JPS5946042A - Observing method for pin hole, crack and coverage of semiconductor device - Google Patents

Observing method for pin hole, crack and coverage of semiconductor device

Info

Publication number
JPS5946042A
JPS5946042A JP15850582A JP15850582A JPS5946042A JP S5946042 A JPS5946042 A JP S5946042A JP 15850582 A JP15850582 A JP 15850582A JP 15850582 A JP15850582 A JP 15850582A JP S5946042 A JPS5946042 A JP S5946042A
Authority
JP
Japan
Prior art keywords
crack
coverage
semiconductor device
pigment
pin hole
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP15850582A
Other languages
Japanese (ja)
Inventor
Masakazu Nakabayashi
正和 中林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Electric Corp
Original Assignee
Mitsubishi Electric Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Electric Corp filed Critical Mitsubishi Electric Corp
Priority to JP15850582A priority Critical patent/JPS5946042A/en
Publication of JPS5946042A publication Critical patent/JPS5946042A/en
Pending legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor

Abstract

PURPOSE:To decide acceptable or defective coverages with high accuracy by immersing a semiconductor device in a pigment solution at high atmospheric pressure and observing the pigment by a fluorescence microscope after washing the device. CONSTITUTION:The pigment solution 7 in which Rhodamine 6G is used as the pigment and benzyl alcohol is used as a solvent is prepared. The device 6 in contg. the crack 5 and the pin hole 4 is immersed in the solution 7 at high atmospheric pressure. When the solution permeates and a sample is washed by pure water and observed by the fluorescence microscope, the pigment in the pin hole 4 and the crack 5 fluoresces, and acceptable or defective coverages can be decided at low cost with high accuracy.

Description

【発明の詳細な説明】 この発明は、半4体デバイスのオーツく−コート114
1のクラック、ピンホール、カバーレッジを評価するた
めのピンホール、クラック、力1<−レッジ%J?、 
%方法tこ関するものである。
DETAILED DESCRIPTION OF THE INVENTION The present invention describes
Pinhole, crack, force 1<-ledge %J to evaluate the crack, pinhole, coverage of 1? ,
This is related to the % method.

従来・この神のl+J1.察を行なうJJ、−合、半導
体デバイスをリン酸エツ手してクラック、ビンよ−Iレ
イノ)評価を行なっていた。
Conventional・This God's l+J1. JJ, who was conducting an inspection, was evaluating semiconductor devices for cracks and cracks by using phosphoric acid.

ここでリン酸エッチ方式は、半・jf休体l−eイスを
リン酸に浸しsAt配線の上部のクラ°ツク、ピンポー
ルを、Atがエツチングさitたことから、金14顕微
鏡で観だず2.ものであった。
Here, the phosphoric acid etching method involves soaking a semi-JF-free chair in phosphoric acid and etching the cracks and pin poles at the top of the sAt wiring, which can then be observed with a gold-14 microscope. 2. It was something.

しかしながら、この方/JEてI#、At配線J: +
;(<のビンホーlし、クラ゛ンクl;t 114見察
できるが、七れ1ツタ)の部分ではイ硯察ができず、ま
た、カバーレッジの悪い部分についても締、察できない
という犬点かあつ lこ 。
However, this person/JE I#, At wiring J: +
;(<'s bottle hole l, crank l; t 114 can be observed, but the dog cannot make a thorough inspection in the part where the coverage is poor.) It's hot.

この発明は上記のような従来のものの失点を除去するた
めになされたもので、半導体デバイスを高気圧の下で色
素l谷液中に浸し、これを洗浄したのち、そのピンホー
ル、クラック、カバーレッジの悪い部分に#潰した色素
をけい光)IJ+i微鏡にて観、察することにより、A
t配線以外の部分のピンホール、クラックをも、さらに
カバーレッジの悪い部分をも観察することができる半導
体デバ・イスのピンポール、クラック、カバーレッジh
1(、察方θモを提供することを目的としている。
This invention was made in order to eliminate the disadvantages of the conventional devices as described above. After immersing a semiconductor device in a dye solution under high pressure and cleaning it, pinholes, cracks, and coverage are removed. By observing and observing the crushed pigment in the bad part of
t Pinholes, cracks, and coverage of semiconductor device chairs that allow you to observe pinholes and cracks in areas other than wiring, as well as areas with poor coverage.
1 (, the purpose is to provide a method of observation θmo).

