추출되는 말톨추출물을 여과후 농축하여 농축액을 얻는 단계(S500')를 거쳐 얻는 것을 특징으로 한다. On the other hand, the red ginseng maltol extract, step of crushing red ginseng fine powder (S100 '); Adding an ethanol aqueous solution having a ratio of 55% to 70% of ethanol to the powdered red ginseng and water to a heating tank (S200 '); Heating the heating tank at a temperature of 75 ° C. to 85 ° C. for 1 hour to 2 hours, extracting and cooling red ginseng maltol as an extraction tank (S300 ′); Repeating the step of extracting and cooling the red ginseng maltol (S400 ′); The maltol extract is concentrated after filtration to obtain a concentrate (S500 ').
한편, 상기 가열탱크에 투입되는 에탄올 수용액은 물에 대한 에탄올의 비율이 55%이하 또는 70%이상일 경우에는 말톨(Maltol)성분의 산화가 급격히 증가하기 때문에 물에 대한 에탄올의 비율은 55%에서 70%가 바람직하고, 상기 가열탱크를 75℃~85℃온도로 가열하는 단계는 경제성을 고려하여 1시간 내지 2시간 동안인 것을 특징으로 한다.On the other hand, the ethanol solution in the heating tank is ethanol to water is less than 55% or more than 70%, since the oxidation of the maltol (Maltol) component rapidly increases because the ratio of ethanol to water is 55% to 70 % Is preferable, and the step of heating the heating tank to a temperature of 75 ℃ ~ 85 ℃ is characterized in that for 1 to 2 hours in consideration of economics.
또한, 가열탱크에 투입된 에탄올수용액과 홍삼분말은 75℃이하 또는 85℃이상으로 가열할 경우 말톨(Maltol)성분의 산화가 급격히 증가하기 때문에 75℃~85℃온도로 가열하는 것이 바람직한 것으로 나타났다.In addition, the ethanol aqueous solution and red ginseng powder in the heating tank was heated to 75 ℃ ~ 85 ℃ temperature because the oxidation of the maltol (Maltol) component is rapidly increased when heated below 75 ℃ or 85 ℃.
또한, 상기 홍삼말톨을 추출 및 냉각시키는 단계의 반복은 홍삼말톨을 추출 하는 시간 및 비용 등을 고려하면 3회 정도가 바람직한데, 상기와 같은 조건으로 3회정도 반복하여 엑기스를 추출하면 홍삼에 있던 말톨성분의 90%이상이 상기 엑기스로 추출되는 것으로 나타난다.In addition, the repetition of the step of extracting and cooling the red ginseng maltol is preferably three times in consideration of the time and cost of extracting the red ginseng maltol, and the extract is repeated three times under the same conditions. More than 90% of the maltol component appears to be extracted with the extract.
이와 관련하여 본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져 제조방법의 구체적인 일실시예는 다음과 같다. In this regard, a specific embodiment of the body cleanser manufacturing method using the red ginseng maltol extract according to the present invention is as follows.
