JPS5742661A - Preparation of n- dialkylaminoalkyl acrylamide - Google Patents

Preparation of n- dialkylaminoalkyl acrylamide

Info

Publication number
JPS5742661A
JPS5742661A JP11920180A JP11920180A JPS5742661A JP S5742661 A JPS5742661 A JP S5742661A JP 11920180 A JP11920180 A JP 11920180A JP 11920180 A JP11920180 A JP 11920180A JP S5742661 A JPS5742661 A JP S5742661A
Authority
JP
Japan
Prior art keywords
formula
dialkylaminoalkylamine
mole
alkyl
double
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11920180A
Other languages
Japanese (ja)
Inventor
Osamu Kamata
Shigeru Sawayama
Makoto Watanabe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Kasei Corp
Original Assignee
Mitsubishi Kasei Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Kasei Corp filed Critical Mitsubishi Kasei Corp
Priority to JP11920180A priority Critical patent/JPS5742661A/en
Publication of JPS5742661A publication Critical patent/JPS5742661A/en
Pending legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To obtain the titled compound useful as a raw material for a cationic polymer in high purity and in high yield, by reacing an acrylic acid or its ester with double or more mole dialkylaminoalkylamine, followed by hydrolysis.
CONSTITUTION: An acrylic acid shown by the formula I (R1 is H or 1W3C alkyl) or an acrylic ester is reacted with double or more mole dialklaminoalkylamine shown by the formula II (R2 and R3 are 1W3C alkyl; n is an integer of 2W5), to give a compound shown by the formula III, which is decomposed at 150W300°C under heating, and only an N-(dialkyl aminoalkyl)acrylamide shown by the formula IV, a decomposition product under heating, is obtained in extremely high yield by a condenser which is simultaneously heated.
EFFECT: The excess addition of the dialkylaminoalkylamine carries out simultaneously amidation and protection of vinyl group, and prevents the polymerization and size reactions during the reaction.
COPYRIGHT: (C)1982,JPO&Japio
JP11920180A 1980-08-29 1980-08-29 Preparation of n- dialkylaminoalkyl acrylamide Pending JPS5742661A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11920180A JPS5742661A (en) 1980-08-29 1980-08-29 Preparation of n- dialkylaminoalkyl acrylamide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11920180A JPS5742661A (en) 1980-08-29 1980-08-29 Preparation of n- dialkylaminoalkyl acrylamide

Publications (1)

Publication Number Publication Date
JPS5742661A true JPS5742661A (en) 1982-03-10

Family

ID=14755422

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11920180A Pending JPS5742661A (en) 1980-08-29 1980-08-29 Preparation of n- dialkylaminoalkyl acrylamide

Country Status (1)

Country Link
JP (1) JPS5742661A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58170741A (en) * 1982-03-18 1983-10-07 ケミシエ・フアブリ−ク・シユトツクハウゼン・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング Manufacture of n-(tertiary aminoalkyl)acrylamide
JP2010505890A (en) * 2006-10-09 2010-02-25 クラリアント・ファイナンス・（ビーブイアイ）・リミテッド Method for producing basic (meth) acrylamide

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS58170741A (en) * 1982-03-18 1983-10-07 ケミシエ・フアブリ−ク・シユトツクハウゼン・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング Manufacture of n-(tertiary aminoalkyl)acrylamide
JPH0237913B2 (en) * 1982-03-18 1990-08-28 Hemitsushu Fuaburitsuku Shutotsukuhauzen Gmbh
JP2010505890A (en) * 2006-10-09 2010-02-25 クラリアント・ファイナンス・（ビーブイアイ）・リミテッド Method for producing basic (meth) acrylamide

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