JPS621168B2 - - Google Patents

Info

Publication number
JPS621168B2
JPS621168B2 JP13019280A JP13019280A JPS621168B2 JP S621168 B2 JPS621168 B2 JP S621168B2 JP 13019280 A JP13019280 A JP 13019280A JP 13019280 A JP13019280 A JP 13019280A JP S621168 B2 JPS621168 B2 JP S621168B2
Authority
JP
Japan
Prior art keywords
furnace body
crucible
melting
rotating container
lower furnace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP13019280A
Other languages
Japanese (ja)
Other versions
JPS5755389A (en
Inventor
Katsuyuki Ootsuka
Ryukichi Mizuno
Katsumi Kuwana
Masahisa Sawada
Fumiaki Komatsu
Atsushi Takusagawa
Takayoshi Masaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Doryokuro Kakunenryo Kaihatsu Jigyodan
Kobe Steel Ltd
Original Assignee
Doryokuro Kakunenryo Kaihatsu Jigyodan
Kobe Steel Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Doryokuro Kakunenryo Kaihatsu Jigyodan, Kobe Steel Ltd filed Critical Doryokuro Kakunenryo Kaihatsu Jigyodan
Priority to JP13019280A priority Critical patent/JPS5755389A/en
Publication of JPS5755389A publication Critical patent/JPS5755389A/en
Publication of JPS621168B2 publication Critical patent/JPS621168B2/ja
Granted legal-status Critical Current

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  • Gasification And Melting Of Waste (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)
  • Furnace Details (AREA)
  • Constitution Of High-Frequency Heating (AREA)

Description

【発明の詳細な説明】 本発明は、バツチ溶解式マイクロ波溶解炉の改
良に関する。さらに詳しくは、本発明は被処理物
の加熱溶解を効率良くかつ円滑に行なえるように
したバツチ溶解式マイクロ波溶解炉に関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to improvements in batch melting type microwave melting furnaces. More specifically, the present invention relates to a batch melting type microwave melting furnace that can efficiently and smoothly heat and melt materials to be processed.

マイクロ波照射により生起する誘電加熱現象を
利用した各種物質の加熱溶融法は、幅射熱や伝熱
による加熱などの他の形式にくらべ、被処理物の
均一かつ効率良い加熱溶融が可能であり、またマ
イクロ波印加電力の調整により、緩急任意の溶融
処理を行なうことができる利点を有する。
The method of heating and melting various substances that utilizes the dielectric heating phenomenon caused by microwave irradiation enables uniform and efficient heating and melting of the processed material compared to other methods such as heating by radiation heat or heat transfer. Moreover, it has the advantage that melting can be performed at any speed or speed by adjusting the power applied to the microwave.

このマイクロ波照射による加熱溶融の原理は、
各種分野においてさまざまな目的に利用すること
ができる。例えば、各種産業施設からスラリー等
として排出される廃棄物に対し、マイクロ波照射
による乾燥あるいは溶融固化処理を施せば、その
容積を大幅に減少させることができ、爾後の処理
に好都合である。また、原子力施設から排出され
る放射性物質含有廃棄物は、回収後、人間環境か
ら隔離し、格納施設に長期間貯蔵しておく必要が
あるため、貯蔵に先立つてマイクロ波照射により
溶融固化する「減容処理」を施せば、貯蔵容器個
数・格納施設スペース等の節減、収容能力の増
大、取扱作業量の減少等をもたらし、経済的にも
極めて有利である。
The principle of heating and melting by microwave irradiation is as follows:
It can be used for various purposes in various fields. For example, if waste discharged as slurry or the like from various industrial facilities is subjected to drying or melt-solidification treatment by microwave irradiation, its volume can be significantly reduced, which is convenient for subsequent processing. In addition, waste containing radioactive materials discharged from nuclear facilities must be isolated from the human environment and stored in a containment facility for a long period of time after collection. If "volume reduction treatment" is applied, it will reduce the number of storage containers and storage facility space, increase storage capacity, reduce the amount of handling work, etc., and is extremely advantageous economically.

