KR100404927B1 - Process for purifying sulfur usable for Health care - Google Patents
Process for purifying sulfur usable for Health care Download PDFInfo
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- KR100404927B1 KR100404927B1 KR10-2000-0018316A KR20000018316A KR100404927B1 KR 100404927 B1 KR100404927 B1 KR 100404927B1 KR 20000018316 A KR20000018316 A KR 20000018316A KR 100404927 B1 KR100404927 B1 KR 100404927B1
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- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B57/00—Golfing accessories
- A63B57/10—Golf tees
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- A—HUMAN NECESSITIES
- A63—SPORTS; GAMES; AMUSEMENTS
- A63B—APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT
- A63B2102/00—Application of clubs, bats, rackets or the like to the sporting activity ; particular sports involving the use of balls and clubs, bats, rackets, or the like
- A63B2102/32—Golf
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- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
본 발명은 건강보조식품용 유황의 가공방법에 관한 것으로 유황(硫黃)을 동용기(銅容器)에 넣어 500∼700℃에서 20∼50분간 가열한 다음 상온으로 냉각시킨 후 다시 상기 고온으로 재가열 및 냉각을 5∼15회 반복 실시하여 회백색의 무독성 유황 응괴물을 얻고 이를 분밀도 200∼500메쉬로 분말화한 다음 여기에 탄산칼슘(CaCO3)을 중량비 1∼2배 첨가한 후 120∼180℃의 온도로 가열 용해하여 pH 12 이상이 되도록 액화(liquidfying)시킨 다음 초산(CH3COOH)을 첨가하여 pH 7.0 이하가 되도록 중화시키면 백색침전물(precipitate)이 형성되는데 이를 증류수로 30회 이상 세척한 후 건조시켜 얻는 특징이 있다.The present invention relates to a processing method of sulfur for health supplement foods, and put sulfur (硫 黃) in the same container (銅 容器), heated at 500 to 700 ° C. for 20 to 50 minutes, and then cooled to room temperature and then reheated to the high temperature again. 5-15 cycles of cooling to obtain an off-white, non-toxic sulfur coagulum, powdered to 200-500 mesh and then adding calcium carbonate (CaCO 3 ) 1 to 2 times by weight to 120 to 180. Liquefying to pH 12 or more by dissolving at a temperature of ℃ and neutralizing the solution to pH 7.0 or less by adding acetic acid (CH 3 COOH) to form a white precipitate (precipitate) washed more than 30 times with distilled water There is a characteristic obtained by drying after.
Description
본 발명은 건강보조식품용 유황의 가공방법에 관한 것이다. 더욱 상세하게는 황색 유황을 500∼700℃에서 가열 냉각을 반복하여 백색의 무독성 유황 응괴물을 얻고 여기에 탄산칼슘을 첨가하여 120∼180℃에서 가열하여 액화한 다음 초산을 첨가하여 중화처리 함으로써 얻어짐을 특징으로 하는 건강보조식품용 유황의 가공방법에 관한 것이다.The present invention relates to a processing method of sulfur for dietary supplements. More specifically, yellow sulfur is obtained by repeating heating and cooling at 500 to 700 ° C. to obtain a white non-toxic sulfur agglomerate, adding calcium carbonate to it and liquefying by heating at 120 to 180 ° C., followed by neutralization by adding acetic acid. The present invention relates to a processing method of sulfur for health supplements characterized by baggage.
유황(硫黃)은 원소기호 S로서 자연계에서는 4종류의 동위원소(isotope)가 발견되며 Sulfide나 Sulfate형태로 존재한다. 이와같은 유황은 수불용성(insoluble in water)이며 알코올, 에테르 등 유기용매 내에 극미량이 용해될 뿐이다.Sulfur is an element symbol S. In nature, four kinds of isotopes are found and exist in the form of sulfides or sulfates. Such sulfur is insoluble in water and only a very small amount is dissolved in an organic solvent such as alcohol or ether.
또한, 유황은 과용하면 눈, 코, 목구멍을 가렵게 하거나 심하면 눈이나 피부를 데게하는 독성(Toxic)을 나타낸다.Sulfur can also cause toxic effects on the eyes, nose and throat when overdose, or severely on the eyes or skin.
본 발명은 상기와 같은 유황의 특성을 감안하여 안출한 것으로 무독성의 회백색 분말상의 건강보조식품용 유황을 제공하는데 그 목적이 있다.The present invention has been made in view of the characteristics of the sulfur as described above is to provide a non-toxic gray-white powder for health supplement food sulfur.
본 발명의 다른 목적은 상기 유황의 신규한 제조방법을 제공하는데 있다.Another object of the present invention is to provide a novel method for producing the sulfur.