以下、この発明の一実施例を図について説明する。第1
図は本発明方法により観察しようと4−るピンホール、
クラックを有する半尋体デ/XIイスを示し、1閲にお
いて、(1)は半8参休基板、+21 Lf A を配
線、(3)は5iU2からなる表面保護11シ’i(オ
ーツく一コート11ネ) 、+61は以上の(1)〜に
31からなる半導+r’iデ/イイスである。そして(
4)はこの半・i^1本デlくイス(6)lこできたピ
ンホール、(5)は同じくクラ゛ンクで、v)る。
An embodiment of the present invention will be described below with reference to the drawings. 1st
The figure shows four pinholes to be observed using the method of the present invention.
In the first review, (1) is a half-8 board, +21 Lf A is wired, and (3) is a surface protection 11 board made of 5iU2 (auto board). Coat 11), +61 is a semiconductor +r'i de/iis consisting of 31 in (1) above. and(
4) is the pinhole made by this half-I^1 pinhole (6) l, and (5) is the same crank, v).

そして上記半導体デノくイス(6)のピン;l= −/
しく4)、クラック(5)を観察す乙には、@2図番こ
示i−よう番こ、ビー力(8]に色素溶液(′l)を入
れたも+/)υ)中(こ、上J己試ぜ1(6)を書妬気
圧F下で漬し、その後、試本・l +61 E 7i1
=浄すると、弔3図のようになり、ピン1トー?しく4
)オよびクラック(5)に色素(9)が4+¥噴する0
ここで・色素溶液の例としてtま、色素としてjId)
し効率の高いローダシン6にを、m”某としてベンジI
Lアルコール、純水等を用G)ること7Jsで゛きる。
And the pin of the semiconductor device (6); l= −/
4), to observe the crack (5), @2 figure number is shown. Soak the sample 1 (6) under pressure F, then sample 1 +61 E 7i1
= When purified, it will look like the picture 3, pin 1 toe? Work 4
) Dye (9) sprays 4+¥ on O and crack (5) 0
Here, t as an example of a dye solution, jId as a dye)
The highly efficient Rhodashin 6 was used as a Venge I.
It can be done in 7Js by using L alcohol, pure water, etc.

またクラック(5)の小さいも0)を+4祭−〇きるプ
こW)+こは分子構造0)小さな1へ素を)l<4−る
こと力S賢1ザ4であるO このように木賽施例では、晶気1−f下で6武生・1(
6)を色素溶液(7) +tニー f 4−と、・t′
1.41木デ/<イス(6)σ)クラ゛ンク(5)、ピ
ンホール(4)に、色素溶液がしみこんで行くので、該
色素溶液がしみこんだ後、試ネil f(3)を純水で
洗浄してクラック(5)、ピンホール(41Di ’y
l−についた色素を洗い落とし、その後、試料16)を
けい光顕敬鏡で繞トすると、ピンホー/l/+41.ク
ラック(5)中に残った色素がりい光を発し、ピンポー
ル(4)・クラック+51 ) #μ察することができ
る。
Also, the small part of crack (5) is 0) +4 festival -〇kirupuko W) + this is the molecular structure 0) small 1 element) l<4- is the force S wise 1 the 4 O like this In the Nimokusai example, 6 Takefu・1(
6) to the dye solution (7) +t knee f 4- and ・t'
1.41 The dye solution soaks into the crank (5) and pinhole (4), so after the dye solution soaks in, test nail f (3). Wash with pure water to remove cracks (5) and pinholes (41Di 'y
After washing off the dye attached to l-, and then looking at sample 16) with a fluorescent microscope, the result was pinho/l/+41. The dye remaining in the crack (5) emits bright light, allowing the pinpole (4)/crack +51) #μ to be detected.