본 발명에 의한 홍삼말톨추출액을 이용한 바디클린져는 증류수 50.00%중량부에 EDTA-2Na 0.05%중량부, 부틸히드록시톨루엔(B.H.T) 0.02%중량부, 디소디움 코코암포디아세테이트(Disodium Cocoamphodiacetate) 10.00%중량부, 코카미도프로필 베타인(Cocamidopropyl Betaine) 10.00%중량부, 농도가 85%인 KOH 3.63%중량부, 디메틸폴리실록산 혼합물(Dimethylpolysiloxane Mixture) 0.10%중량부, 에틸렌글리콜 모노스테아레이트(Ethylene Glycol Monostearate) 1.30%중량부, 라우라마이드 디메틸아인(Lauramide DEA) 2.65%중량부를 희석한 후; 상기 희석액에 70℃~80℃온도에서 라우린산(Lauric acid) 10.00%중량부와, 알란토인(Allantoin) 0.05%중량부, 미리스틱산(Myristic acid) 3.00%중량부, 동백유 2.00%중량부, 알로에(Aloe) 0.50%중량부와, 해초추출물(Marine Ext) 0.60%중량부와, 참깨오일(Sasame Oil) 3.00%중량부를 혼합 믹싱하고; 상기 믹싱된 물질을 약 3시간동안 숙성후 2.50%중량부의 홍삼말톨추출액(Maltol Ext)과 진공상태에서 50℃~60℃온도로 약 30분간 가열하며 배합한 후; 상기 배합물에 향수(Perfume), 허브에센스오일(Herb Essential Oil)을 혼합하며 자연 냉각하여 제조한다.Body cleanser using red ginseng maltol extract according to the present invention is 0.05% by weight of EDTA-2Na, 0.02% by weight of butylhydroxytoluene (BHT), 10.00% of disodium coco amphodiacetate in 50.00% by weight of distilled water Parts by weight, 10.00% by weight of Cocamidopropyl Betaine, 3.63% by weight of KOH having a concentration of 85%, 0.10% by weight of dimethylpolysiloxane Mixture, ethylene glycol monostearate 1.30% by weight, 2.65% by weight of lauramide dimethylaine (Lauramide DEA) was diluted; 10.00% by weight of lauric acid, 0.05% by weight of allantoin, 3.00% by weight of myristic acid, 2.00% by weight of camellia oil, in the diluent at 70 ° C. to 80 ° C. 0.50% by weight of aloe, 0.60% by weight of seaweed extract (Marine Ext), and 3.00% by weight of sesame oil (Sasame Oil) are mixed and mixed; After mixing the mixed material for about 3 hours and 2.50% by weight of red ginseng maltol extract (Maltol Ext) in a vacuum at 50 ℃ ~ 60 ℃ temperature for 30 minutes to mix; Perfume, herbal essence oil (Herb Essential Oil) is mixed with the formulation and prepared by cooling.
한편, 상기 홍삼말톨추출액은, 홍삼 5kg을 잘게 부수어 분말로 만들고, 분말화된 홍삼과 물에 대한 에탄올의 비율이 60%인 에탄올수용액 50ℓ를 가열탱크에 넣어, 상기 가열탱크를 80℃온도로 1시간동안 가열하며 홍삼말톨을 추출탱크로 추출 및 냉각시키는 과정을 3회 반복한 후, 상기 추출액을 여과하여 75℃에서 감압(500~700mmHg) 농축하여 얻는다.On the other hand, the red ginseng maltol extract, finely crushed 5kg red ginseng into a powder, and put 50 liters of ethanol aqueous solution 60% of ethanol to the powdered red ginseng and water in a heating tank, the heating tank at 80 ℃ temperature 1 After heating three times, the process of extracting and cooling red ginseng maltol into an extraction tank was repeated three times, and the extract was filtered and concentrated under reduced pressure (500 to 700 mmHg) at 75 ° C.
결국, 본 발명은 새로운 방법으로 특히 홍삼에 존재하는 노화방지성분인 말톨의 산화를 특수공법으로 줄이며 추출한 추출액에, 보습과 각질 연화작용에 효과가 있는 라우린산(Lauric acid)과, 피부진정 및 가려움 완화효과가 있는 알란토인(Allantoin), 미리스틱산(Myristic acid), 아토피치료에 효과가 있는 동백유, 피부 수분공급 및 아토피치료 보조효과가 있는 알로에(Aloe)와, 피부 영양 공급 및 피부 재생의 효과가 있는 해초추출물(Marine Ext)과, 보습효과가 탁월한 참깨오일(Sasame Oil)을 혼합하여 만든 혼합물에, 향수(Perfume), 허브에센스오일(Herb Essential Oil)을 정제 희석하여 함유시킴으로써, 홍삼추출물과 피부에 이로운 성분들을 결합하여 노화방지, 보습 및 아토피관련 피부진정작용에 효능이 있는 바디클린져 제조방법 및 그 방법을 이용한 바디클린져에 관한 것이다.After all, the present invention is a new method, especially the oxidation of maltol, an anti-aging ingredient present in red ginseng, reduced to a special method to extract, lauric acid (Lauric acid) effective in moisturizing and keratin softening, skin soothing and itching Allantoin, Myristic acid, Camellia oil for atopic dermatitis, Aloe for supplementing skin hydration and atopy treatment, and skin nourishment and skin regeneration Red ginseng extract and skin by diluting and diluting Perfume and Herb Essential Oil into the mixture made by mixing seaweed extract (Marine Ext) and sesame oil (Sasame Oil) with excellent moisturizing effect. A method of manufacturing a body cleanser that is effective in anti-aging, moisturizing and atopic skin by combining beneficial ingredients and a body cleanser using the method A.
