KR100344147B1 - Healthy drink comprising Xylem Sap from Kiwifruit as main material and The process for preparation there of - Google Patents

Abstract

The present invention relates to a functional health drink mainly based on a sap sap collected from a stalk tree, and a method for manufacturing the same, the step of collecting sap sap from the branches of the stalk tree and freezing and storing the collected sap sap; Melting and storing the frozen Tara sap through a filter and preparing other beverage compositions, and 75 to 80 parts by weight of the Tadasu sap through the above steps, 10 to 15 parts by weight of the tuna rapeseed, 5 parts by weight of fructose, 5 The health beverage based on the taraye sap of the present invention prepared by mixing the parts by weight and adding the excipient to the mixed solution is high blood pressure, menopausal women due to the various minerals, such as calcium, cary, magnesium and amino acids contained in It is effective in preventing various diseases such as osteoporosis.

Description

Healthy drink comprising Xylem Sap from Kiwifruit as main material and The process for preparation there of}

The present invention relates to a functional health beverage mainly based on a sap sap collected from the wood and a method of manufacturing the same.

In recent years, interest in health is increasing, but researches on functional health drinks that can be easily consumed for busy modern people without time to consume health foods are continuing.

Conventional health drinks are commercially available in the form of synthetic beverages made of synthetic ingredients or beverages using herbal medicines such as red ginseng or ganoderma lucidum, but in the case of synthetic beverages, consumers do not prefer to use natural ingredients. There are few problems, and the beverage using herbal medicines has a problem that the production cost is high due to the high cost of the ingredients and the satisfactory taste of the herbal medicines does not satisfy the taste of consumers.

The inventors of the present invention continue to study health beverages made with natural ingredients, and the components of the fruit trees of the fruit (fruit tree) contains various nutrients necessary for the growth and development of fruit trees. Taking into account the fact that it is widely used in the sap, especially the sap components of the tree (including the taraxacum and wild thigh), the sap component of the tree, 17 kinds of amino acids, calcium, carry, It was confirmed that various minerals such as magnesium and appropriate sugars were contained and developed it as a health beverage to complete the present invention.

Accordingly, it is an object of the present invention to provide a health beverage and a method for producing the same, which are mainly composed of natural rapeseed sap.

The above object of the present invention has been achieved by providing a healthy drink mainly made of Tadasu sap containing various minerals and sugars, such as amino acids, calcium, carry, magnesium and the like and a method for producing the same.

Hereinafter, the specific configuration and operation of the present invention will be described in detail step by step.

In order to investigate the components of Tara sap, the predominant health beverage of the present invention, the sap characteristics, sap free sugars, mineral and amino acid content changes, and harmful substances according to the sap collection time in sesame and wild thigh were investigated.

The amount of sap according to the time of sap collection in sesame and wild larvae tends to decrease significantly later.

And, as can be seen from the following Table 1, the moisture content of the thigh sap is 99.49 to 99.76%, and the sugar content is relatively high, 0.8 to 0.9 and 0.6 to 0.7, respectively, in the sesame and wild thigh. The faster the trend, the higher the pH, and the faster the time to collect the sap, the more alkaline the weak acidic acid can act to neutralize the gastric acid can prevent gastrointestinal disease, so it is preferable that the time of collection of the thigh sap.

As a result of investigating the sugar components contained in the thigh sap, as shown in the following Table 2, the sap of sesame was fructose, glucose, sucrose, galactose, and manitol, and the sap of wild thigh contained fructose and glucose. there was.

In addition, as shown in the following Table 3, Darae sap helps carry out skeletal formation of children and is effective in preventing osteoporosis of the elderly and inhibits the absorption of calcium and sodium in the body to prevent hypertension, magnesium, which inhibits myocardial infarction, and It contains a significant amount of iron minerals to prevent anemia, and as shown in Table 4 below, it contains 17 kinds of amino acids that are difficult to ingest through conventional health drinks, while heavy metal residues and pesticides harmful to humans are detected. It wasn't.

