KR100344003B1 - Manufacturing method of antibiotic detergent by silver and charcoal - Google Patents

Manufacturing method of antibiotic detergent by silver and charcoal Download PDF

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Publication number
KR100344003B1
KR100344003B1 KR1019990026295A KR19990026295A KR100344003B1 KR 100344003 B1 KR100344003 B1 KR 100344003B1 KR 1019990026295 A KR1019990026295 A KR 1019990026295A KR 19990026295 A KR19990026295 A KR 19990026295A KR 100344003 B1 KR100344003 B1 KR 100344003B1
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silver
charcoal
detergent
powdered
artificial zeolite
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KR1019990026295A
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Korean (ko)
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KR20010008455A (en
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최귀분
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심홍필
최귀분
최명부
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

본 발명은 은과 숯을 이용한 항균세제에 관한 것으로서 특히 항균세제비누 및 샴푸로 사용할 경우 세제에 함유된 은.분말숯 및 인조제오라이트의 살균, 흡착 및 탈취작용으로 각종 피부질환이나 피부염, 여드름, 무좀 등의 치료예방은 물론 주방용 세제로 사용시 살균탈취작용으로 위생적인 세척효과가 있도록 한 것이다.The present invention relates to an antimicrobial detergent using silver and charcoal. Especially, when used as an antibacterial detergent soap and shampoo, various skin diseases, dermatitis, acne, athlete's foot by sterilization, adsorption and deodorization of silver and powder charcoal and artificial zeolite contained in the detergent. Preventive treatment, etc., of course, when used as a detergent for the disinfection of the sanitary effect to have a hygienic cleaning effect.

상기 목적을 달성하기 위하여 본 발명은 정제된 은과 분말화된 숯 및 인조제오라이트를 혼합 반죽한 다음 건조하고, 미분쇄하여 분말가루를 얻고, 상기 분말가루를 비누나 샴푸, 주방용 세제류등의 제조공정에 투입하여 항균세제류를 제조하는 것이다.In order to achieve the above object, the present invention is a mixture of refined silver and powdered charcoal and artificial zeolite, and then dried and pulverized to obtain powdered powder, and the powdered powder is produced in soap, shampoo, kitchen detergent, etc. It is put in to prepare antibacterial detergents.

Description

은과 숯을 이용한 항균세제의 제조방법{Manufacturing method of antibiotic detergent by silver and charcoal}Manufacturing method of antibiotic detergent using silver and charcoal {Manufacturing method of antibiotic detergent by silver and charcoal}

본 발명은 은과 숱 및 인조제오라이트를 합성하여 제조한 항균세제(비누, 샴푸, 주방용세제등)에 관한 것으로서, 특히 항균세제를 사용토록 하므로서 항균세제에 함유된 은의 살균 작용과 숯의 흡착작용 그리고 인조제오라이트의 탈취 및 흡착작용에 의해 바이러스성 피부질환인 비듬, 여드름, 냄새, 각종 피부염이나 무좀에 탁월한 효과가 있도록 할 뿐 아니라, 주방용세제로 사용시 살균탈취효과에 의해 위생적인 세척이 될 수 있도록 한 것이다.The present invention relates to antimicrobial detergents (soaps, shampoos, kitchen detergents, etc.) prepared by synthesizing silver and thinning and artificial zeolites, and in particular, by using antibacterial detergents, the bactericidal action of silver contained in the antimicrobial detergents and adsorption of charcoal and By deodorizing and adsorbing artificial zeolite, it has excellent effect on viral skin diseases such as dandruff, acne, odor, various dermatitis and athlete's foot, and it can be hygienic cleaning by sterilizing deodorizing effect when used as kitchen detergent. will be.

종래에도 은을 이용한 항균비누가 제공된 바 있으나 효과적인 항균작용이 되고 있지 못한 등의 문제점이 있는 것이었다.Conventional antibacterial soap has been provided using silver, but there was a problem such as not being an effective antibacterial action.

