KR100379974B1 - Method for extracting distillate from pine needles - Google Patents

Method for extracting distillate from pine needles Download PDF

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Publication number
KR100379974B1
KR100379974B1 KR10-2000-0060195A KR20000060195A KR100379974B1 KR 100379974 B1 KR100379974 B1 KR 100379974B1 KR 20000060195 A KR20000060195 A KR 20000060195A KR 100379974 B1 KR100379974 B1 KR 100379974B1
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South Korea
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heating
steamer
cooling
distilled water
minutes
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KR10-2000-0060195A
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Korean (ko)
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KR20020029461A (en
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김용주
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배광석
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08—Concentrating or drying of juices
    • A23L2/10—Concentrating or drying of juices by heating or contact with dry gases
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23N—MACHINES OR APPARATUS FOR TREATING HARVESTED FRUIT, VEGETABLES OR FLOWER BULBS IN BULK, NOT OTHERWISE PROVIDED FOR; PEELING VEGETABLES OR FRUIT IN BULK; APPARATUS FOR PREPARING ANIMAL FEEDING- STUFFS
    • A23N1/00—Machines or apparatus for extracting juice
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23N—MACHINES OR APPARATUS FOR TREATING HARVESTED FRUIT, VEGETABLES OR FLOWER BULBS IN BULK, NOT OTHERWISE PROVIDED FOR; PEELING VEGETABLES OR FRUIT IN BULK; APPARATUS FOR PREPARING ANIMAL FEEDING- STUFFS
    • A23N15/00—Machines or apparatus for other treatment of fruits or vegetables for human purposes; Machines or apparatus for topping or skinning flower bulbs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid

Abstract

내통(6)과 외통(7)으로 구성된 증숙기(5)와 증숙기(5)를 가열하기 위한 수관보일러(8) 그리고 증숙기에서 증숙된 기체를 농축하는 증류수농축관(9)과 증숙기(5)에 생수를 공급하기 위한 생수공급관(10)이 결합 구성되고, 상기 증류수농축관(9)의 끝단에는 코일상의 냉각관(13)의 외주를 물통(14)이 외주를 감싸는 구조로 구성된 냉각기(15)가 결합구성 되고, 냉각기에서 냉각된 액체를 여과하기 위한 휠타(16)로 구성된 솔잎 액기스 추출장치를 가지고 컷터기(3)에서 컷터된 솔잎과 생수를 1대1의 비율로 증숙기(5)에 넣고Steamer (5) consisting of inner cylinder (6) and outer cylinder (7), water pipe boiler (8) for heating steamer (5), distilled water condenser (9) and steamer for condensing the vaporized gas in steamer The bottled water supply pipe 10 for supplying the bottled water to the (5) is configured, the end of the distilled water condensation tube (9) is composed of a structure in which the outer periphery of the cooling tube 13 on the coil, the bucket 14 wraps around the outer periphery The cooler 15 is coupled and has a pine needle extracting device composed of a filter 16 for filtering the liquid cooled in the cooler. The pine needles and bottled water cut in the cutter 3 are steamed in a ratio of one to one. 5) Put it in

보일러(8)를 가동하여 증숙기(5)의 온도를 90℃까지 상승시킨 후 보일러를 끄고 10시간 냉각하는 1차가열단계와;A first heating step of operating the boiler 8 to raise the temperature of the steamer 5 to 90 ° C. and then turning off the boiler and cooling for 10 hours;

100℃에서 증숙기(5)의 압력을 2㎏/㎠을 유지하는 상태로 1시간 20분 동안 가열하는 2차가열단계;A secondary heating step of heating at 100 ° C. for 1 hour and 20 minutes while maintaining the pressure of the steamer 5 at 2 kg / cm 2;

온도를 110℃로 올리고 압력은 2.7㎏/㎠을 유지시키는 상태로 1시간 가열하는 3차가열단계;A third heating step of heating the temperature to 110 ° C. for 1 hour while maintaining the pressure at 2.7 kg / cm 2;

120℃로 올리고 압력은 3.4㎏/㎠을 유지하는 상태로 40분간 가열하는 4차가열 단계;A fourth heating step of heating at 120 ° C. for 40 minutes while maintaining a pressure of 3.4 kg / cm 2;

가열된 최초 증기가 증류수농축라인을 통과한 30분간의 증기를 외부로 배출시키는 드레인단계;A drain step of discharging the steam for 30 minutes when the first heated steam passed through the distilled water concentration line to the outside;

이후 증류수농축라인을 통과한 증기를 냉각기에서 냉각하는 냉각단계;A cooling step of cooling the steam passing through the distilled water concentration line in a cooler;

냉각된 액기스를 휠타로 여과하는 단계를 거치도록 하여 제조된 액기스에 다량의 테라반유와 약품성분이 함유되게 되고 색상이 맑은 액기스를 제공할 수 있도록 한 것이다.The filtered solution is subjected to the step of filtering the filter with a filter, so that a large amount of teraban oil and a chemical ingredient are contained in the manufactured solution, and a clear color solution can be provided.

