JPS5948435A - ジクロルアセチルクロライドの製造方法 - Google Patents
ジクロルアセチルクロライドの製造方法Info
- Publication number
- JPS5948435A JPS5948435A JP15772282A JP15772282A JPS5948435A JP S5948435 A JPS5948435 A JP S5948435A JP 15772282 A JP15772282 A JP 15772282A JP 15772282 A JP15772282 A JP 15772282A JP S5948435 A JPS5948435 A JP S5948435A
- Authority
- JP
- Japan
- Prior art keywords
- dichloroacetyl chloride
- reaction
- trichlorethylene
- oxidation
- tertiary amine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- FBCCMZVIWNDFMO-UHFFFAOYSA-N dichloroacetyl chloride Chemical compound ClC(Cl)C(Cl)=O FBCCMZVIWNDFMO-UHFFFAOYSA-N 0.000 title claims abstract description 33
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims abstract description 29
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000006243 chemical reaction Methods 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 14
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 14
- 230000003647 oxidation Effects 0.000 claims abstract description 13
- 150000003512 tertiary amines Chemical class 0.000 claims abstract description 12
- 239000007791 liquid phase Substances 0.000 claims abstract description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 230000008707 rearrangement Effects 0.000 abstract description 8
- 230000006698 induction Effects 0.000 abstract description 6
- 239000003054 catalyst Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 239000004009 herbicide Substances 0.000 abstract description 2
- 239000002917 insecticide Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 abstract 2
- 230000002363 herbicidal effect Effects 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- 238000004821 distillation Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- UAOMVDZJSHZZME-UHFFFAOYSA-N diisopropylamine Chemical compound CC(C)NC(C)C UAOMVDZJSHZZME-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- -1 aliphatic ketones Chemical class 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 230000020169 heat generation Effects 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 238000006462 rearrangement reaction Methods 0.000 description 2
- CMMXCVYESRODNH-UHFFFAOYSA-N trichloroepoxyethane Chemical compound ClC1OC1(Cl)Cl CMMXCVYESRODNH-UHFFFAOYSA-N 0.000 description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical group ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- XENVCRGQTABGKY-ZHACJKMWSA-N chlorohydrin Chemical compound CC#CC#CC#CC#C\C=C\C(Cl)CO XENVCRGQTABGKY-ZHACJKMWSA-N 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 229940043279 diisopropylamine Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002118 epoxides Chemical class 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15772282A JPS5948435A (ja) | 1982-09-10 | 1982-09-10 | ジクロルアセチルクロライドの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15772282A JPS5948435A (ja) | 1982-09-10 | 1982-09-10 | ジクロルアセチルクロライドの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5948435A true JPS5948435A (ja) | 1984-03-19 |
| JPH0316937B2 JPH0316937B2 (enrdf_load_stackoverflow) | 1991-03-06 |
Family
ID=15655935
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP15772282A Granted JPS5948435A (ja) | 1982-09-10 | 1982-09-10 | ジクロルアセチルクロライドの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5948435A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6351352A (ja) * | 1986-08-20 | 1988-03-04 | Daicel Chem Ind Ltd | ジクロルアセチルクロライドの製造方法 |
| US5433831A (en) * | 1993-05-01 | 1995-07-18 | Hoechst Aktiengesellchaft | Process for the preparation of dichloroacetyl chloride |
| WO2011122341A1 (ja) * | 2010-03-29 | 2011-10-06 | セントラル硝子株式会社 | ジフルオロ酢酸クロライドの製造方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6783128B2 (ja) * | 2016-12-06 | 2020-11-11 | 三菱電機株式会社 | リード加工装置 |
-
1982
- 1982-09-10 JP JP15772282A patent/JPS5948435A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6351352A (ja) * | 1986-08-20 | 1988-03-04 | Daicel Chem Ind Ltd | ジクロルアセチルクロライドの製造方法 |
| US5433831A (en) * | 1993-05-01 | 1995-07-18 | Hoechst Aktiengesellchaft | Process for the preparation of dichloroacetyl chloride |
| WO2011122341A1 (ja) * | 2010-03-29 | 2011-10-06 | セントラル硝子株式会社 | ジフルオロ酢酸クロライドの製造方法 |
| US8716526B2 (en) | 2010-03-29 | 2014-05-06 | Central Glass Company, Limited | Method for producing difluoroacetyl chloride |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0316937B2 (enrdf_load_stackoverflow) | 1991-03-06 |
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