本発明は、上記のごときマイクロ波加熱溶解処
理の工業的実用化のための新規溶解炉を提供する
ものであり、本発明者らが先に発明した溶解炉
(特許願昭和54−49599号を参照)の改良に関す
る。特許願昭和54−49599号には、ルツボ内に装
入された被処理物にマイクロ波を照射して該被処
理物を加熱溶解するマイクロ波溶解炉であつて、
マイクロ波発振機に連結された導波管およびチユ
ーナならびに被処理物供給管を備えかつ支持体に
固定された上部炉体と、底部に垂直方向の軸芯を
有する回転台を備え該回転台に溶解用ルツボを載
置するようにした下部炉体とから成り、さらに該
下部炉体を前記上部炉体に着脱可能なようにし、
あるいはさらに下部炉体に不活性ガス導入管を備
え該不活性ガス導入管から供給される不活性ガス
にて前記下部炉体内壁とルツボとの間の圧力を炉
内圧に対して正圧とすることを特徴とするバツチ
溶解式マイクロ波溶解炉が開示されている。上記
発明は、このような構成を有するため、溶解用ル
ツボが炉内で回転し、被処理物に対し照射が均一
に施される結果、被処理物の加熱溶解が効率よく
円滑に行なわれ、また炉内を不活性ガス雰囲気に
できるため、溶融固体化の化学的・物理的諸性質
に対する要求により被処理物と炉内雰囲気との反
応を防止することが必要な場合はこれが可能とな
り、さらにルツボ自体の酸化損耗を軽減する効果
も得られる。
The present invention provides a new melting furnace for the industrial practical application of microwave heating melting treatment as described above, and is based on the melting furnace previously invented by the present inventors (Patent Application No. 1983-49599). (Reference) related to improvements. Patent application No. 1987-49599 discloses a microwave melting furnace that heats and melts a workpiece charged in a crucible by irradiating microwaves to the workpiece,
An upper furnace body is provided with a waveguide and a tuner connected to a microwave oscillator, and a processing material supply pipe and fixed to a support, and a rotary table having a vertical axis at the bottom. a lower furnace body on which a melting crucible is mounted, and the lower furnace body is detachably attached to the upper furnace body,
Alternatively, the lower furnace body is further provided with an inert gas introduction pipe, and the inert gas supplied from the inert gas introduction pipe is used to make the pressure between the inner wall of the lower furnace body and the crucible positive with respect to the pressure inside the furnace. A batch melting type microwave melting furnace is disclosed. Since the above invention has such a configuration, the melting crucible rotates in the furnace and irradiation is uniformly applied to the workpiece, so that the workpiece can be heated and melted efficiently and smoothly. In addition, since the inside of the furnace can be made into an inert gas atmosphere, it is possible to prevent reactions between the processed material and the atmosphere inside the furnace due to the chemical and physical properties required for melting and solidification. The effect of reducing oxidative wear and tear on the crucible itself can also be obtained.

しかし上記発明においても1局部加熱などによ
りルツボに穴があき溶融した被処理物が流出して
回転台上で固化しルツボの取出しを不能とした
り、さらに流出物が回転軸芯にまで達して回転を
不能とする可能性が皆無ではないこと、2回転台
上のルツボが熱膨張により上方に伸びても上部炉
体と接触しないよう相当の間隙を設ける必要があ
り、マイクロ波の漏洩がなお存在すること、さら
に3回転台上に載置されたルツボの底面は不活性
ガスと接触不良で酸化しやすいなどの問題が残
る。
However, even in the above invention, a hole is made in the crucible due to local heating, etc., and the molten material to be processed flows out and solidifies on the rotating table, making it impossible to take out the crucible. However, even if the crucible on the two-turn table extends upward due to thermal expansion, it is necessary to provide a considerable gap so that it does not come into contact with the upper furnace body, and microwave leakage still exists. In addition, there remain problems such as the bottom surface of the crucible placed on the three-turn table being susceptible to oxidation due to poor contact with the inert gas.

