JPS6227545A - Manufacture of sintered soft-magnetic parts - Google Patents

Manufacture of sintered soft-magnetic parts

Info

Publication number
JPS6227545A
JPS6227545A JP16805985A JP16805985A JPS6227545A JP S6227545 A JPS6227545 A JP S6227545A JP 16805985 A JP16805985 A JP 16805985A JP 16805985 A JP16805985 A JP 16805985A JP S6227545 A JPS6227545 A JP S6227545A
Authority
JP
Japan
Prior art keywords
powder
iron
sintered
silicon
magnetic parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP16805985A
Other languages
Japanese (ja)
Inventor
Shuji Matsumoto
修二 松本
Kunpei Kobayashi
薫平 小林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp filed Critical Toshiba Corp
Priority to JP16805985A priority Critical patent/JPS6227545A/en
Publication of JPS6227545A publication Critical patent/JPS6227545A/en
Pending legal-status Critical Current

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  • Powder Metallurgy (AREA)
  • Soft Magnetic Materials (AREA)

Abstract

PURPOSE:To manufacture iron-silicon sintered soft-magnetic parts of good quality in high yield by mixing an iron powder and an ion-silicon powder each having a specific grain size, forming the resulting mixture into a green compact and sintering it. CONSTITUTION:At first, the iron powder with a grain size of -100-+325mesh and the iron-silicon powder with a grain size of 5-44mu are mixed to form a powdered raw material, in which silicon content is regulated to 10-40wt%. Then the above powdered raw material is compacted to be formed into the green compact of a prescribed shape, which is sintered. In this way, a sintered compact causing no crack initiation and suitable for soft-magnetic parts having a complicated shape, such as head cores for dot printers, can be obtained.

Description

【発明の詳細な説明】 〔発明の技術分野〕 本発明は焼結軟磁性部品の製造方法に関する。[Detailed description of the invention] [Technical field of invention] The present invention relates to a method for manufacturing sintered soft magnetic components.

〔発明の技術的背景とその問題点〕[Technical background of the invention and its problems]

一般に、鉄−けい素合金からなる軟磁性部品は広く用い
られているが、近時、この鉄−けい素軟磁性部品を、粉
末冶金法にょシ焼結品として製造することが検討されて
いる。
In general, soft magnetic parts made of iron-silicon alloys are widely used, but recently, it has been considered to manufacture these iron-silicon soft magnetic parts as sintered products using powder metallurgy. .

そして、この鉄−けい素糸の焼結軟磁性部品を製造する
場合には、鉄粉と、鉄−けい素合金粉(母合金粉)とを
混合してなる原料粉末を用いる方法、いわゆる母合金法
を採用することが考えられている。このような母合金法
は、原料粉末として鉄−けい素の合金粉末を用いる合金
法に比して、粉末が軟らかく、粉末を加圧成形する時の
成形密度が大きく、浸れた磁気特性を有する軟磁性部品
を粉末冶金法で製造する上で大変有利である。
When producing sintered soft magnetic parts of iron-silicon yarn, a method using a raw material powder made by mixing iron powder and iron-silicon alloy powder (master alloy powder), the so-called master alloy powder, is used. Consideration is being given to adopting the alloy method. Compared to the alloying method that uses iron-silicon alloy powder as the raw material powder, such a master alloy method produces softer powder, a higher compaction density when the powder is pressure-molded, and has immersed magnetic properties. This is very advantageous in manufacturing soft magnetic parts using powder metallurgy.

しかして、この母合金法によシ鉄−けい素糸焼結軟磁性
部品ヲ徊造する方法では、粒度が一100メツシ:L(
mesh )の7トマイズ鉄粉と、粒度が一350メッ
シェの鉄−けい紫合金粉とを組合せた原料粉末を用いて
いる。
However, in the method of manufacturing iron-silicon yarn sintered soft magnetic parts using this master alloy method, the particle size is 1100 mesh: L (
The raw material powder is a combination of 7 tomized iron powder (mesh) and iron-silica alloy powder with a particle size of 1350 mesh.

しかしながら、このような方法によれば、前記の粒度を
もつ鉄粉と鉄−けい素合金粉とを混合してなる原料粉末
を加圧して圧粉体を成形する場合に、加圧されfc原料
粉末に大きなスプリングバックが発生し、これによシ粉
末すなわち圧粉体にクラックが発生し易く、正常な圧粉
体を歩留シ良く成形することが困難であるという問題が
ある。従って、良質な鉄−けい素糸焼結軟磁性部分を歩
留シ良ぐ製造することが難しい。
However, according to such a method, when pressing raw material powder made by mixing iron powder and iron-silicon alloy powder having the above particle size to form a compact, the pressed fc raw material There is a problem in that large springback occurs in the powder, which tends to cause cracks in the powder, that is, the green compact, and that it is difficult to mold a normal green compact with a good yield. Therefore, it is difficult to produce high-quality iron-silicon yarn sintered soft magnetic parts with a good yield.

