JPS58111649A - Preparation of aqueous gel - Google Patents

Preparation of aqueous gel

Info

Publication number
JPS58111649A
JPS58111649A JP56212470A JP21247081A JPS58111649A JP S58111649 A JPS58111649 A JP S58111649A JP 56212470 A JP56212470 A JP 56212470A JP 21247081 A JP21247081 A JP 21247081A JP S58111649 A JPS58111649 A JP S58111649A
Authority
JP
Japan
Prior art keywords
gel
solution
stirring
carrageenan
add
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP56212470A
Other languages
Japanese (ja)
Inventor
Shiro Ohashi
司郎 大橋
Kenji Masutake
憲二 増竹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
San Ei Kagaku Co Ltd
Sanei Kagaku Kogyo KK
Original Assignee
San Ei Kagaku Co Ltd
Sanei Kagaku Kogyo KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by San Ei Kagaku Co Ltd, Sanei Kagaku Kogyo KK filed Critical San Ei Kagaku Co Ltd
Priority to JP56212470A priority Critical patent/JPS58111649A/en
Publication of JPS58111649A publication Critical patent/JPS58111649A/en
Pending legal-status Critical Current

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Abstract

PURPOSE:To prepare an aqueous gel of cocoa, decocted coffee, milk, etc., economically and industrially, by adding a solution of kappa-carrageenan to an aqueous system containing ions of K, Ca, Mg and NH3. CONSTITUTION:Cocoa, decocted coffee, milk, fermented milk, cheese, or fruit juice usually containing ions of K, Ca, Mg and NH3, is mixed with a hot solution of kappa-carrageenan, and the mixture is left to stand at room temperature for a definite time interval to obtain the aqueous gel of the above raw material liquid.

Description

【発明の詳細な説明】 この発明は、食品に係るものであり、水性ゲルを工業的
に有利に製造することを目的とする。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to foods and aims to industrially advantageously produce an aqueous gel.

寒天、カラギーナン、ゼラチン、七の他のゲル化物質を
主材とする水性ゲルは既に、多くが知られているがこの
ようなものを製造するには、これらのゲル化物質と水と
の混合糸を加熱して均質ゾルにし、ついでこれら物質の
ゲル化点以下の温度に冷却することが必要である。即ち
、従来法による限り、加熱、冷却の両2工程を必要とす
る。
Many aqueous gels based on agar, carrageenan, gelatin, and other gelling substances are already known, but in order to produce such gels, these gelling substances must be mixed with water. It is necessary to heat the yarn to a homogeneous sol and then cool it to a temperature below the gelling point of these materials. That is, the conventional method requires both heating and cooling steps.

ここにおいて、これら両2工程を必要としない即ちイン
スタントな水性ゲルの製法の開発が必要となる。
Here, it is necessary to develop a method for producing an instant aqueous gel that does not require these two steps.

この発明は、この要望に応える一試みであり、それに成
功したものである。
This invention was an attempt to meet this demand, and was successful.

この発明の適用対象は、K、 Oa、 Mg、 N)I
llのイオン1種以上を含む水系である。
The objects to which this invention is applied are K, Oa, Mg, N)I
It is an aqueous system containing one or more types of ions.

このようなものとしては、ココア、コーヒー前液、牛乳
、果汁、醗酵孔、その他が挙げられる。
These include cocoa, coffee pre-liquid, milk, fruit juices, fermenters, and the like.

この究明のゲル化物質としては、カラギーナン中特定の
ものが採用される。 即ちカッパー型カラギーナンに限
って採用される。ラムダ−型、アイオーl−型のものは
、使用することが出来ない。
A specific carrageenan is used as the gelling substance in this investigation. That is, it is adopted only for copper-type carrageenan. Lambda type and IOL type cannot be used.

カッパー型のものの水溶液は、常温下で液状を呈するも
のであってゾルに属し、ゲルには属さな°い。
Copper-type aqueous solutions exhibit a liquid state at room temperature and belong to sol and do not belong to gel.

つぎに目的物水性ゲ〃の製造工程を説明する。Next, the manufacturing process of the target aqueous gel will be explained.

まず、ココア、コーヒー前液、牛乳、醗酵孔、チーズ及
び又は果汁を用意する。これらは何れもに、Ca、Mg
及び又はNH,s  イオンを含む水系である。
First, cocoa, coffee preliquid, milk, fermentation hole, cheese and/or fruit juice are prepared. All of these include Ca, Mg
and/or an aqueous system containing NH,s ions.