And the healthy drink of the present invention mainly based on the sputum sap,

(1) Tara sap collection step,

(2) freezing and storing the collected taupe sap,

(3) dissolving and filtering frozen thaw sap;

(4) preparing other beverage compositions

(5) preparing a beverage,

(6) It is manufactured through the can injection and sterilization step.

The sputum sap used in the step (1) is obtained from the Actinidia chinensis Planch tree or the wild stalk ( Acinidia aguta (Sieb. Et Zucc.) Planch) tree, but is not limited to one species.

The water content, sugar content, viscosity and pH of sap of wild tuna and wild larva are not different between the two species, but in the sugar content, amino acid content and mineral content, the tuna of wild oyster is superior to that of wild larvae. It is more preferable to use the sap of sesame seed than the sap of sap.

In addition, the mineral and amino acid content increases as the sap collection time is late, while the free sugar content decreases and the sampling amount of the sap is significantly reduced, so the harvesting time of the thigh sap used in the present invention is from March 20 to April 10 A period of days is preferred.

The reason for cryopreserving the collected Tara sap as in step (2) is to use the sap of the state immediately collected when using the sap collected in the most time of sap collection in the beverage production.

Filtering the sap frozen and stored as in step (3), which receives various foreign matter (bark, etc.) and frozen sap that were mixed together during sap collection and left in the container for 2 to 3 days, the precipitate becomes cloudy. Therefore, it is to remove it.

In the step (4) is used as an absent ingredient of the health beverage of the present invention is processed sugar type and a fructose to replenish sugar as a beverage and processed in the puree form of vitamins containing a lot of vitamins, vitamin C as necessary And fruity fragrances are also good to use.

The health beverage of the present invention in the step (5) was changed to the content of the thigh sap prepared in step (1) to (3) to tasting 400 people as a result of the following results As shown in Table 5, 60% of the subjects use 75 to 80 parts by weight, which is the preferred content of sputum,

10 to 15 parts by weight of the frozen sesame juice, which is washed with dried crushed sesame and dried and then crushed using a grinder and then juiced with a juicer to remove seeds and shells, and 5 weight of commercial fructose And 5 parts by weight of sugar are added and mixed to prepare a beverage of the present invention. Then, if necessary, about 0.3 parts by weight of vitamin C or 0.001 parts by weight of flavoring agent may be added to the mixed solution.

The health beverage of the present invention prepared in step (5) is put into an enamel coated can, heat treated at 80 ° C. for 10 minutes, sterilized, sealed, inverted for 5 minutes and then cooled.

Hereinafter, the specific configuration and operation of the present invention will be described in more detail by examples. However, the following experimental examples and examples are only for illustrating the present invention, and the scope of the present invention is not limited thereto.

Example 1 Sampling of Sesame Sap

The tuna used in the present invention is a hayward cultivar using a tree that is 8 years old, planted in an orchard in Okcheon-myeon, Haenam-gun, Haenam-gun, Jeonnam, and the sap is on March 10, 1997, April 1, April 24, and April 24. After cutting one branch 1cm in diameter on the main extension of each tree per day, the sap flowing out was collected for 24 hours.

Example 2 Collection of Wild Thigh Sap

The wild sage used in the present invention used a tree that is about 10 years old, which is wild at about 200m above sea level of Mandaesan, Okcheon-myeon, Haenam-gun, Haenam-gun, Jeonnam, and the sap of 1997 and March 10, 1998, April 1, 4 On the 24th of each month, 1 branch 1cm in diameter was cut from the main extension of each tree, and the sap flowing out was collected for 24 hours.

Component Investigation Experiment

In order to investigate the constituents of the sputum sap was used as the sesame and wild sap sap was collected in Example 1 and Example 2, and the collected sap immediately stored in a freezer (-70 ℃) and dissolved before use did.

The sap characteristics, free sugars in the sap, inorganic components and amino acid contents were measured after three weeks of treatment for two years in 1996 and 1997. As a result, the sap characteristics and amino acid contents were not significantly different between the measurement years. The sugar and inorganic components showed data for 2 years.

Experimental Example 1: Investigation of the characteristics of Tara sap

The specific gravity, pH, viscosity, water content, and turbidity of the sap were measured in order to know the characteristics of the Darae sap used as the main ingredient in the health beverage of the present invention.