〔発明の目的〕[Purpose of the invention]

本発明は前記事情に基づいてなされたもので、母合金法
を採用して良質な鉄−けい素糸焼結軟磁性部品を歩留シ
良く得ることができる焼結軟磁性部品の製造方法を提供
することを目的とするものである。
The present invention has been made based on the above-mentioned circumstances, and provides a method for manufacturing sintered soft magnetic parts that can obtain high quality iron-silicon yarn sintered soft magnetic parts with a high yield by adopting the master alloy method. The purpose is to provide

〔発明の概要〕[Summary of the invention]

本発明の焼結軟磁性部品の製造方法は、粒度が−100
ないし+325メツシユの鉄粉と、粒度が5〜44II
の鉄−けい素合金粉とを混合してなる原料粉末を加圧し
て圧粉体を成形し、この圧粉体を焼結して焼結体を得る
ことを特徴とするものである。
In the method for manufacturing sintered soft magnetic parts of the present invention, the particle size is -100
Iron powder of to +325 mesh and particle size of 5 to 44 II
The method is characterized in that a raw material powder prepared by mixing iron-silicon alloy powder is pressed to form a green compact, and this green compact is sintered to obtain a sintered body.

すなわち、本発明の発明者は、圧粉体に発生するスプリ
ングバックは粉末の粒度に影響されることに着目し、種
々研究を重ねた結果、原料粉末を形成する鉄粉と鉄−合
金粉の夫々の粒度を前記した範囲の大きさに設定するこ
とにより。
That is, the inventor of the present invention focused on the fact that the springback that occurs in a green compact is affected by the particle size of the powder, and as a result of various studies, it was found that By setting the respective particle sizes to sizes within the ranges described above.

圧粉体を加圧成形する時に加圧された原料粉末に発生す
るスプリングバックを小さく抑えて、粉末にクラックが
発生することを防止し、よって正常な圧粉体を歩留り良
く加圧成形することができるようにしたものである。
To suppress the springback that occurs in the pressurized raw material powder when press-molding a powder compact, to prevent the generation of cracks in the powder, and to press-form a normal powder compact with a high yield. It was made so that it could be done.

本発明による焼結軟磁性部品の創造方法では、まず粒度
が−100ないし+325メツシユの鉄粉と、粒度が5
μないし44μの鉄−けい素合金粉とを混合して原料粉
末を得る。鉄粉の粒度を前記の範囲の大きさとする理由
は、+ 10100rlsを越える粉末では製品形状で
狭い箇所に充てんされにくく、+ 325 meshと
するのは、Fe −81粉と混合したときの適切粒度分
布を確保するなめである。また、鉄−けい素合金粉の粒
度を前記の範囲の大きさに設定する理由け、44μ以上
では焼結時のF・この反応性が悪く、密度があがらず、
5μ以下では微細すぎて酸化されやすくなるためである
。鉄−けい素合金粉け、重量比でけい素を10〜40優
含むものである。これは44μ以下の粉末を401以下
に抑えるためである。原料粉末における鉄−けい素合金
粉の割合は、重量比で10〜40%とする。この理由は
、101以下では母合金法の効果が少なく、40優を越
えると焼結し念後のStの均質性が悪ぐなシ磁気特性が
劣る。
In the method of creating a sintered soft magnetic component according to the present invention, first, iron powder with a grain size of -100 to +325 mesh and a grain size of 5
A raw material powder is obtained by mixing with iron-silicon alloy powder of μ to 44 μ. The reason why the particle size of the iron powder is set in the above range is that powder exceeding +10100 rls is difficult to fill in a narrow part of the product shape, and +325 mesh is set to have an appropriate particle size when mixed with Fe-81 powder. This is a lick to ensure distribution. In addition, the reason why the particle size of the iron-silicon alloy powder is set within the above range is that if it exceeds 44 μm, the reactivity of F during sintering will be poor and the density will not increase.
This is because if it is less than 5 μm, it will be too fine and will be easily oxidized. Iron-silicon alloy powder, containing 10-40% silicon by weight. This is to suppress the powder size of 44μ or less to 401 or less. The proportion of iron-silicon alloy powder in the raw material powder is 10 to 40% by weight. The reason for this is that if it is less than 101, the effect of the master alloy method is small, and if it exceeds 40, it will sinter, resulting in poor homogeneity of St and poor magnetic properties.