본 발명은 이러한 종래의 문제점을 시정하고자 은과 숯 및 인조제오라이트를 합성하여 효과적인 항균력을 얻을 수 있는 항균세제를 제공받을 수 있도록 하는 것이다.The present invention is to be able to be provided with an antimicrobial detergent to obtain an effective antimicrobial power by synthesizing silver and charcoal and artificial zeolite to correct these problems.

옛부터 은은 인체에 무해한 무기항균제로 널리 사용되고 있을 뿐 아니라, 지상의 모든 단세포 병균을 살균하는 효과가 있다고 보고되고 있다.Since ancient times, silver has been widely used as an inorganic antimicrobial that is harmless to the human body, and has been reported to have the effect of killing all single cell germs on the ground.

은의 살균작용은 활성산소에 의한 항균작용 즉 은이 방출하는 산소는 촉매작용에 의하여 부분적으로 활성화산소(O2+O2-.O)로 전환되고, 이 활성화산소는 오존, 과산화수소, 염소와 같은 강력한 살균작용을 하게 된다.The bactericidal action of silver is an antibacterial action by active oxygen, that is, oxygen released by silver is partially converted into activated oxygen (O 2+ O 2- .O) by catalytic action, and this activated oxygen is strong like ozone, hydrogen peroxide and chlorine. It will be sterilized.

숯은 1g의 표면적이 약 100평 정도로써, 미세구멍의 흡착력에 의해 해로운 바이러스나 박테리아, 독소, 냄새 등을 흡착하며, 주성분은 탄소로서, 음전자가 많기 때문에 물질의 부패를 막아주고, 몸과 피부의 산성화 현상을 막아주는 역활을 하게 된다.The charcoal has a surface area of 1g, about 100 pyeong, and it adsorbs harmful viruses, bacteria, toxins, and odors by the adsorption power of micropores.Its main component is carbon, which contains many negative electrons, preventing the decay of substances and It acts to prevent acidification of the skin.

인조제오라이트는 잘 발달된 포리(PORE)를 가지고 있기 때문에 비표면적이 매우 크며, 또한 박테리아균, 유기물 등을 흡착하는 기능을 보유하고 있고, 탈취작용에 효과적이다.Since artificial zeolite has a well-developed PORE, its specific surface area is very large, and it has a function of adsorbing bacteria, organic matters, etc., and is effective for deodorization.

본 발명은 은, 숯, 인조제오라이트가 가지고 있는 효과를 최대한 활용하여 항균세제를 얻을 수 있도록 한 것이다.The present invention is to take advantage of the effect of silver, charcoal, artificial zeolite to obtain an antibacterial detergent.

상기 목적을 달성하기 위하여 본 발명은 고순도 은괴를 용융, 소립하여 용해조에 넣고, 가열하면서 질산을 서서히 투입하면서 은용액을 만들고, 은용액을 물에 투입한 다음 알미늄산 소다를 넣고 교반하면서 가열하여 수분을 증발시켜 고체화되게 하고, 여기에 다시 물을 넣고, 빙초산을 투입하여 끓여 물이 증발되게 하므로서, 결창은을 얻고, 상기 결창은을 물에 녹여 분말숯과 인조제오라이트를 혼합한 혼합물을 투입 교반하여 반고체의 반죽물을 얻은 다음 건조하고, 분쇄하여 분말가루를 얻고, 상기 분말가루를 통상의 비누분에 투입하여 비누를 제조하므로서, 본 발명에서 얻고자 하는 항균세제의 제조가 완료된다.In order to achieve the above object, the present invention melts and granulates a high purity silver ingot into a dissolution tank, and slowly adds nitric acid while heating to make a silver solution, and then adds a silver solution to water, and then adds sodium aluminate to it and heats it while stirring. To evaporate to solidify, add water again, and add glacial acetic acid to boil to allow water to evaporate, thereby obtaining changchang silver, and dissolve the changchang in water and add a mixture of powdered charcoal and artificial zeolite Semi-solid dough is obtained and then dried and pulverized to obtain powdered powder, and the powdered powder is added to a conventional soap powder to prepare a soap, thereby preparing the antibacterial detergent to be obtained in the present invention.

