JPS63368B2 - - Google Patents
Info
- Publication number
- JPS63368B2 JPS63368B2 JP58178337A JP17833783A JPS63368B2 JP S63368 B2 JPS63368 B2 JP S63368B2 JP 58178337 A JP58178337 A JP 58178337A JP 17833783 A JP17833783 A JP 17833783A JP S63368 B2 JPS63368 B2 JP S63368B2
- Authority
- JP
- Japan
- Prior art keywords
- chlorosilane
- reaction
- lithium hydride
- molten salt
- salt mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000203 mixture Substances 0.000 claims description 55
- 239000005046 Chlorosilane Substances 0.000 claims description 50
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 claims description 50
- SIAPCJWMELPYOE-UHFFFAOYSA-N lithium hydride Chemical compound [LiH] SIAPCJWMELPYOE-UHFFFAOYSA-N 0.000 claims description 49
- 229910000103 lithium hydride Inorganic materials 0.000 claims description 49
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims description 47
- 239000011833 salt mixture Substances 0.000 claims description 33
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 26
- 229910000077 silane Inorganic materials 0.000 claims description 26
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 18
- 238000000034 method Methods 0.000 claims description 18
- 230000005496 eutectics Effects 0.000 claims description 13
- 239000001103 potassium chloride Substances 0.000 claims description 9
- 235000011164 potassium chloride Nutrition 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 229910001514 alkali metal chloride Inorganic materials 0.000 claims description 4
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- -1 salt compound Chemical class 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims 6
- FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical compound Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 description 3
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 3
- 239000005052 trichlorosilane Substances 0.000 description 3
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910003902 SiCl 4 Inorganic materials 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 description 1
- 229910001626 barium chloride Inorganic materials 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- SLLGVCUQYRMELA-UHFFFAOYSA-N chlorosilicon Chemical compound Cl[Si] SLLGVCUQYRMELA-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052701 rubidium Inorganic materials 0.000 description 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/04—Hydrides of silicon
- C01B33/043—Monosilane
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/09—Reaction techniques
- Y10S423/12—Molten media
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8216434A FR2533906A1 (fr) | 1982-09-30 | 1982-09-30 | Procede et dispositif pour la preparation de silane pur par reaction de chlorosilanes avec l'hydrure de lithium |
| FR82.16434 | 1982-09-30 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5983924A JPS5983924A (ja) | 1984-05-15 |
| JPS63368B2 true JPS63368B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1988-01-06 |
Family
ID=9277870
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58178337A Granted JPS5983924A (ja) | 1982-09-30 | 1983-09-28 | クロロシランと水素化リチウムの反応により純粋なシランを製造する方法および装置 |
Country Status (6)
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5075092A (en) * | 1987-07-20 | 1991-12-24 | Ethyl Corporation | Process for preparation of silane |
| US4847061A (en) * | 1987-07-20 | 1989-07-11 | Ethyl Corporation | Process for preparation of silane |
| US6467947B1 (en) * | 1997-08-19 | 2002-10-22 | Commonwealth Scientific And Industrial Research Organisation | Method and apparatus for mixing |
| RU2173297C2 (ru) * | 1999-03-10 | 2001-09-10 | Открытое акционерное общество "Новосибирский завод химконцентратов" | Способ получения моносилана из тетрахлорида кремния |
| RU2194009C1 (ru) * | 2001-04-10 | 2002-12-10 | Открытое акционерное общество "Новосибирский завод химконцентратов" | Способ получения силана |
| RU2245299C2 (ru) * | 2003-02-11 | 2005-01-27 | Открытое акционерное общество "Новосибирский завод химконцентратов" | Способ получения силана |
| GB0312749D0 (en) * | 2003-06-04 | 2003-07-09 | Optimed Ltd | Improvements in and relating to trial lens |
| RU2412902C2 (ru) * | 2008-03-21 | 2011-02-27 | Юрий Константинович Кварацхели | Способ получения моносилана и устройство для его осуществления |
| RU2390494C1 (ru) * | 2009-02-20 | 2010-05-27 | Виктор Иванович Петрик | Способ получения моносилана |
| DE102009037155B3 (de) * | 2009-08-04 | 2010-11-04 | Schmid Silicon Technology Gmbh | Verfahren und Anlage zur Herstellung von Trichlorsilan |
| DE102009056731A1 (de) | 2009-12-04 | 2011-06-09 | Rev Renewable Energy Ventures, Inc. | Halogenierte Polysilane und Polygermane |
| RU2466089C1 (ru) * | 2011-04-20 | 2012-11-10 | Владимир Александрович Ольшанский | Способ получения моносилана |
| RU2551511C1 (ru) * | 2013-10-24 | 2015-05-27 | Открытое акционерное общество "Ведущий научно-исследовательский институт химической технологии" | Способ получения моносилана и устройство для его осуществления |
| US11002255B2 (en) | 2019-08-20 | 2021-05-11 | Lowry Inheritors Trust | Carbon negative clean fuel production system |
| CN113481383B (zh) * | 2021-07-21 | 2022-07-19 | 合肥学院 | 一种金属钾的制备方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL230341A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1957-08-08 | 1900-01-01 | ||
| US3078218A (en) * | 1958-08-04 | 1963-02-19 | Union Carbide Corp | Hydrogenation of halogen compounds of elements of groups iii and iv of the periodic system |
| FR1323193A (fr) * | 1961-04-27 | 1963-04-05 | Union Carbide Corp | Hydrogénation des éléments des groupes iii, iv et v |
| NL277704A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1961-04-27 | |||
| ES462575A1 (es) * | 1976-09-24 | 1978-07-16 | Union Carbide Corp | Un procedimiento para la obtencion de silano. |
| JPS591211B2 (ja) * | 1980-06-02 | 1984-01-11 | 小松電子金属株式会社 | モノシラン連続発生方法およびその装置 |
| FR2504109A1 (fr) * | 1981-04-17 | 1982-10-22 | Rhone Poulenc Spec Chim | Procede de preparation de silane en milieu sels fondus |
-
1982
- 1982-09-30 FR FR8216434A patent/FR2533906A1/fr active Granted
-
1983
- 1983-09-16 DE DE8383401812T patent/DE3360846D1/de not_active Expired
- 1983-09-16 EP EP83401812A patent/EP0105778B1/fr not_active Expired
- 1983-09-27 US US06/536,240 patent/US4499063A/en not_active Expired - Fee Related
- 1983-09-28 JP JP58178337A patent/JPS5983924A/ja active Granted
- 1983-09-29 CA CA000437973A patent/CA1214022A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2533906A1 (fr) | 1984-04-06 |
| DE3360846D1 (en) | 1985-10-24 |
| US4499063A (en) | 1985-02-12 |
| CA1214022A (fr) | 1986-11-18 |
| JPS5983924A (ja) | 1984-05-15 |
| FR2533906B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1985-02-08 |
| EP0105778B1 (fr) | 1985-09-18 |
| EP0105778A1 (fr) | 1984-04-18 |
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