In this experiment, specific gravity was measured using a hydrometer, pH was a pH meter, and viscosity was measured using an Ostwald viscometer. The moisture content was dried at 105 ° C. for 2 hours and then placed in a desiccator and quantified. Turbidity was measured at the absorbance of 480 ~ 520nm using a spectrophotometer, the results are shown in Table 1 below.

Collection Water content Soluble solids pH Acidity Turbidity Viscosity Species time (%) ( ^o Brix) (%) 10.March 99.49a ^z 0.9a 6.5a 0.16b 0.51b 1.01a Blueberry 1 April 99.62a 0.8a 6.2a 0.15b 0.64a 1.02a24 April 99.54a 0.8a 6.2a 0.20a 0.67a 1.02a10. March 99.75a 0.7a 6.9a 0.10b 0.21b 1.01a Wild Twister 1 April 99.75a 0.7a 6.6a 0.11b 0.27b 1.01a24 April 99.76a 0.7a 6.5a 0.14a 0.38a 1.01a ^Z Mean separation within columns by Duncan's multiple range test, p ≤0.05.

Experimental Example 2 Investigation of Organic Sugars in Tara sap

The free sugars of the sesame tangle sap of Example 1 and the wild thigh of Example 2 were pre-treated in a Bio-Rex 5 analytical column (100-200mesh, chloride form anion exchange) and then filtered (0.45 ml) using HPLC using RI detector. Measured by (Waters). The column was a Carbohydrate Anaiysis Column (3.9 X 25cm, 10ml), and the temperature was maintained at 25 ° C. The solvent was used 75% acetonitrile and the flow rate was 1ml / min. The results are shown in Table 2 below. .

Kinds Harvest time Free sugar (mg / ml) Fructose Glucose Sucrose Galactose Manitol 1996 Blue sky 10 March 1.16a ^z 0.15a 0.10a 0.01a 0.04a 1 April 0.95b 0.12a 0.08a 0.01a 0.03a 24 April 0.90b 0.10a 0.08a 0.01a 0.03a Wild Thigh 10 March 0.04a 0.02a 0.00a 0.00a 0.00a 1 April 0.04a 0.01b 0.00a 0.00a 0.00a 24 April 0.01b 0.01b 0.00a 0.00a 0.00a 1997 Blue sky 10 March 1.14a 0.08a 0.06a 0.00a 0.00a 1 April 1.10a 0.08a 0.04a 0.00a 0.00a 24 April 0.98a 0.06a 0.03a 0.00a 0.00a Wild Thigh 10 March 0.08a 0.01a 0.00a 0.00a 0.00a 1 April 0.06a 0.01a 0.00a 0.00a 0.00a 24 April 0.06a 0.01a 0.00a 0.00a 0.00a ^Z Mean separation within columns by Duncan's multiple range test, p ≤0.05.

Experimental Example 3 Investigation of Minerals in Tara sap

In order to investigate the minerals in the thigh sap, 50 ml of the sap of sapling of Example 1, the sap of wild thigh of Example 2, and 30 ml of concentrated nitric acid were added to a triangle flask, and slowly heated until dark red color appeared. 20 mL was added to completely decompose the organics. The digested solution was filtered and analyzed using an Atomic Absorption Spectrophotometer. The results are shown in Table 3 below.

Inorganic Ingredients (mg / L) Blue sky Wild Thigh 10 March 1 April 24 April 10 March 1 April 24 April 1996 Fe 0.08a ^z 0.09a 0.08a 0.02a 0.02a 0.02a Cu 0.17b 0.20ab 0.24a 0.03a 0.03a 0.03a Zn 0.20a 0.24a 0.21a 0.01a 0.01a 0.01a Mn 0.61a 0.33b 0.66a 0.06a 0.06a 0.06a Ca 100.62a 109.15a 115.50a 90.10a 97.11a 101.80a K 64.22a 71.40a 75.65a 58.40a 66.81a 70.02a Mg 61.01a 66.05a 71.83a 48.50a 48.66a 48.11a Na 0.26a 0.31a 0.30a 0.25a 0.21a 0.22a 1997 Fe 0.08a 0.06ab 0.04b 0.02b 0.06a 0.06a Cu 0.13b 0.15b 0.21a 0.03a 0.03a 0.03a Zn 0.17b 0.24a 0.22a 0.01a 0.02a 0.02a Mn 0.40a 0.43a 0.51a 0.08a 0.08a 0.08a Ca 110.10b 114.62ab 134.45a 90.24a 84.10a 98.00a K 64.8a 66.84a 69.50a 66.41a 71.82a 79.34a Mg 54.8b 68.13ab 79.71a 50.41a 54.6a 52.68a Na 0.31a 0.36a 0.40a 0.24a 0.24a 0.22a ^Z Mean separation within columns by Duncan's multiple range test, p ≤0.05.

