JPS59141420A - 連続法によるアルミニウムヒドロキシカーボネートゲルの製法 - Google Patents
連続法によるアルミニウムヒドロキシカーボネートゲルの製法Info
- Publication number
- JPS59141420A JPS59141420A JP58011619A JP1161983A JPS59141420A JP S59141420 A JPS59141420 A JP S59141420A JP 58011619 A JP58011619 A JP 58011619A JP 1161983 A JP1161983 A JP 1161983A JP S59141420 A JPS59141420 A JP S59141420A
- Authority
- JP
- Japan
- Prior art keywords
- solution
- reaction mixture
- gel
- reaction vessel
- aluminum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MPRVXUYAJZZBHG-UHFFFAOYSA-K dicarbonoperoxoyloxyalumanyl hydroxy carbonate Chemical compound [Al+3].OOC([O-])=O.OOC([O-])=O.OOC([O-])=O MPRVXUYAJZZBHG-UHFFFAOYSA-K 0.000 title claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 91
- 239000011541 reaction mixture Substances 0.000 claims description 67
- 239000000243 solution Substances 0.000 claims description 67
- 239000000499 gel Substances 0.000 claims description 44
- 238000000034 method Methods 0.000 claims description 44
- 239000000376 reactant Substances 0.000 claims description 37
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical group Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 30
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 claims description 28
- 239000007788 liquid Substances 0.000 claims description 28
- 238000002347 injection Methods 0.000 claims description 25
- 239000007924 injection Substances 0.000 claims description 25
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 20
- 239000012266 salt solution Substances 0.000 claims description 20
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 18
- 239000000047 product Substances 0.000 claims description 16
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 16
- -1 bicarbonate anions Chemical class 0.000 claims description 13
- 239000007864 aqueous solution Substances 0.000 claims description 12
- 150000002500 ions Chemical class 0.000 claims description 11
- 238000005406 washing Methods 0.000 claims description 10
- 230000002378 acidificating effect Effects 0.000 claims description 9
- 239000002244 precipitate Substances 0.000 claims description 9
- 238000000926 separation method Methods 0.000 claims description 9
- UIIMBOGNXHQVGW-UHFFFAOYSA-M sodium bicarbonate Substances [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 8
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 239000012670 alkaline solution Substances 0.000 claims description 7
- 239000006228 supernatant Substances 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 239000003929 acidic solution Substances 0.000 claims description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims description 3
- 150000008041 alkali metal carbonates Chemical class 0.000 claims description 3
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- 229910000028 potassium bicarbonate Inorganic materials 0.000 claims description 2
- 235000015497 potassium bicarbonate Nutrition 0.000 claims description 2
- 239000011736 potassium bicarbonate Substances 0.000 claims description 2
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 2
- 235000011181 potassium carbonates Nutrition 0.000 claims description 2
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims description 2
- 239000011240 wet gel Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims 2
- 150000008043 acidic salts Chemical class 0.000 claims 1
- 229910001413 alkali metal ion Inorganic materials 0.000 claims 1
- 238000010936 aqueous wash Methods 0.000 claims 1
- 238000005755 formation reaction Methods 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 239000011259 mixed solution Substances 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 235000015424 sodium Nutrition 0.000 claims 1
- 229940001593 sodium carbonate Drugs 0.000 claims 1
- 239000007863 gel particle Substances 0.000 description 13
- 230000032683 aging Effects 0.000 description 9
- 239000000203 mixture Substances 0.000 description 9
- 230000005070 ripening Effects 0.000 description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 8
- 239000002562 thickening agent Substances 0.000 description 8
- 238000007792 addition Methods 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000001556 precipitation Methods 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 4
