JPS62252307A - 水酸アパタイトを湿式合成する方法 - Google Patents
水酸アパタイトを湿式合成する方法Info
- Publication number
- JPS62252307A JPS62252307A JP9463486A JP9463486A JPS62252307A JP S62252307 A JPS62252307 A JP S62252307A JP 9463486 A JP9463486 A JP 9463486A JP 9463486 A JP9463486 A JP 9463486A JP S62252307 A JPS62252307 A JP S62252307A
- Authority
- JP
- Japan
- Prior art keywords
- phosphoric acid
- calcium
- hydroxyapatite
- calcium hydroxide
- suspension
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052588 hydroxylapatite Inorganic materials 0.000 title claims abstract description 22
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 title claims abstract description 22
- 230000015572 biosynthetic process Effects 0.000 title claims 4
- 238000003786 synthesis reaction Methods 0.000 title claims 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims abstract description 38
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims abstract description 19
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 13
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 13
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 10
- 238000006243 chemical reaction Methods 0.000 claims abstract description 10
- 239000002244 precipitate Substances 0.000 claims abstract description 7
- 239000000725 suspension Substances 0.000 claims abstract description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 5
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000292 calcium oxide Substances 0.000 claims abstract description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims abstract 3
- 238000000034 method Methods 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 13
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 230000000887 hydrating effect Effects 0.000 claims description 2
- 239000011575 calcium Substances 0.000 abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 abstract description 2
- 238000003756 stirring Methods 0.000 abstract description 2
- 239000002245 particle Substances 0.000 abstract 2
- 239000012895 dilution Substances 0.000 abstract 1
- 238000010790 dilution Methods 0.000 abstract 1
- 238000002441 X-ray diffraction Methods 0.000 description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 6
- 229910052791 calcium Inorganic materials 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 239000001506 calcium phosphate Substances 0.000 description 5
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 5
- 229910000389 calcium phosphate Inorganic materials 0.000 description 3
- 235000011010 calcium phosphates Nutrition 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000012258 stirred mixture Substances 0.000 description 3
- 102100036850 C-C motif chemokine 23 Human genes 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 101000713081 Homo sapiens C-C motif chemokine 23 Proteins 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001308 synthesis method Methods 0.000 description 2
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 2
- 235000019731 tricalcium phosphate Nutrition 0.000 description 2
- 229940078499 tricalcium phosphate Drugs 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229910052586 apatite Inorganic materials 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000000635 electron micrograph Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- VSIIXMUUUJUKCM-UHFFFAOYSA-D pentacalcium;fluoride;triphosphate Chemical compound [F-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O VSIIXMUUUJUKCM-UHFFFAOYSA-D 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Dental Preparations (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9463486A JPS62252307A (ja) | 1986-04-25 | 1986-04-25 | 水酸アパタイトを湿式合成する方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9463486A JPS62252307A (ja) | 1986-04-25 | 1986-04-25 | 水酸アパタイトを湿式合成する方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62252307A true JPS62252307A (ja) | 1987-11-04 |
| JPH0461807B2 JPH0461807B2 (enrdf_load_stackoverflow) | 1992-10-02 |
Family
ID=14115697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9463486A Granted JPS62252307A (ja) | 1986-04-25 | 1986-04-25 | 水酸アパタイトを湿式合成する方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62252307A (enrdf_load_stackoverflow) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01168872A (ja) * | 1987-12-23 | 1989-07-04 | Sumitomo Chem Co Ltd | ヒドロキシアパタイト皮膜の形成方法 |
| JP2013513703A (ja) * | 2009-12-11 | 2013-04-22 | ラティテュード・１８，インコーポレイテッド | 無機リン酸塩組成物および方法 |
| JP2014509294A (ja) * | 2011-01-27 | 2014-04-17 | シリム バーハド | 石灰石をリン酸三カルシウム及びリン酸テトラカルシウム粉末に同時に転化する方法 |
| US10422041B2 (en) | 2009-12-18 | 2019-09-24 | Latitude 18, Inc | Inorganic phosphate corrosion resistant coatings |
| WO2023209788A1 (ja) * | 2022-04-26 | 2023-11-02 | ブレイニー株式会社 | 抗菌性金属含有ハイドロキシアパタイトの作製装置及び方法 |
| JP2024012323A (ja) * | 2022-04-26 | 2024-01-30 | ブレイニー株式会社 | 抗菌性金属含有ハイドロキシアパタイトの作製装置 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5645814A (en) * | 1979-09-25 | 1981-04-25 | Kureha Chem Ind Co Ltd | Hydroxyapatite, its ceramic material and its manufacture |
-
1986
- 1986-04-25 JP JP9463486A patent/JPS62252307A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5645814A (en) * | 1979-09-25 | 1981-04-25 | Kureha Chem Ind Co Ltd | Hydroxyapatite, its ceramic material and its manufacture |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01168872A (ja) * | 1987-12-23 | 1989-07-04 | Sumitomo Chem Co Ltd | ヒドロキシアパタイト皮膜の形成方法 |
| JP2013513703A (ja) * | 2009-12-11 | 2013-04-22 | ラティテュード・１８，インコーポレイテッド | 無機リン酸塩組成物および方法 |
| US10422041B2 (en) | 2009-12-18 | 2019-09-24 | Latitude 18, Inc | Inorganic phosphate corrosion resistant coatings |
| JP2014509294A (ja) * | 2011-01-27 | 2014-04-17 | シリム バーハド | 石灰石をリン酸三カルシウム及びリン酸テトラカルシウム粉末に同時に転化する方法 |
| WO2023209788A1 (ja) * | 2022-04-26 | 2023-11-02 | ブレイニー株式会社 | 抗菌性金属含有ハイドロキシアパタイトの作製装置及び方法 |
| JPWO2023209788A1 (enrdf_load_stackoverflow) * | 2022-04-26 | 2023-11-02 | ||
| JP2024012323A (ja) * | 2022-04-26 | 2024-01-30 | ブレイニー株式会社 | 抗菌性金属含有ハイドロキシアパタイトの作製装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0461807B2 (enrdf_load_stackoverflow) | 1992-10-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |