JPS5824098B2 - Process for producing water-soluble cocoa - Google Patents

Process for producing water-soluble cocoa

Info

Publication number
JPS5824098B2
JPS5824098B2 JP53067004A JP6700478A JPS5824098B2 JP S5824098 B2 JPS5824098 B2 JP S5824098B2 JP 53067004 A JP53067004 A JP 53067004A JP 6700478 A JP6700478 A JP 6700478A JP S5824098 B2 JPS5824098 B2 JP S5824098B2
Authority
JP
Japan
Prior art keywords
cocoa
cocoa powder
water
amount
fatty acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP53067004A
Other languages
Japanese (ja)
Other versions
JPS54157880A (en
Inventor
奥村誠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sanei Kagaku Kogyo KK
Original Assignee
Sanei Kagaku Kogyo KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sanei Kagaku Kogyo KK filed Critical Sanei Kagaku Kogyo KK
Priority to JP53067004A priority Critical patent/JPS5824098B2/en
Publication of JPS54157880A publication Critical patent/JPS54157880A/en
Publication of JPS5824098B2 publication Critical patent/JPS5824098B2/en
Expired legal-status Critical Current

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  • Confectionery (AREA)

Description

【発明の詳細な説明】 この発明は、ココア粉末の水溶層ないし水分散方法に係
るものであって、水にココア粉末を容易に溶解ないし分
散させる方法の創出を目的とする。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for dissolving or dispersing cocoa powder in water, and aims to create a method for easily dissolving or dispersing cocoa powder in water.

ココア粉末は周知の通り水ないし約3.5°C以下。As is well known, cocoa powder can be used in water or at temperatures below about 3.5°C.

の温水に溶解ないし分散(以下、溶解と論う)すること
が極めて困難なものである。
It is extremely difficult to dissolve or disperse (hereinafter referred to as dissolution) in warm water.

この困難を解決する方法としては、水とココア粉末との
混合系に、ココア粉末に対する約3係(重量、以下同じ
)前後のレシチンを添加するという方法が知られて。
As a method for solving this difficulty, a method is known in which lecithin of approximately 3 parts (by weight, same hereinafter) relative to cocoa powder is added to a mixed system of water and cocoa powder.

いる。There is.

レシチンはこの際、溶解助剤であるが、その使用量が多
すぎること、融点が高いことから、ココア粉末への添加
に当っては、高温を用いて溶解するか、アルコールその
他の溶剤の溶液にして、これを添加しなければならない
こと等の工業的実施に不利な点を有する。
In this case, lecithin is a solubilizing agent, but because it is used in too large a quantity and has a high melting point, when adding it to cocoa powder, it must be dissolved using high temperature or in a solution of alcohol or other solvent. It has disadvantages in industrial implementation, such as the fact that it must be added.

又、ショ糖脂肪酸エステルの添加が知られているが、満
足な結果が得られない。
Furthermore, although it is known to add sucrose fatty acid ester, satisfactory results cannot be obtained.

すなわち、完全に溶解せず、ココア液面に浮上した状態
で一部が残るという欠点を示す。
In other words, it has the disadvantage that it is not completely dissolved and a portion remains floating on the surface of the cocoa liquid.

この発明は、このような欠点のないものである。The present invention is free from such drawbacks.

この発明を以下に説明する。This invention will be explained below.

ココア粉末を用意する。Prepare cocoa powder.

つぎに このもっと水と次のエステルの1種又は2種以
上との混合系を用意する。
Next, a mixed system of water and one or more of the following esters is prepared.

この際、水の使用量は、ココア粉末の容量と等量販上量
ないし10倍以下量でよい。
At this time, the amount of water to be used may be an amount equal to or less than 10 times the volume of cocoa powder.

採用するエステルとしては、多価アルコールの不飽和脂
肪酸エステルである。
The ester employed is an unsaturated fatty acid ester of a polyhydric alcohol.

例えば、多価アルコールとしては、グリセリン、ソルビ
タン、グロピレングリコールがあげられる。
For example, polyhydric alcohols include glycerin, sorbitan, and glopylene glycol.

不飽和脂肪酸としては、パルミトオレイン酸、オレイン
酸、リノール酸、リルン酸、その他があげられる。
Examples of unsaturated fatty acids include palmitooleic acid, oleic acid, linoleic acid, linoleic acid, and others.

併用するエステルとしては、多価アルコールの飽和脂肪
酸エステルである。
The ester used in combination is a saturated fatty acid ester of polyhydric alcohol.