본 발명의 상기 목적은 유황(硫黃)을 동용기(銅容器)에 넣어 고온가열한 다음 냉각하는 과정을 다수회 반복하고 분말화한 후 pH12이하의 알칼리성 액체를 제조한 후 중화시킨 다음 세척하고 건조처리한 후 건강보조식품을 제조함으로써 달성하였다.The object of the present invention is to put sulfur (硫 黃) in a copper container (銅 容器) high temperature heating and then repeat the process of cooling many times and powdered and then prepared an alkaline liquid of pH 12 or less, neutralized and washed Achieved by preparing a dietary supplement after drying.
이하, 본 발명의 구체적인 구성 및 작용을 설명한다.Hereinafter, the specific configuration and operation of the present invention.
도 1은 황색의 원료 유황으로부터 무독성 백색 유황 건조 분말을 제조하기까지의 공정의 전체 흐름을 보인 도면이다.1 is a diagram showing the overall flow of a process from producing yellow non-toxic sulfur to dry white powder.
본 발명은 바람직한 실시예를 도 1에 도시한 바와 같으며 유황을 고온가열하는 단계와 상온냉각하는 단계를 수회 반복하는 공정과; 분말하여 탄산칼슘을 첨가하여 120∼180℃의 온도로 용해하는 단계와; 초산을 첨가하여 주오하시키는 단계와; 증류수로 세척하는 단계와; 건조시키는 단계로 구성된다.The present invention is a preferred embodiment as shown in Figure 1 and the step of repeating the step of heating the sulfur at high temperature and the room temperature cooling several times; Powder to add calcium carbonate to dissolve at a temperature of 120 to 180 캜; Adding acetic acid to shroud; Washing with distilled water; Drying step.
본 발명의 유황은 독성이 있으므로 고온가열 처리함으로써 독성을 제거한다. 고열처리시 유황을 동용기(銅容器)에 투입하면 가장 바람직하지만, 알루미늄 용기라도 무방하며 내열성 유리제 용기도 가능하다. 동용기에 투입한 유황은 500∼700℃에서 20∼50분간 바람직하게는 600℃에서 30분간 가열하는 것이 좋다. 가열 후 15℃가 될 때까지 냉각한 다음 가열과 냉각을 5∼15회 바람직하게는 9회 반복하는 것이 좋다. 이렇게 하면 유황 응괴물이 형성되는데 이를 분말도 200∼500 메쉬로 분쇄한다. 상기 분쇄물을 다른 용기에 넣은 다음 탄산칼슘(CaCO3)을 첨가하여 가열용해시킨다. 이때 사용하는 용기는 원적외선을 방사할 수 있는 어떠한 용기라도 좋으며 상기 유황 응괴물과 탄산칼슘의 혼합비율은 중량비로 1 : 1∼2 바람직하게는 1 : 1.5가 좋다. 이들 물질이 반응하기 바람직한 온도는 100∼200℃이며 150℃에서 30분이 가장 좋으며 pH는 12 이상의 강알칼리 용액이 생성된다.Sulfur of the present invention is toxic and thus removes the toxicity by high temperature heating treatment. It is most preferable to add sulfur to the copper container during the high heat treatment, but it may be an aluminum container and a heat resistant glass container is also possible. Sulfur added to the same container is preferably heated at 500 to 700 ° C for 20 to 50 minutes, preferably at 600 ° C for 30 minutes. After heating, the mixture is cooled to 15 ° C., and then heating and cooling are repeated 5 to 15 times, preferably 9 times. This forms a sulfur coagulum, which is also ground to a powder of 200 to 500 mesh. The pulverized product is placed in another container and then dissolved by heating by adding calcium carbonate (CaCO 3 ). At this time, the container to be used may be any container capable of emitting far infrared rays, and the mixing ratio of the sulfur agglomerate and calcium carbonate is 1: 1 by weight, preferably 1: 1.5 by weight. The preferred temperature for these materials to react is 100-200 ° C., 30 min at 150 ° C., and a pH of 12 or higher strong alkali solution.
생성된 용액에 초산(CH3COOH)을 첨가하여 pH 6.0 이하가 되도록 중화시키면 회백색 가루가 침전된다. 이때, 초산 대신 과일식초나 현미식초를 사용할 수 있다. 상기 중화반응 결과 형성된 회백색 침전물(precipitate)에 증류수를 가하여 30회 이상 세척하여 최종 침전된 회백색 분말을 완전히 건조시킨다.To the resulting solution was added acetic acid (CH 3 COOH) and neutralized to pH 6.0 or lower, which gave off-white powder. At this time, fruit vinegar or brown rice vinegar may be used instead of acetic acid. Distilled water was added to the off-white precipitate formed as a result of the neutralization reaction, and washed 30 times or more to completely dry the final precipitated off-white powder.