また第4区口ま木腎明ノj法1こより1+i見奈しよう
ノニJ−るメカバーレッジの患いt$分をl’(4−る
半・!1(体デバイスを示し、14薯こ2いて、fil
+はシリコンH’:、 &Jz 該シリコン基板fll
+ 11こ形成されたシリコン酸化11弾(S4021
1i )、(1:nは該5i02膜Q21上に部分的ニ
j内戊されプこAt等による蛍1萬配線、(14)は」
二gL!S +02 II外(121および欲属配線(
I:4−ヒlこ形成された5iL)2あるいはSiNか
らなるオーバーコート1嘆であり% (1151は以上
の曲〜(14)からなる半4i体デバイスである。そし
て(1,fll)(16b)は金属I妃線tllの側部
の1才差のある部分において、カバーレッジか餠いfk
 果#  t< −−3−ト膜114)に生じた回部で
ある。
In addition, the 4th Ward Kuchimagi Kidney Akinoj method 1 + i Minayo noni J-ru mechanical coverage amount of t$ l' (4-ru half ! 1 (indicates the body device, 14 yam 2 and , fil
+ is silicon H':, &Jz the silicon substrate full
+11 silicon oxide bullets (S4021
1i), (1:n is 10,000 wires partially etched into the 5i02 film Q21 by At, etc., (14) is
2gL! S +02 II outside (121 and greedy wiring (
1151 is a semi-4i body device consisting of the above songs ~(14).And (1,fl)( 16b) is the coverage or thick fk in the part with a one-year difference on the side of the metal I line tll.
This is a turning portion generated in the result #t<--3-t film 114).

−大第5図は第4図と同様の構成になる半導体デバイス
で、カバーレッジの良い例を示しており、この場合オー
バーコート膜(14)には(つ1萬配線(I31による
段差がある所においてもカバーレッジは良く、第4因に
示すような凹部(16a)(16b)は生じていな(1
゜ 」二記第4図、第51火1に示すような半+、l’、I
:体デバイス(161について、カバーレッジの+a否
5r−I覗、察4−る場r會、」二連のクラック、ピン
ホーlしの観俗の1いγ〉と全く同じように、−!11
0体デバイス(lIil G−、1!V+メ(圧下で1
△素l容岐中に浸し、その後資料(16)をl走電ずA
]は、第4図番こ示すデバイス(16)では凹部0.6
1 ) (liil))に色素が蓄積すスので、これを
りい光に’li r+’、l鏡で、11.lJ察するこ
とにより、カバーレッジの良否を判定することかできる
- Large Figure 5 shows a semiconductor device with the same configuration as Figure 4, and shows an example of good coverage. The coverage was good even in some places, and there were no recesses (16a) (16b) as shown in the fourth factor (1).
Half+, l', I as shown in ゜''2, Figure 4, 51st Tue 1
: body device (for 161, coverage +a or no 5r-I peek, observation 4-ru meeting, ``double crack, pinhole l observation 1 gamma>'', -! 11
0 body device (IIil G-, 1!V+Me (1 under pressure)
△Immerse it in water and then add material (16) to it.
] is a recess of 0.6 in the device (16) shown in Figure 4.
1) Pigment accumulates in (liil)), so it is exposed to a bright light 'li r+' and a mirror. 11. By observing lJ, it is possible to judge whether the coverage is good or bad.

なお上記実歴(例では、半導体デバイνFj +++l
J、桜を行なった場合を説明したが、本発明では他の重
子部品、ハイブリッドIC,コンデンサー、低抗等の表
面観察にも利用できる。
Note that the above actual history (in the example, semiconductor device νFj +++l
J. Although the case where cherry blossoms were carried out has been described, the present invention can also be used for surface observation of other heavy-duty components, hybrid ICs, capacitors, low resistance, etc.

以上のよう番こ、この発明によイ1ば% +!4気化下
で色素溶液中に半々一体デバイスを浸し、該半導体デバ
イスを洗浄したのち、該半導体デバイスのピンホール、
クラック、カバーレッジ(ハ爬い部分に糸情した色素を
けい光顕微鏡で観察することにより、色素とけい光顕微
鏡を使用するだけであるので、安価に観察を行なうこと
ができ、かっt聞良の良いものか得られる効果がある。
As described above, this invention has improved by 1% +! 4. After immersing the half-integrated device in a dye solution under vaporization and cleaning the semiconductor device, pinholes in the semiconductor device,
By observing the pigment in the cracks and coverage areas using a fluorescence microscope, it is possible to conduct the observation at low cost because only the pigment and fluorescence microscope are used. There are good things and effects that can be obtained.