- 229940069428 antacid Drugs 0.000 description 4
- 239000003159 antacid agent Substances 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 4
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical class [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
- 230000001458 anti-acid effect Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 239000000523 sample Substances 0.000 description 3
- 238000004448 titration Methods 0.000 description 3
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 2
- 240000007124 Brassica oleracea Species 0.000 description 2
- 235000003899 Brassica oleracea var acephala Nutrition 0.000 description 2
- 235000012905 Brassica oleracea var viridis Nutrition 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229940024545 aluminum hydroxide Drugs 0.000 description 2
- SMYKVLBUSSNXMV-UHFFFAOYSA-K aluminum;trihydroxide;hydrate Chemical group O.[OH-].[OH-].[OH-].[Al+3] SMYKVLBUSSNXMV-UHFFFAOYSA-K 0.000 description 2
- 239000001099 ammonium carbonate Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000010348 incorporation Methods 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 238000011017 operating method Methods 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 1
- 241000512259 Ascophyllum nodosum Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229940024546 aluminum hydroxide gel Drugs 0.000 description 1
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 1
- 235000012501 ammonium carbonate Nutrition 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 210000004211 gastric acid Anatomy 0.000 description 1
- 238000002523 gelfiltration Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 150000004687 hexahydrates Chemical class 0.000 description 1
- 239000007970 homogeneous dispersion Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000693 micelle Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 238000001139 pH measurement Methods 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 210000004894 snout Anatomy 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58011619A JPS59141420A (ja) | 1983-01-28 | 1983-01-28 | 連続法によるアルミニウムヒドロキシカーボネートゲルの製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58011619A JPS59141420A (ja) | 1983-01-28 | 1983-01-28 | 連続法によるアルミニウムヒドロキシカーボネートゲルの製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59141420A true JPS59141420A (ja) | 1984-08-14 |
| JPH0331643B2 JPH0331643B2 (cg-RX-API-DMAC7.html) | 1991-05-08 |
Family
ID=11782934
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58011619A Granted JPS59141420A (ja) | 1983-01-28 | 1983-01-28 | 連続法によるアルミニウムヒドロキシカーボネートゲルの製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59141420A (cg-RX-API-DMAC7.html) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016163444A1 (ja) * | 2015-04-07 | 2016-10-13 | 日産化学工業株式会社 | 液状の培地組成物の製造方法、およびそのための製造装置とキット |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS50144699A (cg-RX-API-DMAC7.html) * | 1974-05-04 | 1975-11-20 | ||
| JPS5119439A (cg-RX-API-DMAC7.html) * | 1974-08-09 | 1976-02-16 | Hitachi Ltd | |
| JPS51103035U (cg-RX-API-DMAC7.html) * | 1975-02-18 | 1976-08-18 | ||
| JPS51140900A (en) * | 1975-05-29 | 1976-12-04 | Agency Of Ind Science & Technol | Process for production of aluminum carbonate hydroxide:ammonium |
-
1983
- 1983-01-28 JP JP58011619A patent/JPS59141420A/ja active Granted
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS50144699A (cg-RX-API-DMAC7.html) * | 1974-05-04 | 1975-11-20 | ||
| JPS5119439A (cg-RX-API-DMAC7.html) * | 1974-08-09 | 1976-02-16 | Hitachi Ltd | |
| JPS51103035U (cg-RX-API-DMAC7.html) * | 1975-02-18 | 1976-08-18 | ||
| JPS51140900A (en) * | 1975-05-29 | 1976-12-04 | Agency Of Ind Science & Technol | Process for production of aluminum carbonate hydroxide:ammonium |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016163444A1 (ja) * | 2015-04-07 | 2016-10-13 | 日産化学工業株式会社 | 液状の培地組成物の製造方法、およびそのための製造装置とキット |
| JPWO2016163444A1 (ja) * | 2015-04-07 | 2018-02-01 | 日産化学工業株式会社 | 液状の培地組成物の製造方法、およびそのための製造装置とキット |
| US11345762B2 (en) | 2015-04-07 | 2022-05-31 | Nissan Chemical Industries, Ltd. | Method for preparing liquid medium composition, and preparation device and kit therefor |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0331643B2 (cg-RX-API-DMAC7.html) | 1991-05-08 |
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