本発明は、内部に懸垂収納されるルツボを有し
かつ軸芯と着脱可能に係合する回転容器を下部炉
体内に備えることを基本として前記問題点を解決
しうるマイクロ波溶解炉の提供を目的とする。
The present invention provides a microwave melting furnace which can solve the above-mentioned problems by basically equipping the lower furnace body with a rotary container which has a crucible suspended therein and which is removably engaged with the shaft core. purpose.

以下本発明の一実施例を図面により説明する。 An embodiment of the present invention will be described below with reference to the drawings.

第1図に示すように、本発明の溶解炉は、上部
炉体1と下部炉体2とからなり、両者合して溶解
炉本体を構成する。各炉体の外周部には、炉体冷
却手段として冷媒配管(図示せず)が配設され
る。該上部炉体1は、マイクロ波導波管3、チユ
ーナ4、および被処理物供給管5を備えるととも
に、支持体6にて下部炉体2とは独立に固定され
る。チユーナ4は、駆動用モータm1によつてベ
ベルギヤ噛咬機構20を介して炉内における高さ
方向の位置調節がなされる。なお、本実施例にお
いては該上部炉体1には、溶解炉内で発生するダ
ストやヒユーム等のマイクロ波照射効率に有害な
浮遊物を炉外に排除するための排気管7が設けら
れている。一方、下部炉体2は、支腕11を介し
て保持機10により、前記上部炉体1に対して着
脱可能に保持される。該保持機10は、モータ
m2を備えた回転機構部10aと油圧により伸縮
するシリンダ(図示せず)を備えたリフト機構部
10bとからなり、該回転機構部10aは、第1
図1(図中、保持機10はA−A断面を示す)に
示されるようにモータm2により駆動されるギヤ
23を備え、支腕11を側設した支軸21に固着
されたギヤ22に噛合する。したがつて、モータ
m2の駆動により支腕11を支軸21を中心とし
て水平面内で回動させることにより、下部炉体2
を上部炉体1から2′の位置まで退避させ得る。
前記下部炉体2は、第2図に示すごとく、下部炉
体本体21と、これに回転自在に収納される回転
容器12と、さらに該回転容器12とともにこれ
に収納されて回転するルツボ8を備える。下部炉
体本体21の周壁は、外壁21aと内壁21bと
から成る二重構造を有し、外壁21aと内壁21
bの間隙および内壁21bの内面には断熱材13
aおよび13b(例えばカオール)がそれぞれ設
けられている。一方、下部炉体底面21cは略円
盤状をなし、中央の軸受21dの周辺に環状突起
21eが突設される。回転容器12は、略円筒状
をなし、周壁12a上部より外方へ断面L字状に
突出した外縁12bと、底面12cより垂設さ
れ、前記下部炉体底面21cの環状突起21eと
組合わされてマイクロ波の漏洩を防止しうるチヨ
ーク回路を形成する環状垂壁12dと、駆動装置
(図示せず)より前記軸受21dを貫通して下部
炉体2内方へ伸び回転容器12中央の透孔12e
に対接し螺着されアルゴン、窒素等の不活性ガス
導入管15を兼ねる中空の軸芯14とを備える。
なお、回転容器12の底面には断熱材13c(例
えばアルミナブロツク或いは繊維状のカオール)
が敷設され、該断熱材の中心部には、前記不活性
ガスが通過しやすいように開孔等を設けることが
望ましい。また回転容器12の周壁12aの上端
近傍には、不活性ガスを通す複数の透孔を設けて
も良い。ルツボ8は、回転容器12の内径よりや
や小さな外径と回転容器12の内部深さよりやや
浅い深さを有するルツボ本体8aおよびルツボ本
体8a上縁より断面L字状に外方へ突出し回転容
器周壁12aと略同径を有する張出部8bを具備
し、該張出部8b下部が回転容器周壁12aの上
端にて支持されて回転容器12内部に懸垂状態に
て収納される。なお、張出部8bは上部炉体1下
面に設けた環状溝1aと組み合わせてチヨーク回
路を形成してマイクロ波の漏洩による回転容器の
焼付きを防止する。なお、溶解用ルツボとしては
ステンレス鋼などの金属製あるいはカーボン材質
(黒鉛製)のものが挙げられるが、好ましくは金
属製ルツボが用いられ、被処理物の融点が高い場
合には、ルツボ内面に、例えばアルミナセメント
などの高融点断熱性物質の層をコーテイングした
ものを用いることができる。
As shown in FIG. 1, the melting furnace of the present invention consists of an upper furnace body 1 and a lower furnace body 2, which together constitute a melting furnace body. A refrigerant pipe (not shown) is provided around the outer periphery of each furnace body as a means for cooling the furnace body. The upper furnace body 1 includes a microwave waveguide 3, a tuner 4, and a processing material supply pipe 5, and is fixed independently of the lower furnace body 2 with a support 6. The tuner 4 is adjusted in position in the height direction in the furnace by the drive motor m 1 via the bevel gear engagement mechanism 20 . In this embodiment, the upper furnace body 1 is provided with an exhaust pipe 7 for removing floating substances such as dust and fumes generated in the melting furnace that are harmful to the efficiency of microwave irradiation from the furnace. There is. On the other hand, the lower furnace body 2 is detachably held with respect to the upper furnace body 1 by a holding device 10 via a support arm 11 . The holding machine 10 includes a motor
m2 , and a lift mechanism section 10b equipped with a cylinder (not shown) that expands and contracts with hydraulic pressure.
