JPS61134366A - 界面活性剤中の油分分離方法 - Google Patents
界面活性剤中の油分分離方法Info
- Publication number
- JPS61134366A JPS61134366A JP25652784A JP25652784A JPS61134366A JP S61134366 A JPS61134366 A JP S61134366A JP 25652784 A JP25652784 A JP 25652784A JP 25652784 A JP25652784 A JP 25652784A JP S61134366 A JPS61134366 A JP S61134366A
- Authority
- JP
- Japan
- Prior art keywords
- olefin
- sulfonation
- unreacted
- sulfonate
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004094 surface-active agent Substances 0.000 title claims description 5
- 238000000926 separation method Methods 0.000 title abstract description 26
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims abstract description 79
- 150000001336 alkenes Chemical class 0.000 claims abstract description 71
- 238000000034 method Methods 0.000 claims abstract description 15
- 150000001335 aliphatic alkanes Chemical class 0.000 claims abstract description 11
- -1 olefin sulfonate Chemical class 0.000 claims description 30
- 125000004432 carbon atom Chemical group C* 0.000 claims description 8
- 230000003301 hydrolyzing effect Effects 0.000 claims description 3
- 230000003472 neutralizing effect Effects 0.000 claims description 3
- 238000006277 sulfonation reaction Methods 0.000 abstract description 24
- 238000006243 chemical reaction Methods 0.000 abstract description 10
- 238000006460 hydrolysis reaction Methods 0.000 abstract description 5
- 238000006386 neutralization reaction Methods 0.000 abstract description 5
- 239000003599 detergent Substances 0.000 abstract description 4
- 230000007062 hydrolysis Effects 0.000 abstract description 4
- 230000009257 reactivity Effects 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 239000008346 aqueous phase Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract description 2
- 150000003839 salts Chemical class 0.000 abstract description 2
- 150000008054 sulfonate salts Chemical class 0.000 abstract description 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- 239000012071 phase Substances 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 9
- 239000000203 mixture Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 6
- 239000007795 chemical reaction product Substances 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- GGQQNYXPYWCUHG-RMTFUQJTSA-N (3e,6e)-deca-3,6-diene Chemical compound CCC\C=C\C\C=C\CC GGQQNYXPYWCUHG-RMTFUQJTSA-N 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 150000005846 sugar alcohols Polymers 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000004711 α-olefin Substances 0.000 description 2
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000008282 halocarbons Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006772 olefination reaction Methods 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000008053 sultones Chemical class 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25652784A JPS61134366A (ja) | 1984-12-06 | 1984-12-06 | 界面活性剤中の油分分離方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25652784A JPS61134366A (ja) | 1984-12-06 | 1984-12-06 | 界面活性剤中の油分分離方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61134366A true JPS61134366A (ja) | 1986-06-21 |
| JPH0443904B2 JPH0443904B2 (en, 2012) | 1992-07-20 |
Family
ID=17293859
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP25652784A Granted JPS61134366A (ja) | 1984-12-06 | 1984-12-06 | 界面活性剤中の油分分離方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61134366A (en, 2012) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014046176A1 (ja) * | 2012-09-20 | 2014-03-27 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| WO2014046175A1 (ja) * | 2012-09-20 | 2014-03-27 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| WO2014119726A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| WO2014119727A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| WO2014119728A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| WO2014125940A1 (ja) | 2013-02-13 | 2014-08-21 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| JP2015028123A (ja) * | 2012-09-20 | 2015-02-12 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| US9725676B2 (en) | 2012-09-20 | 2017-08-08 | Kao Corporation | Cleansing composition for skin or hair |