このものに、カッパー型カラギーナンの水性ゾルを添加
する。カラギーナンの除加量は、ココア、牛乳、コーヒ
ー前液、醗酵孔及び又は果汁の全量の含有するに、 C
a、Mg、 NHa  イオンを1とする場合、その含
有する物質カラギーナンが1〜200であるようにすれ
ばよい。
To this is added an aqueous sol of copper-type carrageenan. The amount of carrageenan added is based on the total amount of cocoa, milk, coffee preliquid, fermentation hole, and/or fruit juice.C
When the a, Mg, and NHa ions are 1, the content of the substance carrageenan contained therein may be 1 to 200.

この系は、攪拌して均質系とし、これを常温下に静置す
ると、系は安定な水性ゲル状物となる。
This system is stirred to become a homogeneous system, and when this system is left to stand at room temperature, the system becomes a stable aqueous gel.

ここにこの発明は、その目的を達し得る。Herein, the invention can achieve its purpose.

実施例1 水9B、5fを湯浴中で攪拌しながらカラギーナン1.
5?を加え液温か80℃になる迄加温攪拌し溶解する。
Example 1 While stirring water 9B and 5f in a hot water bath, carrageenan 1.
5? Add and stir until the liquid temperature reaches 80°C to dissolve.

この溶液を10℃迄冷却する。この時、この溶液はゲル
にならないゾルである。この溶液100?を軽く攪拌し
ながら10℃の牛乳401を加えて混和する。25℃の
室温で10分間放置するとゲル状となる。このゲルを販
尾式カードメーター、荷重1001、層圧軸8IIII
+で18℃のゲルの破断力を測定すると66y/lIN
であった。このゲルは糊状感を呈せず口溶けがよく風味
の放出性も良好なゲルが得られ庭。
Cool this solution to 10°C. At this time, this solution is a sol that does not form a gel. This solution 100? Add milk 401 at 10°C and mix while stirring lightly. When left at room temperature of 25°C for 10 minutes, it becomes gel-like. This gel is sold using a tail-type card meter, load 1001, layer pressure axis 8III.
When the breaking force of gel at 18°C is measured at +, it is 66y/lIN
Met. This gel does not have a pasty feel, melts in the mouth, and releases flavor well.

実施例2 水98fを湯浴中で攪拌しながらカラギーナン2?を加
え液温が80℃になる迄加温攪拌し溶解する。この溶液
を25℃迄冷却する。この時この溶液はゲルにならない
ゾルである。この溶液100?を軽く攪拌しながら10
℃の10%ココア溶液100?を加えて混和する。25
℃の室温で10分間放置するとゲル状となる。このゲル
を成馬式カードメーター荷重100P1感圧軸8■で1
9℃のゲルの破断力を測定すると50t/−であった。
Example 2 While stirring 98 f of water in a hot water bath, carrageenan 2? Add and dissolve by heating and stirring until the liquid temperature reaches 80°C. Cool this solution to 25°C. At this time, this solution is a sol that does not form a gel. This solution 100? 10 while stirring gently.
10% cocoa solution at 100°C? Add and mix. 25
When left for 10 minutes at room temperature (°C), it becomes gel-like. Apply this gel to an adult card meter with a load of 100P and a pressure-sensitive shaft of 8cm.
The breaking force of the gel at 9°C was measured to be 50t/-.

このゲルは糊状感を呈せず口溶けがよく風味の放出性も
良好なゲルが得られた。
This gel did not have a pasty feel, melted well in the mouth, and had good flavor release properties.

実施例8 水98.5rを湯浴中で攪拌しながらカラギーナン1.
IM’を加え液温が80’Cになる迄加温攪拌し溶解す
る。この溶液t−25℃迄冷却する。この時、この溶液
はゲルにならないゾルである。この溶液100tを軽く
攪拌しながら25℃の8%インスタントコーヒー液10
02を加えて混和する。   ′26℃の室温で10分
間放置するとゲル状となる。
Example 8 While stirring 98.5 r of water in a hot water bath, carrageenan 1.
Add IM' and dissolve by heating and stirring until the liquid temperature reaches 80'C. This solution is cooled to t-25°C. At this time, this solution is a sol that does not form a gel. While gently stirring 100 tons of this solution, 10 tons of 8% instant coffee liquid at 25℃ was added.
Add 02 and mix. 'If left at room temperature of 26°C for 10 minutes, it becomes gel-like.

このゲルを飯尾弐カートメーシー、荷重100F。Apply this gel to Iio Ni cart Macy and load 100F.