이하 본 발명의 실시예를 공정별로 상세히 설명하면 다음과 같다.Hereinafter, an embodiment of the present invention will be described in detail by process.

실시예Example

제1공정: 결창은 제조공정1st step: Changchang manufacturing process

순도99.9%의 은괴 100g을 용융, 소립하여 용해조에 넣고, 서서히 열을 가하면서 질산 100㎖를 투입하여 은용액을 얻는다.100 g of silver ingot having a purity of 99.9% is melted and small, put into a dissolution tank, and 100 ml of nitric acid is added while gradually heating to obtain a silver solution.

상기 은용액을 물 200㎖에 넣은 다음 알미늄산 소다 100g을 넣어 100℃로 가열 교반하여 PH 7정도로 중화되게 하고, 계속 가열하여 수분을 증발시켜 다시 고체가 되게 한다.The silver solution was added to 200 ml of water, and then 100 g of sodium aluminate was added thereto, stirred at 100 ° C. to be neutralized to pH 7, and the heating was continued to evaporate moisture to become solid again.

고체화된 은에 다시 물 200㎖을 넣고 여기에 적량의 빙초산을 투입하여 PH 5정도로 조정되게 한 다음 100℃로 끓여 물이 증발되게 하므로서 결창의 은을 얻는다.200 ml of water is added to the solidified silver, and an appropriate amount of glacial acetic acid is added thereto to adjust the pH to about 5, and then boiled at 100 ° C. to allow the water to evaporate, thereby obtaining silver of the window.

제2공정 : 분말 숯과 인조제오라이트 및 결창은의 혼합분말 제조공정2nd process: manufacturing process of mixed powder of powder charcoal, artificial zeolite and changchang silver

참나무 숯을 1000메쉬로 분쇄한 분말숯 1kg과 인조제오라이트 5kg을 혼합하여 분말숯과 인조제오라이트가 충분히 혼합된 혼합물을 얻는다.1 kg of powdered charcoal pulverized with oak charcoal and 1000 kg of artificial zeolite are mixed to obtain a mixture of powdered charcoal and artificial zeolite.

다시 제1공정에서 얻어진 결창은을 물2ℓ에 넣고, 상기에서 얻어진 분말 숯과 인조제오라이트의 혼합물을 투입하여 충분히 교반하여 반고체의 반죽상태로 한 다음 건조하고, 건조완료된 혼합물은 분쇄기를 통하여 500메쉬정도로 분쇄하여 분말화된 은과 숯 및 인조제오라이트가 혼합된 분말가루를 얻는다.Then, the resulting ingot was added to 2 l of water, and the mixture of powdered charcoal and artificial zeolite obtained above was added and stirred sufficiently to make a semi-solid dough state, and then dried, and the dried mixture was about 500 mesh through a grinder. Grinding to obtain powdered powder mixed with powdered silver, charcoal and artificial zeolite.

제3공정 : 세제의 제조공정Third Step: Manufacturing Process of Detergent

제2공정에서 얻어진 은과 숯 및 인조제오라이트 혼합분말가루를 세제 50kg에 넣고 혼합 성형하므로서 본 발명에서 얻고자 하는 은과 숯을 이용한 항균세제를 제조 완성하게 된다.Silver and charcoal and artificial zeolite mixed powder powder obtained in the second step is mixed into 50kg of detergent and molded to produce an antimicrobial detergent using silver and charcoal to be obtained in the present invention.

이때 세제류로서는, 비누, 샴푸, 주방용세제 등 여러물품에 적용가능하다.In this case, the detergents may be applied to various articles such as soaps, shampoos and dish detergents.