Description

솔잎 투명 액기스 추출방법{Method for extracting distillate from pine needles}Method for extracting distillate from pine needles}

본 발명은 솔잎 투명 액기스 추출방법에 관한 것으로, 보다 상세하게는 증류를 이용하여 투명 액기스를 추출할 때 동파이프 코일에 기체가 통과하면 동파이프 내부에 2mm가량 솔잎 성분이 동맥경화 현상과 같이 농축되게 되고, 연속적으로 기체가 지나가면서 동맥경화처럼 농축된 성분과 뜨거운 기체가 혼합되면서 기체가 냉각되도록 하여 액체를 얻을 수 있도록 개발한 것이다.The present invention relates to a pine needle transparent extract extraction method, and more specifically, when gas is passed through the copper pipe coil when extracting the transparent extract using distillation so that about 2mm pine needle components inside the copper pipe is concentrated like arteriosclerosis phenomenon As the gas passes continuously, the concentrated component and the hot gas are mixed, such as arteriosclerosis, and the gas is cooled to obtain a liquid.

일반적으로 솔잎은 약명으로 송염이라 일컬어지고 있으며 노화와 암 같은 성인병 예방을 하고 베타카토틴을 비롯하여 각종 영양소인 비타민 A, B, P, K가 함유되어 있으며 아미노산에는 22가지 종류가 있고 그 중 8가지가 성인에게 필요하고 성장기의 어린이들에게는 10가지가 필요하다. 놀랍게도 솔잎에는 성인에게 필요한 8가지 필수 아미노산이 모두 들어있다. 이 중에서 알라닌, 그리신, 로이신, 스레오닌, 아스파라긴산, 글루타민산, 세린, 프룰린 등의 태초의 생명물질로 알려져 있다.In general, pine needles are known as pine salt, which is known as pine salt. It prevents adult diseases such as aging and cancer, and contains beta-catototin and various nutrients such as vitamins A, B, P, and K. There are 22 kinds of amino acids, 8 of which are Is needed for adults and 10 for children in growth. Surprisingly, pine needles contain all eight essential amino acids needed by adults. Among them, alanine, glycine, leucine, threonine, aspartic acid, glutamic acid, serine, and prulin are known as the original life substances.

솔잎에 있는 특수 비타민 P 루틴이라는 성분은 고혈압을 예방하고 노화를 막는데 탁월한 효과가 있는 것으로 밝혀졌다. 바로 이 작용으로 뇌졸증을 예방하는 동시 피를 맑게 하고 모세혈관이 좁아지는 것을 억제하며 또 지방질이 산화됨으로써 인체가 늙어가는 것을 막는 항산화작용도 있는 것으로 밝혀졌다.The special vitamin P rutin found in pine needles has been shown to be effective in preventing hypertension and preventing aging. This action has been shown to prevent stroke, simultaneously clearing blood, inhibiting capillary narrowing, and oxidizing fat, which has been shown to have antioxidant activity that prevents the body from growing old.

현재 숙취제거용으로 다른 음료나 약이 판매되고 있으나 실험결과, 본 고안의 음료가 월등히 좋다는 것이 밝혀졌다.Currently, other beverages or drugs are sold for the removal of the hangover, but experiments have shown that the beverage of the present invention is much better.

현재 각종 솔잎 액기스 종류의 제품을 생산하고 있으나 그 제조과정이 잎을 쪄서 짜는 방법과 솔잎의 향만으로 음료를 생산하며 잎을 쪄서 짜낸 것은 복용하기도 곤란하고 향만으로는 약효를 얻을 수 없는 실정이다.Currently, the production of various types of pine needle extract, but the manufacturing process of the method of squeezing the leaves and producing the drink only by the scent of the pine needles and squeezing the leaves squeezing is difficult to take and the medicinal effect is not obtained only by the fragrance.

