JPS6148548B2 - - Google Patents

Info

Publication number

JPS6148548B2

JPS6148548B2 JP16820580A JP16820580A JPS6148548B2 JP S6148548 B2 JPS6148548 B2 JP S6148548B2 JP 16820580 A JP16820580 A JP 16820580A JP 16820580 A JP16820580 A JP 16820580A JP S6148548 B2 JPS6148548 B2 JP S6148548B2

Authority

JP

Japan

Prior art keywords

dye

water

add

black

formula

Prior art date

1980-11-28

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

• Espacenet
• Global Dossier
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• 239000000975 dye Substances 0.000 claims description 49
• 239000000203 mixture Substances 0.000 claims description 10
• CZDZQGXAHZVGPL-UHFFFAOYSA-M sodium;1-hydroxyethanesulfonate Chemical compound [Na+].CC(O)S([O-])(=O)=O CZDZQGXAHZVGPL-UHFFFAOYSA-M 0.000 claims description 7
• QEYMMOKECZBKAC-UHFFFAOYSA-N 3-chloropropanoic acid Chemical compound OC(=O)CCCl QEYMMOKECZBKAC-UHFFFAOYSA-N 0.000 claims description 6
• 239000002253 acid Substances 0.000 claims description 6
• 150000001875 compounds Chemical class 0.000 claims description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
• LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 18
• 239000000243 solution Substances 0.000 description 16
• 239000000843 powder Substances 0.000 description 12
• 239000000976 ink Substances 0.000 description 9
• 238000000034 method Methods 0.000 description 9
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
• 238000003756 stirring Methods 0.000 description 8
• 239000000047 product Substances 0.000 description 7
• 238000004040 coloring Methods 0.000 description 6
• 239000007788 liquid Substances 0.000 description 6
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
• 235000017550 sodium carbonate Nutrition 0.000 description 4
• 229910000029 sodium carbonate Inorganic materials 0.000 description 4
• 229920000742 Cotton Polymers 0.000 description 3
• KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
• ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
• 239000002518 antifoaming agent Substances 0.000 description 3
• MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
• -1 glycol monoalkyl ether Chemical class 0.000 description 3
• 239000010985 leather Substances 0.000 description 3
• 238000004519 manufacturing process Methods 0.000 description 3
• 238000002156 mixing Methods 0.000 description 3
• 239000004094 surface-active agent Substances 0.000 description 3
• IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
• ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
• UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
• WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
• 125000000129 anionic group Chemical group 0.000 description 2
• 238000006243 chemical reaction Methods 0.000 description 2
• 239000003086 colorant Substances 0.000 description 2
• 239000003085 diluting agent Substances 0.000 description 2
• 239000000982 direct dye Substances 0.000 description 2
• 238000001035 drying Methods 0.000 description 2
• 238000009472 formulation Methods 0.000 description 2
• 238000001879 gelation Methods 0.000 description 2
• 235000011187 glycerol Nutrition 0.000 description 2
• WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
• 239000012263 liquid product Substances 0.000 description 2
• 125000000896 monocarboxylic acid group Chemical group 0.000 description 2
• 239000003960 organic solvent Substances 0.000 description 2
• RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
• WLXGQMVCYPUOLM-UHFFFAOYSA-N 1-hydroxyethanesulfonic acid Chemical compound CC(O)S(O)(=O)=O WLXGQMVCYPUOLM-UHFFFAOYSA-N 0.000 description 1
• KHDYBVQANLNECY-UHFFFAOYSA-N 1-hydroxyethanesulfonic acid;sodium Chemical compound [Na].CC(O)S(O)(=O)=O KHDYBVQANLNECY-UHFFFAOYSA-N 0.000 description 1
• 229920001353 Dextrin Polymers 0.000 description 1
• 239000004375 Dextrin Substances 0.000 description 1
• FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
• XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
• 229920013820 alkyl cellulose Polymers 0.000 description 1
• 125000003277 amino group Chemical group 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• SUMDYPCJJOFFON-UHFFFAOYSA-N beta-hydroxyethanesulfonic acid Natural products OCCS(O)(=O)=O SUMDYPCJJOFFON-UHFFFAOYSA-N 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• 239000004202 carbamide Substances 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 238000007796 conventional method Methods 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 230000003247 decreasing effect Effects 0.000 description 1
• 235000019425 dextrin Nutrition 0.000 description 1
• 229940113088 dimethylacetamide Drugs 0.000 description 1
• UZZFFIUHUDOYPS-UHFFFAOYSA-L disodium 4-amino-3,6-bis[[4-[(2,4-diaminophenyl)diazenyl]phenyl]diazenyl]-5-oxido-7-sulfonaphthalene-2-sulfonate Chemical compound [Na+].[Na+].Nc1ccc(N=Nc2ccc(cc2)N=Nc2c(N)c3c(O)c(N=Nc4ccc(cc4)N=Nc4ccc(N)cc4N)c(cc3cc2S([O-])(=O)=O)S([O-])(=O)=O)c(N)c1 UZZFFIUHUDOYPS-UHFFFAOYSA-L 0.000 description 1
• 238000004043 dyeing Methods 0.000 description 1
• 230000000694 effects Effects 0.000 description 1
• CCIVGXIOQKPBKL-UHFFFAOYSA-M ethanesulfonate Chemical compound CCS([O-])(=O)=O CCIVGXIOQKPBKL-UHFFFAOYSA-M 0.000 description 1
• 239000004744 fabric Substances 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 150000002440 hydroxy compounds Chemical class 0.000 description 1
• 230000007935 neutral effect Effects 0.000 description 1
• 230000003647 oxidation Effects 0.000 description 1
• 238000007254 oxidation reaction Methods 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000005185 salting out Methods 0.000 description 1
• 235000017557 sodium bicarbonate Nutrition 0.000 description 1
• 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• HCJLVWUMMKIQIM-UHFFFAOYSA-M sodium;2,3,4,5,6-pentachlorophenolate Chemical compound [Na+].[O-]C1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl HCJLVWUMMKIQIM-UHFFFAOYSA-M 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• 238000001694 spray drying Methods 0.000 description 1
• YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
• YODZTKMDCQEPHD-UHFFFAOYSA-N thiodiglycol Chemical compound OCCSCCO YODZTKMDCQEPHD-UHFFFAOYSA-N 0.000 description 1
• 229950006389 thiodiglycol Drugs 0.000 description 1