As shown in FIG. 1 (in the drawing, the holder 10 shows the A-A cross section), the gear 22 is equipped with a gear 23 driven by a motor m 2 and fixed to a support shaft 21 with a support arm 11 on the side. mesh with. Therefore, the motor
By rotating the support arm 11 in a horizontal plane around the support shaft 21 by driving the lower furnace body 2
can be retracted from the upper furnace body 1 to the position 2'.
As shown in FIG. 2, the lower furnace body 2 includes a lower furnace body 21, a rotary container 12 that is rotatably housed in the lower furnace body, and a crucible 8 that is housed in the rotary vessel 12 and rotates. Be prepared. The peripheral wall of the lower furnace main body 21 has a double structure consisting of an outer wall 21a and an inner wall 21b.
A heat insulating material 13 is provided in the gap b and the inner surface of the inner wall 21b.
a and 13b (eg, caol) are provided, respectively. On the other hand, the bottom surface 21c of the lower furnace body has a substantially disk shape, and an annular protrusion 21e protrudes around the central bearing 21d. The rotating container 12 has a substantially cylindrical shape, has an outer edge 12b projecting outward from the upper part of the peripheral wall 12a in an L-shaped cross section, and is suspended from the bottom surface 12c, and is combined with an annular protrusion 21e on the bottom surface 21c of the lower furnace body. An annular hanging wall 12d forming a chiyoke circuit that can prevent leakage of microwaves, and a through hole 12e in the center of the rotating container 12 extending from a drive device (not shown) through the bearing 21d and extending inward to the lower furnace body 2.
It is provided with a hollow shaft core 14 which is screwed against the shaft core 14 and also serves as an inert gas introduction pipe 15 such as argon or nitrogen.
Note that a heat insulating material 13c (for example, alumina block or fibrous carbon) is provided on the bottom of the rotating container 12.
It is desirable that a hole be provided in the center of the heat insulating material so that the inert gas can easily pass through. Further, near the upper end of the peripheral wall 12a of the rotating container 12, a plurality of through holes may be provided to allow inert gas to pass therethrough. The crucible 8 has an outer diameter slightly smaller than the inner diameter of the rotating container 12 and a depth slightly shallower than the internal depth of the rotating container 12, and a crucible body 8a that protrudes outward from the upper edge of the crucible main body 8a in an L-shaped cross section and extends from the rotating container peripheral wall. The lower part of the projecting part 8b is supported by the upper end of the rotating container peripheral wall 12a and is housed in the rotating container 12 in a suspended state. The projecting portion 8b is combined with the annular groove 1a provided on the lower surface of the upper furnace body 1 to form a chi-yoke circuit to prevent seizure of the rotating container due to leakage of microwaves. The melting crucible may be made of metal such as stainless steel or carbon material (graphite), but preferably a metal crucible is used, and if the melting point of the material to be processed is high, the inner surface of the crucible may be For example, a material coated with a layer of a high melting point insulating material such as alumina cement can be used.