본 발명은 추출방법을 연구하여 투명의 추출물을 얻고 복용하기 좋게 하고 약효를 발휘할 수 있도록 개발한 것이다.The present invention has been developed to study the extraction method to obtain a transparent extract to take and take good effect.

상기 목적을 달성하기 위하여 본 발명은 증숙기와 증숙된 기체에 포함되어 있는 성분이 유실되지 않도록 하기 위한 증류수농축관 그리고 냉각기로 구성되는 본 발명장치를 제공하였다.In order to achieve the above object, the present invention provides a device of the present invention consisting of a distilled water condenser and a cooler to prevent the components contained in the steamer and the steamed gas from being lost.

상기 증류수 농축관은 동파이프 코일의 형태로 이루어져 있는데 코일의 감긴 지름과 길이에 따라 증기가 물로 변환되지 않는 상태로 냉각기로 이동할 수 있게 되는 데 거듭하여 실험을 해본 결과 ø12×9m로 설정하고 코일외형은 ø300으로 하고 증기가 지나가는 속도를 시간당 60㎞였을 때 막히지 않으면서 유실되지 않는 상태로 냉각기로 공급할 수 있게 됨을 알았다.The distilled water condenser tube is made of copper pipe coil, and according to the coil diameter and length of the coil, the steam can be moved to the cooler without being converted into water. Was set to ø300, and when the speed at which the steam passed was 60 km per hour, it was found that it could be supplied to the cooler without being blocked without being blocked.

또한 처음 농축 30분간은 가동하여 배출되는 액기스는 폐기한다. 그 이유는 동파이프 내부에 2mm 가량의 솔잎성분이 동맥경화와 같이 농축되도록 하기 위함이며 30분이 지난 후 뜨거운 증기가 지나가면서 30분간 농축된 성분과 증기가 혼합되어 좋은 약효를 가진 증기가 냉각기까지 이송되도록 도달하여 냉각을 시키면 투명하게 된 좋은 약성분을 얻을 수 있도록 한 것이다.In addition, wastes that are discharged by running for the first 30 minutes of concentration are discarded. The reason is that 2mm pine needle components inside the copper pipe are concentrated like arteriosclerosis. After 30 minutes, the hot steam passes and the concentrated ingredients and steam are mixed for 30 minutes, and the steam with good effect is transferred to the cooler. When it reaches as much as possible and cools, it is possible to obtain a good chemical ingredient that becomes transparent.

도1은 본 발명의 구성을 보인 작용도 이다.1 is a functional diagram showing the configuration of the present invention.

***도면의 주요 부분에 대한 부호의 설명****** Description of the symbols for the main parts of the drawings ***

1 : 세척기 2 : 탈수기1: washing machine 2: dehydrator

3 : 세절기 5 : 증숙기6 : 내통 7 : 외통8 : 수관보일러 9 : 증류수농축관10 : 생수공급관 11, 12 : 밸브13 : 냉각관 14 : 물통15 : 냉각기 16 : 휠타DESCRIPTION OF SYMBOLS 3 Flushing machine 5 Steaming machine 6 Inner cylinder 7 Outer cylinder 8 Water pipe boiler 9 Distilled water concentrate tube 10 Bottled water supply pipe 11, 12 Valve 13 Cooling tube 14 Water tank 15 Cooler 16 Filter

이하 본 발명을 첨부된 도면에 따라 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail with reference to the accompanying drawings.

첨부된 도면 도 1 은 본 발명장치의 구성을 보인 것이다.1 is a view showing the configuration of the present invention.

솔잎을 세척하는 세척기(1)와 세척한 솔잎에 포함된 물을 탈수하는 탈수기(2)그리고 탈수된 솔잎을 2-3mm로 잘게 세절하는 세절기(3)를 통과한 솔잎을 증숙기(5)로 투입한다.Steaming the pine needles through a washer (1) for washing the pine needles, a dehydrator (2) for dehydrating the water contained in the washed pine needles (2), and a thinner (3) for finely dipping the dehydrated pine needles into 2-3 mm (5). )

이때, 상기 세척기(1)와 탈수기(2) 그리고 세절기(3)는 시중에 널리 사용되고 있는 공지의 기계들을 사용한다.상기 증숙기(5)는 내통(6)과 외통(7)으로 구성되어 수관보일러(8)에 의해 가열되는 물이 내통(6)과 외통(7)사이의 공간 부로 공급되어 내통을 가열하여 증숙기(5)의 온도를 상승시키는 구조로 이루어져 있다.At this time, the washing machine (1), the dehydrator (2) and the shredder (3) use known machines widely used in the market. The steamer (5) is composed of an inner cylinder (6) and an outer cylinder (7) The water heated by the water pipe boiler (8) is supplied to the space portion between the inner cylinder (6) and the outer cylinder (7) to heat the inner cylinder to increase the temperature of the steam generator (5).

