JPS5943861A - Louver type chemical vapor deposition device - Google Patents
Louver type chemical vapor deposition deviceInfo
- Publication number
- JPS5943861A JPS5943861A JP15269982A JP15269982A JPS5943861A JP S5943861 A JPS5943861 A JP S5943861A JP 15269982 A JP15269982 A JP 15269982A JP 15269982 A JP15269982 A JP 15269982A JP S5943861 A JPS5943861 A JP S5943861A
- Authority
- JP
- Japan
- Prior art keywords
- gas
- substrates
- reaction
- vapor deposition
- chemical vapor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Vapour Deposition (AREA)
Abstract
Description
【発明の詳細な説明】
本発明はルーツモ一式化学的蒸着(CVD)装置に係り
、本発明におけるOVD装置はプラズマ0VD装置及び
減圧OVD装置の両者を包含するものである。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a Rootsmo chemical vapor deposition (CVD) apparatus, and the OVD apparatus in the present invention includes both a plasma OVD apparatus and a reduced pressure OVD apparatus.
OVD方式では生成物(又は蒸着物質)とともに無用の
、場合によっては有害な副生物が生成され、広い面積又
は範囲の被覆すべき基体上に一様に蒸着することができ
ず、装置を大型化してもこれらの欠点は解消できず、有
効な面積としては反応ガスの流量、流速等によシ若干の
差異はあるもはtAOOtnm−φであることは当業者
によく知られているところである。In the OVD method, useless and sometimes harmful by-products are generated along with the product (or deposition material), and it is not possible to uniformly deposit a large area or range of substrates, which increases the size of the equipment. However, these drawbacks cannot be overcome, and it is well known to those skilled in the art that the effective area is tAOOtnm-φ, although there are some differences depending on the flow rate, flow rate, etc. of the reaction gas.
本発明者は上記の如き従来方式による蒸着有効面積を拡
大することを検討した結果、被覆すべき基体群をルーツ
マー状(すだれ状)に保持し、反応ガスがルーツマー状
に配設した基体間の隙間から後方に流れるような反応ガ
ス流とすることにより解決し得ることを知見したもので
あり、本発明の要旨とするところは前記特許請求の範囲
各項に明記したとおりの構成からなるものである。As a result of considering expanding the effective area for vapor deposition by the conventional method as described above, the inventors of the present invention have found that the substrates to be coated are held in a Rootsmer shape (blinding), and the reactive gas is distributed between the substrates arranged in the Rootsmer shape. The inventors have discovered that this problem can be solved by making the reaction gas flow flow backward from the gap, and the gist of the present invention is to have the structure as specified in each claim. be.
本発明の構成並びに作用効果を従来方式と対比して以下
に詳述する。The configuration and effects of the present invention will be explained in detail below in comparison with the conventional system.
第1図は従来方式のOVD装置の一例であり、lは反応
室であり、被覆すべき基体2はホルダー3に担持されて
矢印り方向九移動する機構としである。グは反応ガス噴
出機構(プラズマ0VD装置の場合は電極も兼ねる)で
あり、前記基体λに対向する面に多数の反応ガス噴出孔
を図示の如く設けである。jは反応済ガスの排出孔であ
り、tは基体λ用のヒーターである。この種従来方式で
は反応ガス(JG)が反応ガス噴出機構弘から矢印Gの
如く噴出し、基体λ上に蒸着層を生成するが、その際に
反応副生物が当然生成され、反応領域周辺に流れる反応
ガスにはこの副生物が含有されることになり、従って反
応有効領域は前述の如く#1ソロ00簡φ1呈度に限定
され、装置自体を大型化してもこの有効領域を拡大する
ことは不可能である。FIG. 1 shows an example of a conventional OVD apparatus, in which 1 is a reaction chamber, and the substrate 2 to be coated is supported by a holder 3 and is moved in the direction of the arrow. Reference numeral 1 is a reactive gas ejection mechanism (also serves as an electrode in the case of a plasma 0VD device), and a large number of reaction gas ejection holes are provided on the surface facing the substrate λ as shown in the figure. j is a discharge hole for the reacted gas, and t is a heater for the substrate λ. In this kind of conventional method, the reaction gas (JG) is ejected from the reaction gas ejection mechanism Hiroshi in the direction of arrow G and forms a vapor deposited layer on the substrate λ, but at this time, reaction by-products are naturally generated and are distributed around the reaction area. The flowing reaction gas will contain this by-product, so the effective reaction area is limited to #1 solo 00 simple φ1 degree as mentioned above, and even if the device itself is enlarged, this effective area cannot be expanded. is not possible.
第λ図〜第グ図は本発明装置の概略図金示す数例であり
、以下本発明装置の具体例f図示に基いて説明する。Figures λ to 7 are several examples showing schematic diagrams of the apparatus of the present invention, and the following description will be given based on the illustration of a specific example of the apparatus of the present invention.