感圧軸8關で、25℃のゲルの破断力を測定すると54
.2r/lJであった。このゲルは糊状感を呈せず口溶
けがよく風味の放出性も良好なゲルが得られた。
When the breaking force of gel at 25°C is measured with 8 pressure sensitive axis, it is 54
.. It was 2r/lJ. This gel did not have a pasty feel, melted well in the mouth, and had good flavor release properties.

実施例4 水98Fを湯浴中で攪拌しながらカラギーナン21を加
え液温が80゛Cになる迄加温攪拌し溶解する。この溶
液f、80℃迄冷却する。この溶液はゲルにならないゾ
ルである。この溶液1001を軽く攪拌しながら10℃
のオレンジ果汁1001を加えて混和する。25℃の室
温で10分間放置するとゲル状となる。このゲルを成馬
式カードメーター荷重100?、感圧軸8mで22℃の
ゲルの破断力を測定すると68f/dであった。このゲ
ルは糊状感を呈せず口溶けがよく風味の放出性も良好な
ゲルが得られた。
Example 4 Carrageenan 21 was added to 98F water while stirring in a hot water bath, and the mixture was heated and stirred until the liquid temperature reached 80°C to dissolve. This solution f is cooled to 80°C. This solution is a sol that does not form a gel. This solution 1001 was heated to 10℃ while stirring lightly.
Add orange juice 1001 and mix. When left at room temperature of 25°C for 10 minutes, it becomes gel-like. This gel has an adult card meter load of 100? When the breaking force of the gel was measured at 22° C. with a pressure-sensitive axis of 8 m, it was 68 f/d. This gel did not have a pasty feel, melted well in the mouth, and had good flavor release properties.

実施例5 水98.51を湯浴中で攪拌しながらカラギーナン1.
5fを加え液温が80゛Cになる迄加温攪拌し溶解する
。この溶液を20℃迄冷却する。この時この溶液はゲル
にならないゾルである。この溶液1001を軽く攪拌し
ながら20℃のヨーグルト60fを加えて混和する。2
5℃の室温で10分間放置するとゲル状となる。このゲ
ルを叙尾弐カードメーター、荷重toof、感圧軸8■
で20℃のゲルの破断力を測定すると89.6f/lj
であった。このゲルは糊状感を呈せず口溶けがよく風味
の放出性も良好なゲルが得られた。
Example 5 While stirring 98.51 liters of water in a hot water bath, 1.
Add 5f and dissolve by heating and stirring until the liquid temperature reaches 80°C. Cool this solution to 20°C. At this time, this solution is a sol that does not form a gel. While lightly stirring this solution 1001, 20° C. yogurt 60f is added and mixed. 2
When left at room temperature of 5°C for 10 minutes, it becomes gel-like. Add this gel to the card meter, load toof, pressure sensitive axis 8■
When the breaking force of the gel at 20°C was measured, it was 89.6f/lj
Met. This gel did not have a pasty feel, melted well in the mouth, and had good flavor release properties.

実施例6 水98Fを湯浴中で攪拌しながらカラギーナン2?を加
え液温か80℃になる迄加温攪拌し溶解する。この溶液
を40℃迄冷却する。この時この溶液はゲルにならない
ゾルである。この溶液100?を軽く攪拌しながら40
℃の10%チーズ溶液100?を加えて混和する。25
℃の室温で10分間放置するとゲル状となる。このゲル
を成馬式カードメーター、荷重100F、感圧軸8■で
88℃のゲルの破断力を測定すると48.2f/−であ
った。このゲルは糊状惑を呈せず口溶けがよく風味の放
出性も良好なゲルが得られた。
Example 6 While stirring 98F water in a hot water bath, carrageenan 2? Add and stir until the liquid temperature reaches 80°C to dissolve. Cool this solution to 40°C. At this time, this solution is a sol that does not form a gel. This solution 100? 40 while stirring gently.
10% cheese solution at 100°C? Add and mix. 25
When left for 10 minutes at room temperature (°C), it becomes gel-like. The breaking force of this gel at 88 DEG C. was measured using an adult card meter with a load of 100 F and a pressure sensitive axis of 8 mm, and it was found to be 48.2 f/-. This gel did not exhibit pasty texture, melted in the mouth, and had good flavor release properties.

