JPS6116501B2 - - Google Patents
Info
- Publication number
- JPS6116501B2 JPS6116501B2 JP51155193A JP15519376A JPS6116501B2 JP S6116501 B2 JPS6116501 B2 JP S6116501B2 JP 51155193 A JP51155193 A JP 51155193A JP 15519376 A JP15519376 A JP 15519376A JP S6116501 B2 JPS6116501 B2 JP S6116501B2
- Authority
- JP
- Japan
- Prior art keywords
- tubular member
- reactor
- tubular
- reaction mixture
- vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000011541 reaction mixture Substances 0.000 claims description 56
- 239000000376 reactant Substances 0.000 claims description 43
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 42
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 30
- 238000006243 chemical reaction Methods 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 18
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 5
- 239000004254 Ammonium phosphate Substances 0.000 claims description 4
- 230000002378 acidificating effect Effects 0.000 claims description 4
- 229910000148 ammonium phosphate Inorganic materials 0.000 claims description 4
- 235000019289 ammonium phosphates Nutrition 0.000 claims description 4
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 4
- 239000007791 liquid phase Substances 0.000 claims description 2
- 239000012808 vapor phase Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 239000007789 gas Substances 0.000 description 32
- 239000000047 product Substances 0.000 description 28
- 229910021529 ammonia Inorganic materials 0.000 description 18
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- 239000002585 base Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000005192 partition Methods 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- 238000004176 ammonification Methods 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 2
- 239000012265 solid product Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000011800 void material Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000010943 off-gassing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- -1 wet sulfuric acid Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/28—Ammonium phosphates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
- B01J19/246—Stationary reactors without moving elements inside provoking a loop type movement of the reactants internally, i.e. the mixture circulating inside the vessel such that the upward stream is separated physically from the downward stream(s)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/004—Sparger-type elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/405—Polyphosphates of ammonium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/0077—Baffles attached to the reactor wall inclined
- B01J2219/00774—Baffles attached to the reactor wall inclined in the form of cones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00777—Baffles attached to the reactor wall horizontal
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB52765/75A GB1550214A (en) | 1975-12-24 | 1975-12-24 | Process for carrying out a chemical reaction |
| GB4305376 | 1976-10-16 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5281074A JPS5281074A (en) | 1977-07-07 |
| JPS6116501B2 true JPS6116501B2 (en:Method) | 1986-04-30 |
Family
ID=26265041
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP51155193A Granted JPS5281074A (en) | 1975-12-24 | 1976-12-24 | Reaction and reactor for two reactants |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4166840A (en:Method) |
| JP (1) | JPS5281074A (en:Method) |
| AU (1) | AU510357B2 (en:Method) |
| DE (1) | DE2658893A1 (en:Method) |
| EG (1) | EG12996A (en:Method) |
| ES (1) | ES454538A1 (en:Method) |
| FR (1) | FR2336174A1 (en:Method) |
| IL (1) | IL51131A (en:Method) |
| NL (1) | NL7614251A (en:Method) |
| OA (1) | OA05522A (en:Method) |
| TR (1) | TR19769A (en:Method) |
| YU (1) | YU312176A (en:Method) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2736872B2 (de) * | 1977-08-16 | 1979-07-19 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Hydroxylammoniumsalzen |
| NL7805957A (nl) * | 1978-06-01 | 1979-12-04 | Unie Van Kunstmestfab Bv | Werkwijze en inrichting voor de bereiding van een ammoniumorthofosfaat bevattend produkt, alsmede produkt verkregen met deze werkwijze. |