このものは、多価アルコールの不飽和脂肪酸エステルの
50%以下の任意量において併用することができる。
This product can be used in any amount up to 50% of the unsaturated fatty acid ester of polyhydric alcohol.

飽和脂肪酸としては、カプリン酸、ラウリン酸、ミリス
チン酸、バルミチン酸、ステアリン酸、その他があげら
れる。
Saturated fatty acids include capric acid, lauric acid, myristic acid, valmitic acid, stearic acid, and others.

これらのエステルの使用量は、ココア粉末の0.0OL
%以上の任意量でよい。
The amount of these esters used is 0.0OL of cocoa powder.
% or more may be used.

これらの併用により、多価アルコールの不飽和脂肪酸単
独よりも、さらに水に速かに溶解し、液面浮上部分が全
くなくなる。
By using these in combination, the polyhydric alcohol dissolves more quickly in water than the unsaturated fatty acid alone, and there is no floating portion on the liquid surface.

この混合系にココア粉末を添加し、ココア粉末の含有す
るカカオ脂の融点以上に加温する。
Cocoa powder is added to this mixed system and heated to a temperature higher than the melting point of cocoa butter contained in the cocoa powder.

この際採用するエステルの融点が、上記カカオ脂の融点
以下のものであるときは、加熱温度はカカオ脂の融点以
上範囲内の任意のものとすればよい。
When the melting point of the ester employed at this time is below the melting point of the cocoa butter, the heating temperature may be any temperature within the range above the melting point of the cocoa butter.

加温系について、カカオ脂が溶融し、ココア粉末が、溶
解を終了した時点で加温を止め直ちに均質にし、この系
を冷却せずに又は冷却し乾燥する。
For the heating system, once the cocoa butter has melted and the cocoa powder has finished dissolving, heating is stopped and the system is immediately homogenized, and the system is dried without cooling or after cooling.

乾燥温度は、ココア粉成分が炭化しない範囲内での任意
のものとする。
The drying temperature is arbitrary within a range that does not carbonize the cocoa powder component.

例えば、噴霧乾燥、大気圧下にあるいは減圧下に水分を
除去する等適宜の方法を採用してよい。
For example, an appropriate method such as spray drying, removing moisture under atmospheric pressure or reduced pressure may be employed.

かくして、得た粉末が目的の水溶性ココア粉末である。The powder thus obtained is the desired water-soluble cocoa powder.

収得物は冷水(例えば、0℃)に極めて速かに溶解する
The yield dissolves very quickly in cold water (eg 0°C).

以下にこの、実験例を記す。An example of this experiment is described below.

〔実験例〕[Experiment example]

溶解方法 A法 100m1のメスシリンダーに水(0°C〜5°
C)95部(重量、以下同じ)、ココア末5部投入、2
0回手で振盪する。
Dissolution method A: Add water (0°C to 5°C) to a 100ml graduated cylinder.
C) Add 95 parts (weight, same below), 5 parts of cocoa powder, 2
Shake by hand 0 times.

室温に静置し10分後浮上した部分を不溶解部として、
残りを溶解部として%で表わす。
The part that floated to the surface after 10 minutes at room temperature was designated as the undissolved part.
The remainder is expressed as a % dissolved portion.

B法 ビーカーに水(0°C〜5°C)95部、コア末
5部投入。
Method B: Add 95 parts of water (0°C to 5°C) and 5 parts of core powder to a beaker.

撹拌棒で20回攪拌、浮上している部分を不溶解部とし
て10点法で表わす。
Stir 20 times with a stirring bar, and indicate on a 10-point scale that the floating portion is considered an undissolved portion.

全部浮上している物を 0点 浮上していない物を 10点とする 実施例 1 ココアパウダー(カカオ脂22〜24%含有)19.7
部 グリセリンモノオレエー) 0.3 温水
80.0部グリセリン
モノオレエートを50℃の温水に分散させココアパウダ
ーを投入し、50℃で約10分間攪拌混合する。
Example 1 Cocoa powder (contains 22-24% cacao butter) 19.7
Part glycerin monooleate) 0.3 Hot water
Disperse 80.0 parts of glycerin monooleate in warm water at 50°C, add cocoa powder, and stir and mix at 50°C for about 10 minutes.

直ちに均質にし、液温40〜50℃でスプレィドライ法
で乾燥した。
It was immediately homogenized and dried by spray drying at a liquid temperature of 40 to 50°C.