次いで、プレスによシ原料粉末を加圧して所定形状の圧
粉体を成形する。この加圧成形時に、原料粉末を加圧し
念プレス型を引上げた後に原料粉末に発生するスプリン
グバックは小さく、このため加圧され念原料粉末にクラ
ックが発生せず、正常な圧粉体を成形できる。
Next, the raw material powder is pressed by a press to form a compact into a predetermined shape. During this pressure molding, the springback that occurs in the raw material powder after it is pressurized and the pneumatic press mold is pulled up is small, so no cracks occur in the pneumatic raw material powder when it is pressurized, and a normal compact is formed. can.

次いで、圧粉体を焼結して焼結体を形成し、鉄−けい素
糸焼結軟磁性部品を製造する。
Next, the green compact is sintered to form a sintered body, and an iron-silicon yarn sintered soft magnetic component is manufactured.

従って、本発明の創造方法によれば、圧粉体を加圧成形
する時にクラックの発生を防止するので、圧粉体を歩留
り良く成形でき、この圧粉体を用いて良質な鉄−けい素
糸焼結磁性部品を歩留り良く製造できる。
Therefore, according to the creative method of the present invention, since the generation of cracks is prevented when the green compact is pressure-formed, the green compact can be formed with a high yield, and this green compact can be used to produce high-quality iron-silicon. Yarn sintered magnetic parts can be manufactured with high yield.

本発明の製造方法は、軟磁性部品を製造する場合に広く
適用できるが、特にドツトプリンタ用ヘッドコアなどの
複雑な形状をなす軟磁性部品を製造する場合に適してい
る。
The manufacturing method of the present invention can be widely applied to manufacturing soft magnetic parts, but is particularly suitable for manufacturing soft magnetic parts with complicated shapes such as head cores for dot printers.

〔発明の実施例〕[Embodiments of the invention]

次に本発明の実施例について説明する。 Next, examples of the present invention will be described.

重量比で、水アトマイズ鉄粉(粒度−100ないし+3
25メツシz)s21鉄−17%けい素合金粉(粒度−
325メツシユ)18%、潤滑剤1チを40分間混合し
て混合粉(本発明例粉)を作成する。また、水アトマイ
ズ鉄粉(粒度−100メツシエ)82チ、鉄−17%け
い素合金粉(粒度、44μ以下)11%、潤滑剤1チを
40分間混合して混合粉(比較例粉)を作成する。そし
て、各混合粉を6トン/dの成形圧で加圧して、直径4
0a+X厚さllaの形状で圧粉体を成形し、これら圧
粉体のスプリングバックを測定した。その結果、本発明
例粉からなる圧粉体でFiO,2Ls、比較例粉からな
る圧粉体では0.4 %であシ、本発明方法にょれば圧
粉体に発生するスプリングバックを小さく抑制できるこ
とが判る。
Water atomized iron powder (particle size -100 to +3) by weight
25 mesh z) S21 iron-17% silicon alloy powder (particle size -
325 mesh) and 1 g of lubricant were mixed for 40 minutes to prepare a mixed powder (invention example powder). In addition, mixed powder (comparative example powder) was prepared by mixing 82 g of water atomized iron powder (particle size -100 mesh), 11% iron-17% silicon alloy powder (particle size, 44 μ or less), and 1 g of lubricant for 40 minutes. create. Then, each mixed powder was pressurized with a molding pressure of 6 tons/d, and the diameter was 4
Green compacts were molded into a shape of 0a+X thickness lla, and the springback of these green compacts was measured. As a result, it was found that the FiO,2Ls was 0.4% in the powder compact made of the powder of the example of the present invention and 0.4% in the compact of the powder of the comparative example, and the springback occurring in the compact was reduced by the method of the present invention. It turns out that it can be suppressed.

さらに、前記本発明例粉と比較例粉を夫々用いて、第1
図および第2図で示す形状をなし且つ寸法が外径40m
5+X内径30mX高さ115mであるドツトプリンタ
用へラドヨークコア1を加圧成形すると、本発明例粉を
用いた場合には正常に成形できたが、比較例粉を用いた
場合には、ヨークコア1における吸着部の根元にクラッ
クを生じて成形が行なえなかった。
Furthermore, using the powder of the example of the present invention and the powder of the comparative example, the first
It has the shape shown in Figures and Figure 2 and has an outer diameter of 40 m.
When rad yoke core 1 for dot printers with 5+X inner diameter 30 m x height 115 m was pressure molded, the molding could be performed normally when using the powder of the example of the present invention, but when the powder of the comparative example was used, the adsorption in the yoke core 1 Molding could not be carried out due to cracks occurring at the base of the part.