実施例7 水98.5ft−湯浴中で攪拌しながらカラギーナン1
.5ftl−加え液温か80℃になる迄加温攪拌し溶解
する。この溶液を10℃迄冷却する。この時この溶液は
ゲルにならないゾルである。この溶液toorfi−軽
く攪拌しながら10℃の牛乳20rと10℃のオレンジ
果汁801を加えて混和する。
Example 7 98.5 ft of water - Carrageenan 1 was added while stirring in a hot water bath.
.. Add 5 ftl and dissolve by heating and stirring until the liquid temperature reaches 80°C. Cool this solution to 10°C. At this time, this solution is a sol that does not form a gel. To this solution, add 20 liters of milk at 10°C and 801ml of orange juice at 10°C and mix while stirring lightly.

25″Cの室温で10分間放置するとゲル状となる。When left at room temperature of 25''C for 10 minutes, it becomes gel-like.

このゲlvを成馬式カードメーター、荷11toor感
圧軸8閣で18℃のゲルの破断力を測定すると52.6
1/lylであった。このゲμは糊状感を呈せず口溶け
がよく風味の放出性も良好なゲルが得られ九。
The breaking force of this gel at 18°C was measured using an adult type card meter with a load of 11 torr and 8 pressure-sensitive shafts, and it was 52.6.
It was 1/lyl. This gel has no pasty texture, melts in the mouth, and has good flavor release properties.9.

実施例8 水98.5Fを湯浴中で攪拌しながらカラギーナン1.
5tf加え液温が80゛Cになる迄加温攪拌し溶解する
。この溶液を20℃迄冷却する。この時この溶液はゲル
にならないゾルである。この溶液100?を軽く攪拌し
ながら20゛Cの10%チーズ溶液50?と20℃のオ
レンジ果汁50rを加えて混和する。25℃の室温で1
0分間放置するとゲル状となる。このゲルを成馬式カー
ドメーター、荷重100?、感圧軸8mで20℃のゲ〃
の破断力を測定すると452/−であった、このゲルは
糊状感を呈せず口溶けがよく風味の放出性も良好々ゲル
が得られた。
Example 8 While stirring water at 98.5F in a hot water bath, carrageenan 1.
Add 5tf and dissolve by heating and stirring until the liquid temperature reaches 80°C. Cool this solution to 20°C. At this time, this solution is a sol that does not form a gel. This solution 100? Add 50% of the 10% cheese solution at 20°C while stirring gently. Add 50 liters of orange juice at 20°C and mix. 1 at room temperature of 25℃
When left for 0 minutes, it becomes gel-like. Use this gel with an adult card meter, load 100? , 20℃ temperature with 8m pressure sensitive axis
When the breaking force of the gel was measured, it was 452/-.This gel did not exhibit a pasty feeling, melted well in the mouth, and had good flavor release properties.

実施例9 水98.5Fを湯浴中で攪拌しながらカラギーナン1.
51を加え液温か80℃になる迄加温攪拌し溶解する。
Example 9 While stirring water at 98.5F in a hot water bath, carrageenan 1.
Add 51 and dissolve by heating and stirring until the liquid temperature reaches 80°C.

この溶液を20℃迄冷却する。この時この溶液はゲルに
ならないゾルである。この溶液100?を軽く攪拌しな
がら10℃のヨーグルト801と10℃のオレンジ果汁
70rを加えて混和する。25℃の室温で10分間放置
するとゲル状となる。このゲ/1/l−販尾式カードメ
ーター、荷重1004、感圧軸8Ialで17℃のゲル
の破断力を測定すると55.8r/J  であった。こ
のゲμは糊状感を呈せず口溶けがよく風味の放出性壷良
好なゲルが得られた。
Cool this solution to 20°C. At this time, this solution is a sol that does not form a gel. This solution 100? Add and mix 10°C yogurt 801 and 10°C orange juice 70ml while stirring gently. When left at room temperature of 25°C for 10 minutes, it becomes gel-like. The breaking force of this gel at 17 DEG C. was measured using a G/1/L-tailor type card meter with a load of 1004 and a pressure-sensitive shaft of 8Ial, and it was found to be 55.8 r/J. This gel did not have a pasty feel, melted in the mouth, and had a good flavor and release properties.