상기한 바와 같은 구성 및 작용은 하나의 실시예로서 본 발명의 청구범위를 제한하는 것은 아니며, 본 발명의 기술적 사상을 변경하지 아니하는 범위 내에서 다양한 변경과 수정이 가능함은 본 발명이 속하는 분야에 종사하는 자에게는 자명한 것이다.The configuration and operation as described above are not limited to the claims of the present invention as an embodiment, and various changes and modifications are possible within the scope of not changing the technical spirit of the present invention. It is obvious to those who are engaged.
상기와 같은 본 발명에 의하면, 홍삼말톨추출액에 동백유, 참깨오일, 허브에센스오일, 해초추출물 등을 혼합함으로써, 그에 함유된 말톨(Maltol)성분에 의한 피부노화방지는 물론 아토피증상의 완화 및 보습효과에 탁월한 효과가 있는 바디클린져를 제공한다.According to the present invention as described above, by mixing red ginseng maltol extract, camellia oil, sesame oil, herbal essence oil, seaweed extract, etc., to prevent skin aging by the maltol component contained therein as well as relieve and moisturize the atopic symptoms Provides a body cleanser with excellent effects.
또한, 홍삼에 함유된 노화억제에 뛰어난 효능이 있는 항산화물질중 노화억제의 효능이 가장 뛰어난 말톨(Maltol)성분의 산화를 줄이며 추출한 홍삼추출물을 이용하여 피부노화방지에 탁월한 효과가 있는 바디클린져를 제공할 수 있다.In addition, it provides a body cleanser that has an excellent effect in preventing skin aging by using red ginseng extract extracted by reducing the oxidation of maltol component, which is the most effective anti-aging agent among antioxidants, which has excellent efficacy in inhibiting aging contained in red ginseng. can do.
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KR101566474B1 (en) | 2012-07-12 | 2015-11-12 | 전북대학교산학협력단 | Foot shampoo composition comprising red ginseng |
KR20160024223A (en) * | 2014-08-25 | 2016-03-04 | 주식회사 코리아나화장품 | Paste Type Cosmetic Composition for Washing with Thermostability |
KR20170120224A (en) | 2016-04-20 | 2017-10-31 | 재단법인 진안홍삼연구소 | Manufacturing method of body scrub containing a red ginseng extract |
KR101935371B1 (en) * | 2018-05-17 | 2019-01-07 | 부산대학교 산학협력단 | Composition for preventing or treating atopic dermatitis comprising maltol, isosoyamaloside I or mixture thereof |
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KR20030066079A (en) * | 2002-02-04 | 2003-08-09 | 박상도 | Manufacturing method of Red Ginseng Soap |
KR20050025454A (en) * | 2003-09-08 | 2005-03-14 | 한불화장품주식회사 | Cosmetic compositions with adsorber stabilized with concentrated red ginseng extract |
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KR20030066079A (en) * | 2002-02-04 | 2003-08-09 | 박상도 | Manufacturing method of Red Ginseng Soap |
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Publication number | Priority date | Publication date | Assignee | Title |
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KR101566474B1 (en) | 2012-07-12 | 2015-11-12 | 전북대학교산학협력단 | Foot shampoo composition comprising red ginseng |
KR20160024223A (en) * | 2014-08-25 | 2016-03-04 | 주식회사 코리아나화장품 | Paste Type Cosmetic Composition for Washing with Thermostability |
KR101628252B1 (en) * | 2014-08-25 | 2016-06-08 | 주식회사 코리아나화장품 | Paste Type Cosmetic Composition for Washing with Thermostability |
KR20170120224A (en) | 2016-04-20 | 2017-10-31 | 재단법인 진안홍삼연구소 | Manufacturing method of body scrub containing a red ginseng extract |
KR101935371B1 (en) * | 2018-05-17 | 2019-01-07 | 부산대학교 산학협력단 | Composition for preventing or treating atopic dermatitis comprising maltol, isosoyamaloside I or mixture thereof |
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