第2図は本発明装置の一例を示す平面略図、第3図は第
2図1[[−111線に沿った断面略図であって、IO
は反応室を示し、該反応室ioの一方に反応ガス噴出機
構l/を配設する。該反応室IOの他方側には反応済ガ
ス(副生物を含有する)年収室7.2がスリット等を設
けた隔壁13を介しで設けてあり、該年収室/コは排ガ
ス排出孔lグを設けである。被覆すべきノ、に体/jは
保持具1lKa数個保持してあり、図示の如く適当な間
隔の間隙17をあけてルーツモー状に多数個でかつ枚数
列配設しである。FIG. 2 is a schematic plan view showing an example of the device of the present invention, and FIG. 3 is a schematic cross-sectional view taken along line 1 [[-111] of FIG.
indicates a reaction chamber, and a reaction gas blowout mechanism l/ is disposed in one side of the reaction chamber io. On the other side of the reaction chamber IO, a reaction chamber 7.2 containing reacted gas (containing by-products) is provided via a partition wall 13 provided with slits, etc. This is provided. Several holders 1lKa are held to cover the parts to be covered, and as shown in the figure, they are arranged in large numbers in rows in a roots-like manner with appropriate gaps 17 between them.
上記の如き機構した本発明装置では1反応ガス(R,G
、 )がガス噴出機構l/の噴出孔から矢印Gの如く噴
出され、第1列の基体11表面に蒸着膜を生成し、反応
副生物と共に間隙17を通過して前進し、第2列の基体
is表面上に蒸着膜を生成し、しかる後筒コ列の隙間/
7を通過し、隔壁/3のスリットを通って排ガス年収室
12に集められ、排出孔l≠を経て排出される。In the apparatus of the present invention configured as described above, one reaction gas (R, G
, ) is ejected from the ejection hole of the gas ejection mechanism l/ as shown by arrow G, forms a vapor deposited film on the surface of the substrate 11 in the first row, passes through the gap 17 together with the reaction by-products, and advances. A vapor deposited film is generated on the surface of the substrate is, and then the gap between the rows of cylinders/
7, passes through the slit in the partition wall /3, is collected in the annual income chamber 12, and is discharged through the exhaust hole l≠.
従って、本発明装置によれば、装置内に配設した基体l
!の被蒸着面には常に新鮮な反応ガスが到達することと
なり、ルーツ々−全体として見れば広い範囲の領域に配
設された基体/!全全体亘って一様かつ均一な蒸着膜を
生成することが可能である。Therefore, according to the device of the present invention, the substrate l disposed in the device
! Fresh reactive gas always reaches the surface to be evaporated, and the roots of the substrate/! It is possible to produce a uniform and uniform deposited film over the entire area.
第≠図はルーツモー状に配設する基体群を反応ガス流に
対して一定角度に傾斜して配設する例を示す略図である
。Figure ≠ is a schematic diagram showing an example in which a group of substrates arranged in a Roots-Maw shape is arranged at a constant angle with respect to the flow of the reactant gas.
上記具体例はノ々ツチ式操作を説明したが、基体群はそ
れらの相互関係(間隔及び傾斜角度)を保持し、反応ガ
スの流れに対向しながら該ガス流の直角方向に移動方式
とすることによりインライン(INLINE)方式とし
得ることは当業者に容易に理解し得るところである。The above specific example describes the Nototsuchi type operation, but the base group maintains their mutual relationship (spacing and inclination angle) and moves in the direction perpendicular to the flow of the reactant gas while facing the flow of the gas. Those skilled in the art will easily understand that this allows an inline method.
第5図に本発明の竪型インライン方式の断面略図を示す
。この方式では図示の如く1反応室10の中央部に反応
ガス噴出孔/2を設け、例えば図示の如く排ガスは排ガ
ス排出孔/4’より下方え排出する。尚、排ガスは上方
に吸引してもよい。FIG. 5 shows a schematic cross-sectional view of the vertical in-line system of the present invention. In this system, as shown in the figure, a reaction gas blowout hole /2 is provided in the center of one reaction chamber 10, and exhaust gas is discharged downward from the exhaust gas discharge hole /4', for example, as shown in the figure. Note that the exhaust gas may be sucked upward.
被覆すべき基体/!は紙面に垂直方向に移動可能とした
保持具16上に担持しである。該保持具16は所望によ
り反応ガス流方向に対向して復数列重複して配置しても
よい。Substrate to be coated/! is supported on a holder 16 which is movable in a direction perpendicular to the plane of the paper. The holders 16 may be arranged in multiple rows and overlappingly, facing each other in the flow direction of the reactant gas, if desired.