또한 증숙기(5)에는 증류수농축관(9)과 생수공급관(10)이 결합되어 있으며 각 관은 밸브(11,12)에 의해 동작된다.In addition, the steamer 5 is coupled to the distilled water condensation tube 9 and the bottled water supply pipe 10, each tube is operated by the valve (11, 12).

상기 증류수 농축관(9)은 ø12×9m로 설정하고 코일외형은 ø300mm으로 하고 증기가 지나가는 속도를 시간당 60㎞였을 때 막히지 않고 유실되지 않는 상태로 냉각기로 공급하도록 이루어져 있다.The distilled water condenser tube 9 is set to ø12 × 9m, the coil appearance is ø300mm, and is supplied to the cooler without being blocked and lost when the speed at which the steam passes is 60 km per hour.

상기 증류수농축관(9)의 끝단에는 코일상의 냉각관(13)의 외주를 물통(14)이 외주를 감싸는 구조로 구성된 냉각기(15)가 결합 구성된다.At the end of the distilled water condensation tube (9), the outer circumference of the coil-shaped cooling tube (13) is coupled to the cooler (15) configured to have a structure in which a bucket (14) surrounds the outer circumference.

이때 냉각관(13)은 ø12×18m 외경은 ø500mm으로 구성되고 냉각수의 온도는 12℃로 이루어진 것이 바람직하다.At this time, the cooling tube 13 is composed of ø12 × 18m outer diameter of ø500mm and the temperature of the cooling water is preferably made of 12 ℃.

이후 냉각기(15)를 통과한 액체는 휠타(16)를 통과하여 액기스 집착기에 집착되는 구조로 이루어져 있다.After that, the liquid passing through the cooler 15 is configured to pass through the filter 16 and adhere to the extractor.

이와 같은 본 발명의 장치를 사용한 액기스추출방법에 대하여 설명하고자 한다.This will be described with respect to the extraction method using the apparatus of the present invention.

먼저 세절기(3)에서 컷터된 솔잎과 생수를 1대1의 비율로 증숙기(5)의 내부에 넣는다.First, pine needles and bottled water cut in the shredder 3 are placed in the steamer 5 at a ratio of 1 to 1.

이후 보일러(8)를 가동하여 증숙기(5)의 온도를 90℃까지 상승시킨다(1차가열) 이후 보일러를 끄고 10시간 기다렸다가 보일러(8)를 재 점화한다.Thereafter, the boiler 8 is operated to raise the temperature of the steamer 5 to 90 ° C. (primary heating). Then, the boiler is turned off and waits for 10 hours to re-ignite the boiler 8.

100℃에서 증숙기(5)의 압력을 2㎏/㎠을 유지하는 상태로 1시간 20분 동안 가열한다(2차가열).It heats for 1 hour and 20 minutes, maintaining the pressure of the steamer 5 at 100 degreeC in 2 kg / cm <2> (secondary heating).

다시 온도를 110℃로 올리고 압력은 2.7㎏/㎠을 유지시키는 상태로 1시간 가열 한다(3차가열).The temperature is again raised to 110 ° C. and the pressure is heated for 1 hour while maintaining the pressure of 2.7 kg / cm 2 (tertiary heating).

다시 120℃로 올리고 압력은 3.4㎏/㎠을 유지하는 상태로 40분간 가열한다(4차가열).The temperature was raised to 120 ° C. and heated for 40 minutes while maintaining a pressure of 3.4 kg / cm 2 (fourth heating).

이와 같이 온도를 달리하면서 가열할 때 솔잎에 함유되어 있는 테라반유및 솔잎약품성분이 충분하게 물에 함유되게 되는 것이다.As such, when heated at different temperatures, the teraban oil and pine needle chemical components contained in pine needles are sufficiently contained in water.

이후 밸브(11)가 자동"온"되어 증류수농축라인을 통과하도록 하며 이때 30분간은 외부로 드레인(드레인단계) 시킨다.After that, the valve 11 is automatically “on” to pass through the distilled water concentration line, and the drain is drained to the outside (drain step) for 30 minutes.