이상과 같은 공정과 단계로 거쳐 제조된 무독성 회백색 유황분말은 건강보조식품용 또는 의약조성물의 원료로 사용할 수 있으며 이하에서는 건강보조식품 및 의약적 용도를 제시하지만, 본 발명 제품의 용도는 이에만 제한되지 아니하며 당업자간에 얼마든지 변경 사용할 수 있음은 물론이다.Non-toxic gray-white sulfur powder prepared by the above process and steps can be used as a raw material for dietary supplements or medicinal compositions and the following suggests dietary supplements and medicinal uses, but the use of the present invention is limited to this Of course, it can be used as many changes among those skilled in the art.
사용예 1 : 강알칼리성 건강보조식품의 제조Use Example 1 Preparation of Strong Alkaline Health Supplements
상기 설명한 바와 같이 제조된 원료물질(명칭:금액단)을 중량비율로 산호초분말과 1 : 1.5 비율로 혼합하고 그 중량의 3배가 되도록 증류수를 가수한 다음 100℃에서 30분간 가열하여 용해하였다. 용해된 액체에 수세 건조한 측백잎사귀와 복분자(산딸기) 건조물을 중량비 1 : 1로 혼합한 것을 다시 중량비 1 : 1로 혼합하여 다시 100℃에서 6시간 가열하였다. 이를 냉각한 다음 여과하여 액체건강보조식품(명칭:SALLINDA)으로 하였다. 이 액체건강보조식품의 pH는 13.5였다.The raw material prepared as described above (name: end of the solution) was mixed with coral reef powder in a weight ratio of 1: 1.5 ratio, distilled water was added to three times its weight, and then heated at 100 ° C. for 30 minutes to dissolve. The lyophilized dried baekbip leaf and bokbunja (raspberry) dried to the dissolved liquid in a weight ratio of 1: 1 was mixed again in a weight ratio of 1: 1, and heated again at 100 ℃ for 6 hours. It was cooled and then filtered to give a liquid health food (name: SALLINDA). The pH of this liquid dietary supplement was 13.5.
이를 사용하기 위해서는 생수 20cc에 1∼5방울(drop)을 떨어뜨려 조석 1일 2회 식후 30분에 복용하면 된다.To use this, drop 1 to 5 drops (drop) in 20cc of bottled water and take it 30 minutes after eating twice a day.
본 발명에서는 이밖의 어떠한 시품원료를 사용하여 건강보조식품을 제조하여 식용화할 수 있음은 물론이다.In the present invention, of course, it is possible to prepare a dietary supplement by using any other raw material and edible.
본 발명은 이상 실시예와 사용예를 통하여 설명한 바와 같이, 인체에 유해한 독성이 있는 유황(硫黃)으로부터 무독성 회백색 건강보조식품용 가공방법을 제공하는 효과가 있으며, 본 발명 무독성 회백색 유황을 이용한 신규한 건강보조식품을 제공하는 뛰어난 효과가 있으므로 식품산업상 매우 유용한 발명인 것이다.The present invention has the effect of providing a non-toxic gray-white dietary supplement for processing from the sulfur (硫 黄) harmful to the human body as described through the above examples and use examples, the present invention using a non-toxic gray-white sulfur It is a very useful invention in the food industry because it has an excellent effect of providing a dietary supplement.
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| KR10-2000-0018316A KR100404927B1 (en) | 2000-04-07 | 2000-04-07 | Process for purifying sulfur usable for Health care |
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| KR10-2000-0018316A KR100404927B1 (en) | 2000-04-07 | 2000-04-07 | Process for purifying sulfur usable for Health care |
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| KR100404927B1 true KR100404927B1 (en) | 2003-11-07 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100795663B1 (en) * | 2006-08-30 | 2008-01-21 | 고순호 | A sulfur |
| KR100901064B1 (en) | 2008-08-21 | 2009-06-04 | 한태석 | Method for manufacturing of nonpoisonous sulfur |
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2000
- 2000-04-07 KR KR10-2000-0018316A patent/KR100404927B1/en not_active IP Right Cessation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100795663B1 (en) * | 2006-08-30 | 2008-01-21 | 고순호 | A sulfur |
| KR100901064B1 (en) | 2008-08-21 | 2009-06-04 | 한태석 | Method for manufacturing of nonpoisonous sulfur |
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| Publication number | Publication date |
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| KR20010094906A (en) | 2001-11-03 |
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