本発明装置は以上詳述した如き4tζ成に基づき、均一
に被覆し・潜る領域を拡大することが可能となり%従米
0OVD方式の作業性を向」ニし得る秀れた作用効果f
、発揮し得るものである。The device of the present invention is based on the 4tζ structure as detailed above, and has an excellent operational effect that can uniformly cover and expand the diving area, improving the workability of the 0% OVD method.
, it can be demonstrated.
第1図は従来方式のOVD装置の一例を示す概略断面図
、第2図は本発明装置の−yIJ e示す断面略図、第
3図は第2図のIN−nr線に沿った被蒸着基体と保持
具のみを示す略図、第参図は被蒸着基体を反応ガス流に
対し傾斜して配設した略図、第3図は本発明装置の竪型
インライン方式を示す略図であり1図中、i、ioは反
応室、2./よは被蒸着基体、J、/lは保持具、≠、
11は反応ガス喰出機構、j、/弘はガス排出孔、/3
は開孔隔壁、/7は間隙、Gはガス流方向を示す矢印、
几、Gは反応ガスを夫々示す。
第2図
、」
第3図
5
b
第4図
/−−
\−
/−FIG. 1 is a schematic cross-sectional view showing an example of a conventional OVD apparatus, FIG. 2 is a schematic cross-sectional view of the apparatus of the present invention, shown in FIG. and a schematic diagram showing only the holder; Figure 1 is a schematic diagram showing the substrate to be deposited inclined with respect to the flow of the reactant gas; Figure 3 is a schematic diagram showing the vertical in-line system of the apparatus of the present invention; i and io are reaction chambers, 2. /yo is the substrate to be deposited, J, /l is the holder, ≠,
11 is the reaction gas ejection mechanism, j, /Hiro is the gas exhaust hole, /3
is an open-hole partition wall, /7 is a gap, G is an arrow indicating the gas flow direction,
几 and G indicate reactive gases, respectively. Figure 2, Figure 3 5 b Figure 4/-- \- /-
Claims (1)
出する構造からなる反応室内に、被覆すべき基体を該反
応ガスの流れに対してルーツマー状に保持することを特
徴とするルーツク一式化学的蒸着装置。 (2) 被覆すべき基体表面を反応ガス流に対して垂
直又は一定角度に保持する特If/[請求の範囲第1項
記載のルーツク一式化学的蒸着装置!L0(3)被覆す
べき基体を反応ガスの流れ方向に対して複数列配列する
特許請求の範囲第1項記載のルーツク一式化学的蒸着装
置。 (4)被覆すべき基体を反応室内の反応ガス流方向を横
切って移動させる機構とする特許請求の範囲第1項記載
のルーツク一式化学的蒸着装置。[Scope of Claims] (1) A substrate to be coated is held in a roots form with respect to the flow of the reaction gas in a reaction chamber configured to charge a reaction gas from one side and exhaust gas from the other side. Lutsk complete chemical vapor deposition equipment featuring: (2) If the surface of the substrate to be coated is held perpendicularly or at a constant angle to the flow of the reactant gas. L0(3) The Lutsk complete chemical vapor deposition apparatus according to claim 1, wherein the substrates to be coated are arranged in multiple rows in the flow direction of the reaction gas. (4) A Lutsk complete chemical vapor deposition apparatus as claimed in claim 1, characterized in that the substrate to be coated is moved across the reaction gas flow direction within the reaction chamber.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15269982A JPS5943861A (en) | 1982-09-03 | 1982-09-03 | Louver type chemical vapor deposition device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15269982A JPS5943861A (en) | 1982-09-03 | 1982-09-03 | Louver type chemical vapor deposition device |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5943861A true JPS5943861A (en) | 1984-03-12 |
JPS619389B2 JPS619389B2 (en) | 1986-03-22 |
Family
ID=15546206
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15269982A Granted JPS5943861A (en) | 1982-09-03 | 1982-09-03 | Louver type chemical vapor deposition device |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5943861A (en) |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1991014798A1 (en) * | 1990-03-20 | 1991-10-03 | Diamonex, Incorporated | An improved hot filament chemical vapor deposition reactor |
US5160544A (en) * | 1990-03-20 | 1992-11-03 | Diamonex Incorporated | Hot filament chemical vapor deposition reactor |
WO1992020464A1 (en) * | 1991-05-10 | 1992-11-26 | Celestech, Inc. | Method and apparatus for plasma deposition |
US5188672A (en) * | 1990-06-28 | 1993-02-23 | Applied Materials, Inc. | Reduction of particulate contaminants in chemical-vapor-deposition apparatus |
US5204144A (en) * | 1991-05-10 | 1993-04-20 | Celestech, Inc. | Method for plasma deposition on apertured substrates |
US5551983A (en) * | 1994-11-01 | 1996-09-03 | Celestech, Inc. | Method and apparatus for depositing a substance with temperature control |