【図面の簡単な説明】[Brief explanation of drawings]

嘱1図は本発明によるイ蜆祭試料であるピンホール、ク
ラックを奮する半導体デバイスの断面図、第2図はその
試−1を商気圧下で色素溶液中に浸した状態を示す図、
@3図は該試料を#!!J素溶rll中に浸した後純水
で洗浄した状態を示す断面図、第4図は本発明による観
察試料であるカバーレッジの悪い半導体デバイスの1新
面図、第5図イ」カバーレッジのdい半46体デバイス
の断面図である。 (6)・・・半導体デバイス、(3)・・・オーバーコ
ー+−+HB・(4)・・・ピンホール、(5)・・・
クラック、(7)・・・1色素frf液、(9)・・・
色素、63)・・・半747.休デバイス、1141・
・・オーバーコ−) 11!、(16a)(16b)・
・・カバーレッジか悪いため生ずる凹部。 第1 図 ρ 第2 図 第3図 第4図 第5図 4 S;O2
Figure 1 is a cross-sectional view of a semiconductor device that exhibits pinholes and cracks, which is a test sample according to the present invention, and Figure 2 is a diagram showing the sample 1 immersed in a dye solution under commercial pressure.
@Figure 3 indicates the sample with #! ! A cross-sectional view showing the state after being immersed in J Soluble Rll and then washed with pure water. Fig. 4 is a new view of a semiconductor device with poor coverage, which is an observation sample according to the present invention. Fig. 5 FIG. 3 is a cross-sectional view of a small half-46 body device. (6)...Semiconductor device, (3)...Overcoat +-+HB, (4)...Pinhole, (5)...
Crack, (7)...1 dye frf liquid, (9)...
Pigment, 63)...Half 747. Closed device, 1141・
...overco-) 11! , (16a) (16b)・
...Concavities caused by poor coverage. Figure 1 ρ Figure 2 Figure 3 Figure 4 Figure 5 Figure 4 S; O2

Claims (1)

【特許請求の範囲】[Claims] (1)  6気圧下で色素溶液中に半ノ)一体デバイス
を浸し、該半導体デバイスを洗浄したのち、該半導体デ
バイスのビンポール、クラック、あるいはカバーレッジ
の悪い部分に蓄1ぼした色素をけい毘順微鏡で観察する
ことを特徴とする!I算14ネ体デ/くイスのピンホー
ル、クラック、カバーレッジMM <6 方法。
(1) After immersing the semi-integrated device in a dye solution at 6 atmospheres and cleaning the semiconductor device, remove the dye that has accumulated in the holes, cracks, or areas with poor coverage of the semiconductor device. It is characterized by observation using a forward microscope! Pinholes, cracks, and coverage of I calculation 14 body design/cutting machine MM <6 Method.
JP15850582A 1982-09-09 1982-09-09 Observing method for pin hole, crack and coverage of semiconductor device Pending JPS5946042A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15850582A JPS5946042A (en) 1982-09-09 1982-09-09 Observing method for pin hole, crack and coverage of semiconductor device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15850582A JPS5946042A (en) 1982-09-09 1982-09-09 Observing method for pin hole, crack and coverage of semiconductor device

Publications (1)

Publication Number Publication Date
JPS5946042A true JPS5946042A (en) 1984-03-15

Family

ID=15673197

Family Applications (1)

Application Number Title Priority Date Filing Date
JP15850582A Pending JPS5946042A (en) 1982-09-09 1982-09-09 Observing method for pin hole, crack and coverage of semiconductor device

Country Status (1)

Country Link
JP (1) JPS5946042A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63131303A (en) * 1986-11-21 1988-06-03 Hitachi Ltd Drive system for magneto-resistance effect head
CN112185839A (en) * 2020-10-27 2021-01-05 上海华虹宏力半导体制造有限公司 Passivation layer test structure

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5454583A (en) * 1977-10-11 1979-04-28 Toshiba Corp Inspecting method of sealing bodies
JPS54101677A (en) * 1978-01-27 1979-08-10 Hitachi Ltd Detecting method for leak presence in resin seal-type semiconductor device

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5454583A (en) * 1977-10-11 1979-04-28 Toshiba Corp Inspecting method of sealing bodies
JPS54101677A (en) * 1978-01-27 1979-08-10 Hitachi Ltd Detecting method for leak presence in resin seal-type semiconductor device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63131303A (en) * 1986-11-21 1988-06-03 Hitachi Ltd Drive system for magneto-resistance effect head
CN112185839A (en) * 2020-10-27 2021-01-05 上海华虹宏力半导体制造有限公司 Passivation layer test structure

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