〔発明の効果〕〔Effect of the invention〕

以上説明したように本発明の焼結軟磁性部品の製造方法
によれば、鉄粉と鉄−けい素合金粉とを混合してなる原
料粉末を加圧して、クラックの発生がない正常な圧粉体
を成形でき、従って良質な鉄−けい素糸焼結軟磁性部品
を歩留シ良く製造できる。
As explained above, according to the method for manufacturing sintered soft magnetic parts of the present invention, raw material powder made of a mixture of iron powder and iron-silicon alloy powder is pressurized to a normal pressure without cracking. Powder can be molded, and therefore high-quality iron-silicon yarn sintered soft magnetic parts can be manufactured with good yield.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図および第2図は焼結軟磁性部品の一例であるドツ
トプリンタ用へラドヨークコアを示す正面図および断面
図である。 I・・・ヘッドヨークコア。 出願人代理人  弁理士 鈴 江 武 彦第2国
FIGS. 1 and 2 are a front view and a sectional view showing a hard yoke core for a dot printer, which is an example of a sintered soft magnetic component. I...Head yoke core. Applicant's agent Patent attorney Takehiko Suzue Second country

Claims (2)

【特許請求の範囲】[Claims] (1)粒度が−100ないし+325メッシュの鉄粉と
、粒度が5〜44μの鉄−けい素合金粉とを混合してな
る原料粉末を加圧して圧粉体を成形し、この圧粉体を焼
結して焼結体を得ることを特徴とする焼結軟磁性部品の
製造方法。
(1) A raw material powder made by mixing iron powder with a particle size of -100 to +325 mesh and iron-silicon alloy powder with a particle size of 5 to 44μ is pressed to form a green compact, and this green compact is 1. A method for producing a sintered soft magnetic component, the method comprising obtaining a sintered body by sintering.
(2)原料粉末における鉄−けい素合金粉の割合は重量
比で10〜40%である特許請求の範囲第1項に記載の
焼結軟磁性部品の製造方法。
(2) The method for manufacturing a sintered soft magnetic component according to claim 1, wherein the proportion of iron-silicon alloy powder in the raw material powder is 10 to 40% by weight.
JP16805985A 1985-07-30 1985-07-30 Manufacture of sintered soft-magnetic parts Pending JPS6227545A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16805985A JPS6227545A (en) 1985-07-30 1985-07-30 Manufacture of sintered soft-magnetic parts

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16805985A JPS6227545A (en) 1985-07-30 1985-07-30 Manufacture of sintered soft-magnetic parts

Publications (1)

Publication Number Publication Date
JPS6227545A true JPS6227545A (en) 1987-02-05

Family

ID=15861062

Family Applications (1)

Application Number Title Priority Date Filing Date
JP16805985A Pending JPS6227545A (en) 1985-07-30 1985-07-30 Manufacture of sintered soft-magnetic parts

Country Status (1)

Country Link
JP (1) JPS6227545A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01136308A (en) * 1987-11-24 1989-05-29 Daido Steel Co Ltd Sintered body of magnetic alloy and manufacturing thereof
JPH01136307A (en) * 1987-11-24 1989-05-29 Daido Steel Co Ltd Powdered magnetic alloy for sintering
EP1734141A1 (en) * 2004-03-29 2006-12-20 Hitachi Powdered Metals Co., Ltd. Sintered soft magnetic member and method for manufacture thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01136308A (en) * 1987-11-24 1989-05-29 Daido Steel Co Ltd Sintered body of magnetic alloy and manufacturing thereof
JPH01136307A (en) * 1987-11-24 1989-05-29 Daido Steel Co Ltd Powdered magnetic alloy for sintering
EP1734141A1 (en) * 2004-03-29 2006-12-20 Hitachi Powdered Metals Co., Ltd. Sintered soft magnetic member and method for manufacture thereof
EP1734141A4 (en) * 2004-03-29 2007-10-10 Hitachi Powdered Metals Sintered soft magnetic member and method for manufacture thereof
US7470332B2 (en) 2004-03-29 2008-12-30 Hitachi Powdered Metals Co., Ltd. Production method for soft magnetic sintered member

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