JPS6223989B2 - - Google Patents
Info
- Publication number
- JPS6223989B2 JPS6223989B2 JP56195143A JP19514381A JPS6223989B2 JP S6223989 B2 JPS6223989 B2 JP S6223989B2 JP 56195143 A JP56195143 A JP 56195143A JP 19514381 A JP19514381 A JP 19514381A JP S6223989 B2 JPS6223989 B2 JP S6223989B2
- Authority
- JP
- Japan
- Prior art keywords
- slurry
- titanium dioxide
- pigment
- surface treatment
- dispersant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 50
- 239000002002 slurry Substances 0.000 claims description 38
- 239000004408 titanium dioxide Substances 0.000 claims description 22
- 239000002270 dispersing agent Substances 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000007730 finishing process Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 238000000034 method Methods 0.000 description 24
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 17
- 239000000049 pigment Substances 0.000 description 14
- 229910010413 TiO 2 Inorganic materials 0.000 description 10
- 239000002893 slag Substances 0.000 description 10
- 230000032683 aging Effects 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 239000012756 surface treatment agent Substances 0.000 description 7
- 238000001238 wet grinding Methods 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 230000018044 dehydration Effects 0.000 description 5
- 238000006297 dehydration reaction Methods 0.000 description 5
- 238000004381 surface treatment Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 239000011324 bead Substances 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 239000012065 filter cake Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003973 paint Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 239000004576 sand Substances 0.000 description 3
- 235000019832 sodium triphosphate Nutrition 0.000 description 3
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 239000000976 ink Substances 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 239000011164 primary particle Substances 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 2
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 229960004029 silicic acid Drugs 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 238000009283 thermal hydrolysis Methods 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
- JUWGUJSXVOBPHP-UHFFFAOYSA-B titanium(4+);tetraphosphate Chemical compound [Ti+4].[Ti+4].[Ti+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O JUWGUJSXVOBPHP-UHFFFAOYSA-B 0.000 description 1
Landscapes
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP19514381A JPS5899121A (ja) | 1981-12-04 | 1981-12-04 | 二酸化チタンスラリ−の製造法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP19514381A JPS5899121A (ja) | 1981-12-04 | 1981-12-04 | 二酸化チタンスラリ−の製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5899121A JPS5899121A (ja) | 1983-06-13 |
JPS6223989B2 true JPS6223989B2 (es) | 1987-05-26 |
Family
ID=16336153
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP19514381A Granted JPS5899121A (ja) | 1981-12-04 | 1981-12-04 | 二酸化チタンスラリ−の製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5899121A (es) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0566112U (ja) * | 1992-02-17 | 1993-08-31 | 公成商事株式会社 | 可動式間仕切構造 |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3411759C1 (de) * | 1984-03-30 | 1985-04-25 | Th. Goldschmidt Ag, 4300 Essen | An ihrer Oberflaeche durch hydrophile und hydrophobe Gruppen modifizierte Teilchen |
US4801509A (en) * | 1985-07-05 | 1989-01-31 | Mitsubishi Paper Mills, Ltd. | Photographic resin coated paper |
US5356470A (en) * | 1990-06-25 | 1994-10-18 | E. I. Du Pont De Nemours And Company | Media milling pigment slurries to eliminate or reduce oversize particles |
US5501732A (en) * | 1994-02-28 | 1996-03-26 | E. I. Du Pont De Nemours And Company | Process for preparing silanized TiO2 pigments using a media mill |
US5653793A (en) * | 1995-08-01 | 1997-08-05 | E. I. Du Pont De Nemours And Company | TiO2 slurry process |
DE19536657A1 (de) * | 1995-09-30 | 1997-04-10 | Metallgesellschaft Ag | Verfahren zur Herstellung von Ti0¶2¶-Pigmenten aus Ti0¶2¶-Klinker |
US5908498A (en) * | 1996-02-16 | 1999-06-01 | Kerr-Mcgee Chemical Llc | Process for preparing an improved low-dusting, free-flowing pigment |
WO1997030127A1 (en) * | 1996-02-16 | 1997-08-21 | Kerr-Mcgee Chemical Corporation | Process for preparing an improved low-dusting, free-flowing pigment |
JP2003342528A (ja) * | 2002-05-27 | 2003-12-03 | Kikusui Chemical Industries Co Ltd | スラリー原料を利用した水系塗料の製造方法 |
DE10236366A1 (de) * | 2002-08-08 | 2004-02-19 | Kronos International, Inc. | Verfahren zur Oberflächenbehandlung eines Titandioxid-Pigments |
WO2013062781A1 (en) * | 2011-10-28 | 2013-05-02 | E. I. Du Pont De Nemours And Company | Treated inorganic pigments having improved dispersability and use thereof in coating compositions |
CN104828861B (zh) * | 2015-05-13 | 2016-11-09 | 攀枝花学院 | 一种工业偏钛酸粒度分级生产颜料钛白的方法 |
EP3199595A1 (de) * | 2016-01-27 | 2017-08-02 | Kronos International, Inc. | Herstellung von titandioxidpigment nach dem sulfatverfahren mit enger partikelgrössenverteilung |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3702773A (en) * | 1971-07-21 | 1972-11-14 | Du Pont | Alkanolamine stabilized high solids titanium dioxide slurry |
-
1981
- 1981-12-04 JP JP19514381A patent/JPS5899121A/ja active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3702773A (en) * | 1971-07-21 | 1972-11-14 | Du Pont | Alkanolamine stabilized high solids titanium dioxide slurry |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0566112U (ja) * | 1992-02-17 | 1993-08-31 | 公成商事株式会社 | 可動式間仕切構造 |
Also Published As
Publication number | Publication date |
---|---|
JPS5899121A (ja) | 1983-06-13 |
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