이와 같이 하면 증류수 농축라인에는 테라반유 및 솔잎약품 성분이 농축되어 달라붙게 되며 이후 증류수농축라인을 통과하는 증류수는 기체인 상태로서 통과하게 된다.In this way, the teraban oil and pine needle chemical components are concentrated and adhered to the distilled water concentration line, and then the distilled water passing through the distilled water concentration line passes as a gas.

통과되는 기체는 증류수농축라인을 통과하면서 벽면에 부딪치게 되는 데 이때 기체에 포함된 테라반유와 솔잎약품이 먼저 달라붙어 있던 테라반유와 솔잎약품이 포함되거나 일부는 벽면에 빼앗기면서 통과되게 되어 농축라인을 통과한 기체는 결과적으로는 증숙기를 통과할 때와 같은 함량의 테라반유와 솔잎약품성분을 간직하게 되는 것이다.Passing gas passes through the distilled water concentration line and hits the wall surface. At this time, the teraban oil and pine needle chemicals contained in the gas are included. The gas passed will eventually retain the same amount of terraban oil and pine needles as they pass through the steamer.

이후 냉각기(15)에서 냉각이 이루어지게 되며(냉각단계) 휠타(16)에 의해 냉각기에서 냉각되어 액체로 변한 농축엑에 포함된 덩어리를 여과하여(여과단계) 투명하고 맑은 증류액을 얻을 수 있게 되는 것이다.After the cooling is performed in the cooler 15 (cooling step) and the lump contained in the concentrated liquid cooled in the cooler by the filter (16) is filtered (filtration step) to obtain a clear and clear distillate Will be.

상기와 같은 솔잎 투명 액기스 추출장치에 의해 제조된 액기스는 다량의 약품성분이 함유되게 되고 색상이 투명한 액기스를 제공할 수 있게 되는 효과가 있는 것이다.The extract prepared by the pine needle transparent extract extracting device as described above is effective to be able to provide a large amount of the chemical component and the color is transparent.

Claims (3)

삭제delete 삭제delete 세절기(3)에서 컷터된 솔잎과 생수를 1대1의 비율로 증숙기(5)에 넣고Pine needles and bottled water cut in the seasoning machine (3) are placed in the steamer (5) at a ratio of 1 to 1. 보일러(8)를 가동하여 증숙기(5)의 온도를 90℃까지 상승시킨 후 보일러를 끄고 10시간 냉각하는 1차가열단계와;A first heating step of operating the boiler 8 to raise the temperature of the steamer 5 to 90 ° C. and then turning off the boiler and cooling for 10 hours; 100℃에서 증숙기(5)의 압력을 2㎏/㎠을 유지하는 상태로 1시간 20분 동안 가열하는 2차가열단계;A secondary heating step of heating at 100 ° C. for 1 hour and 20 minutes while maintaining the pressure of the steamer 5 at 2 kg / cm 2; 온도를 110℃로 올리고 압력은 2.7㎏/㎠을 유지시키는 상태로 1시간 가열하는 3차가열단계;A third heating step of heating the temperature to 110 ° C. for 1 hour while maintaining the pressure at 2.7 kg / cm 2; 120℃로 올리고 압력은 3.4㎏/㎠을 유지하는 상태로 40분간 가열하는 4차가열 단계;A fourth heating step of heating at 120 ° C. for 40 minutes while maintaining a pressure of 3.4 kg / cm 2; 가열된 최초 증기가 증류수농축라인을 통과한 30분간의 증기를 외부로 배출시키는 드레인단계;A drain step of discharging the steam for 30 minutes when the first heated steam passed through the distilled water concentration line to the outside; 이후 증류수농축라인을 통과한 증기를 냉각기에서 냉각하는 냉각단계;A cooling step of cooling the steam passing through the distilled water concentration line in a cooler; 냉각된 액기스를 휠타로 여과하는 여과단계에 의해 솔잎 액기스를 추출하는 것을 특징으로 솔잎 투명 액기스 추출방법.A pine needle transparent extract extraction method, characterized in that to extract the pine needle extract by the filtration step of filtering the cooled extract with a filter.
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KR970009723U (en) * 1995-08-30 1997-03-27 심재홍 Mokchosan Extraction Device
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KR890004716A (en) * 1987-09-30 1989-05-09 한양주 Manufacturing method of antidote based on herbal herbal medicine
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