따라서 본 발명의 항균세제성분내에 은과 분말숯 및 인조제오라이트 성분이 함유되어 있어, 세제를 사용하게 되면 은의 강력한 항균력과, 숯의 뛰어난 흡착성과, 산화방지성 및 인조제오라이트의 탈취작용에 의해 피부의 변원체 피지성분을 제거하고, 바이러스성 피부질환, 비듬, 여드름, 냄새, 무좀 등을 자연스럽게 예방치료할 수 있게 되고, 외출후 손발을 씻으면 대장균등의 세균을 멸균하는 효과와 함께 피부의 유해한 중금속등을 깨끗히 세척할 수 있게 되며, 또한 주방용세제로 사용시에도 살균과 탈취, 흡착작용에 의해 위생적인 세척이 가능케 되는 등의 효과가 있는 것이다.Therefore, silver and powder charcoal and artificial zeolite component are contained in the antibacterial detergent component of the present invention. When the detergent is used, the strong antibacterial activity of silver, excellent adsorption of charcoal, antioxidant and deodorization of artificial zeolite It removes the sebaceous constituents of the body, and can prevent and treat viral skin diseases, dandruff, acne, odor, athlete's foot, etc. Naturally, when you wash your hands and feet after going out, you can sterilize bacteria such as E. coli and harmful heavy metals. Being able to wash cleanly, and also when used as a dishwashing detergent, sterilization, deodorization, by the adsorption action is hygienic cleaning is possible.

Claims (2)

고순도 은100g을 용융소립하여 용해조에 넣고 가열하면서 질산 100㎖를 투입하여 은용액을 얻고, 상기 은용액을 200㎖의 물에 넣은 다음 100g의 알미늄소다를 투입 100℃로 가열교반하면서 수분을 증발시켜 고체화되게 하고, 고체화된 은에 빙초산을 투입 PH 5정도로 조정하고, 가열하여 물이 증발되게 하므로서, 결창은을 얻고, 상기 결창은과, 분말숯 1kg과 인조제오라이트5kg을 혼합교반한 혼합물을 2ℓ의 물에 넣고 혼합교반한 다음 건조하고, 건조된 혼합물을 약500메쉬로 분쇄하여 분말가루를 얻고, 상기 분말가루를 통상의 세제액 50kg내에 넣고 제조하는 것을 특징으로 하는 은과 숯을 이용한 항균세제의 제조방법.100 g of high-purity silver is melted and granulated in a dissolution tank, and 100 ml of nitric acid is added while heating to obtain a silver solution. Then, the silver solution is added to 200 ml of water and 100 g of aluminum soda is added. To solidify, add glacial acetic acid to the solidified silver to adjust the pH to about 5, and heat to evaporate the water, to obtain a spear, the spear was mixed with 2 liters of a mixture of 1 kg of powdered charcoal and 5 kg of artificial zeolite After mixing and stirring in water and drying, the dried mixture was pulverized to about 500 mesh to obtain powdered powder, and the powdered powder was prepared in 50 kg of a normal detergent solution. Manufacturing method. 삭제delete
KR1019990026295A 1999-07-01 1999-07-01 Manufacturing method of antibiotic detergent by silver and charcoal KR100344003B1 (en)

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Publication number Priority date Publication date Assignee Title
KR20010069644A (en) * 2001-04-24 2001-07-25 오성근 Manufacturing of highly concentrated Antibiotic Silver Soap
KR20030045412A (en) * 2001-12-04 2003-06-11 김동욱 Method for washing diaper using silver
KR20030083038A (en) * 2002-04-19 2003-10-30 이언섭 The detergent comprising Ag-ion
KR20040085132A (en) * 2004-09-14 2004-10-07 이현숙 Functional soap including pearl powder and nano silver and method thereof
KR101699271B1 (en) 2014-11-25 2017-01-24 주식회사 지엘머티리얼즈 method for manufacturing soap having finely dispersed rare metal nano-particles, and soap manufactured using the same

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