US5679404A (en) * | 1995-06-07 | 1997-10-21 | Saint-Gobain/Norton Industrial Ceramics Corporation | Method for depositing a substance with temperature control |
US6173672B1 (en) | 1997-06-06 | 2001-01-16 | Celestech, Inc. | Diamond film deposition on substrate arrays |
JP2002168530A (en) * | 2000-11-30 | 2002-06-14 | Daiwa House Ind Co Ltd | Construction method for roof panel with solar heat hot water device and solar heat hot water device |
US6406760B1 (en) | 1996-06-10 | 2002-06-18 | Celestech, Inc. | Diamond film deposition on substrate arrays |
DE102008044024A1 (en) * | 2008-11-24 | 2010-05-27 | Robert Bosch Gmbh | Coating method and coating device |
US20160306088A1 (en) * | 2013-12-27 | 2016-10-20 | 3M Innovative Properties Company | Uniform chemical vapor deposition coating on a 3-diminsional array of uniformly shaped articles |
JP2020100877A (en) * | 2018-12-21 | 2020-07-02 | 富士ゼロックス株式会社 | Film forming apparatus and film forming method |
-
1982
- 1982-09-03 JP JP15269982A patent/JPS5943861A/en active Granted
Cited By (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1991014798A1 (en) * | 1990-03-20 | 1991-10-03 | Diamonex, Incorporated | An improved hot filament chemical vapor deposition reactor |
US5160544A (en) * | 1990-03-20 | 1992-11-03 | Diamonex Incorporated | Hot filament chemical vapor deposition reactor |
US5397596A (en) * | 1990-06-28 | 1995-03-14 | Applied Materials, Inc. | Method of reducing particulate contaminants in a chemical-vapor-deposition system |
US5188672A (en) * | 1990-06-28 | 1993-02-23 | Applied Materials, Inc. | Reduction of particulate contaminants in chemical-vapor-deposition apparatus |
US5322567A (en) * | 1990-06-28 | 1994-06-21 | Applied Materials, Inc. | Particulate reduction baffle with wafer catcher for chemical-vapor-deposition apparatus |
US5204144A (en) * | 1991-05-10 | 1993-04-20 | Celestech, Inc. | Method for plasma deposition on apertured substrates |
EP0969120B1 (en) * | 1991-05-10 | 2003-07-30 | Celestech, Inc. | Method for plasma deposition |
US5435849A (en) * | 1991-05-10 | 1995-07-25 | Celestech, Inc. | Apparatus for plasma deposition |
US5487787A (en) * | 1991-05-10 | 1996-01-30 | Celestech, Inc. | Apparatus and method for plasma deposition |
WO1992020464A1 (en) * | 1991-05-10 | 1992-11-26 | Celestech, Inc. | Method and apparatus for plasma deposition |
EP0969120A2 (en) * | 1991-05-10 | 2000-01-05 | Celestech, Inc. | Method and apparatus for plasma deposition |
US5551983A (en) * | 1994-11-01 | 1996-09-03 | Celestech, Inc. | Method and apparatus for depositing a substance with temperature control |
US5683759A (en) * | 1994-11-01 | 1997-11-04 | Celestech, Inc. | Method for depositing a substance with temperature control |
US5679404A (en) * | 1995-06-07 | 1997-10-21 | Saint-Gobain/Norton Industrial Ceramics Corporation | Method for depositing a substance with temperature control |
US6099652A (en) * | 1995-06-07 | 2000-08-08 | Saint-Gobain Industrial Ceramics, Inc. | Apparatus and method for depositing a substance with temperature control |
US6406760B1 (en) | 1996-06-10 | 2002-06-18 | Celestech, Inc. | Diamond film deposition on substrate arrays |
US6173672B1 (en) | 1997-06-06 | 2001-01-16 | Celestech, Inc. | Diamond film deposition on substrate arrays |
JP2002168530A (en) * | 2000-11-30 | 2002-06-14 | Daiwa House Ind Co Ltd | Construction method for roof panel with solar heat hot water device and solar heat hot water device |
DE102008044024A1 (en) * | 2008-11-24 | 2010-05-27 | Robert Bosch Gmbh | Coating method and coating device |
US20160306088A1 (en) * | 2013-12-27 | 2016-10-20 | 3M Innovative Properties Company | Uniform chemical vapor deposition coating on a 3-diminsional array of uniformly shaped articles |
US10739503B2 (en) * | 2013-12-27 | 2020-08-11 | 3M Innovative Properties Company | Uniform chemical vapor deposition coating on a 3-dimensional array of uniformly shaped articles |
JP2020100877A (en) * | 2018-12-21 | 2020-07-02 | 富士ゼロックス株式会社 | Film forming apparatus and film forming method |
Also Published As
Publication number | Publication date |
---|---|
JPS619389B2 (en) | 1986-03-22 |
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