JPS588042A - アクリル酸メチルの蒸留方法 - Google Patents
アクリル酸メチルの蒸留方法Info
- Publication number
- JPS588042A JPS588042A JP10622881A JP10622881A JPS588042A JP S588042 A JPS588042 A JP S588042A JP 10622881 A JP10622881 A JP 10622881A JP 10622881 A JP10622881 A JP 10622881A JP S588042 A JPS588042 A JP S588042A
- Authority
- JP
- Japan
- Prior art keywords
- acrylic acid
- methyl acrylate
- water
- methyl
- methyl alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 title claims abstract description 94
- 238000000034 method Methods 0.000 title claims description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 105
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 44
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 42
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 40
- 239000000203 mixture Substances 0.000 claims abstract description 22
- 238000004821 distillation Methods 0.000 claims abstract description 17
- 238000005886 esterification reaction Methods 0.000 claims description 18
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 description 9
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- -1 furinol and octatool Chemical class 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- CAAULPUQFIIOTL-UHFFFAOYSA-N methyl dihydrogen phosphate Chemical compound COP(O)(O)=O CAAULPUQFIIOTL-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229950000688 phenothiazine Drugs 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10622881A JPS588042A (ja) | 1981-07-09 | 1981-07-09 | アクリル酸メチルの蒸留方法 |
| US06/393,484 US4464229A (en) | 1981-07-09 | 1982-06-29 | Process for producing acrylic or methacrylic esters |
| FR8211987A FR2509294A1 (fr) | 1981-07-09 | 1982-07-08 | Procede de fabrication d'esters de l'acide acrylique ou methacrylique |
| BR8203983A BR8203983A (pt) | 1981-07-09 | 1982-07-08 | Processo para produzir ester acrilico ou metacrilico |
| MX193511A MX163005B (es) | 1981-07-09 | 1982-07-08 | Procedimiento mejorado para producir un ester acrilico o metacrilico |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10622881A JPS588042A (ja) | 1981-07-09 | 1981-07-09 | アクリル酸メチルの蒸留方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS588042A true JPS588042A (ja) | 1983-01-18 |
| JPS6320416B2 JPS6320416B2 (enrdf_load_stackoverflow) | 1988-04-27 |
Family
ID=14428264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10622881A Granted JPS588042A (ja) | 1981-07-09 | 1981-07-09 | アクリル酸メチルの蒸留方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS588042A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59181239A (ja) * | 1983-03-30 | 1984-10-15 | Mitsubishi Rayon Co Ltd | 含フツ素アクリル酸エステル又はメタクリル酸エステルの製造方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63144505A (ja) * | 1986-12-09 | 1988-06-16 | Mitsubishi Electric Corp | 漏洩磁界キヤンセル装置 |
-
1981
- 1981-07-09 JP JP10622881A patent/JPS588042A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59181239A (ja) * | 1983-03-30 | 1984-10-15 | Mitsubishi Rayon Co Ltd | 含フツ素アクリル酸エステル又はメタクリル酸エステルの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6320416B2 (enrdf_load_stackoverflow) | 1988-04-27 |
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