しかして、本発明の溶解炉により溶解処理を行
なうには、まず回転容器12を軸芯14に螺着固
定して下部炉体2内に収納し、つぎにルツボ8を
回転容器12内に懸垂収納したのち、該下部炉体
2を保持機10の回転操作および昇降操作にて上
部炉体1に装着する。次に不活性ガスを軸芯14
を通じて回転容器12内に導入する。該不活性ガ
スは、例えば断熱材13cがアルミナブロツクの
場合は該断熱材と回転容器12との境界部を通し
て、繊維状のカオールの場合は該断熱材内部を通
して回転容器12に導入されるが、断熱材中心部
の開孔を通して導入しても良い。ついで、前記不
活性ガスは、回転容器12とルツボ8の接触部を
通して、前記環状溝に導入される。また、回転容
器12の周壁12aの上端近傍に設けた複数の透
孔を通して不活性ガスを導入しても良い。このよ
うにして、ルツボ8と回転容器12の間隙、ルツ
ボ8内、下部炉体2内面を不活性ガス雰囲気とし
たのち、被処理物を供給管5よりルツボ8内へ導
入する。チユーナ4を駆動用モータm1によつて
位置調節し、マイクロ波発振機(図示せず)から
導波管3を経て炉内にマイクロ波を導き、回転容
器12とともにルツボ8を回転させつつ被処理物
の照射を行なう。発生するダストやヒユームは不
活性ガスとともに排気管7より排出される。
Therefore, in order to perform a melting process using the melting furnace of the present invention, the rotating container 12 is first screwed and fixed to the shaft core 14 and housed in the lower furnace body 2, and then the crucible 8 is suspended in the rotating container 12. After storing, the lower furnace body 2 is attached to the upper furnace body 1 by rotating and raising/lowering the holding machine 10. Next, inert gas is applied to the shaft core 14.
is introduced into the rotating container 12 through. The inert gas is introduced into the rotating container 12 through the boundary between the heat insulating material and the rotating container 12 when the heat insulating material 13c is an alumina block, or through the inside of the heat insulating material when the heat insulating material 13c is made of fibrous carbon. It may also be introduced through an opening in the center of the insulation material. The inert gas is then introduced into the annular groove through the contact between the rotating container 12 and the crucible 8. Alternatively, the inert gas may be introduced through a plurality of through holes provided near the upper end of the peripheral wall 12a of the rotating container 12. In this way, the gap between the crucible 8 and the rotating container 12, the inside of the crucible 8, and the inner surface of the lower furnace body 2 are made into an inert gas atmosphere, and then the object to be treated is introduced into the crucible 8 through the supply pipe 5. The position of the tuner 4 is adjusted by the driving motor m1 , and microwaves are guided into the furnace from a microwave oscillator (not shown) through the waveguide 3, and the crucible 8 is rotated together with the rotary container 12. The object to be treated is irradiated. The generated dust and fumes are discharged from the exhaust pipe 7 together with the inert gas.