| US9877906B2 (en) | 2012-09-20 | 2018-01-30 | Kao Corporation | Cleansing composition for skin or hair |
| US10039702B2 (en) | 2012-09-20 | 2018-08-07 | Kao Corporation | Cleansing composition for skin or hair |
| US10071039B2 (en) | 2012-09-20 | 2018-09-11 | Kao Corporation | Cleansing composition for skin or hair |
-
1984
- 1984-12-06 JP JP25652784A patent/JPS61134366A/ja active Granted
Cited By (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108498361A (zh) * | 2012-09-20 | 2018-09-07 | 花王株式会社 | 内烯烃磺酸盐组合物和包含该组合物的清洁组合物 |
| US10201488B2 (en) | 2012-09-20 | 2019-02-12 | Kao Corporation | Internal olefin sulfonate composition and cleansing composition containing same |
| JP2014077126A (ja) * | 2012-09-20 | 2014-05-01 | Kao Corp | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| JP2014076988A (ja) * | 2012-09-20 | 2014-05-01 | Kao Corp | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| CN104603251B (zh) * | 2012-09-20 | 2018-12-28 | 花王株式会社 | 内烯烃磺酸盐组合物及含有其的洗净剂组合物 |
| EP3388051A1 (en) * | 2012-09-20 | 2018-10-17 | Kao Corporation | Internal olefin sulfonate composition and detergent composition containing same |
| US10071039B2 (en) | 2012-09-20 | 2018-09-11 | Kao Corporation | Cleansing composition for skin or hair |
| CN108498361B (zh) * | 2012-09-20 | 2021-10-12 | 花王株式会社 | 内烯烃磺酸盐组合物和包含该组合物的清洁组合物 |
| WO2014046175A1 (ja) * | 2012-09-20 | 2014-03-27 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| US9725676B2 (en) | 2012-09-20 | 2017-08-08 | Kao Corporation | Cleansing composition for skin or hair |
| US10039702B2 (en) | 2012-09-20 | 2018-08-07 | Kao Corporation | Cleansing composition for skin or hair |
| US9877906B2 (en) | 2012-09-20 | 2018-01-30 | Kao Corporation | Cleansing composition for skin or hair |
| JP2015028123A (ja) * | 2012-09-20 | 2015-02-12 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| CN104603251A (zh) * | 2012-09-20 | 2015-05-06 | 花王株式会社 | 内烯烃磺酸盐组合物及含有其的洗净剂组合物 |
| US10196587B2 (en) | 2012-09-20 | 2019-02-05 | Kao Corporation | Cleansing composition for skin or hair |
| JP2018009189A (ja) * | 2012-09-20 | 2018-01-18 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| WO2014046176A1 (ja) * | 2012-09-20 | 2014-03-27 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物及びこれを含有する洗浄剤組成物 |
| US9713584B2 (en) | 2012-09-20 | 2017-07-25 | Kao Corporation | Internal olefin sulfonate composition and cleansing composition containing same |
| CN104955932A (zh) * | 2013-02-01 | 2015-09-30 | 花王株式会社 | 内部烯烃磺酸盐组合物 |
| US9789045B2 (en) | 2013-02-01 | 2017-10-17 | Kao Corporation | Internal olefin sulfonate composition |
| US9861566B2 (en) | 2013-02-01 | 2018-01-09 | Kao Corporation | Internal olefin sulfonate composition |
| US9861567B2 (en) | 2013-02-01 | 2018-01-09 | Kao Corporation | Internal olefin sulfonate composition |
| CN104955933A (zh) * | 2013-02-01 | 2015-09-30 | 花王株式会社 | 内部烯烃磺酸盐组合物 |
| US10328008B2 (en) | 2013-02-01 | 2019-06-25 | Kao Corporation | Internal olefin sulfonate composition |
| JP2014167108A (ja) * | 2013-02-01 | 2014-09-11 | Kao Corp | 内部オレフィンスルホン酸塩組成物 |
| JP2018115329A (ja) * | 2013-02-01 | 2018-07-26 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| JP2014167107A (ja) * | 2013-02-01 | 2014-09-11 | Kao Corp | 内部オレフィンスルホン酸塩組成物 |
| JP2014167106A (ja) * | 2013-02-01 | 2014-09-11 | Kao Corp | 内部オレフィンスルホン酸塩組成物 |
| WO2014119728A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| WO2014119727A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| WO2014119726A1 (ja) * | 2013-02-01 | 2014-08-07 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
| US9622952B2 (en) | 2013-02-13 | 2017-04-18 | Kao Corporation | Internal olefin sulfonate composition |
| US9877907B2 (en) | 2013-02-13 | 2018-01-30 | Kao Corporation | Internal olefin sulfonate composition |
| JP2014177620A (ja) * | 2013-02-13 | 2014-09-25 | Kao Corp | 内部オレフィンスルホン酸塩組成物 |
| WO2014125940A1 (ja) | 2013-02-13 | 2014-08-21 | 花王株式会社 | 内部オレフィンスルホン酸塩組成物 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0443904B2 (en, 2012) | 1992-07-20 |
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