実施例1O 水98?を湯浴中で攪拌しながらカラギーナン2fを加
え液温か80℃になる迄加温攪拌し溶解する。この溶液
を20℃迄冷却する。この時、この溶液はゲルにならな
いゾルである。この溶液toorを軽く攪拌しながら1
0℃の牛乳201と20℃の8%インスタントコーヒ液
80re加えて混和する。25℃の室温で10分間放置
するとゲル状となる。このゲ/l’を成馬式カードメー
ター、荷重100F、感圧軸8mmで20℃のゲルの破
断力を測定すると、42F/−であった。このゲルは糊
状感を呈せず口溶けがよく風味の放出性も良好なゲルが
得られた。
Example 1O Water 98? While stirring in a water bath, add 2 f of carrageenan, and dissolve by heating and stirring until the liquid temperature reaches 80°C. Cool this solution to 20°C. At this time, this solution is a sol that does not form a gel. While stirring this solution toor lightly,
Add 201 re of milk at 0°C and 80 re of 8% instant coffee liquid at 20°C and mix. When left at room temperature of 25°C for 10 minutes, it becomes gel-like. When the breaking force of the gel at 20° C. was measured using an adult card meter, a load of 100 F, and a pressure-sensitive shaft of 8 mm, the gel/l' was 42 F/-. This gel did not have a pasty feel, melted well in the mouth, and had good flavor release properties.

実施例11 水97.5 Fを湯浴中で攪拌しながらカラギーナン2
.5vを加え液温か80℃になる迄加温攪拌し溶解する
。この溶液を40℃迄冷却する。この時この溶液はゲル
にならないゾルである。この溶液100fを軽く攪拌し
ながら40℃の10%チーズ溶液802と40℃のヨー
グルト701を加えて混和する。25°Cの室温で10
分間放置するとゲル状となる。このゲルを販尾式カード
メーター荷重1001、感圧軸8鴎で88℃のゲルの破
断力を測定すると、201/cdであるた、このグμは
糊状感を呈せず口溶けがよく風味の放出性も良好なゲル
が得られた。
Example 11 Carrageenan 2 was added while stirring 97.5 F water in a hot water bath.
.. Add 5v and stir to dissolve until the liquid temperature reaches 80°C. Cool this solution to 40°C. At this time, this solution is a sol that does not form a gel. 10% cheese solution 802 at 40°C and yogurt 701 at 40°C are added to and mixed with this solution 100f while stirring lightly. 10 at room temperature of 25°C
Leave it for a minute and it will turn into a gel. When we measured the breaking force of this gel at 88°C using a sales-type card meter with a load of 1001 and a pressure-sensitive shaft of 8, it was 201/cd. A gel with good release properties was obtained.

特許出願人 三栄化学工業株式会社Patent applicant: Sanei Chemical Industry Co., Ltd.

Claims (1)

【特許請求の範囲】[Claims] に、Ca’、 Mg’、 NHaの1種以上のイオンを
含む常温下ノ水系にカッパー型カラギーナン水系を添加
することを特徴とするココア・コーヒー前液、牛乳、醗
酵孔、チーズ及び又は果汁系の製法。
A cocoa/coffee preliquid, milk, fermentation hole, cheese and/or fruit juice system, characterized in that a copper carrageenan aqueous system is added to a room temperature aqueous system containing one or more types of ions of Ca', Mg', and NHa. manufacturing method.
JP56212470A 1981-12-26 1981-12-26 Preparation of aqueous gel Pending JPS58111649A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP56212470A JPS58111649A (en) 1981-12-26 1981-12-26 Preparation of aqueous gel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP56212470A JPS58111649A (en) 1981-12-26 1981-12-26 Preparation of aqueous gel

Publications (1)

Publication Number Publication Date
JPS58111649A true JPS58111649A (en) 1983-07-02

Family

ID=16623173

Family Applications (1)

Application Number Title Priority Date Filing Date
JP56212470A Pending JPS58111649A (en) 1981-12-26 1981-12-26 Preparation of aqueous gel

Country Status (1)

Country Link
JP (1) JPS58111649A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6322841B1 (en) 2000-02-09 2001-11-27 Kraft Foods, Inc. Cheese-like dairy gels
JP2011000051A (en) * 2009-06-18 2011-01-06 Sanei Gen Ffi Inc Liquid base for preparing instant dessert
WO2013115257A1 (en) * 2012-01-30 2013-08-08 株式会社明治 Insoluble mineral fortified milk beverage

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6322841B1 (en) 2000-02-09 2001-11-27 Kraft Foods, Inc. Cheese-like dairy gels
JP2011000051A (en) * 2009-06-18 2011-01-06 Sanei Gen Ffi Inc Liquid base for preparing instant dessert
WO2013115257A1 (en) * 2012-01-30 2013-08-08 株式会社明治 Insoluble mineral fortified milk beverage
JPWO2013115257A1 (en) * 2012-01-30 2015-05-11 株式会社明治 Insoluble mineral-enriched milk beverage

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