従つて、本発明のマイクロ波溶解炉によれば、
回転軸芯に対して着脱可能な回転容器を有するた
め、万一、局部加熱によりルツボに穴があき、溶
融物が流出しても軸芯にまで達せず回転容器内に
留まり、ルツボを回転容器とともに取りはずせば
良く稼動率の低下をおこすことがない。また、ル
ツボは上縁の張出部により回転容器上端に懸垂支
持されるので、溶解中の熱による上方への膨張が
ほとんどなく、したがつて、ルツボと上部炉体と
の間隙(前記実施例においてはチヨーク回路を形
成する)を極めて小さくでき、マイクロ波の漏洩
を確実に防止して回転容器の焼付を防止し得る。
さらに、ルツボが懸垂支持されているので、ルツ
ボ底面をはじめ全面が不活性ガス雰囲気となり酸
化損耗が防止されうる。
Therefore, according to the microwave melting furnace of the present invention,
Since it has a rotating container that can be attached to and removed from the rotating shaft core, even if a hole is made in the crucible due to local heating and the melt flows out, it will not reach the shaft core and will remain within the rotating container. It can be removed together with the holder without reducing the operating rate. In addition, since the crucible is suspended and supported on the upper end of the rotating container by the overhanging part of the upper edge, there is almost no upward expansion due to heat during melting. In this case, it is possible to make the circuit (which forms the chain yoke circuit) extremely small, reliably prevent leakage of microwaves, and prevent seizure of the rotating container.
Furthermore, since the crucible is suspended and supported, the entire surface including the bottom surface of the crucible becomes an inert gas atmosphere, thereby preventing oxidative damage.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明溶解炉の一実施例を示し、同図
は平面概要図、は側面概面図、第2図はその
下部炉体内のルツボおよび回転容器の収納状況を
示す断面概要図である。図面中の主な符号は次の
とおりである。 1:上部炉体、2:下部炉体、6:支持体、
8:ルツボ、12:回転容器、14:軸芯、1
5:不活性ガス導入管。
Fig. 1 shows an embodiment of the melting furnace of the present invention, which is a schematic plan view, a schematic side view, and Fig. 2 is a schematic cross-sectional view showing how the crucible and rotating container are housed in the lower furnace body. be. The main symbols in the drawings are as follows. 1: Upper furnace body, 2: Lower furnace body, 6: Support body,
8: Crucible, 12: Rotating container, 14: Axial core, 1
5: Inert gas introduction pipe.

Claims (1)

【特許請求の範囲】[Claims] 1 ルツボ内に装入された被処理物にマイクロ波
を照射して該被処理物を加熱溶解するための、支
持体に固定された上部炉体とこれに着脱可能な下
部炉体とからなるマイクロ波溶解炉であつて、該
下部炉体は、下部炉体本体、該本体に回転自在に
収納される回転容器、該回転容器内に懸垂収納さ
れるルツボおよび前記回転容器を回転自在に支持
し且つ不活性ガス導入管を兼ねる軸芯を備えるこ
とを特徴とするバツチ溶解式マイクロ波溶解炉。
1 Consists of an upper furnace body fixed to a support and a lower furnace body that is detachable from the upper furnace body, for heating and melting the workpiece charged in the crucible by irradiating the workpiece with microwaves. The lower furnace body is a microwave melting furnace, and the lower furnace body includes a lower furnace body, a rotating container rotatably housed in the main body, a crucible suspended and housed in the rotating vessel, and rotatably supporting the rotating vessel. A batch melting type microwave melting furnace characterized by having a shaft that also serves as an inert gas introduction pipe.
JP13019280A 1980-09-18 1980-09-18 Patch melting type microwave melting furnace Granted JPS5755389A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP13019280A JPS5755389A (en) 1980-09-18 1980-09-18 Patch melting type microwave melting furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP13019280A JPS5755389A (en) 1980-09-18 1980-09-18 Patch melting type microwave melting furnace

Publications (2)

Publication Number Publication Date
JPS5755389A JPS5755389A (en) 1982-04-02
JPS621168B2 true JPS621168B2 (en) 1987-01-12

Family

ID=15028280

Family Applications (1)

Application Number Title Priority Date Filing Date
JP13019280A Granted JPS5755389A (en) 1980-09-18 1980-09-18 Patch melting type microwave melting furnace

Country Status (1)

Country Link
JP (1) JPS5755389A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU6836087A (en) * 1985-12-30 1987-07-28 Ebara Corporation Dehydration method and apparatus
JP5162181B2 (en) * 2007-08-01 2013-03-13 国立大学法人東京工業大学 Microwave iron furnace
CN108731475B (en) * 2017-04-20 2019-10-18 南京理工大学 A kind of ceramic material microwave sintering attemperator

Also Published As

Publication number Publication date
JPS5755389A (en) 1982-04-02

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