| US4286982A (en) * | 1979-07-02 | 1981-09-01 | Bremmer James S | Process of manufacturing stable ammonium polyphosphate fertilizers |
| US6989113B1 (en) * | 2001-04-30 | 2006-01-24 | No-Burn Investments, L.L.C. | Fire retardant |
| US6982049B1 (en) * | 2003-12-03 | 2006-01-03 | No-Burn Investments, L.L.C. | Fire retardant with mold inhibitor |
| US20050022466A1 (en) * | 2004-10-04 | 2005-02-03 | No-Burn Investments, L.L.C. | Fire resistance rating system |
| US7587875B2 (en) * | 2004-10-04 | 2009-09-15 | No-Burn Investments, L.L.C. | Fire resistance rating system |
| US7482395B2 (en) | 2005-01-24 | 2009-01-27 | No-Burn Investments, L.L.C. | Intumescent fire retardant latex paint with mold inhibitor |
| US20060189232A1 (en) * | 2005-02-23 | 2006-08-24 | No-Burn Investments, L.L.C. | Fire retarding, stain and/or mold protecting composition |
| US20070170404A1 (en) * | 2006-01-20 | 2007-07-26 | No-Burn Investments, Llc | Fire retardant with mold inhibitor and insecticide |
| US9005642B2 (en) * | 2006-01-24 | 2015-04-14 | No-Burn Investments, L.L.C. | Intumescent fire retardant paint with insecticide |
| US20070176156A1 (en) * | 2006-02-02 | 2007-08-02 | No-Burn Investments, Llc | Fire retardant composition with insecticide |
| US20070185238A1 (en) * | 2006-02-06 | 2007-08-09 | No-Burn Investments, Llc | Paint with mold inhibitor and insecticide |
| GB2465554B (en) * | 2008-11-18 | 2013-03-13 | Gtl F1 Ag | Slurry bubble column reactor |
| GB2466315B (en) | 2008-12-22 | 2013-01-09 | Gtl F1 Ag | Apparatus and method for conducting a Fischer-Tropsch synthesis reaction |
| GB2471338B (en) | 2009-06-26 | 2014-12-24 | Gtl F1 Ag | Apparatus and process for three-phase reacton |
| CA3094383C (en) | 2013-03-15 | 2022-04-12 | William B. Coe | Pavement repair system |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA557623A (en) * | 1958-05-20 | P. Ward Alfred | Manufacture of sodium and potassium phosphates | |
| US2902342A (en) * | 1955-01-27 | 1959-09-01 | Jr Bernard J Kerley | Method and apparatus for producing ammonium salts |
| US3419378A (en) * | 1965-04-01 | 1968-12-31 | Swift & Co | Method of producing monoammonium phosphate by reacting phosphoric acid and ammonia under pressure |
| US3502441A (en) * | 1966-11-25 | 1970-03-24 | United States Steel Corp | Apparatus for neutralizing acids with ammonia |
| DE1667389B1 (de) * | 1967-08-10 | 1970-10-15 | Benckiser Knapsack Gmbh | Verfahren zur Herstellung von Alkalimono-,di- und triphosphaten |
| US3957442A (en) * | 1968-10-23 | 1976-05-18 | Asahi Denka Kogyo Kabushiki Kaisha | Apparatus for the production of glycerol dichlorohydrin |
| US3758277A (en) * | 1971-06-11 | 1973-09-11 | Mississippi Chem Corp | Ammonium nitrate neutralizer |
| IT1026662B (it) * | 1974-11-29 | 1978-10-20 | Montedison Spa | Procedimento per l assorbimento di ammoniaca in soluzioni o torbile acide |
| FR2310798A1 (fr) * | 1975-05-12 | 1976-12-10 | Lykov Mikhail | Appareil pour la neutralisation des acides |
-
1976
- 1976-11-30 US US05/746,148 patent/US4166840A/en not_active Expired - Lifetime
- 1976-12-14 EG EG767/76A patent/EG12996A/xx active
- 1976-12-21 IL IL51131A patent/IL51131A/xx unknown
- 1976-12-22 TR TR19769A patent/TR19769A/xx unknown
- 1976-12-22 NL NL7614251A patent/NL7614251A/xx not_active Application Discontinuation
- 1976-12-22 YU YU03121/76A patent/YU312176A/xx unknown
- 1976-12-23 OA OA56024A patent/OA05522A/xx unknown
- 1976-12-23 AU AU20871/76A patent/AU510357B2/en not_active Expired
- 1976-12-23 ES ES454538A patent/ES454538A1/es not_active Expired
- 1976-12-24 FR FR7639051A patent/FR2336174A1/fr not_active Withdrawn
- 1976-12-24 JP JP51155193A patent/JPS5281074A/ja active Granted
- 1976-12-24 DE DE19762658893 patent/DE2658893A1/de not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| OA05522A (fr) | 1981-04-30 |
| AU510357B2 (en) | 1980-06-19 |
| ES454538A1 (es) | 1977-12-01 |
| IL51131A0 (en) | 1977-02-28 |
| YU312176A (en) | 1983-02-28 |
| NL7614251A (nl) | 1977-06-28 |
| US4166840A (en) | 1979-09-04 |
| JPS5281074A (en) | 1977-07-07 |
| AU2087176A (en) | 1978-06-29 |
| EG12996A (en) | 1980-03-31 |
| FR2336174A1 (fr) | 1977-07-22 |
| IL51131A (en) | 1979-10-31 |
| TR19769A (tr) | 1979-11-30 |
| DE2658893A1 (de) | 1977-07-07 |
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