Experimental Example 4 Investigation of Amino Acids in Tara sap

In order to investigate the amino acids in the sap from sap, sap from sap of sapling of Example 1 and sap from wild sap of Example 2 were analyzed by modifying the analysis method of Anderson and Brodbeck (1989).

That is, the sample was filtered (0.45 ml), 50 ml of the filtrate was placed in a sample tube and dried at the workstation. The dried sample was re-dried after adding 20 ml of a mixture of methanol, water, and trifluoroacetic acid (TEA) in a 2: 2: 1 ratio. 20 ml of a mixture of methanol, water, TEA, and phenylisothiocyate in a 7: 1: 1: 1 mixture was added to the dried sample and derivatized at room temperature, followed by vacuum drying. 250 μL of the sample dilution reagent was added to the dried sample, followed by filtration, and 10 mL was injected into HPLC (Waters). The column was a Pico-Tag Column (3.9mm x 150mm, 4ml) and the temperature was maintained at 50 ℃. The solvents were 20 g sodium acetate trihydrate, water containing 500-600 ml of TEA and 65 ml of CH ₃ CN (solution A), and water containing 60% CH ₃ CN (solution B). After the first 100% to 0% was measured by using a UV detector while again flowing 100% A solution for 10 minutes, the results are shown in Table 4 below.

Amino Acid (mg / L) Blue sky Wild Thigh 10 March 1 April 24 April 10 March 1 April 24 April Glutamic acidAsparticGlycineSerineThreonineProlineAlanineValineleucineIsoleucineArginineLysineTyrosinePhenylalanineCystineHistidineMethionine 520b ^z 72a11a52a147a37a29a211a242a366a171a312a57a151a61b190a84a 570ab68a12a57a140a35a28a210a262a377a184a303a50a141a57b196a83a 640a67a13a61a153a45a31a220a266a381a162a316a64a148a84a186a93a 530a55a15a53a129a23a21a73a188a180a131a290a107a138a41a203a54b 533a50a15a43a120a20a19a63a181a186a136a281a111a130a45a201a64ab 560a51a16a53a128a21a16a60a170a171a126a286a120a149a49a211a77a ^Z Mean separation within columns by Duncan's multiple range test, p ≤0.05

Example 3 Preparation of Blue Sap

The frozen sesame sap collected in Example 1 was immediately frozen in a freezer at a temperature of -70 to -100 ° C., and the frozen sesame sap stored at room temperature was dissolved, and then, a filter using Whatman Paper size four-ply cheese cloth was used. The frozen sesame seed sap is filtered and the remaining residue is filtered to prepare sesame seed sap.

Example 4 Preparation of Wild Thigh Sap

The frozen wild tuna sap collected in Example 2 was immediately frozen in a freezer at a temperature of -70 to -100 ° C, and the frozen blue tuna sap was dissolved at room temperature, and then used as a filter with four layers of Whatman Paper size cheese cloth. Filter the frozen wild sap sap and remove the remaining filtered residue to prepare wild sap sap.

Example 5 Preparation of Other Beverage Ingredients

Champarae puree used in the present invention is a 'Hayward' cultivar used in cultivated from a tree that is 10 years old in the orchard of Okcheon-myeon, Haenam-gun, Haenam-gun, Korea. After drying the water, apply the full speed 1,600 times per minute using a grinder. Break the sesame seeds and use a juicer (0.84mm net) to immediately juice the sesame juice obtained by separating the seeds and husks at 100 degrees Celsius. After heat treatment using a heat exchanger for 30 seconds and immediately cooled to prepare, commercially available fructose, sugar, vitamin C and fruit flavors from the fruit was prepared.