収得物は0℃の水に速かに全量溶解し、液面浮上部分が
全ぐなかった。
The entire amount of the obtained product was quickly dissolved in water at 0°C, and there was no floating portion on the liquid surface.

実施例 2 ココアパウダー(カカオ脂22〜24係含有)19.6
0部 ソルビタンモノオレエート 0.38部グリセ
リンモノステアレー) 0.02部水
so、oo部メソルビタンモノ
オレエートグリセリンモノステアレートを70〜75℃
の温水に分散させ、ココアパウダーを投入し、70〜7
5℃で約10分間攪拌混合する。
Example 2 Cocoa powder (containing 22 to 24 parts of cocoa fat) 19.6
0 parts sorbitan monooleate 0.38 parts glycerin monostearate) 0.02 parts water
so, oo part mesorbitan monooleate glycerol monostearate at 70-75℃
Disperse in warm water, add cocoa powder, and heat to 70-7
Stir and mix for about 10 minutes at 5°C.

直ちに均質にし、液温70〜75℃でスプレィドライ法
で乾燥した。
The mixture was immediately homogenized and dried by spray drying at a liquid temperature of 70 to 75°C.

収得物は、0℃の水に速かに全量溶解し、液面浮上部分
が全くなかった。
The entire amount of the obtained product was quickly dissolved in water at 0° C., and there was no portion floating on the liquid surface.

Claims (1)

【特許請求の範囲】 1 ココア粉末にその0.001%以上量の多価アルコ
ール不飽和脂肪酸エステルと、その等量販上量の水を添
加し、ココア粉末含有カカオ脂及び該エステルの融点以
上温度に加温し、均質系を得、これを乾燥することを特
徴とする水溶性ココアの製法。 2 ココア粉末にその0.001%以上量の多価アルコ
ール不飽和脂肪酸エステル、このエステルの。 半量以下量の多価アルコール飽和脂肪酸エステル、及び
ココア粉末の等量販上の水を添加し、ココア粉末含有カ
カオ脂及び該エステル類の融点以上温度に加温して均質
系を得、これを乾燥することを特徴とする水溶性ココア
の製法。
[Scope of Claims] 1. A polyhydric alcohol unsaturated fatty acid ester in an amount of 0.001% or more of the cocoa powder and an equivalent commercial amount of water are added to the cocoa powder, and the temperature is equal to or higher than the melting point of the cocoa butter containing the cocoa powder and the ester. A method for producing water-soluble cocoa, which is characterized by heating it to obtain a homogeneous system and drying this. 2 Cocoa powder with an amount of 0.001% or more of polyhydric alcohol unsaturated fatty acid ester, and this ester. A homogeneous system is obtained by adding less than half the amount of polyhydric alcohol saturated fatty acid ester and the same amount of water as the amount of cocoa powder, and heating to a temperature above the melting point of the cocoa powder-containing cocoa butter and the esters, which is then dried. A method for producing water-soluble cocoa characterized by:
JP53067004A 1978-06-02 1978-06-02 Process for producing water-soluble cocoa Expired JPS5824098B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP53067004A JPS5824098B2 (en) 1978-06-02 1978-06-02 Process for producing water-soluble cocoa

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP53067004A JPS5824098B2 (en) 1978-06-02 1978-06-02 Process for producing water-soluble cocoa

Publications (2)

Publication Number Publication Date
JPS54157880A JPS54157880A (en) 1979-12-13
JPS5824098B2 true JPS5824098B2 (en) 1983-05-19

Family

ID=13332340

Family Applications (1)

Application Number Title Priority Date Filing Date
JP53067004A Expired JPS5824098B2 (en) 1978-06-02 1978-06-02 Process for producing water-soluble cocoa

Country Status (1)

Country Link
JP (1) JPS5824098B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0345198Y2 (en) * 1985-03-08 1991-09-24
JPH0431547Y2 (en) * 1984-07-20 1992-07-29

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3347579B2 (en) * 1996-04-10 2002-11-20 理研ビタミン株式会社 Oil composition for improving wettability of cocoa powder
JP7072979B2 (en) * 2018-03-29 2022-05-23 日清オイリオグループ株式会社 Beverage chocolate

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0431547Y2 (en) * 1984-07-20 1992-07-29
JPH0345198Y2 (en) * 1985-03-08 1991-09-24

Also Published As

Publication number Publication date
JPS54157880A (en) 1979-12-13

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