Example 6 Preparation of Healthy Beverages Based on Sesame Sap, Can Injection, and Sterilization

75 to 80 parts by weight of the sesame sap prepared in Example 3, 10 to 15 parts by weight of sesame fungus prepared in Example 5, 5 parts by weight of fructose and 5 parts by weight of sugar were added to prepare a beverage of the present invention. About 0.3 parts by weight of vitamin C or 0.001 parts by weight of perfume is added to the mixed solution to prepare a health beverage mainly composed of Tadasu sap, and then heat-treated at 80 ° C. for 10 minutes for sterilization and sealing. Turn over for 5 minutes and let cool.

Example 7 Preparation of Healthy Beverages Based on Wild Thigh Sap, Can Injection, and Sterilization

75 to 80 parts by weight of wild sap sap prepared in Example 4 as the sputum sap, and other conditions were prepared in the same manner as in Example 6 to prepare a health beverage mainly containing wild sap sap and then put in an enamel coated can Heat treatment at 80 ℃ for 10 minutes to sterilize, seal and invert for 5 minutes and then cool.

Experimental Example 5: Investigation of the Preference According to the Change of Content

The results of tasting 400 people in the Agricultural Cooperatives on December 5, 1998 by changing the content of the Tara sap to apply the beverage of the present invention by investigating the preference according to the content change of the Tara sap is shown in Table 5 below. .

Content of Sesame Sap Content of Celadon Puree Preferred (persons) 90 wt% 10% by weight 24 85 wt% 15 wt% 37 80 wt% 20 wt% 130 75 wt% 25% by weight 110 70 wt% 30 wt% 46 65% by weight 35 wt% 33 60% by weight 40 wt% 8 55 wt% 45 wt% 2

As can be seen from the detailed description of the present invention, the health beverage of the present invention uses 17 kinds of amino acids and various minerals such as calcium, cary, magnesium, and dalnae sap, which contains appropriate sugars, as a main component, and thus the growth period is due to the calcium component. It has the effect of promoting the skeletal formation and growth of children and the prevention of osteoporosis in the elderly, the effect of inhibiting the absorption of sodium in the body due to the carry component to prevent hypertension, and the effect of inhibiting myocardial infarction due to the magnesium component It is not only able to prevent anemia due to iron components, but also to promote blood circulation due to the arginine and gdamic acid component among the 17 kinds of amino acids contained. It is a natural substance of domestic Darae Since the present invention can be obtained is a very useful invention in the food industry and public health.

Claims (4)

Collecting the stalk sap from the branch of the stalk tree in early March to the middle of April, and storing the stalk sap collected at -70 ° C. to -100 ° C. until the sesame puree is ready; Dissolving the Tara sap at room temperature and then filtering through a filter; Sesame seeds harvested from October to November were washed with drinking water containing 5ppm of free chlorine, and then crushed using a grinder, and then juiced to separate seeds and husks.The obtained sesame juice was heat-treated at 100 ° C. for 30 seconds. After cooling to prepare a sesame seed fungus; Mixing 75 to 80 parts by weight of the Tadasu sap prepared in the above step, 10 to 15 parts by weight of sesame seeds, 5 parts by weight of fructose, and 5 parts by weight of sugar; Method for producing a healthy drink, mainly based on the Darae sap characterized in that it comprises the step of adding 0.3 parts by weight of vitamin C, 0.001 parts by weight to the mixed solution. It is prepared by the method of claim 1, 75 to 80 parts by weight of Tadasu sap, 10 to 15 parts by weight of sesame seed, 5 parts by weight of fructose, 5 parts by weight of sugar, 0.3 parts by weight of vitamin C, 0.001 parts by weight of fragrance Healthy drink mainly made of dairae sap. The health beverage of claim 2, wherein the stalk is the sap of the thorn tree. The health beverage of claim 2, wherein the thigh sap is a sap of wild thigh tree.